The present invention relates to a device and method for mixing a multiphase fluid, as well as a device and a method for measuring physical properties of a multiphase fluid.
This invention is in particular applicable in oil production, for example in the extraction of heavy oils (i.e. with a high viscosity). In this context, there may be a need for PVT data (pressure, volume, and temperature) on the heavy oils under tank conditions so as to better predict their behavior during production.
It is currently impossible to make a multiphase oil-gas mixture rise from a tank under the tank's conditions. In fact, during transport, the gas dissipates in the air. Obtaining a regassed heavy oil sample is thereof an important aim for oil companies today.
The use of magnetic agitation is very widespread in traditional PVT measuring cells. In fact, for traditional fluids, which are therefore not very viscous, i.e. with a viscosity in the vicinity of 10 mPa.s (i.e. 10 milli pascal-seconds), magnetic bars are used driven by a rotary magnetic agitator outside the PVT cell. A similar solution is described in patent WO 2007/027100 with an agitator included in the piston of the PVT cell. A similar solution is also described in the article “Reservoir Fluid Analysis using PVT Express” by I. A. Kahn, K. McAndrews, J. P. Jose, and A. K. M. Jamaluddin.
However, these solutions are not suitable in the case of heavy oil because of the high viscosity (of the heavy oil phase) of the fluid to be mixed. Indeed, for a fluid with a viscosity of about 10,000 mPa.s, i.e. 10 Pa.s (e.g. for temperatures of about 0° C. to 100° C., and/or a pressure of between 1 and 200 bar), different problems can emerge, e.g. dead volumes or too weak agitating force.
At this time, a manual and time-consuming technique is therefore used to mix heavy oil+gas. This technique involves injecting the gas into the oil and waiting for homogenization of the mixture. The manipulations consist of changing the orientation of the cell in order bring gravity into play. To identify complete homogenization, the pressure prevailing in the PVT cell is observed. It decreases during the homogenization phase, then stabilizes when the gas is dissolved in the mixture. This wait can last several weeks, as heavy oils have very low diffusivity coefficients, the order of 10−10 m2.s−1. There is therefore a need for an improved method of mixing a multiphase fluid.
To that end, the invention proposes a device for mixing a multiphase fluid comprising a mixing chamber; a mixing element translatable along a central axis of the mixing chamber, the distance between a point of the inner surface of the mixing chamber and the central axis being occupied between 85% and 95% by the mixing element along at least one section transverse to the central axis. According to examples, the mixing device can comprise one or more of the following features:
The invention also proposes a device for measuring physical properties of a multiphase fluid, comprising the above mixing device; means for measuring physical properties of the fluid. According to examples, the measuring device can comprise one or more of the following features:
According to examples, the mixing method can comprise one or more of the following features:
Other features and advantages of the invention will appear upon reading the following detailed description of embodiments of the invention, provided solely as an example and in reference to the drawings, which show:
The invention relates to a device for mixing a multiphase fluid. The mixing device comprises a mixing chamber and a mixing element. The mixing element is translatable along a central axis of the mixing chamber. Along at least one section of the mixing element transverse to the axis, the distance between a point of the inner surface of the mixing chamber and the central axis is occupied between 85% and 95% by the mixing element. This mixing device allows faster mixing of a multiphase fluid, in particular when one of the phases has a high viscosity.
The mixing element being translatable, it generally undergoes fewer stresses than in a system with a rotary agitator. In this way, the device is adapted to a multiphase fluid comprising a viscous phase, as the device requires less force for the mobility of the mixing element. The mixing element can in particular have a penetrating front profile and a penetrating rear profile. This further decreases the stresses undergone during mixing and, as a result, the force required to perform the mixing. A penetrating profile designates a monotonous (decreasing) section of the mixing element along the central axis, starting from the central section of the mixer toward the front and back exteriors. In this way, each half (front and rear) of the mixer can have an apex.
In order to ensure mixing with this translational movement, the distance between a point of the inner surface of the mixing chamber and the central axis is occupied between 85% and 95% by the mixing element along at least one section transverse to the axis. In other words, during use of the mixing device, i.e. when the mixing chamber contains the multiphase fluid and the mixing element is in motion, there is at least one point PS of the inner surface of the chamber projected orthogonally on the central axis at a point PA, the distance between PS and PA being occupied at least 85% and at most 95% by the mixing element. In this way, at least at one moment of the movement, at least one segment joining a point of the inner surface and the axis (that joining PS to PA) is made up between 85% and 95% of the mixing element.
The mixing element therefore has a section close to that of the mixing chamber at such a point PS, which involves a small exchange surface. Having a small exchange surface allows rolling of the multiphase fluid, which allows a better transfer of matter, and therefore a more homogenous mixture. This rolling is even more important when the fluid comprises a viscous phase.
The fact that the proportion of the mixer in the distance is comprised between 85% and 95% makes it possible to ensure good mixing while leaving sufficient mobility for the mixing element. In fact, increasing this ratio causes an increase in the viscous force, which is even more pronounced when the fluid comprises a viscous phase. Thus, at the mixing element, the distance from any point of the surface to the central axis is preferably always occupied by the mixing element in a proportion smaller than 95%.
The mixing device can therefore be used for a mixing method comprising conveying the multiphase fluid into the mixing chamber and translating the mixing element in the fluid along the central axis of the mixing chamber. Such a method ensures homogenous and fast mixing of the multiphase fluid. The fluid can comprise a viscous phase, the viscosity coefficient of which is comprised between 1 and 100 Pa.s, preferably between 1 and 60 Pa.s, preferably between 5 and 15 Pa.s. For example, the viscous phase is heavy oil and the fluid also comprises a gaseous phase. The mixing device then makes it possible to obtain a homogenous heavy oil+gas mixture. In such a case, the device is particularly effective in that it ensures a fast and effective homogenization of the mixture between oil and gas. However, all types of very viscous products can be mixed using the mixing device.
The translation of the mixing element can comprise backward and forward movements, e.g. until the mixture is homogenized. The method can comprise detecting the homogenization, for example by the user (e.g. using his experience), or by pressure and/or viscosity measurements of the mixture. For example, the pressure can be measured by a specific sensor, and/or the viscosity can be measured by measuring an intensity of a motorization of the mixing device, as will be exemplified below in reference to
In the case of a gas+oil fluid, the time and appearance of the drop in pressure can also make it possible to obtain the gas diffusion coefficient in the oil and the behavior of the oil. The evolution of the viscosity can also provide information on the behavior of the oil. The device thus makes it possible to obtain a heavy oil+gas sample that is correctly homogenized as quickly as possible, and potentially to know the properties thereof. It is then possible to perform measurements of physical properties on the homogenized multiphase fluid.
For example, the mixing device can be comprised in a device for measuring physical properties of a multiphase fluid also comprising means for measuring physical properties of the fluid. It is thus possible to measure physical properties of the fluid under tank conditions, i.e. with the different homogenized phases. In particular, the mixing chamber can be a PVT cell. Such a measuring device is particularly useful in the context of a hydrocarbon production method that comprises analyzing a hydrocarbon tank by measuring physical properties of a multiphase fluid sample from the tank. In fact, as indicated above, it is difficult to recover the sample under the tank conditions because the gas dissipates. The mixing device makes it possible to mix the sample to then measure the physical properties thereof, traditionally to perform PVT measurements (Pressure, Volume, Temperature).
Examples of the mixing device and the measuring device will now be discussed in reference to the figures.
In this example, the mixing device 10 is shown partially and in longitudinal cross-section, only a segment of the mixing chamber 14 being illustrated. The mixing chamber 14 is made up of a wall that defines an inner volume 12. The mixing chamber 14 therefore comprises an inner surface S that is the surface of the wall opposite the inner volume 12. The mixing chamber 14 is thus adapted to receive the multiphase fluid in the inner volume 12 so that the latter is mixed. To that end, the mixing device 10 comprises the mixing element 16. As shown in
Along section 22, the distance between a point PS of the inner surface S and the central axis 18 is occupied between 85 and 95% by the mixing element 16. In other words, if one considers the point PA resulting from the orthogonal projection of PS on the axis 18, the distance between PS and PA is occupied between 85 and 95% by the mixing element 16 (
The interstice 19 corresponds to the largest transverse section of the mixing element 16 (i.e. the section occupying the most space inside the mixing chamber 14). In that section, the greatest distance between a point of the inner surface of the mixing chamber 14 and the central axis 18 is occupied between 85% and 95% by the mixing element 16 along at least one section 22 transverse to the central axis 18. In other words, at the mixing element 16, along the central axis 18, at most between 85 and 95% of the distance is occupied by the mixing element 16.
In the example of
The above property is in particular verified if the mixing chamber 14 is generally in a cylindrical shape with radius R and the mixing element 16 has at least one section transverse to the central axis 18 with radius r such that r=k*R, with k comprised between 85% and 95%, as is the case in the example of
The spherical shapes, with half-spheres at the ends of the cylinder, and cylindrical with cones at the ends of the cylinder, have the additional advantage of offering a penetrating profile, as previously discussed. This decreases the stresses undergone by the mixing element 16. The sphere is in particular adapted for the mixing element 16 so as to ensure good penetration in the fluid.
In any case, the mixing chamber 14 can have a shape at its ends that is complementary to the mixing element 16 (the ends are not shown in
The mixing element 16 can be movable by magnetic driving. This leaves more space for the multiphase fluid in the mixing chamber 14 by avoiding adding mechanical driving means therein. The mixing device 10 is also easier to make. In the example of
The mixing chamber 14 is then advantageously made from a non-magnetic material so as to avoid magnetic interference, preferably non-magnetic stainless steel (e.g. INOX 316L) or aluminum. The wall of the mixing chamber 14 can have a limited thickness, preferably smaller than 10 mm, or smaller than 5 mm, advantageously in the vicinity of 3 mm. This allows energy savings, the magnetic field created inside the chamber 14 being less disrupted.
Using software with finite element calculation, we can evaluate the induced magnetic field and thus determine the magnetic force that is exerted on the mixing element 16. With the configuration of
It is observed that the forces obtained with the configuration of
We will now refer to
We will now refer to
Tests have been performed on a prototype of the device 100 with silicone oils with viscosities similar to those of heavy oils. A test was in particular done with an oil at 10,000 mPa.s and another with an oil at 60,000 mPas. The tests were carried out at atmospheric pressure (0.1 MPa) and temperature (25° C.). The tests were conclusive, i.e. the multiphase liquid was thoroughly mixed and the measurements were stable. Tests with the same silicone oils for different pressures (0.1 to 20 MPa) were also performed and have also led to conclusive results.
Number | Date | Country | Kind |
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1152061 | Mar 2011 | FR | national |
This application is a National Phase Entry of International Application No. PCT/EP2012/054392, filed on Mar. 13, 2012, which claims priority to French Patent Application Serial No. 1152061, filed on Mar. 14, 2011, both of which are incorporated by reference herein.
Filing Document | Filing Date | Country | Kind | 371c Date |
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PCT/EP12/54392 | 3/13/2012 | WO | 00 | 9/13/2013 |