The present disclosure relates to methods for calibrating one or more heat sources in an apparatus for the layer-by-layer manufacture of three-dimensional (3D) objects from particulate material. A controller and an apparatus for applying the methods are also disclosed as well as a resulting test part.
In applications for forming 3D objects from particulate material, such as so-called “print and sinter” and laser sintering processes, an object is formed layer-by-layer from particulate material that is spread in successive layers across a build bed. Each successive layer of the object is melted or partially melted to fuse or sinter the particulate material over defined regions and in so doing to consolidate it, in order to form a cross section of the 3D object. In the context of particulate polymer materials for example, the process of melting achieves fusion of particles. Such a process requires accurate temperature control over the temperature of the surface that is being processed to achieve high-quality uniform objects with well-defined properties. Temperature control requires use of a thermal sensor, such as a pyrometer or thermal camera, that detects the temperature of the build bed surface. For reliable process control from build to build or between different apparatus, it is desirable to calibrate the input power to the heat sources that contribute to the thermal control of the layer surface. Such heat sources may be infrared bar heaters moved over the build bed surface to heat the particulate material in different power modes. For example, the build process may comprise a preheat step during which the particulate material reaches a temperature near to but below the melting point, and a fuse step during which the material is heated enough so that it melts. The input power of the one or more heat sources that provide these two heating steps requires calibration against a reference such that the desired temperatures are achieved. This for example ensures that fusing occurs as intended. Furthermore, significant temperature differentials may be prevented to subsist or at least be reduced between fused and unfused areas. In the case where two or more different heat sources, or different modes of the same heat source, are used to heat the particulate material, it is desirable to calibrate the power of the sources with respect to one another or with respect to different modes. This adjusts for variability in heat source performance that otherwise causes uncontrollable differences of heating of the layer surface, which in turn causes poor control over object properties. Known methods use a thermal sensor to calibrate heating effects of one or more heat sources on the build bed surface by measuring the temperature of individual regions heated by operating a respective heat source above them at different powers. It was found that such known techniques are however not adequate and frequently lead to unexpected variation in a subsequent build process. It is an object of the present invention to reduce or eliminate such variation by providing improved calibration techniques.
Aspects of the invention are set out in the appended independent claims, while particular embodiments of the invention are set out in the appended dependent claims.
The following disclosure describes, in one aspect, a method for calibrating one or more heat sources in an apparatus for the layer by layer manufacture of a 3D object from particulate material is disclosed, the apparatus comprising at least one heat source and a thermal sensor; the method comprising the layer cycle steps of:
(a) distributing a layer of particulate material over a build bed, the layer providing a build bed surface of the build bed;
(b) heating the build bed surface by operating a first heat source at a first power input over a first period of time, the build bed surface comprising a first region;
(c) measuring a first temperature of the first region using the thermal sensor;
(d) depositing a first amount of absorption modifier in the form of radiation absorber over the first region within the build bed surface; and/or depositing a first amount of absorption modifier in the form of absorption inhibitor over a surrounding area surrounding the first region;
(e) heating the first region, and a second region within the surrounding area, by operating the first heat source or a second heat source at a second power input over a second period of time; and
(f) measuring with the thermal sensor a second temperature of the first region and a third temperature of the second region, wherein the first amount of absorption modifier causes the second temperature to be higher than the third temperature; and
In a second aspect, a method for calibrating one or more heat sources in an apparatus for the layer by layer manufacture of a 3D object from particulate material is disclosed, the apparatus comprising at least one heat source and a thermal sensor; the method comprising: the layer cycle steps of:
(a) distributing a layer of particulate material over a build bed, the layer providing a build bed surface of the build bed;
(b) heating the build bed surface by operating a first heat source at a first power input over a first period of time, the build bed surface comprising a first region;
(c) measuring a first temperature of the first region using the thermal sensor;
(d) depositing a first amount of absorption modifier in form of radiation absorber over the first region and a second amount of absorption modifier over a second region; and/or depositing a first amount of absorption modifier in form of absorption inhibitor over a surrounding area surrounding the first region and a second region and depositing a second amount of absorption modifier in form of absorption inhibitor over the second region;
(e) heating the first region and the second region by operating the first heat source or a second heat source at a second power input over a second period of time; and
(f) measuring with the thermal sensor a second temperature, of the first region, and a third temperature of the second region; wherein the first amount and the second amount of absorption modifier causes the second temperature to be higher than the third temperature and the third temperature to be higher than the temperature of the surrounding area after the step (e) of heating; and
Reference is now directed to the drawings, in which:
In the drawings, like elements are indicated by like reference numerals throughout.
Methods according to the invention for calibrating one or more heat sources in a 3D printing apparatus, an associated apparatus and controller therefor, and a resulting test part, will now be described with reference to
Modules for distributing the particulate material and processing the formed layer are provided on one or more carriages that are moveable across the layer. Accordingly, for illustrative purposes,
A heat source L2 is provided on the carriage 30_2 to heat the region 50 following deposition of the radiation absorbing fluid. The selectivity of preferentially heating the region 50 versus the surrounding area is achieved by providing the heat source L2 with a spectrum of radiation that at least partially overlaps with the absorption spectrum of radiation absorbing fluid but that is not significantly absorbed by the particulate material alone. The radiation-absorbing fluid thus may absorb radiation readily from the first heat source and selectively heat the particulate material it is in thermal contact with (i.e. over the region 50) preferentially over that of the surrounding area. If the combination of absorber amount and power input to first heat source (causing a certain energy input to the region 50) is sufficient, the particulate material of region 50 will, for example, melt/sinter to fuse and form a region 50 of consolidated particulate material. Thus, during a build process of an object, the radiation-absorbing fluid may be deposited over selected portions of the build bed surface 12 so as to define the cross sections of the object over successive layers. During a calibration process, the region 50 may be a section of a test part processed for measurement purposes. During a build process, the region 50 may represent a cross section of an object to be built. The test part may be a single test part in which the different layers may have different visual shades due to changes in the pairs of input powers causing different levels of fusion. In addition, the test part may have different visual shades in the plane of each layer, due to different (first and second) regions having different (first and second) respective amounts of radiation absorber.
In some apparatus, and as exemplified in the apparatus 1 of
The two heat sources will in the following be referred to as “first heat source” L1, which is used to heat the newly distributed particulate material, and “second heat source” L2, which is used to heat the region 50 following deposition of absorption modifier. Providing a further moveable first heat source L1 may be an effective way of returning, or preheating, the temperature of the new and much colder layer (compared to the previous, processed layer) back towards a target build bed temperature. The target temperature may be a predefined temperature that is lower than a melting point and higher than a solidification temperature of the particulate material. This may be done in combination with or in addition to operating the stationary overhead heater 20 provided above the build bed surface 12. The first and second heat sources may be elongate infrared bar heaters, and each may perform differently at identical power inputs due to manufacturing variability or changes in performance as a result of ageing. To adequately control the required heating processes provided by the first and second heat sources L1, L2 therefore, it is necessary to align the performance of the heat sources with respect to one another. If adequately controlled, it may be ensured that the region 50 will consolidate as expected during an object build process, and large temperature differentials between fused and unfused areas may be prevented by operating the first heat source L1 at appropriate power inputs throughout the layer cycle, such that warping or curl of the fused regions may be avoided. This provides reliable control over mechanical and visual properties of a finished object. Furthermore, any subsequent calibration routine relying on the two heat sources may be improved in accuracy of its output, such as a subsequent thermal camera calibration routine.
The inventor has discovered improved methods for calibrating a one or more heat sources in an apparatus for the layer by layer manufacture of a 3D object from particulate material, the apparatus comprising at least one heat source and a thermal sensor; wherein a first method comprises: the layer cycle steps of:
Next, the layer cycle according to the method of the invention is carried out two or more times, each layer cycle using a respective pair of first and second input powers applied to the heat sources L1, L2, wherein each said pair is different to the preceding pairs by at least one of the first and second input powers. From the measured first, second and third temperatures for each layer to which a corresponding pair of input powers was applied, an adjusted input power for at least one of: the first and second heat sources, or the respective steps (b) and (d) of heating when carried out by the first heat source, is determined, so as to calibrate the performance of the first heat source, or of the first and second heat source, at step (b) of heating with respect to step (e) of heating. The adjusted input power(s) may then be applied during the layer cycle of any subsequent process, for example a calibration process for the thermal sensor, or a subsequent build process for an object during a subsequent layer cycle.
In a second method according to the invention, alternatively to the first method, the second region 50_2 may be provided with a second amount of absorption modifier, wherein the surrounding area further surrounds the second region. Where a second amount of absorption modifier is used in addition to the first amount, the temperature measurements of the second region 50_2 may be more accurate, and lead to improved accuracy in determining the adjusted input powers. In this case, the step of depositing comprises depositing either a first amount over the first region 50_1 and a second amount of over a second region 50_2 when the absorption modifier is radiation absorber; and/or, depositing a first amount over a surrounding area surrounding the first region 50_1 and the second region 50_2, and depositing a second amount of absorption modifier over the second region 50_2, when the absorption modifier is absorption inhibitor. The first amount and the second amount of absorption modifier are such that they cause the second temperature T2 to be higher than the third temperature T3, and the third temperature T3 to be higher than the temperature of the surrounding area after the step of heating the first region 50_1 and a second region 50_2 with the second heat source L2, or with the first heat source L1, at the second input power profile. The second amount may thus cause a moderate level of absorption over the second region compared to the first, while the surrounding area is the least absorbing. It is thus not essential that the first region 50_1 is void of inhibitor; instead, the first region may have a third amount of absorption inhibitor deposited over it that is chosen such that the first region still absorbs the highest amount of energy from the second heat source L2. The different amounts of absorption modifier may be achieved in different ways, as will be explained in more detail below. As in the first method, from the measured first, second and third temperatures for each layer to which a corresponding pair of input powers was applied, an adjusted input power for at least one of: the first and second heat sources L1, L2, or the respective steps (b) and (d) of heating when carried out by the first heat source L1, is determined, so as to calibrate the performance of the first heat source L1, or of the first and second heat source L1, L2, at step (b) of heating with respect to step (e) of heating. The adjusted input power(s) may then be applied during the layer cycle of any subsequent process, for example a calibration process for the thermal sensor, or a subsequent build process for an object during a subsequent layer cycle.
The adjusted input power(s) may thus be chosen to narrow a performance difference between the two heat sources and to normalise, or calibrate, their performance with respect to one another. This may be necessary where the two heat sources provide significantly different levels of output power for the same input power. The adjusted input power may for example be determined such that a predetermined temperature difference between the two steps of heating is achieved, for example one of the adjusted power input of the first step of heating may be determined based on the adjusted power input of the second step of heating. Furthermore, the adjusted input power may be such as to limit the duty cycle to the heat sources to below a predefined maximum, and the other. The predetermined temperature difference may be obtained from experimental results for the mechanical and/or aesthetic properties of test objects, for example. For each method, the adjusted first and/or second input powers may be applied to the respective steps of heating for a subsequent layer cycle, so as to operate the first heat source (or the first and second heat source) at calibrated input powers. The input power referred to herein may also be referred to as “input power profile” to indicate a power level applied along at least one dimension of the build bed surface 12, for example in direction of movement of the first and/or second heat source. The input power profile may be a constant input power profile, or an input power profile that varies along the direction of movement, i.e. with distance over the build bed surface 12. The radiation of the first and second heat sources L1, L2 may preferably be infrared radiation, preferably comprising near infrared radiation, and the absorption modifier in general terms may be arranged to cause each region 50_n to heat up more than the surrounding area. An infrared radiation absorber, or absorber, may be carbon black. An absorption inhibitor, or inhibitor, may be water acting as a coolant, or a reflector of the radiation of the second or first heat source L2, L1. However, other wavelength spectra may be suitable in combination with respective absorption modifiers and particulate materials. In some examples, both types of absorption modifier may be provided to achieve the desired selectivity and degree of absorption of radiation from the second heat source L2 by the first and second regions.
In the following, the methods are described with reference to the preferred method comprising a second amount of absorption modifier deposited over the second region 50_2. However alternative variants may easily be envisaged for which only the first amount is deposited over the first region 50_1 (or over the surrounding area surrounding the first region 50_1, in the case of inhibitor). The further features of the variants described herein apply equally to either method. The method is further illustrated in
At block 102, a new layer of particulate material is distributed by distribution module 32 (in the form of a roller, in this example) to form the new build bed surface 12, and at block 104 the build bed surface 12 comprising the first region 50_1 is heated with the first heat source L1. These blocks correspond to
At block 106, the thermal sensor 72 is used to measure the first temperature T1 of the first region 50_1 following heating at block 104, as illustrated in
At block 108A, the first amount of absorber is deposited over the first region 50_1. Preferably, also a second amount of absorber is deposited over the second region 50_2, following which, at block 110, the first and second regions 50_1, and 50_2 are heated by the second heat source L2 while it is operated at a second input power P2. Where the second amount of absorber (or generally, absorption modifier) is deposited, the surrounding area surrounds both the first and second regions.
Finally, at block 112, and as illustrated in
As
Furthermore, each layer may comprise a plurality of sublayers, wherein each sublayer is processed according to the same layer cycle steps for that layer. A respective average temperature is determined for the first, second and third temperature T1, T2, T3 from one or more of the plurality of sublayers. Over, for example, the first few sublayers of a calibration routine layer cycle, thermal stability may be achieved and consequently any measurements for these first few sublayers may be discarded or ignored, and for the remaining sublayers, a respective average temperature is determined for that layer. In such a case, the adjusted input power for at least one of the first and second heat sources L1, L2 is determined from the respective average first, second and third temperatures T1, T2, T3.
Power, Pairs of Power Inputs.
The heating effect by each of the first and second heat sources L1, L2 is determined by factors including the input power to each heat source. Throughout the layer cycle of the first layer of the calibration method, the first heat source L1 is operated at a power P1_1 and the second heat source L2 is operated at a power P2_1. These conditions remain the same for any sublayers comprised within that layer. Throughout the layer cycle of the second layer of the calibration method, the first heat source is operated at a power P1_2 and the second heat source is operated at a power P2_2. These conditions again remain the same for any sublayers comprised within that layer. Throughout the layer cycle of the third layer of the calibration method, the first heat source is operated at a power P1_3 and the second heat source is operated at a power P2_3. Thus three pairs of first and second input powers (P1_1, P2_1), (P1_2, P2_2) and (P1_3, P2_3) are applied in turn, wherein each pair differs from another pair by at least one of the power inputs. The first power and the second power may be the same for at least one of the pairs. These conditions also remain the same for any sublayers comprised within that layer. The first heat source L1 may be used as a preheat source in the apparatus 1 for any subsequent build process. In apparatus variants, the first heat source L1 may instead be arranged so as to provide a second heating step following that of the second heat source L2. In other words, the two heat sources L1, L2 may subsequently be required to be operated to provide very different energy outputs, or similar energy outputs. The three pairs of power inputs may thus span input powers for which preheat and fuse modes may be achieved. For example a fuse mode may be achieved by operating the heat source (for example the second heat source L2) at a high input power, such as 100% duty cycle, and a preheat mode may be achieved by operating the heat source (for example the first heat source L1) at a medium or low input power, such as 70%-50% duty cycle. The three pairs of power inputs may for example be arranged with input power levels (high, high), (medium, high), (low, medium). These power inputs may cause three sets of first, second and third temperatures T1, T2, T3, which allow a determination of an adjustment to one or both of the two heat sources L1, L2.
In some apparatus, the first and second heat sources L1, L2 may be the same, single heat source operated in different ‘modes’, i.e. a preheat mode and a fuse mode. This might require that the same heat source is calibrated against two different modes of operation, represented by very different power inputs, for example, following the procedure as described. For other variants of the apparatus, further moveable heat sources, such as a further second heat source L2_2 following the second heat source L2, the two heat sources may be treated as a single heat source operated at additional pairs of power inputs, such that for each layer the heat sources are operated at respective set of three power inputs (P1, P2, P3) per layer: the first heat source, during the step of heating the first region 50_1, is operated at power P1 as before, and the first and second heat sources L2, L2_2 are operated during the step of heating the first and second regions 50_150_2 at respective power inputs P2, P3. Similarly, where the further heat source is a further first heat source L1_2, for each layer the heat sources are operated at respective set of three power inputs (P1, P2, P3) per layer such that the first heat source L1 and further first heat source L1_2 are operated at powers P1 and P3 during the step of heating the first region 50_1, and the second heat source L2 is operated at power input P2 during the step of heating the first and second regions 50_1, 50_2. In each case, the steps of measuring the first second and third temperature T1, T2, T3 remain the same. The first second and third temperatures T1, T2, T3 measured according to the methods disclosed herein thus allow the determination of an adjustment for the input power to one or both (or any further) of the heat sources that takes into account the heating effect of both first and second (and optionally further) heat sources within the same layer.
First Amount and Second Amount of Absorption Modifier
As described above, a preferred method comprises depositing a first and second amount of absorption modifier, such that the temperatures may be measured with improved accuracy. The second and third temperatures T2, T3 are the result of modifying the absorption differentially between the first and second regions, and between the surrounding area within the build bed surface 12 of the same layer. In the methods disclosed herein furthermore, the speed of the heat sources and the input power over the respective heating steps of the same layer cycle need not be altered so as to achieve the three temperatures T1, T2 and T3. Such changes within the same layer cycle are not preferred since they may lead to unknown variation in heating significant enough to compromise determination of the first, second and third temperatures T1, T2, T3, and thus the reliability of the calibrated input powers.
The absorptive properties of the first and second regions 50_1 and 50_2 may be altered by changing the amount of absorption modifier applied from the first to the second region by one or more of the following:
The absorption modifiers may comprise different colours capable of absorbing or inhibiting a different amount of energy of the radiation spectrum of the second heat source L2. Multiple fluids provided to the apparatus may be deposited in an overlapping multi-fluid pattern to vary the absorption of the energy of the radiation provided by the second heat source L2. The radiation absorber (or absorption modifier) may be deposited in the form of a multi-fluid pattern, wherein the multi-fluid pattern is deposited over the first and second regions 50_1 and 50_2.
In order for the thermal sensor 72 to be able to measure the temperature of the first region 50_1 following heating by the first heat source L1, and to measure the temperature of the first region 50_1 and the second region 50_2 following heating with the second heat source L2, the regions must necessarily be within the field of view of the thermal sensor 72 at the required timing during the layer cycle. From
Furthermore, with reference to
In a preferred method, the steps of heating comprise heating the entire build bed surface 12 comprising the layer-specific region 50. This means that the thermal processes are applied across the entirety of the build bed surface 12, for example by operating the first and second heat sources L1, L2 for at least the duration over which they pass over the build bed surface 12. The thermal stability of the layer cycle may further, or instead, be improved when the calibration methods apply any one, or any combination of, and preferably all, of the following, to the layer cycle disclosed herein, and which may further preferably also apply to the layer cycle of a subsequent layer cycle, such as that of a calibration method for the thermal sensor, or to a build process:
the steps of distributing each layer at block 102 and of passing the first and the second heat source L1, L2 over the first and second regions 50_1, 50_2 at blocks 104 and 110 may be carried out in the same direction; optionally also the step of depositing radiation absorber at block 108A (and optionally at block 108B) is carried out by moving the deposition module 38 in that same direction.
It may be desirable for the layer cycle of the calibration methods to closely resemble that of a subsequent calibration or build process. For example, it may be preferable that significant thermal events of the layer cycle are substantially, or at least predominantly, the same for both the calibration and the build process. In preferred variants of the method, respective time periods between the initiation of two steps, and preferably between each step and the previous step, for each layer cycle remains the same for each corresponding step in each successive layer cycle. A preferred variant may for example comprise initiating the step at block 102 of distributing each further layer after a first time interval following initiating the step at block 110 of heating each layer; and initiating the step at block 110 of heating the first and second regions with the second heat source L2 after a second time interval from the step at block 102 of distributing the layer; preferably wherein the respective first and the second time interval is the same for each layer. This means that the return movements of the heat sources, distribution module and the deposition module are preferably also time controlled and remain the same for each layer.
Furthermore, for each layer, the layer cycle may comprise initiating the step at block 110 of heating each layer with the second heat source L2 after a third time interval from initiating the step at block 104 of heating with the first heat source L1. Additionally, or instead, the layer cycle may comprise initiating the step at block 104 of heating each layer with the first heat source L1 after a further time interval from initiating the step at block 102 of distributing each layer. Still further, the respective first, second, third and/or further time interval may be the same for each layer such that the duration of time of each layer cycle is substantially constant throughout the calibration method. Optionally, the step of depositing absorption modifier over the plurality of regions 50_n for each layer at block 108A/108B (typically carried out synchronously and/or in a single step) may be initiated after a fourth time interval following initiating the step of heating with the first heat source at block 104, wherein the fourth time interval is the same for each layer. However, this step may be considered, in most processes, a less significant thermal event of the layer cycle.
A preferred layer cycle according to the above is further illustrated in
In
The first heat source L1 (in analogy to
In
In
In
In
From these illustrations it can be seen that location A2 experiences the event of heating with the second heat source L2 after a fixed third time interval Δt3 of heating with the first heat source L1. Location A1 near the far end of the build bed surface 12 also experiences the event of heating with the second heat source L2 after a fixed third time interval Δt3 of heating with the first heat source L1. The second time interval and the fourth time interval are fixed as long as the speed v1 is constant, since these time intervals are determined by the respective distance between the distribution module and the first heat source L1, or between the deposition module and the second heat source, and speed v1. In this way, the duration of time of the layer cycle may be substantially the same for each layer. It has been found that this provides for an improved stable thermal cycle and for a more reliable build process when these layer cycle conditions are equally applied to the calibration process. In this way, each location on the build bed surface 12 experiences the same layer cycle steps after the same respective time intervals and for the same respective durations, providing a stable and consistent layer cycle. The same considerations apply for any location of the first and second regions and for an object cross section during a subsequent build process.
The adjusted input power profiles may be determined based on a predefined temperature difference to be achieved between the measured temperatures of a region preheated at a first adjusted power input P1′ at a block 104 following distribution, and next heated at a second adjusted input power profile P2′ at a block 110 following deposition, of for example radiation absorber. Such as condition contributes to the shape of the desired thermal cycle for example. Furthermore, the adjusted input power profiles P1′, P2′ may be determined by limiting them to a below a threshold input power that is below the maximum input to the first (and/or second) heat source L1 (L1, L2).
Third Heat Source Considerations and Effect on Calibration Process
The apparatus 1 may comprise a third heat source 20 arranged stationary above the build bed surface 12, such as the overhead heater 20 in
The first and second regions 50_1, 50_2 may be located at any location over the build bed surface 12, for example in the form of two rectangular regions side by side and arranged perpendicular or parallel to the process direction along x. A plurality of first and second regions 50_1, 50_2 may be provided over different locations of the build bed surface 12. After the completion of the calibration method, i.e. after at least three layer cycles, the processed first and second regions form one or more test objects that may be removed and discarded from the completed build after depowdering.
It should be noted that it is not necessary to immediately proceed from one layer of the layer cycle described herein to the next layer of the calibration method. In addition, a number of unprocessed, blank layers may be distributed without the steps of, for example, depositing absorption modifier and heating with the second heat source L2, such that one or more intermediate layer cycles are applied that are different to the layer cycle of the disclosed calibration method.
The methods and their variants as described may be carried out in part or fully by a controller 70 of the apparatus 1. The controller 70 may for example be configured to control any one or more of the power inputs P1, P2 to the first and second heat sources L1, L2, and to the third heat source 20, the movement of the carriages 30_1, 30_2, the various time intervals between the initiation of the layer cycle steps, and to apply the adjusted input power profiles of the first and/or second heat source L1, L2 during a subsequent process, such as a calibration process for the thermal sensor 72 and/or a build process for a 3D object. A possible sequence of processes is illustrated the flow chart of
Number | Date | Country | Kind |
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2112998.6 | Sep 2021 | GB | national |