The present invention relates to food and beverage processing. In particular, the present invention relates to processing alcoholic beverages by removing contaminants and impurities and achieving desirable designed taste and aroma of beverage by adding variable plant extracts.
Alcoholic beverages, in particular distilled spirits, begin with a fermentation process, which converts sugars into cellular energy thereby producing ethanol and carbon dioxide. Another byproduct of fermentation is fusel oil produced by amino acids during the fermentation and distillation process.
Fusel oil is a mixture of volatile organic acids, higher alcohols, aldehydes, ketones, fatty acids, and esters, including amyl alcohol and n-propyl and isobutyl alcohols. When concentrated, this mixture has an oily consistency and potent odor. During distillation, fusel oil is typically concentrated in the feints or “tails” at the end of the distillation run. Fusel oil can affect the flavor and aroma of the resultant beverage. For example, fusel oil can give off a solvent-like aroma and flavor. Moreover, in certain beverages such as vodka the presence of fusel oil, in addition to alcohols other than ethanol, is considered a fault. As a result, removal of these impurities including fusel oil is desirable.
One proposed method employs nanofiltration and ultrafiltration to filter out the fusel oil. However, this method is limited to rice spirits and requires additional costs in the form of additional pumps, valves, gauges, and temperature control systems, in addition to the routine costs of filters.
Therefore, there is a need in the art for a method for removing impurities, including fusel oil, in a wide range of alcoholic beverages without additional costs and maintenance and in a quick manner to minimize costs.
A method for removing a set of impurities in an alcoholic beverage is disclosed. In one embodiment, the steps include providing a water solution comprising approximately 96%, or less, of pure water and at least 4% or more of honey by volume, providing a spirit base comprising a set of impurities and at least 80% alcohol by volume, creating a mixture from approximately 50% the water solution by volume and approximately 50% the spirit base by volume, adding approximately 1% of a set of extracts by volume to the mixture to achieve designer taste, adding approximately 4% or more of sugar by volume and approximately 0.5% or more of sediment to create two phase colloidal mixture, adsorbing the set of impurities onto the sediments, and separating the sediment from the resultant product. After separation of the two phases, the sediment contains impurities such as fusel oil, and yields a clear liquid final product suitable for consumption without additional purification.
In the detailed description presented below, reference will be made to the following drawing.
Referring to
Method 100 begins at step 101, where a spirit base is provided. In a preferred embodiment, the spirit base is any alcohol suitable for human consumption having at least eighty percent (80%) alcohol by volume (160 proof in the United States), that is mixed with equal amounts of a water solution as described below. For example, the spirit base is a clear high point alcohol such as vodka, rum, gin, or tequila. The components for a spirit base having at least eighty percent (80%) alcohol by volume is described in Table 1 below.
At step 102, a water solution is provided. In a preferred embodiment, the water solution is a mixture of water and honey in the amounts described in Table 2 on the following page.
In a preferred embodiment, the water solution includes approximately up to and including 96% water by volume, approximately 4% or more of honey by volume.
At step 103, a herbal extract is provided. In a preferred embodiment, the set of extracts is extract of walnut dividers, or also known as the partition. The walnut divider is the portion inside of the walnut shell that separates the kernel or “meat” inside the walnut shell. In other embodiments, the set of extracts is a set of fruit extracts that include any number of desired fruits and/or plants. For example, pineapple, or hot pepper extract (for example Pimiento roja.), or various herbs (for example anise) extract. Any type of fruit extract may be employed as desired. In other embodiments, a set of herbal extracts is employed. In a preferred embodiment, the set of herbal extracts is tincture extracts. Other known herbal extracts may be employed as desired.
At step 104, a sugar is provided. In a preferred embodiment, the sugar is ordinary granulated sugar.
At step 105, the water solution is mixed with the spirit base at a ratio of approximately fifty percent (50%) water solution by volume to approximately fifty percent (50%) spirit base. This step is performed using any suitable mixing equipment known in the art. In a preferred embodiment, the mixture of the water solution and the spirit base has an alcohol content of approximately forty percent (40%) alcohol by volume (80 proof in the United States). In a preferred embodiment, the mixture of the water solution and the spirit base is agitated for approximately one (1) hour.
At step 106, the herbal extracts are added to to the mixture of the water solution and the spirit base. In a preferred embodiment, approximately one percent (1%) or more of a set of extracts by volume is added to the resultant product.
At step 107, the sugar is added to the mixture of the water solution, spirit base, and herbal extract for sedimentation. This step is performed using any suitable mixing equipment known in the art. In one embodiment, approximately 4% or more of sugar by volume is added to the mixture. In this embodiment, the mixture of the water solution and the spirit base is agitated continuously for approximately twenty-four (24) hours or until the sugar dissolves.
At step 108, sedimentation occurs and sediment forms in the mixture of the water solution and spirit base. In this step, impurities such as fusel oil are adsorbed on the sediment as it forms. In a preferred embodiment, the sedimentation process takes place over one or more weeks.
At step 109, the sediment is separated by pouring off the liquid, leaving behind the sediment. This sediment can be used to catalyze further sedimentation in the purification process.
Method 200 begins at step 201, where a spirit base is provided. In a preferred embodiment, the spirit base is any alcohol suitable for human consumption having at least eighty percent (80%) alcohol by volume (160 proof in the United States), that is mixed with equal amounts of a water solution as described below. For example, the spirit base is a clear high point alcohol such as vodka, rum, gin, or tequila. The components for a spirit base having at least eighty percent (80%) alcohol by volume is described in Table 3 on the following page.
At step 202, a water solution is provided. In a preferred embodiment, the
water solution is a mixture of water and honey in the amounts described in Table 4 below.
In a preferred embodiment, the water solution includes approximately up to and including 96% water by volume, approximately 4% or more of honey by volume.
At step 203, a herbal extract is provided. In a preferred embodiment, the set of extracts is extract of walnut dividers, or also known as the partition. The walnut divider is the portion inside of the walnut shell that separates the kernel or “meat” inside the walnut shell. In other embodiments, the set of extracts is a set of fruit extracts that include any number of desired fruits and/or plants. For example, pineapple, or hot pepper extract (for example Pimiento roja.), or various herbs (for example anise) extract. Any type of fruit extract may be employed as desired. In other embodiments, a set of herbal extracts is employed. In a preferred embodiment, the set of herbal extracts is tincture extracts. Other known herbal extracts may be employed as desired.
At step 204, a sugar is provided. In a preferred embodiment, the sugar is ordinary granulated sugar.
At step 205, the water solution is mixed with the spirit base at a ratio of approximately fifty percent (50%) water solution by volume to approximately fifty percent (50%) spirit base. This step is performed using any suitable mixing equipment known in the art. In a preferred embodiment, the mixture of the water solution and the spirit base has an alcohol content of approximately forty percent (40%) alcohol by volume (80 proof in the United States). In a preferred embodiment, the mixture of the water solution and the spirit base is agitated for approximately one (1) hour.
At step 206, the herbal extracts are added to to the mixture of the water solution and the spirit base. In a preferred embodiment, approximately one percent (1%) or more of a set of extracts by volume is added to the resultant product.
At step 207, the sugar is added to the mixture of the water solution and the spirit base for sedimentation. This step is performed using any suitable mixing equipment known in the art. In one embodiment, approximately 4% or more of sugar by volume is added to the mixture.
At step 208, approximately 0.5% or more per unit volume of sediment, obtained through Method 100 or through Method 200, is added, and the mixture is agitated to suspend the sediment in the mixture for efficient separation. This creates a colloidal mixture which catalyzes sedimentation. This step is performed using any suitable mixing equipment known in the art. In one embodiment, the mixture is agitated continuously for approximately twenty-four (24) hours or until the sugar dissolves.
At step 209, sedimentation occurs and sediment forms in the mixture of the water solution and spirit base. In this step, impurities such as fusel oil are adsorbed on the sediment. In a preferred embodiment, the sedimentation process takes place for approximately one day, depending on how long it takes for the sediment to fully separate out.
At step 210, the sediment is separated from the resultant product by pouring off the liquid, leaving behind the sediment. The resultant product has been purified and impurities such as fusel oil removed from the resultant product. The extracted sediment can then be further used to catalyze sedimentation of further execution of Method 200.
It will be appreciated by those skilled in the art that modifications can be made to the embodiments disclosed and remain within the inventive concept. Therefore, this invention is not limited to the specific embodiments disclosed, but is intended to cover changes within the scope and spirit of the claims.
This application is a continuation in part application of U.S. application Ser. No. 17/988,437, filed Nov. 16, 2022, which is a continuation U.S. application Ser. No. 16/409,160, filed May 10, 2019, which claims priority to U.S. Provisional Application No. 62/670,356, filed May 11, 2018. Each of these patent applications is incorporated herein by reference in its entirety to provide continuity of disclosure.
Number | Date | Country | |
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Parent | 16409160 | May 2019 | US |
Child | 17988437 | US |
Number | Date | Country | |
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Parent | 17988437 | Nov 2022 | US |
Child | 18481885 | US |