This application is related to the application entitled “Multi-Functional NMR Probe” by Albert P. Zens and James P. Finnigan, which application is being filed on the same date as the present application and is assigned to the assignee of the present application.
The present work is directed to variable capacitor structure and usage particularly optimized for achieving a capacitance value approaching zero at one extreme.
Capacitance coupling between RF circuits comprises a reactive impedance inversely proportional to the product of frequency and capacitance. This reactive impedance component exhibits a frequency dependence, the reactance approaches infinity as the capacitance approaches zero. In situations where a resistive or inductive component can be neglected, the variable coupling capacitor has the properties of an RF switch, imperfect only insofar as determined by the minimum achievable capacitance. Reference to such switch is understood most simply in this context as a functional 2 state device, ignoring intermediate values of capacitance. In other applications, the continuous range of capacitance values is desirable for traditional functions such as the tuning and matching of a resonant circuit to a transmission line.
Specialization in the application for circuit components is related to the specialized environment for these circuits. Of particular interest herein is the NMR instrument, which imposes constraints on materials for both magnetic properties and for certain chemical properties. Intense magnetic fields of carefully controlled spatial distribution characterize magnetic resonance apparatus requiring components of the instrument to comprise materials that will not compromise that controlled spatial distribution. Depending upon the proximity of the component to the measurement volume, the magnetic susceptibility of the material of the component can be an issue for consideration. The chemical properties of the material may also be critical if the material contains an isotope exhibiting nuclear magnetic resonance in the magnetic fields and frequencies prevailing in the instrument. A prior art NMR probe utilizing adjustable capacitance in an axial geometry close to the NMR measurement volume and realizing adjustment through axial displacement is known and described in U.S. Pat. No. 7,064,549 commonly assigned herewith.
Although the discussion herein is conducted in terms of a cylindrical geometry, no such limitation is intended, and the apparatus of this work may be as easily realized in alternate form.
An adjustable capacitor exhibiting minimal capacitance value at one extreme of adjustment, provides an RF impedance approaching infinity as the minimum capacitance approaches zero, and thereby furnishes the basis for an RF switch when the other extreme furnishes a capacitance value to yield an acceptable dynamic range of impedance. It is quantifiable in relative terms that the minimum capacitance value is very small compared to other relevant capacitances of the circuit in which this RF switch is deployed and inclusive of the relevant parasitic capacitances. This component, suitable for general application and a particular application to coupling/decoupling resonant sub-circuits, is implemented with particular attention to use in NMR probe circuits.
Coaxial silica glass (a preferred class of material) tubes are selected of mutual dimensional tolerance to support at least a slip fit therebetween. This option for materials presents an excellent choice for application in the environment of an NMR instrument and is equally appropriate for general application. For ease of description only, consider an outer tube to support a pair of conductive bands, each band having a selected azimuthal extent and spaced axially apart by an amount such that the capacitance between these conductors is can be neglected in comparison with other capacitances. These conductive bands each comprise a stator forming a pair of series connected capacitances in conjunction with a floating conductor supported by the inner tube on a surface thereof that is (obviously) non-adjacent to the conductors supported by the outer tube (for slip fit coaxial tubes). The outer surface is preferred for support of the stators because the inner surface presents additional complication in electrical access to these stators. For the stators on the outer surface of the outer tube, either inner or outer surface of the inner tube may be selected to support the floating conductor which may be conveniently regarded as a moveable capacitor plate for both capacitors. The choice of inner or outer surface of this tube for conductor support is a choice of dielectric thickness (and possibly of disparate dielectric constants). The axial extent of the floating conductor is sufficient to completely overlap the two stator plates in one position of the device, forming two series connected capacitors. Relative displacement of the (assumed moveable) floating conductor progressively decreases the capacitance of one of the series capacitances and continued relative displacement breaks the series connection of the two capacitors. Further relative displacement may be desirable to reduce parasitic capacitance.
It will be understood that reference herein to the present “capacitor unit” encompasses the integral physical combination of a fixed capacitance in series with a variable capacitance and the termination of the series connection beyond the geometrical position for the minimum value of the variable sub-component. In this work, the reference to a “capacitor” will be understood, in appropriate context to refer to the capacitor unit of fixed and variable sub-components.
Various embodiments are conveniently implemented to realize multiple capacitor units in ganged relationships and/or switch selective relationships.
Silica glass materials, e.g., quartz or sapphire, have no adverse effect in certain contexts such as NMR probes. These materials exhibit a low coefficient of static friction and such tubes are available with excellent dimensional tolerances and high finish to support a fit requiring rather little axial force to provide the relative displacement. This permits a wide choice of linear actuators for operation. In some applications, Teflon® may be a desirable material for one or both tubes.
a illustrates an exploded view of a preferred embodiment of the present work.
b is a section through the embodiment of
c is the electrical description of the embodiment of
a is a variation of
b is the electrical description of
a illustrates a section through a prior art capacitor, typical of the subject.
b is the equivalent circuit for
c illustrates a section through the present adjustable capacitor.
d is the equivalent circuit for
a is an exploded view of a dual/ganged pair of adjustable capacitors.
b is the equivalent circuit for
e shows a simple ganging arrangement for two capacitors.
The present work will be described with the aid of exemplary drawings for which the same functional component will bear the same label in the several embodiments.
Turning now to
In figure la, inner coaxial tube 42 is driven by actuator 50 and outer tube 40 is secured to the actuator housing by supporting collar and flange 49.
Insertion of moveable floating conducting surface 48 to fully face each of the spaced-apart conductors 46 and 47 results in a pair of series capacitances 48-46 and 48-47 as shown in the capacitor unit of
g>>ε t L,
where ε is the dielectric constant, assumed here to be air. Conductors 46, 47 and 48 may be applied to their respective substrates by appropriate adhesives or by some suitable deposition process.
The description has been drawn to one example of the selection of surface pairs for conductor support. It is emphasized that non-adjacent surfaces are appropriate, and that the inner surface of the outer tube and outer surface of the inner tube are excluded as a pair of surfaces for conductor support, as this particular pair of adjacent surfaces would simply define a purely resistive path unless the component tubes define a controlled gap therebetween. The stators and floating conductor may be supported on the respective substrates through adhesives, or by a deposition process, or by an embedding procedure. Although the inner substrate is referenced herein as a tube, it may be a solid cylinder, with the floating conductor supported on the cylindrical surface, or embedded therein.
The selection of a particular pair of (non-adjacent) surfaces determines the intervening dielectric properties, especially of the tubular material and wall thickness, neither of which are necessarily identical for the present capacitor structure. In the embodiment of
For the present work, silica glass is the preferred class of material. This includes quartz and sapphire and the like. Such material exhibits satisfactory dielectric properties and the relevant surfaces are susceptible to achieving a high finish and excellent dimensional tolerance to reach the desired degree of fit. The coefficients of static and dynamic friction, magnetic susceptibility and (for NMR usage) freedom from 1H and 19F contaminant are excellent desiderata and the coincidence of excellence for each of these properties is gratifying.
A low coefficient of friction permits utility of a wide range of actuator designs. A piston 52 transmits the force realized in actuator 50 to axially displace the (exemplary) inner tube 42. A common form of actuator is realized in a captive nut and threaded shaft where the captive nut is fixed in relation to the movable member, such as tube 42, and the threaded shaft is fixed in relation to the static member, such as tube 40. An example of this common form of rotary to axial actuator suitable for the present application, is commercially available from Maxon Precision Motors, Inc, Fall River, Mass.
In many applications, and particularly for the case of an NMR probe, a piezo actuator is desirable to produce axial displacement such as is required in the present work. Such piezo actuators are also commercially available. One example is the Squiggle® type actuator available from NewScale Technologies, Victor, N.Y. Additionally, such actuators are further described in U.S. Pat. No. 7,061,745.
Elaboration of the embodiment of
a is another embodiment wherein three stators 46, 47 and 47′ together with floating conductor 48, form (at successive displacements of conductor 48) capacitor pairs 46, 48 and 47, 48; followed by 47, 48 and 47′, 48. This is equivalent to a selector mechanism for selection of either pair of stators forming a pair of capacitor units.
The advantages of the present work are best explained with the aid of
C
max
=C
+
+C
s1
C
min
=C
−
+C
s1
In
C
max=[(CA+CB)·(CsA+CsB)]/[(CA·CB)(CsA+CsB)]
and it is reasonable to make a simplification CA=CB and CsA=CsB (a design choice) after which the total capacitance reduces to
½(CA+CsA)
Consider the relative motion of Mf as it disengages from a geometric projection onto Sp1 and the capacitance CA diminishes while CB remains constant until the capacitive disengagement is complete and the series relationship of CA and CB (first term of the above expression) vanishes. The capacity of the (idealized) network is now reduced to stray capacity Cs1 between the terminal points. For notational convenience assume that Cs1 of
A capacitance similar to that shown in
outertube:o.d.=0.190;i.d.=0.170 length 2.4
innertube:o.d.=0.164;i.d.=0.144 length=2.4
Cmax=1.8 pf Cmin<˜0.01 pf axial displacement=0.7
Measurements were made for comparison of representative prior art and the present capacitor unit incorporated in an NMR probe for which resonances corresponding to both 1H and 19F were observed to obtain observations of performance at respective frequencies. The test circuit is shown at
1H
19F
1H
19F
1H
1H
A comparison of the values for ErBench of the capacitors C3,C4 and C5 of prior art with the present work is interpreted as demonstrating that much less power is required to obtain the same field within the NMR coil.
1H
19F
1H
19F
The parameter PW-90° is the length of the pulse (at constant specified RF power) required to rotate the resonating nuclear spins 90° and this may be taken as a figure of merit for the efficiency of the circuit and here measures the comparison of the capacitors of prior art to components corresponding to the present work. In the test circuit of
The capacitors C3, C4 and C5 of the test circuit of
The test circuit of
The maximum capacitance of C6 is determined by design with the result that the capacitor unit exhibits a dynamic range of about two orders of magnitude.
c illustrates a variation in the embodiment of
Although this invention has been described with reference to particular embodiments and examples, other modifications and variations will occur to those skilled in the art in view of the above teachings. The capacitor unit arrangement disclosed herein is not limited to a particular geometry such as coaxial tubes, and planar substrates and conductors are a straightforward variation of the above described capacitor units. It should be understood that, within the scope of the appended claims, this invention may be practiced otherwise than as specifically described.