1. Field of the Invention
The present invention relates to a planetary ball mill for grinding a matter to be ground, by bringing a mill pot containing grinding medium balls and the matter to be ground into rotation concurrently with revolution.
2. Description of the Related Art
There has been known a planetary ball mill such that revolutional centrifugal forces and rotational centrifugal forces generated in a mill pot (grinding vessel) in rotation during its planetary motion inclusive of rotation and revolution are applied to the matter to be ground and grinding medium balls contained in the mill pot, to cause severe collisions between the matter to be ground and the grinding medium balls, and the matter to be ground is grounded by the resulting compression and shearing.
The planetary ball mill is characterized by an extremely excellent grinding speed owing to the synergistic effect of a high revolutional centrifugal acceleration and a high rotational centrifugal acceleration.
However, the planetary ball mills in the related art have had the following problems. First of all, the planetary ball mill as shown in
In addition, as shown in
The present invention has been made in consideration of the above situations. Accordingly, it is an object of the present invention to provide a planetary ball mill which can be reduced in size and price and which is excellent in grinding efficiency.
In order to attain the above object, according to the present invention, there is provided a planetary ball mill including a revolution turning arm turning about a revolution shaft rotated by a driving force, a mill pot turnably supported on the revolution turning arm through a rotation shaft inclined from the vertical direction toward the side of the revolution shaft, and an outer circumferential pot receiver which is fixedly disposed on the upper side of the revolution turning arm over the whole part of a circumference around the revolution shaft and with which an outer peripheral surface of the mill pot revolving attendantly on the turning of the revolution turning arm makes contact, whereby the mill pot is put into rotation.
The planetary ball mill according to the present invention has a structure in which the mill pot being rotatable and being in revolution makes, under a centrifugal force thereof, contact with the outer circumferential pot receiver so as to be thereby put into a rotating motion. Therefore, there is no need for a large-type transmission gear for putting the mill pot into a rotational motion. Moreover, since the outer circumferential pot receiver bears the centrifugal force in this structure, the bearing for the rotation shaft for the mill pot can also be simplified, permitting reductions in size and cost.
Besides, since the rotation shaft of the mill pot is inclined and the rotating speed of the mill pot put into rotation by the contact between the outer circumferential pot receiver and the mill pot can be set higher than the revolving speed, the grinding medium balls and the matter to be ground in the mill pot are put into fluidization with a tornado motion of climbing up, while spinning at high speed, along the inside surface of the mill pot inclined toward the axis of revolution. As a result, grinding with good fluidity is attained, promising an extremely favorable grinding efficiency.
In the planetary ball mill as above, preferably, the inside bottom of the mill pot has a concaved spherical shape.
Where the inside bottom of the mill pot in the planetary ball mill has a concaved spherical shape, it is ensured that the fluidization with the tornado motion of climbing up, while spinning at high speed, along the inside surface of the mill pot inclined toward the axis of revolution will take place more easily, whereby the grinding efficiency can be enhanced.
In addition, in the planetary ball mill as above, preferably, an inside side wall of the mill pot is provided with a recess.
With the inside side wall of the mill pot provided with the recess, the forces of the grinding medium balls can be concentrated into the recess, so that the grinding efficiency can be enhanced.
Besides, in the planetary ball mill as above, preferably, the part, with which the mill pot makes contact, of the outer circumferential pot receiver has a shape deviated from a locus of revolution around the revolution shaft, and the rotation shaft is supported on the revolution turning arm so as to be swingable relative to the radial direction of a circle centered at the revolution shaft.
This structure ensures that the mill pot is put by a centrifugal force into an oscillating motion while being constantly kept in contact with the outer circumferential pot receiver which has a shape deviated from a locus of revolution. As a result, grinding with good fluidity is attained due to the oscillating motion added to the tornado motion, whereby an extremely high grinding efficiency is promised.
In addition, in the planetary ball mill as above, preferably, an outer peripheral surface, making contact with the outer circumferential pot receiver, of the mill pot has a shape deviated from a circular shape centered at the rotation shaft, and the rotation shaft is supported on the revolution turning arm so as to be swingable relative to the radial direction of a circle centered at the revolution shaft.
Where the mill pot having an outer peripheral surface of a shape deviated from a circular shape is used, the mill pot is put into an oscillating motion by the contact there of with the outer circumferential pot receiver. Therefore, the oscillating motion is added to the tornado motion, so that grinding with good fluidity is achieved, which leads to an extremely high grinding efficiency.
Besides, in the planetary ball mill as above, preferably, the angle of inclination of the rotation shaft from the vertical direction is in the range of 15 to 40 degrees.
Where the angle of inclination of the rotation shaft from the vertical direction is set in the range of 15 to 40 degrees, the tornado motion can be generated effectively.
The planetary ball mill according to the present invention can be reduced in size and price, and is excellent in grinding efficiency.
Now, an embodiment of the planetary ball mill according to the present invention will be described below, but the invention is not to be limited to the following embodiment.
At an outer peripheral portion of the base 101, a hollow cylindrical peripheral wall 140 along an orbit of revolution is provided so as to surround the electric motor 110. A ring-shaped support plate 141 is fixed to the upper end edge of the peripheral wall 140, and the inner circumferential edge of the support plate 141 has a circular shape substantially coinciding with the orbit of revolution. An outer circumferential pot receiver 142 composed of a ring-shaped elastic blank material is attached to the inner circumferential edge of the support plate 141. The outer circumferential pot receiver 142 is disposed fixedly on the upper side of the revolution turning arm 120, over the whole part of the circumference of a circle centered at the revolution shaft (rotating shaft) 111. The inner circumferential edge of the outer circumferential pot receiver 142 is disposed at a position which is located on an orbit of revolution where the outer peripheral surfaces of the mill pots 130 revolving attendant on the turning of the revolution turning arm 120 make contact with the inner circumferential edge and which is minutely spaced from the outer peripheral surfaces of the mill pots 130 being at rest. Examples of the elastic material which can be used to form the outer circumferential pot receiver 142 include synthetic rubbers such as silicone rubbers, urethane rubber, etc. and natural rubber.
Now, operations of the planetary ball mill 100 as above will be described. With the electric motor 110 driven, the rotating shaft 111 of the electric motor 110 rotates, as shown in
In this manner, each of the mill pots 130 is put into the rotating motion about the axis of rotation 133 inclined from the vertical direction, while revolving around the axis of revolution 112; thus, each mill pot 130 performs a planetary motion. In the planetary ball mill 100 according to the present invention, the rotational speed is determined by the ratio of the diameter of the inner circumferential edge, making contact with the mill pots 130, of the outer circumferential pot receiver 142 and the diameter of the outer periphery, making contact with the outer circumferential pot receiver 142, of each mill pot 130. Since the diameter of the inner circumferential edge of the outer circumferential pot receiver 142 is several times as large as the diameter of the outer periphery of each mill pot 130, there is a characteristic feature that the rotational speed is several times as high as the revolutional speed. The ratio of rotational speed to revolutional speed is, for example, from about 2 to about 8. In the planetary ball mills in the related art, for example, the revolutional speed is 2000 rpm, and the rotational speed is 60 rpm; thus, the rotational speed has been by far lower than the revolutional speed.
With the mill pot 130 put into the revolving motion, the matter to be ground P and the grinding medium balls B in the mill pot 130 are strongly pressed against the inside bottom surface and the inside side surface of the mill pot 130 by the revolutional centrifugal acceleration. When the rotational centrifugal acceleration at the rotational speed several times as high as the revolutional speed is additionally exerted, at the inclination angle θ of the rotation shaft 131 of the mill pot 130, the grinding medium balls B and the matter to be ground P climb up, while spinning at high speed, along the inside surface of the mill pot 130 inclined toward the axis of revolution 112, so that they collide against each other while being in the tornado motion. The tornado motion causes a continuous convection motion of the matter to be ground P and the grinding medium balls B. The matter to be ground P is subjected to shearing, grinding, disintegration and dispersion, under the collision with and high compression by the grinding medium balls B, whereby it is converted into a fine powder. Such a grinding mechanism promises grinding with good fluidity and an enhanced grinding efficiency, as compared with a planetary ball mill not having the inclination angle θ.
In addition, the presence of the inclination angle θ ensures that the matter to be ground P and the grinding medium balls B in the mill pot 130 are pressed to the side of the inside bottom surface of the pot body 135, so that they would not rise up to the position of the cap 136. Therefore, the ground powder P would not easily leak through the position of the cap 136.
The inclination angle θ of the axis of rotation 133 from the vertical direction is not particularly limited. It has been empirically confirmed, however, the inclination angle is preferably in the range of 15 to 40 degrees, particularly in the range of 20 to 35 degrees, from the viewpoint of easy occurrence of the tornado motion. It is recognized that it is difficult for the tornado motion to take place when the inclination angle is 45 degrees, though the reason has not yet been elucidated.
In the planetary ball mill 100 according to the present invention, a rotation mechanism is adopted in which the revolving mill pots 130 are pressed against the fixed outer circumferential pot receiver 142 by the revolutional centrifugal force. Since a transmission mechanism such as sprockets and transmission chain is not used in the rotation mechanism, the mechanism is simplified, promising reductions in size and cost. Moreover, a structure is adopted in which the revolutional centrifugal forces of the mill pots 130 are received by the outer circumferential pot receiver 142, so that the revolutional centrifugal forces acting on the mill pots 130 are exerted dispersedly on the bearings 132 and on the outer circumferential pot receiver 142. Therefore, the load on the bearings is lighter, and the mechanism inclusive of the bearings can be simplified, which contributes on reductions in size and cost. Besides, the number of movable parts is small, which is advantageous from the viewpoint of maintenance. The reduced size makes it possible to dispose the planetary ball mill 100 in a thermostat or a freezer, for example; thus, the planetary ball mill 100 can cope with a wide variety of matters to be ground.
As for the operating conditions of the planetary ball mill 100 according to the present invention, for example, the inside volume of the mill pot may be in the range of 100 to 200 ml, the revolutional speed may be 100 to 2000 rpm, and the rotational speed may be 200 to 5000 rpm. In the case where the revolutional speed is 666 rpm, the radius of revolving motion is 126 mm, the rotational speed is 2000 rpm (hence, the ratio of rotational speed to revolutional speed is 3.0), and the rotating vessel inside diameter is 42 mm, the grinding can be performed at a revolutional acceleration of 62 G, a rotational acceleration of 188 G, and a composite acceleration of 250 G.
Examples of use of the planetary ball mill 100 according to the present invention include both dry grinding and wet grinding in pulverization of electronic blank materials, ceramics, metals, etc., cutting of fibers in organism specimens such as soft tissue, etc., extraction pretreatment of soil bacteria DNA, emulsification and dispersion in food, cosmetic and medical fields, production of polymeric toners, etc.
The planetary ball mill 100 according to the present invention can assume various forms, for enhancing the grinding efficiency. For example, a mill pot 130b shown in
In addition, a mill pot 130c shown in
Besides, a mill pot 130d shown in
The grinding by the grinding medium balls B generates a considerable quantity of heat; therefore, a powder weak to heat may be deteriorated by the rise in temperature. In addition, there are matters to be ground which must be ground at low temperatures. On the contrary, grinding under heating may be required in some cases. Therefore, it may be necessary in some cases to cool or heat the mill pots 130 in the planetary ball mill 100 according to the present invention.
The planetary ball mill 100c shown in
Besides, a swing mechanism in which the outer peripheral surface of each mill pot 130e is elliptically shaped, as shown in
While the number of the mill pots is two, and the mill pots are disposed at both ends of the revolution turning arm in the diameter direction, in the above description, the number of mill pots may be three or more, insofar as the mill pots are disposed at positions on equally spaced radial directions from the axis of revolution.
Besides, an anti-slip band composed of an elastic blank material may be provided on the outer peripheral surface of the mill pot.
The planetary ball mill according to the present invention can be reduced in size and price and can pulverize at high speed a variety of matters to be ground, and, therefore, it can be utilized for development of mechanochemical or other novel functional materials.
The present invention is not limited to the details of the above described preferred embodiments. The scope of the invention is defined by the appended claims and all changes and modifications as fall within the equivalence of the scope of the claims are therefore to be embraced by the invention.
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Number | Date | Country | |
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20080197223 A1 | Aug 2008 | US |