PROCESS FOR THE PURIFICATION OF A LIQUID-CRYSTAL MIXTURE

Abstract
In a process for the purification of a liquid-crystal mixture (7), the liquid-crystal mixture (7) is passed through a first electrodialysis cell (2) and a concentrate solution (14) is passed through a second electrodialysis cell (8) which is adjacent to the first electrodialysis cell (2) and is separated by an ion-exchanger membrane (9), and an electric field transverse to a direction of passage of the liquid-crystal mixture (7) through the first electrodialysis cell (2) is generated with the aid of an anode/cathode arrangement (15, 16) arranged outside the electrodialysis cells (2, 8) so that ionised constituents of the liquid-crystal mixture (7) are discharged at the ion-exchanger membrane (9) and removed from the liquid-crystal mixture (7).
Description

The invention relates to a process for the purification of a liquid-crystal mixture.


Liquid-crystal mixtures are fluid substances having crystal-like direction-dependent physical properties which are used, for example, in liquid-crystal displays. Commercially available liquid-crystal mixtures which can advantageously be employed in displays have various components which are mixed with one another in a pre-specified ratio to one another. The properties and advantages of the liquid-crystal mixture that are necessary for the respective application can be achieved specifically by suitable specification of individual components and mixing proportions.


It has been found that even slight contamination of a liquid-crystal mixture can result in the properties of the liquid-crystal mixture that are necessary or desired for the intended application being impaired and economically viable use of a pre-specified liquid-crystal mixture for a particular application being made more difficult or even impossible.


Various purification processes by means of which a liquid-crystal mixture can be purified have therefore been disclosed in practice. The various purification processes are based on different methods. In industrial production and processing processes, mechanical filter processes or the addition and subsequent separation of a sorbent represent purification processes which are frequently employed.


The purification processes known from practice often have only low efficiency for the purification of liquid-crystal mixtures and are nevertheless comparatively expensive.


It is therefore regarded as an object of the present invention to design a process for the purification of a liquid-crystal mixture in such a way that the most efficient purification possible of the liquid-crystal mixture can be carried out as inexpensively and reliably as possible.


This object is achieved in accordance with the invention by a purification process in which the liquid-crystal mixture is passed through a first electrodialysis cell, a concentrate solution is passed through a second electrodialysis cell which is adjacent to the first electrodialysis cell and is separated by an ion-exchanger membrane, and, with the aid of an anode/cathode arrangement arranged outside the electrodialysis cells, an electric field transverse to a direction of passage of the liquid-crystal mixture through the first electrodialysis cell is generated so that ionised constituents of the liquid-crystal mixture are discharged from the first electrodialysis cell and are removed from the liquid-crystal mixture. The process according to the invention consequently essentially corresponds to the performance of electrodialysis on the liquid-crystal mixture. It has been found that many impurities relevant in practice can be separated and removed from the liquid-crystal mixture using electrodialysis. Ionised impurities can be removed reliably and with high effectiveness from the liquid-crystal mixture by suitable pre-specification of the concentrate solution and the ion-exchanger membrane delimiting the first electrodialysis cell.


The process according to the invention can be carried out in continuous operation and enables continuous sampling and control of the purification process, so that, depending on the respective liquid-crystal mixture, the contamination thereof and a target degree of purity of the liquid-crystal mixture to be purified, a suitable process duration can be determined and the purification already achieved can be monitored and if necessary regulated while the purification process is being carried out.


According to an advantageous embodiment of the inventive idea, it is provided that the liquid-crystal mixture is passed through the first electrodialysis cell a number of times. It is likewise possible for the liquid-crystal mixture to be passed successively through a plurality of electrodialysis cells having an arrangement, comparable to the first electrodialysis cell, of an ion-exchanger membrane and an adjacent second electrodialysis cell and a comparable electric field. In both cases, it is thereby possible to achieve the situation where a rate of passage of the liquid-crystal mixture and a total purification duration or a total residence time of the liquid-crystal mixture in the first electrodialysis cell or in a comparable electrodialysis cell arrangement can be pre-specified independently of one another. Thus, for example, it is possible, in the case of an impurity which can be removed highly efficiently, for the process duration to be adapted and kept short. If, by contrast, it is observed that the impurity in the liquid-crystal mixture can only be separated and removed from the liquid-crystal mixture comparatively slowly, the purification process can be carried out for a sufficiently long time in order to achieve and reliably guarantee a pre-specified purification effect. Sampling at time intervals or continuously enables the purification effect that has already been achieved to be determined and controlled. Accordingly, the purification process according to the invention also enables regulated purification of a liquid-crystal mixture, so that it can be ensured that a target or necessarily pre-specified degree of purity is also achieved with the purification according to the invention.


According to an embodiment of the inventive idea, it is provided that the liquid-crystal mixture is passed through the first electrodialysis cell over a period of more than one hour, preferably more than 4 hours. If the liquid-crystal mixture is passed successively through a plurality of comparable electrodialysis cells, it may likewise be provided that the total residence time of the liquid-crystal mixture in these electrodialysis cells is more than one hour and preferably more than four hours. It has been found that the specific resistance, which can be regarded as an expedient criterion for the purity of the liquid-crystal mixture, can be increased by more than a factor of 20, depending on the process duration over a period of about 4 hours to 8 hours.


It has proven advantageous for the concentrate solution used to be deionised water. In addition to comparatively effective charge transport in deionised water, the concentration gradient favours osmosis through the ion-exchanger membrane, which results in an additional purifying effect.


However, it is likewise possible and possibly advantageous, depending on the composition of the liquid-crystal mixture, for the concentrate solution used also to be other suitable solutions, such as, for example, transformer oil, dodecane or another organic solvent.


Investigations have shown that a large potential difference and consequently a large electric field transverse to a flow direction of the liquid-crystal mixture through the first electrodialysis cell is particularly advantageous for an effective purification effect. According to an embodiment of the inventive idea, it is therefore provided that the ion-exchanger membrane used is a membrane having a breakdown voltage of greater than 10 volts, preferably greater than 80 volts and particularly preferably 400 volts or more, and an electric potential difference which effects the greatest possible drop in voltage at the ion-exchanger membrane, but which is below the breakdown voltage, is pre-specified with the aid of the anode/cathode arrangement. The breakdown voltage denotes the voltage from which the membrane no longer reliably acts as insulator and current flow through the membrane could impair the electrodialysis. A drop in voltage between 10 and 1000 volts within the first electrodialysis cell is regarded as suitable for carrying out the purification process. The drop in voltage in the first electrodialysis cell should preferably be in a range between 80 volts and 120 volts, which has proven particularly advantageous for the purification process.


In order to prevent water or other mixture components being destroyed at the electrodes, it is, in accordance with an advantageous embodiment of the inventive idea, provided that the anode and cathode are flushed with transformer oil while the process is being carried out. The accessible active surfaces of the anode and cathode can be flushed with the transformer oil continuously or at time intervals. The electrode material used for the anode and for the cathode can preferably be stainless steel, but also graphite, mixed oxides or other suitable electrode materials.


In order to prevent residues of the purified liquid-crystal mixture remaining adhering and being retained in the first electrodialysis cell after a purification operation, it is provided that if possible all surfaces coming into contact with the liquid-crystal mixture to be purified are made, for example, from perfluoroalkoxy polymers (PFA) or are coated therewith. It is likewise possible for the components which come into contact with product, such as, for example, the electrodialysis cell, but also tubes, ion-exchanger membranes or spacer elements in an electrodialysis cell to be made from an inert polymer, such as, for example, polytetrafluoroethylene (PTFE). The components which come into contact with product are advantageously cleaned with organic solvents, such as, for example, acetone or toluene, before beginning a new purification process.


In order to prevent undesired pressure variations in the first electrodialysis cell while the purification process is being carried out, which may favour or cause leakage between adjacent electrodialysis cells, low-pulsation pumps are used to convey the liquid-crystal mixture and the concentrate solution. It has been found that, for example, the use of gear pumps enables the liquid-crystal mixture to be conveyed with very constant pressure and considerably reduces or entirely prevents undesired effects, such as, for example, leakage or a reduced purification effect.


In order to achieve the most effective purification possible of the liquid-crystal mixture within the shortest possible time, it is provided that the liquid-crystal mixture is thoroughly mixed and homogenised before introduction into the first electrodialysis cell.


A device by means of which the process according to the invention can be carried out has a first electrodialysis cell having a supply line and a discharge line, enabling a liquid-crystal mixture to be passed through the first electrodialysis cell in a direction of passage, and a second electrodialysis cell having a supply line and a discharge line, which is adjacent to the first electrodialysis cell and is separated by a suitable ion-exchanger membrane, enabling a concentrate solution to be passed through the second electrodialysis cell. The first electrodialysis cell and the second electrodialysis cell are arranged between an anode/cathode arrangement in such a way that an electric field transverse to the direction of passage of the liquid-crystal mixture in the first electrodialysis cell can be generated by means of the anode/cathode arrangement.


The anode and the cathode are separated from the first electrodialysis cell and from the second electrodialysis cell in each case by an ion-exchanger membrane, which exchanges dissolved ions having a charge which has an opposite charge sign to the dissolved ions exchanged by the ion-exchanger membrane between the first electrodialysis cell and the second electrodialysis cell. For example, if a cation-exchanger membrane is located between the first electrodialysis cell and the second electrodialysis cell, the anode and the cathode are separated from the first and second electrodialysis cells by anion-exchanger membranes.


The ion-exchanger membranes can preferably have a heterogeneous design and contain ion-exchanger particles embedded in a base polymer, or alternatively can have a homogeneous design and consist of an ionic polymer. The electrode material used is preferably stainless steel, but also graphite or a suitable mixed oxide.


Spacing devices, which are known as spacers and also serve for effective fluid distribution within the electrodialysis cells, are arranged between the respectively adjacent ion-exchanger membranes. The spacers are made from an inert plastic material or plastic-material mixture, such as, for example, polyethylene, polyethylene and polyamide, or from polyvinyl chloride and polyethylene terephthalate. A typical thickness of suitable spacers is between 0.3 mm and 1.5 mm, preferably about 0.5 mm.


Low-pulsation and as far as possible constant-pressure pumps, such as, for example, gear pumps, are advantageously used for conveying the liquid-crystal mixture and the concentrate solution.


All components which come into contact with the liquid-crystal mixture, such as, for example, the electrodialysis cells, the ion-exchanger membranes, the spacers and the tubes used for the supply lines and discharge lines, are preferably made from an inert polymer or provided with a corresponding coating. A suitable inert polymer is, for example, PFA or PTFE.





Illustrative embodiments of the inventive idea are explained in greater detail below and are depicted in the drawing, in which:



FIG. 1 shows a diagrammatic representation of a purification process according to the invention which is carried out with the aid of a suitable electrodialysis device, and



FIG. 2 shows a diagrammatic representation of a change in a specific resistance of a liquid-crystal mixture over time over the duration of performance of the purification process.





A purification device 1, depicted by way of example in FIG. 1, by means of which the process according to the invention for the purification of a liquid-crystal mixture can be carried out has a first electrodialysis cell 2 having a supply line 3 and a discharge line 4, which are connected to a liquid-crystal mixture reservoir 5. With the aid of a gear pump 6, an amount of fluid of a liquid-crystal mixture 7 can be conveyed out of the liquid-crystal mixture reservoir 5, through the first electrodialysis cell 2 and back into the liquid-crystal mixture reservoir 5, so that a circuit is produced and the liquid-crystal mixture 7 is passed continuously through the first electrodialysis cell 2. In the representation in accordance with FIG. 1, the liquid-crystal mixture 7 flows through the first electrodialysis cell 2 in a direction of passage running from top to bottom.


A second electrodialysis cell 8, which is adjacent to the first electrodialysis cell 2, is separated from the first electrodialysis cell 2 by a suitable anion-exchanger membrane 9. The second electrodialysis cell 8 likewise has a supply line 10 and a discharge line 11, which are connected to a concentrate-solution reservoir 12, so that a concentrate solution 14 can be passed through the second electrodialysis cell 8 with the aid of a gear pump 13. The concentrate solution 14 used is deionised water.


The first electrodialysis cell 2 and the second electrodialysis cell 8 are arranged between an anode 15 and a cathode 16 in such a way that an electric field transverse to the direction of passage of the liquid-crystal mixture 7 in the first electrodialysis cell 2 can be generated by means of this anode/cathode arrangement.


The anode 15 and the cathode 16 are separated from the first electrodialysis cell 2 and from the second electrodialysis cell 8 in each case by a cation-exchanger membrane 17 and can be flushed continuously or on demand with transformer oil 19 with the aid of a transformer-oil circuit 18.


All components which come into contact with the liquid-crystal mixture 7, such as, for example, the electrodialysis cells 2 and 8, the ion-exchanger membranes 9 and 17, the spacers and the tubes used for the supply lines 3 and 10 and the discharge lines 4 and 11, are made from an inert polymer or provided with a corresponding coating. A suitable inert polymer is, for example, PFA or PTFE.


In order to carry out the purification process, a potential difference of, for example, 80 volts or 120 volts is generated between the anode 15 and the cathode 16 with the aid of a direct-voltage source. The gear pumps 6 and 13 are started and effect uniform passage of the liquid-crystal mixture 7 through the first electrodialysis cell 2 and of the concentrate solution 14 through the second electrodialysis cell 8. While the liquid-crystal mixture 7 flows through the first electrodialysis cell 2, ionised impurities are diverted by the electric field either in the direction of the second electrodialysis cell 8 at the anion-exchanger membrane 9, or, in the case of an opposite charge sign of the ionised impurity, in the direction of the cathode 16 at the cation-exchanger membrane 17 and are thereby removed from the liquid-crystal mixture 7 flowing through.


The liquid-crystal mixture can be passed through the first electrodialysis cell 2 over a sufficiently long period. While the purification process is being carried out, samples can be taken continuously or at time intervals in order to determine and monitor the purification of the liquid-crystal mixture 7 that has already been achieved.



FIG. 2 depicts diagrammatically a specific resistance ρ in the unit ohm×cm determined while the purification process for a liquid-crystal mixture 7 is being carried out, as a function of the purification duration t in the unit hours. The specific resistance ρ is a measure of the proportion of dissolved ions in the liquid-crystal mixture 7 and thus at least indirectly a measure of the proportion of ionised impurities present in the liquid-crystal mixture 7. The greater the specific resistance p, the smaller the proportion of ionised impurities and the higher the purity of the liquid-crystal mixture 7. It has been found that the specific resistance ρ of a typical liquid-crystal mixture 7 increases by about a factor of 10 after only one hour and by about a factor of 40 after about four hours.


The purification process according to the invention can be carried out using standard laboratory electrodialysis devices and merely requires continuous operation of the gear pumps. Correspondingly, the purification process can be carried out using simple equipment and inexpensively and facilitates very efficient purification of the liquid-crystal mixture 7. The efficiency can be increased further by additionally carrying out further purification processes based on other methods beforehand.


The purification process described above is particularly suitable for liquid-crystal mixtures comprising at least two organic substances, preferably mesogenic, in particular liquid-crystalline substances, where the organic substances are preferably selected from the compounds of the general formula I,




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in which

  • R1 and R2 each, independently of one another, denote H, an alkyl radical having up to 15 C atoms which is unsubstituted, monosubstituted by CN or CF3 or at least monosubstituted by halogen, where, in addition, one or more CH2 groups in these radicals may be replaced by —O—, —S—,




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—C≡C—, —CH═CH—, —CF2O—, —OCF2—, —OC—O— or —O—CO— in such a way that O atoms are not linked directly to one another, and one of the radicals R1 and R2 also denotes F, Cl, CN, SF5, NCS, SCN, OCN,

  • rings A, B, C, D and E each, independently of one another, denote




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  • r, s and t each, independently of one another, denote 0, 1, 2 or 3, where r+s+t≦3,

  • Z1-4 each, independently of one another, denote —CO—O—, —O—CO—, —CF2O—, —OCF2—, —CH2O—, —OCH2—, —CH2CH2—, —(CH2)4—, —CH═CH—CH2O, —C2F4—, —CH2CF2—, —CF2CH2—, —CF═CF—, —CH═CF—, —CF═CH—, —CH═CH—, —C≡C— or a single bond, and

  • L1 and L2 each, independently of one another, denote H or F.



In the case where r+s+t=0, Z1 and Z4 are preferably selected in such a way that, if they do not denote a single bond, they are not linked to one another via two 0 atoms.


The liquid-crystal mixtures employed comprising the individual mesogenic substances may additionally also comprise one or more polymerisable compounds, so-called reactive mesogens (RMs), for example as disclosed in U.S. Pat. No. 6,861,107, in concentrations of, preferably, 0.1-5% by weight, particularly preferably 0.2-2% by weight, based on the mixture. Mixtures of this type can be used for so-called polymer stabilised VA (PS-VA) modes, negative IPS (PS-IPS) or negative FFS (PS-FFS) modes, in which polymerisation of the reactive mesogens is intended to take place in the liquid-crystalline mixture. The prerequisite for this is that the liquid-crystal mixture does not itself comprise any individual polymerisable substances.


The prerequisite for this is that the liquid-crystal mixture itself does not comprise any polymerisable components which likewise polymerise under the conditions where the compounds of the formula M polymerise.


The polymerisation is preferably carried out under the following conditions:


The polymerisable components are polymerised in a cell using a UV-A lamp of defined intensity for a defined period and applied voltage (typically 10 V to 30 V alternating voltage, frequencies in the range from 60 Hz-1 kHz). The UV-A light source employed is typically a metal-halide vapour lamp or high-pressure mercury lamp having an intensity of 50 mW/cm2. These are conditions where, for example, liquid-crystalline compounds containing an alkenyl or alkenyloxy side chain, such as, for example, the compound of the formula




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do not polymerise.


The polymerisable mesogenic or liquid-crystalline compounds, also known as “reactive mesogens” (RMs), are preferably selected from the compounds of the formula II





Ra-A1-(Z1-A2)m-Rb  II


in which the individual radicals have the following meanings:

  • A1 and A2 each, independently of one another, denote an aromatic, heteroaromatic, alicyclic or heterocyclic group, preferably having 4 to 25 C atoms, which may also contain fused rings and which is optionally mono- or polysubstituted by L,
  • Z1 on each occurrence, identically or differently, denotes —O—, —S—, —CO—, —CO—O—, —OCO—, —O—CO—O—, —OCH2—, —CH2O—, —SCH2—, —CH2S—, —CF2O—, —OCF2—, —CF2S—, —SCF2—, —(CH2)n—, —CF2CH2—, —CH2CF2—, —(CF2)n—, —CH═CH—, —CF═CF—, —C≡C—, —CH═CH—COO—, —OCO—CH═CH—, CR0R00 or a single bond,
  • L, Ra and Rb each, independently of one another, denote H, halogen, SF5,


NO2, a carbon group or hydrocarbon group, where the compounds contain at least one radical L, Ra and Rb which denotes or contains a P-Sp-group,

  • R0 and R00 each, independently of one another, denote H or alkyl having 1 to 12 C atoms,
  • P denotes a polymerisable group,
  • Sp denotes a spacer group or a single bond,
  • m denotes 0, 1, 2, 3 or 4,
  • n denotes 1, 2, 3 or 4.


The polymerisable compounds may contain one polymerisable group (monoreactive) or two or more (di- or multireactive), preferably two, polymerisable groups.


Above and below, the following meanings apply:


The term “mesogenic group” is known to the person skilled in the art and is described in the literature, and denotes a group which, due to the anisotropy of its attracting and repelling interactions, essentially contributes to causing a liquid-crystal (LC) phase in low-molecular-weight or polymeric substances. Compounds containing mesogenic groups (mesogenic compounds) do not necessarily have to have an LC phase themselves. It is also possible for mesogenic compounds to exhibit LC phase behaviour only after mixing with other compounds and/or after polymerisation. Typical mesogenic groups are, for example, rigid rod- or disc-shaped units. An overview of the terms and definitions used in connection with mesogenic or LC compounds is given in Pure Appl. Chem. 73(5), 888 (2001) and C. Tschierske, G. Pelzl, S. Diele, Angew. Chem. 2004, 116, 6340-6368.


The term “spacer group”, also referred to as “Sp” above and below, is known to the person skilled in the art and is described in the literature, see, for example, Pure Appl. Chem. 73(5), 888 (2001) and C. Tschierske, G. Pelzl, S. Diele, Angew. Chem. 2004, 116, 6340-6368. Unless indicated otherwise, the term “spacer group” or “spacer” above and below denotes a flexible group which connects the mesogenic group and the polymerisable group(s) in a polymerisable mesogenic compound (“RM”) to one another. Sp preferably denotes a single bond or a 1-16 C alkylene, in which one or more CH2 groups may be replaced by —O—, —CO—, —COO— or —OCO— in such a way that two 0 atoms are not connected directly to one another.


The term “organic group” denotes a carbon or hydrocarbon group.


The term “carbon group” denotes a mono- or polyvalent organic group containing at least one carbon atom which either contains no further atoms (such as, for example, —C≡C—) or optionally contains one or more further atoms, such as, for example, N, O, S, P, Si, Se, As, Te or Ge (for example carbonyl, etc.). The term “hydrocarbon group” denotes a carbon group which additionally contains one or more H atoms and optionally one or more heteroatoms, such as, for example, N, O, S, P, Si, Se, As, Te or Ge.


“Halogen” denotes F, Cl, Br or I.


The terms “alkyl”, “aryl”, “heteroaryl”, etc., also encompass polyvalent groups, for example alkylene, arylene, heteroarylene, etc.


The term “alkyl” in this application encompasses straight-chain and branched alkyl groups having 1 to 9 carbon atoms, preferably the straight-chain groups methyl, ethyl, propyl, butyl, pentyl, hexyl, heptyl, octyl and nonyl. Groups having 1 to 5 carbon atoms are particularly preferred.


The term “alkenyl” in this application encompasses straight-chain and branched alkenyl groups having 2 to 9 carbon atoms, preferably the straight-chain groups having 2 to 7 carbon atoms. Particularly preferred alkenyl groups are C2-C7-1E-alkenyl, C4-C7-3E-alkenyl, C5-C7-4-alkenyl, C6-C7-5-alkenyl and C7-6-alkenyl, in particular C2-C7-1E-alkenyl, C4-C7-3E-alkenyl and C5-C7-4-alkenyl. Examples of preferred alkenyl groups are vinyl, 1E-propenyl, 1E-butenyl, 1E-pentenyl, 1E-hex-enyl, 1E-hept-enyl, 3-butenyl, 3E-pentenyl, 3E-hexenyl, 3E-heptenyl, 4-pentenyl, 4Z-hexenyl, 4E-hexenyl, 4Z-hep-tenyl, 5-hexenyl, 6-heptenyl and the like. Groups having up to 5 carbon atoms are particularly preferred.


The term “fluoroalkyl” in this application encompasses straight-chain groups having a terminal fluorine, i.e. fluoromethyl, 2-fluoroethyl, 3-fluoropropyl, 4-fluoro-butyl, 5-fluoro-pentyl, 6-fluorohexyl and 7-fluoroheptyl. However, other positions of the fluorine are not excluded.


The term “oxaalkyl” or “alkoxy” in this application encompasses straight-chain radicals of the formula CnH2n+1-O—(CH2)m, in which n and m each, independently of one another, denote 1 to 6. Preferably, n=1 and m=1 to 6.


The term “aryl” denotes an aromatic carbon group or a group derived therefrom. The term “heteroaryl” denotes “aryl” in accordance with the above definition containing one or more heteroatoms.


The polymerisable group P is a group which is suitable for a polymerisation reaction, such as, for example, free-radical or ionic chain polymerisation, polyaddition or polycondensation, or for a polymer-analogous reaction, for example addition or condensation onto a main polymer chain. Particular preference is given to groups for chain polymerisation, in particular those containing a C═C double bond or a —C≡C— triple bond, and groups which are suitable for polymerisation with ring opening, such as, for example, oxetane or epoxide groups.


The polymerisable compounds are prepared analogously to processes which are known to the person skilled in the art and are described in standard works of organic chemistry, such as, for example, in Houben-Weyl, Methoden der organischen Chemie [Methods of Organic Chemistry], Thieme-Verlag, Stuttgart.


Typical and preferred reactive mesogens (RMs) are described, for example, in WO 93/22397, EP 0 261 712, DE 195 04 224, WO 95/22586, WO 97/00600, U.S. Pat. No. 5,518,652, U.S. Pat. No. 5,750,051, U.S. Pat. No. 5,770,107 and U.S. Pat. No. 6,514,578. Very particularly referred reactive mesogens are shown on Table E.


The process is used for the preparation of a mixture consisting of organic compounds, one or more of which are preferably mesogenic, preferably liquid-crystalline, per se. The mesogenic compounds preferably include one or more liquid-crystalline compounds. The process product is preferably a homogeneous, liquid-crystalline mixture. In the broader sense, the process also encompasses the preparation of mixtures which consist of organic substances in the homogeneous liquid phase and comprise additives which are insoluble therein (for example small particles). The process can thus also be used for the preparation of suspension-like or emulsion-like mixtures based on a continuous homogeneous organic phase. However, process variants of this type are generally less preferred.


By means of suitable additives, the liquid-crystal mixtures comprising at least two compounds of the formula I can be modified in such a way that they can be employed in any type of LCD display that has been disclosed to date, for example, ECB, VAN, IPS, FFS, TN, TN-TFT, STN, OCB, GH, PS-IPS, PS-FFS, PM-VA, PVA, PSA, PS-VA or ASM-VA displays.


The liquid-crystal mixtures may also comprise further additives known to the person skilled in the art and described in the literature, such as, for example, UV stabilisers, such as, for example, Tinuvin®, for example Tinuvin® 770, from BASF, antioxidants, such as, for example, Irganox®, for example Irganox® 1076 (octadecyl 3-(3,5-di-tert.butyl-4-hydroxyphenyl)propionate), from BASF, free-radical scavengers, nanoparticles, microparticles, one or more dopants, etc. For example, 0-15% of pleochroic dyes may be added, furthermore conductive salts, preferably ethyldimethyldodecylammonium 4-hexoxybenzoate, tetrabutylammonium tetraphenylboranate or complex salts of crown ethers (cf., for example, Haller et al., Mol. Cryst. Liq. Cryst. Volume 24, pages 249-258 (1973)) in order to improve the conductivity, or substances can be added in order to modify the dielectric anisotropy, the viscosity and/or the alignment of the nematic phases. Substances of this type are described, for example, in DE-A 22 09 127, 22 40 864, 23 21 632, 23 38 281, 24 50 088, 26 37 430 and 28 53 728.


Suitable stabilisers and dopants which can be combined with the compounds of the formula I in the electrodialysis cell during the preparation of the liquid-crystal mixtures are indicated below in Tables C and D.


The following examples are intended to explain the invention without limiting it. Above and below, percent data denote percent by weight; all temperatures are indicated in degrees Celsius.


Throughout the patent application, 1,4-cyclohexylene rings and 1,4-phenylene rings are depicted as follows:




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The cyclohexylene rings are trans-1,4-cyclohexylene rings.


In the present application and in the following examples, the structures of the liquid-crystal compounds are indicated by means of acronyms, with the transformation into chemical formulae taking place in accordance with Tables A and B below. All radicals CnH2n+1 and CmH2m+1 are straight-chain alkyl radicals having n and m C atoms respectively; n, m, k and z are integers and preferably denote 0, 1, 2, 3, 4, 5, 6, 7, 8, 9, 10, 11 or 12. The term “(O)CmH2m-1” means OCmH2m+1 or CmH2m+1. The coding in Table B is self-evident.


In Table A, only the acronym for the parent structure is indicated. In individual cases, this is followed, separated from the acronym for the parent structure by a dash, by a code for the substituents R1*, R2*, L1* and L2*:
















Code for R1*,






R2*, L1*, L2*, L3*
R1*
R2*
L1*
L2*







nm
CnH2n+1
CmH2m+1
H
H


nOm
CnH2n+1
OCmH2m+1
H
H


nO.m
OCnH2n+1
CmH2m+1
H
H


n
CnH2n+1
CN
H
H


nN.F
CnH2n+1
CN
F
H


nN.F.F
CnH2n+1
CN
F
F


nF
CnH2n+1
F
H
H


nCl
CnH2n+1
Cl
H
H


nOF
OCnH2n+1
F
H
H


nF.F
CnH2n+1
F
F
H


nF.F.F
CnH2n+1
F
F
F


nOCF3
CnH2n+1
OCF3
H
H


nOCF3.F
CnH2n+1
OCF3
F
H


n-Vm
CnH2n+1
—CH═CH—CmH2m+1
H
H


nV-Vm
CnH2n+1—CH═CH—
—CH═CH—CmH2m+1
H
H









Preferred mesogenic or liquid-crystalline substances which are suitable for the preparation of liquid-crystal mixtures and can be used in the purification process according to the invention are listed, in particular, in Tables A and B:









TABLE A









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PYP







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PYRP







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BCH







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CBC







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CCH







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CCP







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CPTP







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CEPTP







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ECCP







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CECP







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EPCH







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PCH







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CH







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PTP







embedded image




CCPC







embedded image




CP







embedded image




BECH







embedded image




EBCH







embedded image




CPC







embedded image




B







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FET-nF







embedded image




CGG







embedded image




CGU







embedded image




CFU
















TABLE B





(n = 1-15; (O)CnH2n+1 means CnH2n+1 or OCnH2n+1)









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APU-n-OXF







embedded image




ACQU-n-F







embedded image




CPU-n-OXF







embedded image




APUQU-n-F







embedded image




BCH-n.Fm







embedded image




CFU-n-F







embedded image




CBC-nmF







embedded image




CCP-nOCF3







embedded image




CCZU-n-F







embedded image




ECCP-nm







embedded image




ECCP-nF.F







embedded image




PGP-n-m







embedded image




CGU-n-F







embedded image




CGUQU-n-F







embedded image




CLUQU-n-F







embedded image




CDUQU-n-F







embedded image




CDU-n-F







embedded image




DCU-n-F







embedded image




CGG-n-F







embedded image




CPZG-n-OT







embedded image




CC-nV-Vm







embedded image




GPP-n-m







embedded image




CCP-Vn-m







embedded image




CCG-V-F







embedded image




CCP-nV-m







embedded image




CC-n-V







embedded image




CCQU-n-F







embedded image




CC-n-Vm







embedded image




CPPC-nV-Vm







embedded image




CCQG-n-F







embedded image




CQU-n-F







embedded image




CP-1V-m







embedded image




CP-2V-m







embedded image




CP-V2-m







embedded image




CP-1V-N







embedded image




CP-V2-N







embedded image




CCP-nF







embedded image




CCP-nF.F







embedded image




BCH-nF.F.F







embedded image




CCP-nF.F.F







embedded image




Dec-U-n-F







embedded image




CWCU-n-F







embedded image




CPGP-n-m







embedded image




CWCG-n-F







embedded image




CCOC-n-m







embedded image




CPTU-n-F







embedded image




GPTU-n-F







embedded image




PQU-n-F







embedded image




PUQU-n-F







embedded image




PGU-n-F







embedded image




CGZP-n-OT







embedded image




PGU-n-OXF







embedded image




CCGU-n-F







embedded image




CUQU-n-F







embedded image




CCCQU-n-F







embedded image




CPGU-n-OT







embedded image




CPGU-n-F







embedded image




CVCP-1V-OT







embedded image




GGP-n-Cl







embedded image




PP-nV-Vm







embedded image




PP-1-nVm







embedded image




CWCQU-n-F







embedded image




PPGU-n-F







embedded image




PGUQU-n-F







embedded image




GPQU-n-F







embedded image




MPP-n-F







embedded image




PGP-n-kVm







embedded image




PP-n-kVm







embedded image




PCH-nCl







embedded image




GP-n-Cl







embedded image




GGP-n-F







embedded image




PGIGI-n-F







embedded image




AIK-n-F







embedded image




BCH-nm







embedded image




BCN-nm







embedded image




CY-n-Om







embedded image




CP(F,Cl)n-Om







embedded image




CP(Cl,F)-n-Om







embedded image




CCY-n-Om







embedded image




CCY-n-m







embedded image




CCP(Cl,F)-n-Om







embedded image




CCP(F,Cl)n-Om







embedded image




CCY-V-m







embedded image




CCY-Vn-m







embedded image




CCY-n-OmV







embedded image




CBC-nm







embedded image




CCP-V-m







embedded image




CCP-n-m







embedded image




CPYC-n-m







embedded image




CYYC-n-m







embedded image




CCYY-n-(O)m







embedded image




CCY-n-O2V







embedded image




CY-n-m







embedded image




CCH-nm







embedded image




CCH-nOm







embedded image




CEY-n-Om







embedded image




CC-n-V1







embedded image




CY-n-OV







embedded image




CC-2V-V2







embedded image




CVC-n-m







embedded image




CC-n-mV







embedded image




CP-nOmFF







embedded image




CH-nm







embedded image




CEY-V-n







embedded image




CVY-V-n







embedded image




CY-V-On







embedded image




CY-n-OC(CH3)═CH2







embedded image




CY-1V-On







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CY-V1-On







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CY-n-O1V







embedded image




CCN-nm







embedded image




CCPC-nm







embedded image




CCY-n-zOm







embedded image




CPY-n-m







embedded image




CPY-n-Om







embedded image




CPY-1V-Om







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CPY-V-Om







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CPP(Cl,F)-n-(O)m







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CQY-n-(O)m







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CPP(F,Cl)n—(O)m







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CQIY-n-(O)m







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PGIY-n-Om







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CCQY-n-(O)m







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CCQIY-n-(O)m







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CPQY-n-(O)m







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CPQIY-n-(O)m







embedded image




CPYG-n-(O)m







embedded image




CCY-V-Om







embedded image




D-nOmFF







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CY-nV-(O)m







embedded image




PCH-nm







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PCH-nOm







embedded image




CY-nV-OmV







embedded image




DPGU-n-F







embedded image




DPGU-n-OT







embedded image




PP-n-m







embedded image




PYP-n-mV







embedded image




CYLI-n-m







embedded image




CENap-n-Om







embedded image




LY-n-(O)m







embedded image




CCNap-n-Om







embedded image




CNap-n-Om







embedded image




YPY-n-mV







embedded image




CETNap-n-Om







embedded image




CTNap-n-Om







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CK-n-F







embedded image




YPY-n-m







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LYLI-n-m







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C-DFDBF-n-(O)m







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CPYG-n-(O)m







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DFDBC-n(O)-(O)m







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HP-nN.F







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CCY-V2-(O)m







embedded image




CCY-1V2-(O)m







embedded image




CCY-3V-(O)m







embedded image




PYP-nF







embedded image




MEnN.F







embedded image




MUQU-n-F







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NUQU-n-F







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CCY-V2-(O)m







embedded image




CCY-1V2-(O)m







embedded image




CCY-3V-(O)m







embedded image




CCVC-n-V







embedded image




COChrom-n-Om







embedded image




COChrom-n-m







embedded image




CCOChrom-n-Om







embedded image




CCOChrom-n-m







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CONaph-n-Om







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CCONaph-n-Om







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CLY-n-Om







embedded image




CLY-n-m







embedded image




LYLI-n-m







embedded image




CYLI-n-m







embedded image




LY-n-(O)m







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COYOICC-n-m







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COYOIC-n-V







embedded image




CCOY-V-O2V







embedded image




CCOY-V-O3V







embedded image




COY-n-Om







embedded image




CCOY-n-Om







embedded image




PYP-n-m







embedded image




PYP-n-Om







embedded image




YPY-n-m







embedded image




YPY-n-mV







embedded image




Y-nO-Om







embedded image




Y-n-Om







embedded image




PY-n-m







embedded image




PY-n-Om







embedded image




PY-V2-Om







embedded image




PY-3V-Om







embedded image




PY-V-Om







embedded image




PY-1V-Om







embedded image




PY-1V2-Om







embedded image




C-DFDBF-n-(O)m







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DFDBC-n(O)-(O)m







embedded image




B-nO-Om







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DFDBC-n(O)-(O)m







embedded image




CPU-n-VT







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CPU-n-AT







embedded image




DGUQU-n-F







embedded image




C-n-V







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C-n-XF







embedded image




C-n-m







embedded image




CC-n-2V1







embedded image









embedded image




BCH-nF







embedded image




BCH-nF.F







embedded image




PY-n-m







embedded image




PY-n-Om







embedded image




PTP-nOmFF







embedded image




CPTP-nOmFF







embedded image




PPTUI-n-m







embedded image




CPTP-nOm







embedded image




CPTP-nm







embedded image




PTP-nOm







embedded image




PTP-nm







embedded image




Y-nO-Om







embedded image




Y-nO-OmV







embedded image




Y-nO-OmVm′









Particular preference is given to liquid-crystalline mixtures which comprise at least one, two, three, four or more compounds from Table B besides one or more compounds of the formula I.









TABLE C









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Table C indicates possible dopants, which are generally added to the liquid-crystalline mixtures. The mixtures preferably comprise 0-10% by weight, in particular 0.01-5% by weight and particularly preferably 0.01-3% by weight, of dopants.










TABLE D









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STAB-1







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STAB-2







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STAB-3







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STAB-4







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STAB-5







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STAB-6







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STAB-7







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STAB-8







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STAB-9







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STAB-10







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STAB-11







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STAB-12







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STAB-13







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STAB-14







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STAB-15







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STAB-16







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STAB-17







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STAB-18







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STAB-19







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STAB-20







embedded image


STAB-21







embedded image


STAB-22







embedded image


STAB-23







embedded image


STAB-24







embedded image


STAB-25







embedded image


STAB-26







embedded image


STAB-27







embedded image


STAB-28







embedded image


STAB-29







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STAB-30







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STAB-31







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STAB-32







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STAB-33







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STAB-34







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STAB-35







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STAB-36







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STAB-37







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STAB-38









Stabilisers, which can be added, for example, to the liquid-crystalline mixtures in amounts of 0-10% by weight, are shown below.


(n=1-12)


Suitable polymerisable compounds (reactive mesogens) for use in the mixtures according to the invention, preferably in PSA and PS-VA applications or PS-IPS/FFS applications, are shown below in Table E:










TABLE E









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RM-1







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RM-2







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RM-3







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RM-4







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RM-5







embedded image


RM-6







embedded image


RM-7







embedded image


RM-8







embedded image


RM-9







embedded image


RM-10







embedded image


RM-11







embedded image


RM-12







embedded image


RM-13







embedded image


RM-14







embedded image


RM-15







embedded image


RM-16







embedded image


RM-17







embedded image


RM-18







embedded image


RM-19







embedded image


RM-20







embedded image


RM-21







embedded image


RM-22







embedded image


RM-23







embedded image


RM-24







embedded image


RM-25







embedded image


RM-26







embedded image


RM-27







embedded image


RM-28







embedded image


RM-29







embedded image


RM-30







embedded image


RM-31







embedded image


RM-32







embedded image


RM-33







embedded image


RM-34







embedded image


RM-35







embedded image


RM-36







embedded image


RM-37







embedded image


RM-38







embedded image


RM-39







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RM-40







embedded image


RM-41







embedded image


RM-42







embedded image


RM-43







embedded image


RM-44







embedded image


RM-45







embedded image


RM-46







embedded image


RM-47







embedded image


RM-48







embedded image


RM-49







embedded image


RM-50







embedded image


RM-51







embedded image


RM-52







embedded image


RM-53







embedded image


RM-54







embedded image


RM-55







embedded image


RM-56







embedded image


RM-57







embedded image


RM-58







embedded image


RM-59







embedded image


RM-60







embedded image


RM-61







embedded image


RM-62







embedded image


RM-63







embedded image


RM-64







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RM-65







embedded image


RM-66







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RM-67







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RM-68







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RM-69







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RM-70







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RM-71







embedded image


RM-72







embedded image


RM-73







embedded image


RM-74







embedded image


RM-75







embedded image


RM-76







embedded image


RM-77







embedded image


RM-78







embedded image


RM-79







embedded image


RM-80







embedded image


RM-81







embedded image


RM-82







embedded image


RM-83







embedded image


RM-84







embedded image


RM-85







embedded image


RM-86







embedded image


RM-87







embedded image


RM-88







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RM-89







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RM-90







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RM-91







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RM-92







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RM-93







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RM-94







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RM-95









Table E shows example compounds which can preferably be used as reactive mesogenic compounds in the liquid-crystalline mixtures according to the invention. If the liquid-crystalline mixtures comprise one or more reactive compounds, they are preferably employed in amounts of 0.01-5% by weight. It may be necessary also to add an initiator or a mixture of two or more initiators for the polymerisation. The initiator or the initiator mixture is preferably added in amounts of 0.001-2% by weight, based on the mixture. A suitable initiator is, for example, Irgacure (BASF) or Irganox (BASF).


Suitable polymerisable compounds (reactive mesogens) for use in the mixtures according to the invention, preferably in PSA and PS-VA applications or PS-IPS/FFS applications, are shown below in Table E:


In a preferred embodiment, the liquid-crystalline mixtures comprise one or more compounds selected from the group of the compounds from Table E.


EXAMPLES

The following working examples are intended to explain the invention without restricting it.


Above and below, percent data denote percent by weight. All temperatures are indicated in degrees Celsius. m.p. denotes melting point, cl.p.=clearing point. Furthermore, C=crystalline state, N=nematic phase, S=smectic phase and I=isotropic phase. The data between these symbols represent the transition temperatures. Furthermore,

  • Vo denotes threshold voltage, capacitive [V] at 20° C.
  • Δπ denotes the optical anisotropy measured at 20° C. and 589 nm
  • Δ∈ denotes the dielectric anisotropy at 20° C. and 1 kHz
  • cl.p. denotes clearing point [° C.]
  • K1 denotes elastic constant, “splay” deformation at 20° C., [pN]
  • K3 denotes elastic constant, “bend” deformation at 20° C., [pN]
  • γ1 denotes rotational viscosity measured at 20° C. [mPa·s], determined by the rotation method in a magnetic field
  • LTS denotes low-temperature stability (nematic phase), determined in test cells.


The following examples are intended to explain the invention without limiting it.


Above and below, percentages denote percent by weight. All temperatures are indicated in degrees Celsius.


WORKING EXAMPLES
Example 1

A liquid-crystalline mixture, for example for PS-VA applications, of the composition


















CCH-35
9.47%



CCH-501
4.99%



CCY-2-1
9.47%



CCY-3-1
10.47%



CCY-3-O2
10.47%



CCY-5-O2
9.47%



CPY-2-O2
11.96%



CY-3-O4
8.97%



CY-5-O4
10.97%



RM-1
0.30%



PCH-53
13.46%











is purified using the process according to the invention.


Example 2

A liquid-crystalline mixture, for example for PS-VA applications, of the composition


















BCH-32
7.48%



CCH-23
21.93%



CCH-34
3.49%



CCY-3-O3
6.98%



CCY-4-O2
7.98%



CPY-2-O2
10.97%



CPY-3-O2
10.97%



CY-3-O2
15.45%



RM-1
0.30%



PCH-301
12.46%



PCH-302
1.99%











is purified using the process according to the invention.


Example 3

A liquid-crystalline mixture, for example for PS-VA applications, of the composition


















CC-3-V1
7.98%



CCH-23
17.95%



CCH-34
3.99%



CCH-35
6.98%



CCP-3-1
4.99%



CCY-3-O2
12.46%



CPY-2-O2
7.98%



CPY-3-O2
10.97%



CY-3-O2
15.45%



RM-1
0.30%



PY-3-O2
10.97%











is purified using the process according to the invention.


Example 4

A liquid-crystalline mixture, for example for PS-VA applications, of the composition


















CC-3-V1
8.97%



CCH-23
12.96%



CCH-34
6.23%



CCH-35
7.73%



CCP-3-1
3.49%



CCY-3-O2
12.21%



CPY-2-O2
6.73%



CPY-3-O2
11.96%



CY-3-O2
11.47%



RM-1
0.30%



PP-1-2V1
4.24%



PY-3-O2
13.71%











is purified using the process according to the invention.


Example 5

A liquid-crystalline mixture, for example for TN-TFT applications, of the composition


















CBC-33
3.50%



CC-3-V
38.00%



CC-3-V1
10.00%



CCP-V-1
3.00%



CCP-V2-1
9.00%



PGP-2-3
5.00%



PGP-2-4
5.00%



PGU-2-F
8.00%



PGU-3-F
9.00%



PUQU-3-F
9.50%











is purified using the process according to the invention.


Example 6

A liquid-crystalline mixture, for example for IPS or FFS applications, of the composition


















APUQU-3-F
4.50%



CC-3-V
44.00%



CC-3-V1
12.00%



CCP-V-1
11.00%



CCP-V2-1
9.00%



PGP-2-3
6.00%



PGUQU-3-F
6.00%



PP-1-2V1
7.00%



PPGU-3-F
0.50%











is purified using the process according to the invention.


Example 7

A liquid-crystalline mixture, for example for IPS or FFS applications, of the composition


















APUQU-3-F
8.00%



CBC-33
3.00%



CC-3-V
34.00%



CC-3-V1
2.50%



CCGU-3-F
4.00%



CCP-30CF3
4.00%



CCP-3F.F.F
4.50%



CCP-50CF3
3.00%



CCP-V-1
10.00%



CCQU-3-F
10.00%



CPGU-3-OT
6.00%



PGUQU-3-F
4.00%



PUQU-3-F
7.00%











is purified using the process according to the invention.


Example 8

A liquid-crystalline mixture, for example for IPS or FFS applications, of the composition


















APUQU-2-F
5.00%



APUQU-3-F
7.50%



BCH-3F.F.F
7.00%



CC-3-V
40.50%



CC-3-V1
6.00%



CCP-V-1
9.50%



CPGU-3-OT
5.00%



PGP-2-3
6.00%



PGP-2-4
6.00%



PPGU-3-F
0.50%



PUQU-3-F
7.00%











is purified using the process according to the invention.


Example 9

A liquid-crystalline mixture, for example for TN-TFT applications, of the composition


















APUQU-2-F
8.00%



APUQU-3-F
8.00%



BCH-32
7.00%



CC-3-V
43.00%



CCP-V-1
9.00%



PGP-2-3
7.00%



PGP-2-4
6.00%



PUQU-2-F
5.00%



PUQU-3-F
7.00%











is purified using the process according to the invention.


Example 10

A liquid-crystalline mixture, for example for TN-TFT applications, of the composition


















BCH-5F.F
8.00%



CBC-33F
3.00%



CC-3-V
22.00%



CCGU-3-F
6.00%



CCP-3F.F.F
8.00%



CCP-5F.F.F
4.00%



CCP-V-1
13.00%



CCP-V2-1
11.00%



CCQU-3-F
5.00%



CCQU-5-F
4.00%



PUQU-3-F
16.00%











is purified using the process according to the invention.


Example 11

A liquid-crystalline mixture, for example for TN-TFT applications, of the composition


















CBC-33F
3.00%



CBC-53F
3.00%



CC-3-V
17.00%



CC-3-V1
4.00%



CCP-3F.F.F
8.00%



CCPC-33
3.00%



CCPC-34
3.00%



CCP-V-1
5.00%



CCP-V2-1
2.00%



CCQU-2-F
1.50%



CCQU-3-F
10.00%



CCQU-5-F
10.00%



CGU-3-F
6.00%



PGP-2-3
7.50%



PP-1-2V1
7.00%



PUQU-3-F
10.00%











is purified using the process according to the invention.


Example 12

A liquid-crystalline mixture, for example for TN-TFT applications, of the composition


















APUQU-2-F
1.00%



BCH-3F.F.F
15.00%



CC-3-V
33.50%



CC-3-V1
2.00%



CCGU-3-F
1.00%



CCPC-33
2.00%



CCP-V-1
4.50%



BCH-2F
5.00%



BCH-3F
5.00%



PGP-2-3
8.50%



PGUQU-3-F
7.80%



PP-1-2V1
11.00%



PPGU-3-F
0.20%



PUQU-3-F
3.50%











is purified using the process according to the invention.


Example 13

A liquid-crystalline mixture, for example for IPS or FFS applications, of the composition


















APUQU-2-F
2.00%



APUQU-3-F
6.00%



CC-3-V
42.00%



CCP-3-1
3.00%



CCP-3-3
3.00%



CCP-3F.F.F
8.00%



CCP-V-1
1.50%



CCQU-3-F
7.00%



CCQU-5-F
3.00%



CPGU-3-OT
6.50%



PGUQU-3-F
5.00%



PGUQU-4-F
4.00%



PGUQU-5-F
4.00%



PPGU-3-F
0.50%



PUQU-3-F
4.50%











is purified using the process according to the invention.


Example 14

A liquid-crystalline mixture, for example for TN-TFT applications, of the composition


















CC-3-V
49.50%



CCP-3-1
1.50%



CCP-V-1
6.00%



CPGU-3-OT
7.00%



PGP-2-3
8.50%



PGP-2-4
5.50%



PGUQU-3-F
7.00%



PGUQU-4-F
4.00%



PP-1-2V1
2.50%



PPGU-3-F
0.50%



PUQU-3-F
8.00%











is purified using the process according to the invention.


Example 15

A liquid-crystalline mixture, for example for VA applications, of the composition


















BCH-32
6.00%



CCH-23
18.00%



CCH-34
8.00%



CCP-3-1
12.00%



CCP-3-3
3.00%



CCY-3-O2
6.00%



CPY-2-O2
6.00%



CPY-3-O2
7.00%



CY-3-O2
14.00%



CY-3-O4
8.00%



CY-5-O2
9.00%



PYP-2-3
3.00%











is purified using the process according to the invention.


Example 16

A liquid-crystalline mixture, for example for PS-VA applications, of the composition


















CC-3-V1
7.98%



CCH-23
17.95%



CCH-34
3.99%



CCH-35
6.98%



CCP-3-1
4.99%



CCY-3-O2
12.46%



CPY-2-O2
7.98%



CPY-3-O2
10.97%



CY-3-O2
15.45%



RM-17
0.30%



PY-3-O2
10.97%











is purified using the process according to the invention.


Example 17

A liquid-crystalline mixture, for example for VA applications, of the composition


















CC-3-V
29.50%



PP-1-3
11.00%



PY-3-O2
12.00%



CCP-3-1
9.50%



CCOY-2-O2
18.00%



CCOY-3-O2
13.00%



GPP-5-2
7.00%











is purified using the process according to the invention.


Mixture Examples 1 to 17 may additionally also comprise one or more, for example one or two, stabiliser(s) and/or a dopant from Tables C and D.


Example 18

A liquid-crystalline mixture, for example for TN applications, of the composition


















BCH-3F.F
7.50%



BCH-5F.F
7.50%



CC-3-V
35.00%



CCGU-3-F
4.00%



CCP-3F.F.F
12.00%



CCPC-33
3.00%



CCP-V-1
10.00%



PGP-2-4
4.00%



PPGU-3-F
1.00%



PUQU-3-F
16.00%











is purified using the process according to the invention.


Example 19

A liquid-crystalline mixture, for example for TN applications, of the composition


















BCH-2F.F
4.00%



BCH-3F.F.F
8.50%



CC-3-V1
8.00%



CC-4-V
10.00%



CCG-V-F
8.00%



CCP-20CF3
7.00%



CCP-2F.F.F
8.00%



CCP-30CF3
5.00%



CCP-3-1
3.00%



CCPC-33
2.50%



CCP-V-1
11.50%



CCQU-3-F
5.00%



CDU-2-F
7.00%



CDU-3-F
7.00%



PUQU-3-F
5.50%











is purified using the process according to the invention.


Example 20

A liquid-crystalline mixture, for example for PS-VA applications, of the composition


















BCH-32
7.48%



CCH-23
21.93%



CCH-34
3.49%



CCY-3-O3
6.98%



CCY-4-O2
7.98%



CPY-2-O2
10.97%



CPY-3-O2
10.97%



CY-3-O2
15.45%



RM-1
0.30%



PCH-301
12.46%



PCH-302
1.99%











is purified using the process according to the invention.


Example 21

A liquid-crystalline mixture, for example for VA applications, of the composition


















BCH-32
8.50%



CC-3-V
24.00%



CC-3-V1
5.00%



CCP-V-1
2.00%



CCY-3-1
2.50%



CCY-3-O1
7.00%



CCY-3-O2
6.50%



CCY-3-O3
4.00%



CCY-4-O2
4.00%



CPY-2-O2
7.50%



CPY-3-O2
10.00%



CY-3-O2
3.50%



PY-3-O2
8.50%



PYP-2-3
4.00%



PYP-2-4
3.00%











is purified using the process according to the invention.


Example 22

A liquid-crystalline mixture, for example for FFS applications, of the composition


















APUQU-2-F
4.00%



CC-3-V
26.50%



CC-3-V1
7.00%



CCGU-3-F
1.50%



CCP-2F.F.F
1.50%



CCP-30CF3
8.00%



CCP-3-1
2.00%



CCP-V-1
10.00%



CCP-V2-1
7.00%



CDU-2-F
5.00%



CPGU-3-OT
4.50%



PGU-3-F
3.00%



PGUQU-3-F
3.00%



PGUQU-4-F
3.00%



PPGU-3-F
1.50%



PUQU-3-F
12.50%











is purified using the process according to the invention.


Example 23

A liquid-crystalline mixture, for example for FFS applications, of the composition


















BCH-3F.F
7.00%



CBC-33
3.00%



CC-3-V
25.00%



CCGU-3-F
6.00%



CCP-30CF3
8.00%



CCP-3-1
4.50%



CCP-V-1
13.50%



CCP-V2-1
6.00%



CCQU-3-F
8.00%



CPGP-5-2
3.00%



DPGU-4-F
2.50%



PPGU-3-F
1.00%



PUQU-3-F
4.50%



Y-4O-O4
8.00%











is purified using the process according to the invention.


Example 24

A liquid-crystalline mixture, for example for PS-VA applications, of the composition


















CC-3-V1
10.22%



CCH-23
18.44%



Irganox ® 1076
0.01%



RM-1
0.30%



PY-3-O2
12.96%



PP-1-2V1
3.74%



CY-3-O2
11.47%



CPY-3-O2
9.72%



CPY-2-O2
5.98%



CCY-3-O2
11.96%



CCY-3-1
2.49%



CCP-3-1
5.98%



CCH-35
6.73%










is purified using the process according to the invention.


Example 25

A liquid-crystalline mixture, for example for TN applications, of the composition


















APUQU-2-F
2.00%



BCH-3F.F
9.00%



BCH-3F.F.F
9.00%



CC-3-V1
5.00%



CC-4-V
6.00%



CCGU-3-F
7.50%



CCG-V-F
15.50%



CCP-2F.F.F
8.50%



CCP-30CF3
6.00%



CCP-3-1
2.00%



CCP-3F.F.F
10.00%



CCQU-3-F
9.50%



CCQU-5-F
9.00%



PPGU-3-F
1.00%











is purified using the process according to the invention.


Example 26

A liquid-crystalline mixture, for example for PS-VA applications, of the composition


















RM-1
0.199%



Irganox ® 1076
0.001%



PYP-2-4
8.98%



PYP-2-3
8.98%



PCH-53
2.99%



PCH-301
5.99%



CY-3-O4
20.46%



CPY-3-O2
4.49%



CPY-2-O2
9.98%



CCY-4-O2
6.99%



CCY-3-O3
7.98%



CCY-3-O2
6.99%



CCH-35
5.99%



BCH-52
3.99%



CCH-34
5.99%











is purified using the process according to the invention.


Example 27

A liquid-crystalline mixture, for example for FFS applications, of the composition


















CDUQU-3-F
3.00%



CCP-V-1
13.50%



CCP-3-3
2.50%



CC-3-V
44.00%



APUQU-2-F
4.50%



CPGU-3-OT
4.00%



PUQU-2-F
5.00%



PGU-2-F
6.00%



PGU-3-F
6.00%



PGUQU-3-F
3.50%



PGUQU-4-F
3.50%



PPGU-3-F
0.50%



DPGU-4-F
4.00%











is purified using the process according to the invention.


Example 28

A liquid-crystalline mixture, for example for FFS applications, of the composition


















BCH-3F.F
15.00%



BCH-3F.F.F
8.00%



CC-3-V
10.00%



CC-3-V1
10.50%



CC-4-V
10.50%



CCP-30CF3
10.00%



CCP-V-1
15.00%



CDUQU-3-F
6.50%



PGP-2-2V
1.00%



PGU-2-F
8.00%



PPGU-3-F
1.00%



PUQU-3-F
4.50%











is purified using the process according to the invention.


Example 29

A liquid-crystalline mixture, for example for FFS applications, of the composition


















PUQU-3-F
14.00%



PPGU-3-F
1.00%



PGP-2-2V
4.50%



DPGU-4-F
3.00%



CPGU-3-OT
3.00%



STAB-37
0.01%



CCP-V-1
14.00%



CCP-30CF3
6.00%



CC-3-V1
5.50%



CC-3-V
38.99%



APUQU-2-F
4.00%



CCY-3-O2
6.00%











is purified using the process according to the invention.


Example 30

A liquid-crystalline mixture, for example for VA applications, of the composition


















CLY-3-O2
10.00%



CCY-3-O2
9.25%



CCH-35
8.00%



CC-3-V1
10.00%



CC-3-V
27.50%



CPY-3-O2
11.75%



PYP-2-4
0.50%



PY-4-O2
9.00%



PY-3-O2
14.00%











is purified using the process according to the invention.


Example 31

A liquid-crystalline mixture, for example for PVA applications, of the composition


















CCH-23
12.00%



CCH-34
10.00%



CCP-3-1
7.00%



CCY-3-1
10.00%



CCY-3-O2
9.00%



CCY-3-O3
9.00%



CCY-4-O2
9.00%



CPGP-4-3
2.00%



CPY-2-O2
8.00%



CPY-3-O2
8.00%



CY-3-O4
4.50%



PCH-301
10.00%



PYP-2-3
1.50%











is purified using the process according to the invention.


Example 32

A liquid-crystalline mixture, for example for FFS applications, of the composition


















CC-3-V
33.00%



CCY-3-O1
5.00%



CCY-3-O2
6.50%



CCY-4-O2
8.00%



CCY-5-O2
3.50%



CPY-2-O2
9.00%



CPY-3-O2
9.00%



CY-3-O2
10.00%



CY-5-O2
2.00%



PY-3-O2
9.00%



PYP-2-3
5.00%










is purified using the process according to the invention.


Example 33

A liquid-crystalline mixture, for example for FFS applications, of the composition


















CC-3-V
44.50%



CC-3-V1
5.50%



CCP-30CF3
8.00%



CCP-V-1
8.00%



CCQU-3-F
5.00%



PGP-2-3
4.00%



PGP-2-4
5.00%



PGUQU-3-F
3.00%



PGUQU-4-F
9.00%



PGUQU-5-F
5.50%



PUQU-3-F
2.50%











is purified using the process according to the invention.


Example 34

A liquid-crystalline mixture, for example for FFS applications, of the composition


















APUQU-2-F
5.00%



APUQU-3-F
5.00%



CC-3-V
40.00%



CC-3-V1
4.50%



CCGU-3-F
3.50%



CCP-30CF3
5.50%



CCP-V-1
10.50%



CCQU-3-F
5.50%



CPGU-3-OT
3.00%



PGUQU-4-F
6.00%



PGUQU-5-F
4.50%



PUQU-3-F
7.00%











is purified using the process according to the invention.


Example 35

A liquid-crystalline mixture, for example for FFS applications, of the composition


















CC-3-V
23.50%



CC-3-V1
9.00%



CCGU-3-F
5.00%



CCP-30CF3
8.00%



CCP-50CF3
6.00%



CCP-V-1
12.00%



CCP-V2-1
5.00%



CPGP-4-3
3.00%



PCH-301
5.00%



PGP-1-2V
7.50%



PGP-2-2V
8.00%



PUQU-3-F
8.00%











is purified using the process according to the invention.


Example 36

A liquid-crystalline mixture, for example for IPS applications, of the composition


















APUQU-2-F
5.00%



APUQU-3-F
8.00%



CC-3-V
36.00%



CC-3-V1
5.00%



CCP-V-1
8.00%



CCQU-3-F
9.50%



PGP-2-2V
3.00%



PGUQU-3-F
4.00%



PGUQU-4-F
8.00%



PGUQU-5-F
5.00%



PUQU-3-F
8.50%











is purified using the process according to the invention.


Example 37

A liquid-crystalline mixture, for example for IPS applications, of the composition


















APUQU-2-F
7.00%



APUQU-3-F
7.00%



CC-3-2V1
4.50%



CC-3-V
32.00%



CC-3-V1
11.00%



CCP-30CF3
7.50%



CCP-50CF3
1.50%



DGUQU-4-F
8.00%



DPGU-4-F
5.00%



PGUQU-3-F
3.00%



PGUQU-4-F
8.00%



PGUQU-5-F
2.00%



PP-1-2V1
2.00%



PUQU-3-F
1.50%











is purified using the process according to the invention.


Example 38

A liquid-crystalline mixture, for example for PS-VA applications, of the composition


















CCH-23
13.97%



CCH-34
11.98%



CCP-3-1
2.99%



CCY-3-1
7.98%



CCY-3-O2
11.98%



CCY-3-O3
11.98%



CCY-4-O2
9.98%



CPY-2-O2
2.99%



CPY-3-O2
9.98%



PCH-301
9.98%



PYP-2-3
5.99%



RM-1
0.20%











is purified using the process according to the invention.


Example 39

A liquid-crystalline mixture, for example for FFS applications, of the composition


















CC-3-V
29.00%



CCY-3-O1
3.50%



CCY-3-O2
9.00%



CCY-4-O2
9.00%



CCY-5-O2
3.00%



CPY-3-O2
9.50%



CY-3-O2
13.00%



CY-5-O2
2.00%



PY-3-O2
10.00%



PYP-2-3
2.50%



CPY-2-O2
9.50%











is purified using the process according to the invention and 0.005% of STAB-35 is subsequently added.


Example 40

A liquid-crystalline mixture, for example for PS-IPS applications, of the composition


















APUQU-2-F
2.99%



APUQU-3-F
5.99%



BCH-2F.F
2.00%



BCH-3F.F
7.48%



CC-3-V
25.44%



CC-3-V1
5.98%



CCP-V-1
12.97%



CCP-V2-1
5.98%



CCQU-3-F
7.98%



CCQU-5-F
3.98%



PGUQU-3-F
4.99%



PPGU-3-F
0.50%



PUQU-3-F
13.47%



RM-35
0.25%











is purified using the process according to the invention.


Example 41

A liquid-crystalline mixture, for example for PS-IPS applications, of the composition


















APUQU-2-F
2.99%



APUQU-3-F
5.99%



BCH-2F.F
2.00%



BCH-3F.F
7.48%



CC-3-V
25.44%



CC-3-V1
5.98%



CCP-V-1
12.97%



CCP-V2-1
5.99%



CCQU-3-F
7.98%



CCQU-5-F
3.98%



PGUQU-3-F
4.98%



PPGU-3-F
0.50%



PUQU-3-F
13.47%



RM-41
0.25%











is purified using the process according to the invention.


Example 42

A liquid-crystalline mixture, for example for TN applications, of the composition


















PPGU-3-F
0.50%



PP-1-2V1
1.50%



PGUQU-4-F
4.00%



PGUQU-3-F
5.00%



PGP-2-5
2.00%



PGP-2-4
5.00%



PUQU-3-F
6.00%



PCH-302
6.00%



CPGP-5-3
6.00%



CPGP-5-2
6.00%



CC-3-V
30.00%



BCH-3F.F.F
12.00%



BCH-3F.F
10.00%



PGP-2-3
6.00%











is purified using the process according to the invention.


Example 43

A liquid-crystalline mixture, for example for TN-TFT applications, of the composition


















CC-3-V
29.00%



CCGU-3-F
4.00%



CCG-V-F
5.00%



CCP-2F.F.F
5.00%



CCP-3F.F.F
8.00%



CCPC-33
3.00%



CCPC-34
3.00%



CCPC-35
1.50%



CCP-V-1
10.00%



CCP-V2-1
11.00%



CCQU-2-F
1.50%



CCQU-3-F
8.00%



PUQU-3-F
11.00%











is purified using the process according to the invention.


Example 44

A liquid-crystalline mixture, for example for FFS applications, of the composition


















BCH-32
4.50%



CC-3-V
23.50%



CCH-301
4.00%



CCY-3-O2
4.00%



CCY-3-O3
7.00%



CCY-4-O2
8.00%



CLY-3-O2
8.00%



CPY-2-O2
7.00%



CPY-3-O2
11.00%



CY-3-O2
11.00%



PY-3-O2
12.00%











is purified using the process according to the invention.


Example 45

A liquid-crystalline mixture, for example for IPS applications, of the composition


















APUQU-2-F
2.50%



APUQU-3-F
4.50%



CC-3-V
42.00%



CCGU-3-F
4.00%



CCP-30CF3
5.00%



CCP-3-1
3.00%



CCP-V-1
10.00%



CCP-V2-1
2.50%



CCQU-3-F
6.00%



CPGU-3-OT
5.00%



PGUQU-3-F
4.50%



PGUQU-4-F
3.50%



PPGU-3-F
0.50%



PUQU-3-F
7.00%











is purified using the process according to the invention.


Example 46

A liquid-crystalline mixture, for example for IPS applications, of the composition


















BCH-32
2.99%



CCH-303
1.49%



CCH-34
12.93%



CCH-501
5.97%



CCY-2-1
5.97%



CCY-3-1
5.97%



CCY-3-O2
5.97%



CCY-3-O3
5.97%



CCY-4-O2
5.97%



CCY-5-O2
2.99%



CPY-2-O2
6.97%



CPY-3-O2
6.97%



CY-3-O2
14.93%



CY-5-O2
9.46%



PCH-302
4.98%



RM-41
0.30%



S-4011
0.17%











is purified using the process according to the invention.


Example 47

A liquid-crystalline mixture, for example for PM-VA applications, of the composition


















CPY-3-O2
8.00%



CPY-2-O2
8.00%



CH-43
3.00%



CH-35
3.00%



CH-33
3.00%



CCY-5-O2
5.50%



CCY-4-O2
6.50%



CCY-3-O3
6.50%



CCY-3-O2
6.50%



CCPC-35
5.00%



CCPC-34
5.00%



CCPC-33
5.00%



CC-4-V
4.50%



CY-3-O4
15.50%



Y-4O-O4
15.00%











is purified using the process according to the invention.


Example 48

A liquid-crystalline mixture, for example for PS-FFS applications, of the composition


















APUQU-2-F
2.49%



APUQU-3-F
6.98%



CC-3-V
24.94%



CC-3-V1
7.98%



CCGU-3-F
3.49%



CCP-30CF3
4.99%



CCP-V-1
5.99%



CCP-V2-1
13.97%



CCQU-3-F
9.98%



PCH-302
6.48%



PGUQU-3-F
3.99%



PGUQU-4-F
3.99%



PPGU-3-F
0.49%



PUQU-3-F
3.99%



RM-41
0.25%











is purified using the process according to the invention.


Example 49

A liquid-crystalline mixture, for example for FFS applications, of the composition


















APUQU-2-F
3.50%



APUQU-3-F
6.00%



CC-3-V
45.50%



CCP-30CF3
5.00%



CCP-3-1
3.00%



CCP-V2-1
8.50%



CPGU-3-OT
6.00%



PGUQU-3-F
5.00%



PGUQU-4-F
5.00%



PPGU-3-F
0.50%



PUQU-3-F
12.00%











is purified using the process according to the invention.


Example 50

A liquid-crystalline mixture, for example for FFS applications, of the composition


















APUQU-2-F
4.00%



APUQU-3-F
6.00%



CC-3-V
45.00%



CCP-20CF3
4.00%



CCP-30CF3
4.00%



CCP-40CF3
2.50%



CPGP-5-2
7.00%



CPGP-5-3
7.00%



PGP-2-3
5.50%



PGP-2-4
5.00%



PPGU-3-F
0.50%



PUQU-3-F
9.50%











is purified using the process according to the invention.


Example 51

A liquid-crystalline mixture, for example for TN applications, of the composition


















CC-3-V
49.50%



CCP-3-1
1.50%



CCP-V-1
6.00%



CPGU-3-OT
7.00%



PGP-2-3
8.50%



PGP-2-4
5.50%



PGUQU-3-F
7.00%



PGUQU-4-F
4.00%



PP-1-2V1
2.50%



PPGU-3-F
0.50%



PUQU-3-F
8.00%











is purified using the process according to the invention.


Example 52

A liquid-crystalline mixture, for example for PA-VA applications, of the composition


















BCH-32
6.00%



CCH-23
18.00%



CCH-34
8.00%



CCP-3-1
12.00%



CCP-3-3
3.00%



CCY-3-O2
6.00%



CPY-2-O2
6.00%



CPY-3-O2
7.00%



CY-3-O2
14.00%



CY-3-O4
8.00%



CY-5-O2
9.00%



PYP-2-3
3.00%











is purified using the process according to the invention.


Example 53

A liquid-crystalline mixture, for example for FFS applications, of the composition


















CCQU-3-F
8.00%



CCP-V2-1
7.00%



CCP-V-1
10.00%



CC-3-V
32.50%



PGP-2-2V
10.00%



PUQU-3-F
12.50%



PGUQU-5-F
4.00%



PGUQU-4-F
5.00%



PGUQU-3-F
5.00%



APUQU-3-F
6.00%











is purified using the process according to the invention.


Example 54

A liquid-crystalline mixture, for example for FFS applications, of the composition


















APUQU-3-F
1.00%



BCH-3F.F.F
17.00%



CC-3-V
35.00%



CC-3-V1
6.00%



CCP-3F.F.F
2.50%



CCP-V-1
12.00%



CCP-V2-1
8.50%



CPGP-5-2
3.00%



CPGP-5-3
2.50%



DPGU-4-F
4.00%



PGUQU-3-F
4.00%



PGUQU-4-F
2.00%



PGUQU-5-F
2.00%



PPGU-3-F
0.50%











is purified using the process according to the invention.


Example 55

A liquid-crystalline mixture, for example for PM-VA applications, of the composition


















CH-35
3.00%



CH-43
3.00%



CLY-3-O2
3.25%



CPY-2-O2
10.00%



CY-3-O2
15.00%



CH-33
3.00%



CCY-5-O2
4.00%



CCY-4-O2
6.00%



CCY-3-O3
6.00%



CCY-3-O2
6.00%



CCY-3-1
2.00%



CCY-2-1
8.75%



CY-3-O4
20.00%



CCPC-33
3.75%



CCH-34
4.75%



CCPC-34
1.50%











is purified using the process according to the invention.


Example 56

A liquid-crystalline mixture, for example for PS-FFS applications, of the composition


















APUQU-3-F
5.99%



BCH-3F.F
5.49%



CC-3-V
24.94%



CC-3-V1
7.98%



CCGU-3-F
5.98%



CCP-30CF3
2.99%



CCP-V-1
16.96%



CCP-V2-1
13.96%



CCQU-3-F
2.49%



CCQU-5-F
4.99%



PGUQU-4-F
4.49%



PPGU-3-F
0.50%



PUQU-3-F
2.99%



RM-41
0.25%











is purified using the process according to the invention.


The following mixtures are likewise purified using the process according to the invention:


Example 57




















CY-3-O4
14.00%
Clearing point [° C.]:
106.0



CCY-3-O2
8.00%
Δn [589 nm, 20° C.]:
0.1597



CCY-4-O2
7.00%
ε [1 kHz, 20° C.]:
3.9



CCY-3-O3
6.00%
ε [1 kHz, 20° C.]:
8.5



CCY-5-O2
5.00%
Δε [1 kHz, 20° C.]:
−4.6



CPY-2-O2
10.00%
K1 [pN, 20° C.]:
16.6



CPY-3-O2
8.00%
K3 [pN, 20° C.]:
17.6



PYP-2-3
14.00%
V0 [20° C., V]:
2.08



PYP-2-4
14.00%
γ1 [mPa · s, 20° C.]:
316



CCH-301
8.00%



PGP-2-3
6.00%










Example 57a

The mixture according to Example 57 additionally comprises 0.025% of STAB-35.


Example 58




















CY-3-O2
13.00%
Clearing point [° C.]:
111



CY-5-O2
9.00%



CY-5-O4
8.00%



CCY-3-O2
6.00%



CCY-3-O3
5.00%



CCY-4-O2
5.00%



CCY-5-O2
3.50%



CPY-2-O2
7.00%



CPY-3-O2
3.00%



CCH-34
17.50%



CCP-3-1
4.50%



CH-35
3.00%



CH-43
3.00%



CH-45
0.50%



CCPC-33
3.00%



CCPC-34
3.00%



CCPC-35
3.00%










Example 59




















CC-3-V
37.00%
Clearing point [° C.]:
75.2



CCY-3-O1
5.00%
Δn [589 nm, 20° C.]:
0.1014



CCY-3-O2
5.00%
Δε [1 kHz, 20° C.]:
−3.7



CCY-4-O2
4.00%
ε [1 kHz, 20° C.]:
3.7



CLY-3-O2
7.00%
ε [1 kHz, 20° C.]:
7.4



CPY-2-O2
9.00%
K1 [pN, 20° C.]:
13.2



CPY-3-O2
10.00%
K3 [pN, 20° C.]:
15.2



CY-3-O2
11.50%
V0 [20° C., V]:
2.13



PY-3-O2
11.50%










Example 60




















CC-3-V
40.00%
Clearing point [° C.]:
100.3



CC-3-V1
5.00%
Δn [589 nm, 20° C.]:
0.1059



CCP-30CF3
4.00%
Δε [1 kHz, 20° C.]:
3.9



CCP-V-1
13.00%
ε [1 kHz, 20° C.]:
6.7



CCP-V2-1
4.00%
ε [1 kHz, 20° C.]:
2.8



CCVC-3-V
4.00%
K1 [pN, 20° C.]:
14.9



CDUQU-3-F
2.00%
K3 [pN, 20° C.]:
17.0



CPGP-5-2
5.00%
V0 [20° C., V]:
2.07



CPGP-5-3
1.50%
γ1 [mPa · s, 20° C.]:
74



DGUQU-4-F
2.00%



DPGU-4-F
3.00%



PGP-2-3
4.00%



PGP-2-4
4.00%



PPGU-3-F
0.50%



PUQU-3-F
8.00%










Example 61




















CY-3-O4
23.00%
Clearing point [° C.]:
71.3



CCY-3-O1
6.00%
Δn [589 nm, 20° C.]:
0.1197



CCY-3-O2
6.00%
Δε [1 kHz, 20° C.]:
−7.0



CCY-3-O3
7.00%
ε [1 kHz, 20° C.]:
5.0



CCY-4-O2
7.00%
ε [1 kHz, 20° C.]:
12.0



CCY-5-O2
5.00%
K1 [pN, 20° C.]:
11.7



CPY-2-O2
8.00%
K3 [pN, 20° C.]:
13.2



CPY-3-O2
10.00%
V0 [20° C., V]:
1.44



CCY-2-1
3.50%
γ1 [mPa · s, 20° C.]:
246



PYP-2-4
8.50%



PY-1-O4
8.00%



Y-4O-O4
8.00%










Example 62




















PUQU-3-F
9.00%
Clearing point [° C.]:
75.9



PGUQU-3-F
7.00%
Δn [589 nm, 20° C.]:
0.1131



PGUQU-4-F
5.00%
Δε [1 kHz, 20° C.]:
6.1



CPGU-3-OT
4.50%
K1 [pN, 20° C.]:
11.9



PPGU-3-F
0.50%
K3 [pN, 20° C.]:
13.6



CDUQU-3-F
0.05%
V0 [20° C.]:
1.14



CC-3-V
49.95%
γ1 [mPa · s, 20° C.]:
57



CCP-V-1
12.00%



PGP-2-3
8.00%



PGP-2-4
4.00%










Example 63




















PUQU-3-F
8.00%
Clearing point [° C.]:
75.4



PGUQU-3-F
7.00%
Δn [589 nm, 20° C.]:
0.1191



PGUQU-4-F
4.00%
Δε [1 kHz, 20° C.]:
6.1



PPGU-3-F
0.50%
K1 [pN, 20° C.]:
12.6



CPGU-3-OT
7.00%
K3 [pN, 20° C.]:
12.5



CC-3-V
49.50%
V0 [20° C., V]:
1.52



CCP-3-1
1.50%
γ1 [mPa · s, 20° C.]:
57



CCP-V-1
6.00%



PP-1-2V1
2.50%



PGP-2-3
8.50%



PGP-2-4
5.50%










Example 64




















CY-3-O4
12.00%
Clearing point [° C.]:
102.5



CY-5-O4
12.00%
Δn [589 nm, 20° C.]:
0.1605



CCY-3-O2
8.00%
Δε [1 kHz, 20° C.]:
−5.6



CCY-4-O2
7.00%
ε [1 kHz, 20° C.]:
4.0



CCY-3-O3
7.00%
ε [1 kHz, 20° C.]:
9.6



CPY-2-O2
12.00%
K1 [pN, 20° C.]:
16.9



CPY-3-O2
12.00%
K3 [pN, 20° C.]:
17.1



PYP-2-3
15.00%
V0 [V, 20° C.]:
1.84



PYP-2-4
15.00%
γ1 [mPa · s, 20° C.]:
401










Example 65




















BCH-32
8.00%
Clearing point [° C.]:
80.6



CC-3-V
28.00%
Δn [589 nm, 20° C.]:
0.1194



CCY-3-O1
5.00%
Δε [1 kHz, 20° C.]:
−3.9



CCY-3-O2
6.00%
ε [1 kHz, 20° C.]:
4.0



CLY-3-O2
8.00%
ε [1 kHz, 20° C.]:
7.9



CPY-2-O2
10.00%
K1 [pN, 20° C.]:
13.0



CPY-3-O2
10.00%
K3 [pN, 20° C.]:
14.0



PGIY-2-O4
8.00%
V0 [20° C.]:
2.0



PY-3-O2
9.00%
γ1 [mPa · s, 20° C.]:
120



Y-4O-O4
8.00%










Example 66




















CY-3-O2
15.00%
Clearing point [° C.]:
80.1



CY-5-O2
7.00%
Δn [589 nm, 20° C.]:
0.1026



CCY-3-O1
4.00%
Δε [1 kHz, 20° C.]:
−3.5



CCY-3-O2
2.00%
ε [1 kHz, 20° C.]:
3.5



CCY-3-O3
6.00%
ε [1 kHz, 20° C.]:
7.0



CCY-4-O2
6.00%
K1 [pN, 20° C.]:
13.9



CPY-2-O2
8.00%
K3 [pN, 20° C.]:
13.8



CPY-3-O2
8.00%
V0 [20° C.]:
2.11



PYP-2-4
6.50%
γ1 [mPa · s, 20° C.]:
132



CCH-23
15.00%



CCH-34
5.00%



CCH-35
4.00%



CCH-301
6.00%



BCH-32
7.50%










Example 67




















APUQU-2-F
3.00%
Clearing point [° C.]:
100.1



APUQU-3-F
2.50%
Δn [589 nm, 20° C.]:
0.1046



CC-3-2V1
3.00%



CC-3-V
37.00%



CC-3-V1
5.00%



CCP-V-1
13.00%



CCP-V2-1
7.50%



CCVC-3-V
5.00%



CDUQU-3-F
2.00%



CPGP-5-2
4.00%



DGUQU-4-F
2.00%



PGP-2-3
5.00%



PGP-2-4
4.50%



PPGU-3-F
0.50%



PUQU-3-F
6.00%










Example 68




















PCH-3
6.00%
Clearing point [° C.]:
86.0



CC-5-V
20.00%
Δn [589 nm, 20° C.]:
0.1612



PCH-301
14.00%
Δε [1 kHz, 20° C.]:
1.8



PCH-302
15.00%
ε [1 kHz, 20° C.]:
4.7



PPTUI-3-2
15.00%
ε [1 kHz, 20° C.]:
2.9



PPTUI-3-4
15.00%



CCP-V-1
8.00%



CCP-V2-1
7.00%










Example 68a

The mixture according to Example 68 additionally comprises 2% of R-5011.


Example 69




















CY-3-O4
13.00%
Clearing point [° C.]:
92.0



CC-4-V
17.00%
Δn [589 nm, 20° C.]:
0.1598



CC-3-V1
8.00%
Δε [1 kHz, 20° C.]:
−1.9



CCP-V-1
12.00%
ε [1 kHz, 20° C.]:
3.4



CCP-V2-1
12.00%
ε [1 kHz, 20° C.]:
5.3



PPTUI-3-2
10.00%



PTP-302FF
10.00%



PTP-502FF
10.00%



CPTP-302FF
4.00%



CPTP-502FF
4.00%










Example 70




















CY-3-O4
12.50%
Clearing point [° C.]:
75.4



CY-5-O2
10.00%
Δn [589 nm, 20° C.]:
0.1077



CCY-3-O1
4.50%
Δε [1 kHz, 20° C.]:
−3.2



CCY-3-O2
6.00%
ε [1 kHz, 20° C.]:
3.5



CLY-3-O2
7.00%
ε [1 kHz, 20° C.]:
6.7



CPY-2-O2
10.00%
V0 [20° C.]:
2.30



CPY-3-O2
10.00%
γ1 [mPa · s, 20° C.]:
112.9



CC-3-V
27.40%



BCH-32
3.50%



PP-1-2V1
9.00%



CDUQU-3-F
0.10%










Example 71




















CY-3-O2
15.00%
Clearing point [° C.]:
75.8



CY-3-O4
2.50%
Δn [589 nm, 20° C.]:
0.1021



CY-5-O2
10.00%
Δε [1 kHz, 20° C.]:
−3.2



CCY-3-O1
5.00%
ε [1 kHz, 20° C.]:
3.6



CCY-4-O2
5.00%
ε [1 kHz, 20° C.]:
6.8



CPY-2-O2
7.00%
K1 [pN, 20° C.]:
13.4



CPY-3-O2
7.00%
K3 [pN, 20° C.]:
13.5



CCY-2-1
6.00%
V0 [20° C.]:
2.14



CCY-3-1
6.00%
γ1 [mPa · s, 20° C.]:
128



CCH-23
15.50%



CCH-34
5.00%



BCH-32
13.00%



PP-1-4
3.00%










Example 72




















CC-3-V
33.00%
Clearing point [° C.]:
80.2



CCY-3-O1
6.00%
Δn [589 nm, 20° C.]:
0.1116



CCY-3-O2
8.00%
Δε [1 kHz, 20° C.]:
−4.1



CCY-4-O2
2.50%
ε [1 kHz, 20° C.]:
3.7



CPY-2-O2
8.00%
ε [1 kHz, 20° C.]:
7.8



CPY-3-O2
12.00%
K1 [pN, 20° C.]:
14.5



CLY-3-O2
8.00%
K3 [pN, 20° C.]:
16.1



PY-1-O4
1.50%
V0 [20° C.]:
2.09



PY-3-O2
10.00%
γ1 [mPa · s, 20° C.]:
119



PY-4-O2
8.00%



CY-3-O2
3.00%










Example 73




















BCH-32
2.00%
Clearing point [° C.]:
79.7



BCH-52
2.50%
Δn [589 nm, 20° C.]:
0.1036



CCY-2-1
9.50%
Δε [1 kHz, 20° C.]:
−3.7



CCY-3-1
9.50%
ε [1 kHz, 20° C.]:
4.8



CCY-3-O2
10.00%
ε [1 kHz, 20° C.]:
8.5



CCY-5-O2
10.00%
K1 [pN, 20° C.]:
13.9



CPY-2-O2
12.00%
K3 [pN, 20° C.]:
14.1



CY-3-O4
15.00%
V0 [20° C.]:
2.06



CY-5-O4
15.50%



PCH-53
10.50%



APUQU-3-F
3.50%










Example 74




















BCH-32
0.50%
Clearing point [° C.]:
79.2



BCH-52
0.50%
Δn [589 nm, 20° C.]:
0.1037



CCY-2-1
5.00%
Δε [1 kHz, 20° C.]:
−3.8



CCY-3-1
5.00%
ε [1 kHz, 20° C.]:
6.2



CCY-3-O2
13.00%
ε [1 kHz, 20° C.]:
10.0



CCY-5-O2
13.00%
K1 [pN, 20° C.]:
14.8



CPY-2-O2
12.00%
K3 [pN, 20° C.]:
14.5



CY-3-O4
19.50%
V0 [20° C.]:
2.12



CY-5-O4
19.50%



PCH-53
5.00%



APUQU-3-F
7.00%










Example 75




















CY-3-O2
27.50%
Clearing point [° C.]:
80.0



CCY-4-O2
26.50%
Δn [589 nm, 20° C.]:
0.0911



CPY-3-O2
13.50%
Δε [1 kHz, 20° C.]:
−3.6



CC-3-V
25.00%
ε [1 kHz, 20° C.]:
4.4



CCH-34
5.00%
ε [1 kHz, 20° C.]:
8.1



APUQU-3-F
2.50%










Example 76




















APUQU-3-F
7.00%
Clearing point [° C.]:
88.0



CC-3-V
35.00%
Δn [589 nm, 20° C.]:
0.1150



CC-3-V1
5.00%
Δε [1 kHz, 20° C.]:
−2.2



CCP-30CF3
5.00%
ε [1 kHz, 20° C.]:
1.0



CCP-V-1
12.00%
ε [1 kHz, 20° C.]:
3.1



CPGP-5-2
1.00%
K1 [pN, 20° C.]:
14.3



DPGU-4-F
8.00%
K3 [pN, 20° C.]:
14.7



PGP-2-2V
12.00%
V0 [20° C.]:
1.53



PUQU-3-F
10.00%
γ1 [mPa · s, 20° C.]:
66



CC-2-V1
5.00%










Example 77




















BCH-32
6.00%
Clearing point [° C.]:
101.6



CC-3-V
39.50%
Δn [589 nm, 20° C.]:
0.1111



CCP-3-1
6.50%
Δε [1 kHz, 20° C.]:
6.9



CCP-30CF3
1.00%
K1 [pN, 20° C.]:
15.3



CCP-V-1
16.00%
K3 [pN, 20° C.]:
17.3



CDUQU-3-F
9.50%
V0 [20° C.]:
1.57



CPGP-5-2
3.00%
γ1 [mPa · s, 20° C.]:
89



CPGP-5-3
1.00%
LTS [bulk, −30° C.]:
>1000 h



PGU-2-F
7.50%



PGUQU-3-F
3.50%



PGUQU-4-F
2.00%



PGUQU-5-F
3.50%



PPGU-3-F
1.00%










Example 78




















BCH-32
5.00%
Clearing point [° C.]:
102.5



CC-3-V
35.00%
Δn [589 nm, 20° C.]:
0.1207



CC-3-V1
5.00%
Δε [1 kHz, 20° C.]:
7.3



CCP-V-1
15.00%
K1 [pN, 20° C.]:
15.2



CDUQU-3-F
8.00%
K3 [pN, 20° C.]:
16.6



CPGP-4-3
3.00%
V0 [20° C.]:
1.53



CPGP-5-2
3.00%
γ1 [mPa · s, 20° C.]:
96



CPGP-5-3
3.00%
LTS [bulk, −30° C.]:
>1000 h



CPGU-3-OT
4.50%



PGU-2-F
5.50%



PGU-3-F
5.50%



PGUQU-3-F
2.50%



PPGU-3-F
0.50%



PUQU-3-F
4.50%










Example 79




















BCH-32
6.00%
Clearing point [° C.]:
101



CC-3-V
34.50%
Δn [589 nm, 20° C.]:
0.1210



CC-3-V1
6.00%
Δε [1 kHz, 20° C.]:
7.3



CCP-V-1
15.00%
K1 [pN, 20° C.]:
15.1



CDUQU-3-F
6.50%
K3 [pN, 20° C.]:
16.5



CPGP-4-3
3.00%
γ1 [mPa · s, 20° C.]:
92



CPGP-5-2
3.00%
LTS [bulk, −30° C.]:
>1000 h



CPGP-5-3
1.50%



CPGU-3-OT
5.00%



PGU-2-F
5.50%



PGU-3-F
4.50%



PGUQU-3-F
4.00%



PPGU-3-F
0.50%



PUQU-3-F
5.00%










Example 80




















APUQU-3-F
5.00%
Clearing point [° C.]:
104.4



BCH-3F.F
2.50%
Δn [589 nm, 20° C.]:
0.0947



CC-3-V
40.00%
Δε [1 kHz, 20° C.]:
7.2



CCGU-3-F
6.00%
K1 [pN, 20° C.]:
15.5



CCP-3-1
2.50%
K3 [pN, 20° C.]:
18.3



CCP-30CF3
7.00%
V0 [20° C.]:
1.55



CCP-V-1
12.00%
γ1 [mPa · s, 20° C.]:
93



CCP-V2-1
6.00%



CDUQU-3-F
10.00%



CPGP-5-2
2.00%



DPGU-4-F
2.50%



PPGU-3-F
0.50%



PUQU-3-F
4.00%










Example 81




















APUQU-3-F
5.00%
Clearing point [° C.]:
104.5



CC-3-V
39.00%
Δn [589 nm, 20° C.]:
0.0942



CCGU-3-F
10.00%
Δε [1 kHz, 20° C.]:
7.2



CCP-3-1
3.00%
K1 [pN, 20° C.]:
15.3



CCP-30CF3
7.50%
K3 [pN, 20° C.]:
18.5



CCP-V-1
13.00%
V0 [20° C.]:
1.54



CCP-V2-1
5.00%
γ1 [mPa · s, 20° C.]:
94



CDUQU-3-F
8.00%



CPGP-5-2
2.00%



PPGU-3-F
0.50%



PUQU-3-F
7.00%










Example 82




















APUQU-3-F
5.00%
Clearing point [° C.]:
104.5



CC-3-V
34.50%
Δn [589 nm, 20° C.]:
0.0940



CC-3-V1
4.50%
Δε [1 kHz, 20° C.]:
7.3



CCGU-3-F
10.00%
K1 [pN, 20° C.]:
15.5



CCP-3-1
3.00%
K3 [pN, 20° C.]:
18.7



CCP-30CF3
7.50%
V0 [20° C.]:
1.54



CCP-V-1
11.50%
γ1 [mPa · s, 20° C.]:
97



CCP-V2-1
4.00%



CCQU-3-F
4.00%



CDUQU-3-F
6.50%



CPGP-5-2
2.00%



PPGU-3-F
0.50%



PUQU-3-F
7.00%










Example 83




















BCH-3F.F.F
12.00%
Clearing point [° C.]:
101.2



CC-3-V
8.00%
Δn [589 nm, 20° C.]:
0.1079



CC-3-V1
9.00%
Δε [1 kHz, 20° C.]:
6.8



CC-4-V
10.00%
K1 [pN, 20° C.]:
14.2



CCGU-3-F
4.00%
K3 [pN, 20° C.]:
17.0



CCP-1F.F.F
4.50%
V0 [20° C.]:
1.53



CCP-30CF3
8.00%
γ1 [mPa · s, 20° C.]:
100



CCP-3F.F.F
8.00%



CCP-V-1
13.00%



CCP-V2-1
6.00%



CPGP-5-2
3.00%



CPGU-3-OT
1.50%



PGP-2-2V
3.00%



PPGU-3-F
1.00%



PUQU-3-F
9.00%










Example 84




















APUQU-2-F
5.50%
Clearing point [° C.]:
80.5



APUQU-3-F
3.00%
Δn [589 nm, 20° C.]:
0.1017



CC-3-V
36.00%
Δε [1 kHz, 20° C.]:
9.2



CC-3-V1
6.50%
ε [1 kHz, 20° C.]:
12.9



CCP-30CF3
8.00%
ε [1 kHz, 20° C.]:
3.7



CCP-V-1
11.50%
K1 [pN, 20° C.]:
11.8



CDUQU-3-F
5.00%
K3 [pN, 20° C.]:
12.8



DPGU-4-F
5.50%
V0 [20° C.]:
1.20



PGP-2-2V
2.00%
γ1 [mPa · s, 20° C.]:
53



PGU-2-F
7.50%



PUQU-3-F
9.50%










Example 84a

The mixture according to Example 84 additionally comprises 0.4% of RM-1.


Example 85




















BCH-32
3.00%
Clearing point [° C.]:
109.8



CCH-23
15.00%
Δn [589 nm, 20° C.]:
0.1028



CCH-34
3.00%
Δε [1 kHz, 20° C.]:
−3.7



CCH-35
7.00%
ε [1 kHz, 20° C.]:
3.3



CCP-3-1
7.00%
ε [1 kHz, 20° C.]:
7.0



CCY-3-1
8.00%
K1 [pN, 20° C.]:
20.4



CCY-3-O2
12.00%
K3 [pN, 20° C.]:
20.6



CCY-4-O2
10.00%



CCY-5-O2
5.50%



CPY-2-O2
5.00%



CPY-3-O2
11.00%



CY-3-O2
8.00%



PY-3-O2
5.50%










Example 86




















CC-3-V1
10.00%
Clearing point [° C.]:
74.6



CCH-23
18.50%
Δn [589 nm, 20° C.]:
0.1032



CCH-35
8.00%
Δε [1 kHz, 20° C.]:
−3.0



CCP-3-1
7.00%
ε [1 kHz, 20° C.]:
3.4



CCY-3-O2
12.00%
ε [1 kHz, 20° C.]:
6.3



CPY-3-O2
10.50%
K1 [pN, 20° C.]:
15.0



CY-3-O2
15.50%
K3 [pN, 20° C.]:
16.1



PY-3-O2
10.50%
V0 [20° C.]:
2.45



PYP-2-3
8.00%
γ1 [mPa · s, 20° C.]:
103










Example 86a

The mixture from Example 86 additionally comprises 0.001% of Irganox® 1076 (octadecyl 3-(3,5-di-tert-butyl-4-hydroxyphenyl)propionate, BASF) and 0.3% of RM-1.


Example 87

















CDUQU-3-F
7.00%
Clearing point [° C.]:
100


CCP-V-1
2.00%
Δn [589 nm, 20° C.]:
0.0714


CCQU-3-F
5.00%
Δε [1 kHz, 20° C.]:
8.3


CCQU-5-F
5.00%
ε [1 kHz, 20° C.]:
12.0


CCZU-3-F
13.50%
ε [1 kHz, 20° C.]:
3.8


CCZU-5-F
4.00%
K1 [pN, 20° C.]:
11.4


PUQU-3-F
1.00%
K3 [pN, 20° C.]:
15.8


CC-5-V
7.00%
V0 [20° C.]:
1.23


CCG-V-F
7.50%
γ1 [mPa · s, 20° C.]:
118


CCH-301
14.00%


CCP-2F.F.F
5.00%


CCP-30CF3.F
7.00%


CCP-3F.F.F
7.00%


CCP-5F.F.F
7.00%


CCPC-33
1.50%


CCPC-34
2.00%


CH-33
1.50%


CH-35
1.50%


CH-43
1.50%









Example 88




















APUQU-2-F
8.00%
Clearing point [° C.]:
88.9



APUQU-3-F
8.00%
Δn [589 nm, 20° C.]:
0.0987



CC-3-V
30.00%
Δε [1 kHz, 20° C.]:
5.9



CC-3-V1
8.50%
ε [1 kHz, 20° C.]:
8.9



CCP-3-1
4.00%
ε [1 kHz, 20° C.]:
2.9



CCP-V-1
16.00%
K1 [pN, 20° C.]:
13.4



CCP-V2-1
11.00%
K3 [pN, 20° C.]:
16.1



PP-1-2V1
6.00%
V0 [20° C.]:
1.59



PUQU-3-F
8.50%
γ1 [mPa · s, 20° C.]:
56










Example 89




















CC-3-V
28.50%
Clearing point [° C.]:
74.6



CC-3-V1
7.00%
Δn [589 nm, 20° C.]:
0.1040



CCY-3-O2
12.50%
Δε [1 kHz, 20° C.]:
−3.0



CCY-4-O2
5.25%
ε [1 kHz, 20° C.]:
3.5



CPY-3-O2
9.75%
ε [1 kHz, 20° C.]:
6.5



CY-3-O2
15.00%
K1 [pN, 20° C.]:
13.2



CY-3-O4
4.75%
K3 [pN, 20° C.]:
15.5



CY-5-O2
1.00%
V0 [20° C.]:
2.40



PCH-301
3.25%
γ1 [mPa · s, 20° C.]:
98



PPGU-3-F
0.50%



PYP-2-3
12.50%










Example 89a

The mixture from Example 89 additionally comprises 0.001% of Irganox® 1076 (octadecyl 3-(3,5-di-tert-butyl-4-hydroxyphenyl)propionate, BASF) and 0.3% of RM-1.


Example 90




















CC-3-V
15.00%
Clearing point [° C.]:
74.4



CC-3-V1
9.00%
Δn [589 nm, 20° C.]:
0.1086



CCH-23
8.00%
Δε [1 kHz, 20° C.]:
−3.2



CCH-34
7.50%
ε [1 kHz, 20° C.]:
3.5



CCY-3-O2
10.00%
ε [1 kHz, 20° C.]:
6.7



CCY-5-O2
8.00%
K1 [pN, 20° C.]:
14.3



CPY-2-O2
3.00%
K3 [pN, 20° C.]:
15.7



CPY-3-O2
8.50%
V0 [20° C.]:
2.33



CY-3-O2
7.00%
γ1 [mPa · s, 20° C.]:
102



PY-3-O2
16.00%



PYP-2-3
8.00%










Example 90a

The mixture from Example 90 additionally comprises 0.3% of RM-1.


Example 91




















CC-3-V
29.00%
Clearing point [° C.]:
103



CC-3-V1
9.00%
Δn [589 nm, 20° C.]:
0.1176



CC-3-2V1
7.00%
Δε [1 kHz, 20° C.]:
4.8



CCP-V-1
7.00%
ε [1 kHz, 20° C.]:
7.6



CCP-V2-1
7.50%
ε [1 kHz, 20° C.]:
2.9



PP-1-2V1
3.00%
K1 [pN, 20° C.]:
18.0



PGP-1-2V
4.00%
K3 [pN, 20° C.]:
19.6



PGP-2-2V
6.00%
V0 [20° C.]:
2.04



PGP-3-2V
4.00%
γ1 [mPa · s, 20° C.]:
82



CCP-30CF3
5.00%



CCGU-3-F
4.00%



PGUQU-4-F
3.50%



CDUQU-3-F
3.00%



DGUQU-4-F
4.00%



CPGU-3-OT
4.00%










Example 91a

The mixture from Example 91 additionally comprises 0.001% of STAB-35.


Example 92




















PGUQU-3-F
8.00%
Clearing point [° C.]:
82.5



PGUQU-4-F
9.00%
Δn [589 nm, 20° C.]:
0.2143



PGUQU-5-F
9.00%
Δε [1 kHz, 20° C.]:
65.8



PGU-2-F
7.00%
ε [1 kHz, 20° C.]:
73.4



PGU-3-F
8.00%
ε [1 kHz, 20° C.]:
7.6



PGP-2-3
8.00%



PGP-2-4
8.00%



ME2N.F
12.00%



ME3N.F
12.00%



BCH-3F.F
7.00%



BCH-5F.F
7.00%



DPGU-4-F
5.00%










Example 93

















CC-3-V
10.50%
Clearing point [° C.]:
100.8


CC-3-V1
5.50%
Δn [589 nm, 20° C.]:
0.0999


CCP-V-1
6.50%
Δε [1 kHz, 20° C.]:
9.1


PUQU-3-F
7.00%
ε [1 kHz, 20° C.]:
12.6


CCGU-3-F
6.00%
ε [1 kHz, 20° C.]:
3.5


APUQU-3-F
2.50%
K1 [pN, 20° C.]:
13.4


CCP-30CF3
8.00%
K3 [pN, 20° C.]:
17.0


CCP-50CF3
5.00%
V0 [pN, 20° C.]:
1.28


CCP-30CF3.F
12.00%
γ1 [mPa · s, 20° C.]:
126


CCQU-3-F
10.00%


CCP-1F.F.F
9.00%


CCP-3F.F.F
11.00%


PGP-2-2V
6.00%


CDU-2-F
1.00%









Example 94




















CY-3-O2
10.50%
Clearing point [° C.]:
79.7



PY-1-O4
5.00%
Δn [589 nm, 20° C.]:
0.1113



PY-3-O2
7.50%
Δε [1 kHz, 20° C.]:
−4.4



PY-4-O2
4.00%
K1 [pN, 20° C.]:
14.5



CCY-3-O1
5.50%
K3 [pN, 20° C.]:
16.7



CCY-3-O2
5.00%
V0 [20° C.]:
2.05



CCY-4-O2
4.00%



CLY-3-O2
9.00%



CPY-2-O2
9.00%



CPY-3-O2
9.00%



CC-3-V
23.50%



CC-3-V1
7.00%



CBC-33F
1.00%










Example 95




















DU-2-N
2.50%
Clearing point [° C.]:
94.0



ME2N.F
8.00%
Δn [589 nm, 20° C.]:
0.2530



ME3N.F
8.00%
Δε [1 kHz, 20° C.]:
47.6



ME4N.F
16.00%
ε [1 kHz, 20° C.]:
55.7



ME5N.F
8.00%
ε [1 kHz, 20° C.]:
8.1



HP-3N.F
5.00%
K1 [pN, 20° C.]:
11.3



HP-4N.F
5.00%
K3 [pN, 20° C.]:
13.8



HP-5N.F
2.50%
V0 [20° C.]:
0.51



PTP-102
5.00%
γ1 [mPa · s, 20° C.]:
464



PPTUI-3-2
20.00%



PPTUI-3-4
20.00%










Example 95a

The mixture according to Example 95 additionally comprises 5% of RM-41.


Example 96




















CCY-3-O1
7.50%
Clearing point [° C.]:
81.5



CCY-4-O2
3.50%
Δn [589 nm, 20° C.]:
0.1082



CLY-3-O2
7.00%
Δε [1 kHz, 20° C.]:
−2.7



CPY-2-O2
10.00%
ε [1 kHz, 20° C.]:
3.4



CPY-3-O2
10.00%
ε [1 kHz, 20° C.]:
6.1



PYP-2-3
9.00%
γ1 [mPa · s, 20° C.]:
88



CC-3-V
45.00%
K1 [pN, 20° C.]:
13.4



PY-1-O4
4.00%
K3 [pN, 20° C.]:
15.3



PY-3-O2
2.00%
V0 [20° C., V]:
2.53



Y-4O-O4
2.00%










Example 97




















CCY-3-O1
7.50%
Clearing point [° C.]:
81



CCY-4-O2
5.00%
Δn [589 nm, 20° C.]:
0.1054



CLY-3-O2
7.00%
Δε [1 kHz, 20° C.]:
−2.6



CPY-2-O2
10.00%
ε [1 kHz, 20° C.]:
3.4



CPY-3-O2
8.50%
ε [1 kHz, 20° C.]:
6.0



PYP-2-3
9.00%
γ1 [mPa · s, 20° C.]:
86



CC-3-V
45.50%
K1 [pN, 20° C.]:
13.3



PY-1-O4
5.00%
K3 [pN, 20° C.]:
15.1



Y-4O-O4
2.50%
V0 [20° C., V]:
2.54










Example 98




















CC-3-2V1
4.00%
Clearing point [° C.]:
100



CC-3-V
37.50%
Δn [589 nm, 20° C.]:
0.1047



CC-3-V1
5.00%
Δε [1 kHz, 20° C.]:
3.9



CCP-V-1
13.00%
ε [1 kHz, 20° C.]:
6.6



CCP-V2-1
7.50%
ε [1 kHz, 20° C.]:
2.7



CCVC-3-V
6.00%
γ1 [mPa · s, 20° C.]:
72



CDUQU-3-F
1.00%
K1 [pN, 20° C.]:
15.1



CPGP-5-2
3.00%
K3 [pN, 20° C.]:
17.4



DGUQU-4-F
2.00%
V0 [20° C., V]:
2.07



PGP-2-3
5.00%



PGP-2-4
3.00%



PGUQU-3-F
4.00%



PGUQU-4-F
3.50%



PPGU-3F
0.50%



PUQU-3F
5.00%










Example 99




















APUQU-2-F
1.50%
Clearing point [° C.]:
100



APUQU-3-F
5.00%
Δn [589 nm, 20° C.]:
0.1056



CC-3-2V1
4.00%
Δε [1 kHz, 20° C.]:
4.0



CC-3-V
36.00%
ε [1 kHz, 20° C.]:
6.8



CC-3-V1
5.00%
ε [1 kHz, 20° C.]:
2.8



CCP-V-1
13.00%
γ1 [mPa · s, 20° C.]:
71



CCP-V2-1
9.50%
K1 [pN, 20° C.]:
15.4



CCVC-3-V
4.00%
K3 [pN, 20° C.]:
17.7



CDUQU-3-F
3.00%
V0 [20° C., V]:
2.07



DGUQU-4-F
2.00%



PGP-1-2V
5.50%



PGP-2-2V
7.00%



PPGU-3-F
0.50%



PUQU-3-F
4.00%










Example 100




















CC-3-V1
9.00%
Clearing point [° C.]:
74.7



CCH-23
18.00%
Δn [589 nm, 20° C.]:
0.0982



CCH-34
3.00%
Δε [1 kHz, 20° C.]:
−3.4



CCH-35
7.00%
ε|| [1 kHz, 20° C.]:
3.5



CCP-3-1
5.50%
ε [1 kHz, 20° C.]:
6.9



CCY-3-O2
11.50%
γ1 [mPa · s, 20° C.]:
108



CPY-2-O2
8.00%
K1 [pN, 20° C.]:
14.9



CPY-3-O2
11.00%
K3 [pN, 20° C.]:
15.9



CY-3-O2
15.50%
V0 [20° C., V]:
2.28



PY-3-O2
11.50%










Example 100a

The mixture according to Example 100 additionally comprises 0.001% of Irganox® 1076 (octadecyl 3-(3,5-di-tert-butyl-4-hydroxyphenyl)propionate, BASF) and 0.45% of RM-1.


Example 101




















CC-3-V
15.00%
Clearing point [° C.]:
85



CPGP-4-3
2.00%
Δn [589 nm, 20° C.]:
0.1981



CPGP-5-2
2.00%
Δε [1 kHz, 20° C.]:
9.9



CPTP-301
6.00%
ε|| [1 kHz, 20° C.]:
13.6



DGUQU-4-F
3.00%
ε [1 kHz, 20° C.]:
3.7



PCH-301
7.00%
γ1 [mPa · s, 20° C.]:
123



PGP-2-2V
14.50%
K1 [pN, 20° C.]:
15.1



PGUQU-3-F
7.50%
K3 [pN, 20° C.]:
15.1



PGUQU-4-F
7.00%
V0 [20° C., V]:
1.29



PGUQU-5-F
6.00%



PP-1-2V1
12.00%



PTP-102
6.00%



PTP-201
6.00%



PUQU-3-F
6.00%










Example 102




















CC-3-V
28.00%
Clearing point [° C.]:
84.8



CC-3-V1
3.00%
Δn [589 nm, 20° C.]:
0.1078



CCP-3-1
3.00%
Δε [1 kHz, 20° C.]:
−4.1



CCY-3-O2
9.00%
ε|| [1 kHz, 20° C.]:
3.7



CCY-4-O2
9.00%
ε [1 kHz, 20° C.]:
7.8



CLY-3-O2
6.00%
γ1 [mPa · s, 20° C.]:
122



CLY-3-O3
6.00%
K1 [pN, 20° C.]:
14.8



CPY-2-O2
7.00%



CPY-3-O2
9.00%



PY-3-O2
8.00%



PY-4-O2
4.00%



PYP-2-4
2.50%



Y-4O-O4
5.50%










Example 102a

The mixture according to Example 102 additionally comprises 0.04% of




embedded image


and


0.01% of




embedded image


Example 103




















CC-3-V
28.00%
Clearing point [° C.]:
80



CC-3-V1
5.00%
Δn [589 nm, 20° C.]:
0.1082



CCP-3-1
2.50%
Δε [1 kHz, 20° C.]:
−4.1



CCY-3-O2
10.00%
ε|| [1 kHz, 20° C.]:
3.8



CCY-4-O2
2.50%
ε [1 kHz, 20° C.]:
7.9



CLY-3-O2
6.50%
γ1 [mPa · s, 20° C.]:
113



CLY-3-O3
6.50%
K1 [pN, 20° C.]:
14.5



CPY-2-O2
9.00%



CPY-3-O2
10.00%



PY-3-O2
10.00%



PY-4-O2
5.00%



Y-4O-O4
5.00%










Example 103a

The mixture according to Example 103 additionally comprises 0.04% of




embedded image


and 0.01% of




embedded image


Example 104




















CC-3-V
29.00%
Clearing point [° C.]:
75.1



CC-3-V1
5.00%
Δn [589 nm, 20° C.]:
0.1075



CCP-3-1
3.00%
Δε [1 kHz, 20° C.]:
−4.0



CCY-3-O2
10.00%
ε|| [1 kHz, 20° C.]:
3.8



CLY-3-O2
6.00%
ε [1 kHz, 20° C.]:
7.7



CLY-3-O3
6.00%
γ1 [mPa · s, 20° C.]:
103



CPY-2-O2
9.00%
K1 [pN, 20° C.]:
14.3



CPY-3-O2
10.00%



PY-3-O2
10.00%



PY-4-O2
7.00%



Y-4O-O4
5.00%










Example 104a

The mixture from Example 104 additionally comprises 0.04% of




embedded image


and 0.015% of




embedded image


Example 105




















CC-3-V
29.00%
Clearing point [° C.]:
80.1



CCY-3-O1
8.00%
Δn [589 nm, 20° C.]:
0.1052



CCY-3-O2
6.00%
Δε [1 kHz, 20° C.]:
−4.7



CCY-4-O2
2.00%
ε|| [1 kHz, 20° C.]:
3.9



CLY-3-O2
8.50%
ε [1 kHz, 20° C.]:
8.7



CLY-3-O3
7.50%
γ1 [mPa · s, 20° C.]:
125



CPY-2-O2
10.00%
K1 [pN, 20° C.]:
14.0



CPY-3-O2
7.50%



CY-3-O2
6.50%



PY-3-O2
10.00%



Y-4O-O4
5.00%










Example 105a

The mixture according to Example 105 additionally comprises 0.04% of




embedded image


and 0.02% of




embedded image


Example 106




















CC-3-V
37.00%
Clearing point [° C.]:
75.2



CCY-3-O1
5.00%
Δn [589 nm, 20° C.]:
0.1012



CCY-3-O2
5.00%
Δε [1 kHz, 20° C.]:
−3.8



CCY-4-O2
4.00%
ε|| [1 kHz, 20° C.]:
3.6



CLY-3-O2
7.00%
ε [1 kHz, 20° C.]:
7.5



CPY-2-O2
9.00%
γ1 [mPa · s, 20° C.]:
97



CPY-3-O2
10.00%
K1 [pN, 20° C.]:
13.3



CY-3-O2
12.00%
K3 [pN, 20° C.]:
15.3



PY-3-O2
11.00%
V0 [20° C., V]:
2.12










Example 106a

The mixture according to Example 106 additionally comprises 0.04% of




embedded image


and 0.015% of




embedded image


Example 107




















CY-3-O2
15.00%
Clearing point [° C.]:
80.4



CY-5-O2
12.50%
Δn [589 nm, 20° C.]:
0.1038



CCY-3-O1
2.50%
Δε [1 kHz, 20° C.]:
−3.3



CCY-4-O2
5.00%
ε|| [1 kHz, 20° C.]:
3.5



CPY-2-O2
8.00%
ε [1 kHz, 20° C.]:
6.8



CPY-3-O2
8.00%
γ1 [mPa · s, 20° C.]:
137



CCY-2-1
6.00%
K1 [pN, 20° C.]:
14.2



CCY-3-1
6.00%
K3 [pN, 20° C.]:
14.2



CCH-23
15.00%
V0 [20° C., V]:
2.18



CCH-34
5.00%



CCH-301
1.50%



BCH-32
15.50%










Example 107a

The mixture according to Example 107 additionally comprises 0.01% of




embedded image


Example 108




















CY-3-O2
15.00%
Clearing point [° C.]:
100



CY-3-O4
20.00%
Δn [589 nm, 20° C.]:
0.0968



CY-5-O2
7.50%
Δε [1 kHz, 20° C.]:
−5.9



CCY-3-O2
6.50%
ε|| [1 kHz, 20° C.]:
4.0



CCY-3-O3
6.50%
ε [1 kHz, 20° C.]:
9.9



CCY-4-O2
6.50%
γ1 [mPa · s, 20° C.]:
324



CCY-5-O2
6.50%
K1 [pN, 20° C.]:
15.1



CPY-2-O2
5.50%
K3 [pN, 20° C.]:
17.2



CPY-3-O2
5.00%
V0 [20° C., V]:
1.80



CC-4-V
3.00%



CH-33
3.00%



CH-35
2.00%



CH-43
3.00%



CH-45
2.00%



CCPC-33
4.00%



CCPC-34
4.00%










Example 109




















CY-3-O2
11.00%
Clearing point [° C.]:
101



CY-3-O4
18.00%
Δn [589 nm, 20° C.]:
0.1662



CCY-3-O2
6.00%
Δε [1 kHz, 20° C.]:
−6.1



CCY-3-O3
6.00%
ε|| [1 kHz, 20° C.]:
4.2



CCY-4-O2
6.00%
ε [1 kHz, 20° C.]:
10.3



CCY-5-O2
6.00%
γ1 [mPa · s, 20° C.]:
363



CPY-3-O2
6.00%
K1 [pN, 20° C.]:
16.5



CC-4-V
3.00%
K3 [pN, 20° C.]:
22.00



CPTP-3-1
5.00%
V0 [20° C., V]:
2.00



PTP-302FF
10.00%



PTP-502FF
10.00%



CPTP-302FF
5.00%



CPTP-502FF
5.00%



CCPC-33
3.00%










Example 110




















CY-3-O2
8.00%
Clearing point [° C.]:
101



CY-3-O4
13.00%
Δn [589 nm, 20° C.]:
0.0970



CCY-3-O2
6.50%
Δε [1 kHz, 20° C.]:
−2.1



CPY-2-O2
3.50%
ε|| [1 kHz, 20° C.]:
3.2



CPY-3-O2
8.00%
ε [1 kHz, 20° C.]:
5.3



CCH-301
5.00%
γ1 [mPa · s, 20° C.]:
136



CC-4-V
12.00%
K1 [pN, 20° C.]:
14.8



CC-5-V
8.00%
K3 [pN, 20° C.]:
18.3



CCP-V-1
13.00%
V0 [20° C., V]:
3.11



CCP-V2-1
13.00%



BCH-32
5.00%



CCPC-33
5.00%










Example 111




















CY-3-O4
12.00%
Clearing point [° C.]:
101



CC-4-V
13.00%
Δn [589 nm, 20° C.]:
0.1660



CC-5-V
9.50%
Δε [1 kHz, 20° C.]:
−2.1



CCP-V-1
10.50%
ε|| [1 kHz, 20° C.]:
3.4



CCP-V2-1
10.00%
ε [1 kHz, 20° C.]:
5.5



PTP-102
3.00%
γ1 [mPa · s, 20° C.]:
151



CPTP-3-1
5.00%
K1 [pN, 20° C.]:
16.2



CPTP-3-2
5.00%
K3 [pN, 20° C.]:
19.8



PTP-302FF
9.50%
V0 [20° C., V]:
3.25



PTP-502FF
9.50%



CPTP-302FF
6.50%



CPTP-502FF
6.50%










Example 112




















CY-3-O2
15.00%
Clearing point [° C.]:
71.9



CCY-3-O1
6.00%
Δn [589 nm, 20° C.]:
0.1203



CCY-3-O2
8.00%
Δε [1 kHz, 20° C.]:
−8.1



CCY-3-O3
5.50%
ε|| [1 kHz, 20° C.]:
5.2



CCY-4-O2
8.00%
ε [1 kHz, 20° C.]:
13.3



CCY-5-O2
8.00%
γ1 [mPa · s, 20° C.]:
253



CPY-2-O2
1.50%
K1 [pN, 20° C.]:
13.2



CPY-3-O2
10.00%
K3 [pN, 20° C.]:
15.7



CLY-3-O2
8.00%
V0 [20° C., V]:
1.46



PY-3-O2
6.00%



PY-1-O4
8.00%



PY-4-O2
8.00%



Y-4O-O4
8.00%










Example 113




















CC-3-V1
8.00%
Clearing point [° C.]:
75.5



CCH-23
18.00%
Δn [589 nm, 20° C.]:
0.0978



CCH-34
4.00%
Δε [1 kHz, 20° C.]:
−3.5



CCH-35
7.00%
ε|| [1 kHz, 20° C.]:
3.5



CCP-3-1
5.00%
ε [1 kHz, 20° C.]:
6.9



CCY-3-O2
12.50%
γ1 [mPa · s, 20° C.]:
111



CPY-2-O2
8.00%
K1 [pN, 20° C.]:
14.9



CPY-3-O2
11.00%
K3 [pN, 20° C.]:
15.8



CY-3-O2
15.50%
V0 [20° C., V]:
2.26



PY-3-O2
11.00%










Example 113a

The mixture according to Example 113 additionally comprises 0.3% of RM-1.


Example 114




















BCH-32
1.50%
Clearing point [° C.]:
74.8



CC-3-V
15.50%
Δn [589 nm, 20° C.]:
0.1035



CC-3-V1
11.00%
Δε [1 kHz, 20° C.]:
−3.1



CCH-23
12.00%
ε|| [1 kHz, 20° C.]:
3.4



CCH-34
3.50%
ε [1 kHz, 20° C.]:
6.5



CCY-3-O2
11.50%
γ1 [mPa · s, 20° C.]:
95



CCY-5-O2
0.50%
K1 [pN, 20° C.]:
14.1



CPY-2-O2
8.50%
K3 [pN, 20° C.]:
15.4



CPY-3-O2
12.00%
V0 [20° C., V]:
2.36



CY-3-O2
9.50%



PY-3-O2
11.50%



PYP-2-3
3.00%










Example 115a

The mixture according to Example 115 additionally comprises 0.001% of Irganox® 1076 (octadecyl 3-(3,5-di-tert-butyl-4-hydroxyphenyl)propionate, BASF) and 0.3% of RM-1.


Example 116




















CC-3-V
30.50%
Clearing point [° C.]:
79.8



CC-3-V1
4.50%
Δn [589 nm, 20° C.]:
0.1022



CCY-3-O1
5.00%
Δε [1 kHz, 20° C.]:
−4.0



CCY-3-O2
6.00%
ε|| [1 kHz, 20° C.]:
3.6



CCY-3-O3
4.00%
ε [1 kHz, 20° C.]:
7.6



CLY-3-O2
8.00%
γ1 [mPa · s, 20° C.]:
114



CPY-2-O2
8.00%
K1 [pN, 20° C.]:
14.5



CPY-3-O2
11.00%
K3 [pN, 20° C.]:
16.7



CY-3-O2
15.00%
V0 [20° C., V]:
2.14



PY-3-O2
8.00%










Example 117




















CY-3-O2
15.00%
Clearing point [° C.]:
80.4



CY-5-O2
12.50%
Δn [589 nm, 20° C.]:
0.1038



CCY-3-O1
2.50%
Δε [1 kHz, 20° C.]:
−3.3



CCY-4-O2
5.00%
ε|| [1 kHz, 20° C.]:
3.5



CPY-2-O2
8.00%
ε [1 kHz, 20° C.]:
6.8



CPY-3-O2
8.00%
γ1 [mPa · s, 20° C.]:
137



CCY-2-1
6.00%
K1 [pN, 20° C.]:
14.2



CCY-3-1
6.00%
K3 [pN, 20° C.]:
14.2



CCH-23
15.00%
V0 [20° C., V]:
2.18



CCH-34
5.00%



CCH-301
1.50%



BCH-32
15.50%










Example 118




















CY-3-O2
15.00%
Clearing point [° C.]:
80.5



CY-3-O4
4.00%
Δn [589 nm, 20° C.]:
0.1025



CY-5-O2
6.50%
Δε [1 kHz, 20° C.]:
−3.4



CCY-3-O1
5.00%
ε|| [1 kHz, 20° C.]:
3.5



CCY-3-O3
2.00%
ε [1 kHz, 20° C.]:
6.9



CCY-4-O2
6.00%
γ1 [mPa · s, 20° C.]:
141



CPY-2-O2
7.00%
K1 [pN, 20° C.]:
14.0



CPY-3-O2
7.00%
K3 [pN, 20° C.]:
14.1



CCY-2-1
6.00%
V0 [20° C., V]:
2.16



CCY-3-1
6.00%



CCH-23
15.50%



CCH-34
5.00%



BCH-32
13.00%



PP-1-4
2.00%










Example 119




















PGUQU-3-F
4.00%
Clearing point [° C.]:
85.4



CCQU-3-F
7.50%
Δn [589 nm, 20° C.]:
0.1028



PUQU-3-F
15.50%
Δε [1 kHz, 20° C.]:
9.9



APUQU-2-F
4.00%
ε|| [1 kHz, 20° C.]:
13.3



APUQU-3-F
7.50%
ε [1 kHz, 20° C.]:
3.4



CC-3-V
27.50%
γ1 [mPa · s, 20° C.]:
82



CCP-3-V1
6.00%
K1 [pN, 20° C.]:
12.6



CCP-V-1
13.00%
K3 [pN, 20° C.]:
15.3



CCP-V2-1
10.00%
V0 [20° C., V]:
1.19



PPGU-3-F
0.50%



BCH-3F.F
4.50%










Example 119a

The mixture according to Example 119 additionally comprises 0.01% of




embedded image


Example 120




















CC-3-V
30.50%
Clearing point [° C.]:
80.1



CC-3-V1
4.50%
Δn [589 nm, 20° C.]:
0.1033



CCY-3-O1
6.00%
Δε [1 kHz, 20° C.]:
−4.0



CCY-3-O2
8.00%
ε|| [1 kHz, 20° C.]:
3.6



CLY-3-O2
8.00%
ε [1 kHz, 20° C.]:
7.6



CPY-2-O2
8.00%
γ1 [mPa · s, 20° C.]:
113



CPY-3-O2
12.00%
K1 [pN, 20° C.]:
14.4



CY-3-O2
15.00%
K3 [pN, 20° C.]:
17.0



PY-3-O2
8.00%
V0 [20° C., V]:
2.16










Example 120a

The mixture from Example 120 additionally comprises 0.3% of




embedded image


Example 121




















CC-3-V
28.50%
Clearing point [° C.]:
74.6



CC-3-V1
7.00%
Δn [589 nm, 20° C.]:
0.1040



CCY-3-O2
12.50%
Δε [1 kHz, 20° C.]:
−3.0



CCY-4-O2
5.25%
ε|| [1 kHz, 20° C.]:
3.5



CPY-3-O2
9.75%
ε [1 kHz, 20° C.]:
6.5



CY-3-O2
15.00%
γ1 [mPa · s, 20° C.]:
98



CY-3-O4
4.75%
K1 [pN, 20° C.]:
13.2



CY-5-O2
1.00%
K3 [pN, 20° C.]:
15.5



PCH-301
3.25%
V0 [20° C., V]:
2.4



PPGU-3-F
0.50%



PYP-2-3
12.50%










Example 121a

The mixture from Example 121 additionally comprises 0.001% of Irganox® 1076 (octadecyl 3-(3,5-di-tert-butyl-4-hydroxyphenyl)propionate. BASF) and 0.45% of RM-1.


Example 122




















CC-3-V
36.50%
Clearing point [° C.]:
75



CC-3-V1
2.00%
Δn [589 nm, 20° C.]:
0.1015



CCY-3-O1
8.00%
Δε [1 kHz, 20° C.]:
−3.7



CCY-3-O2
6.00%
ε|| [1 kHz, 20° C.]:
3.7



CCY-4-O2
2.50%
ε [1 kHz, 20° C.]:
7.3



CLY-3-O2
8.00%
γ1 [mPa · s, 20° C.]:
97



CLY-3-O3
2.00%
K1 [pN, 20° C.]:
13.8



CPY-2-O2
10.00%
K3 [pN, 20° C.]:
15



CPY-3-O2
3.00%
V0 [20° C., V]:
2.14



CY-3-O2
5.50%



PY-3-O2
13.00%



PY-1-O4
3.50%










Example 123




















BCH-32
4.50%
Clearing point [° C.]:
75.5



CCH-23
14.00%
Δn [589 nm, 20° C.]:
0.0938



CCH-301
7.00%
Δε [1 kHz, 20° C.]:
−2.5



CCH-34
9.00%
ε|| [1 kHz, 20° C.]:
3.3



CCH-35
5.50%
ε [1 kHz, 20° C.]:
5.8



CCP-3-1
10.00%
γ1 [mPa · s, 20° C.]:
89



CY-3-O2
5.00%
K1 [pN, 20° C.]:
13.5



CY-V-O2
7.00%
K3 [pN, 20° C.]:
14.5



CCY-3-O1
5.00%
V0 [20° C., V]:
2.54



CCY-3-O2
9.00%



CPY-V-O2
10.00%



PCH-302
5.00%



PY-V2-O2
9.00%










Example 124




















BCH-32
1.50%
Clearing point [° C.]:
75



CC-3-V
37.00%
Δn [589 nm, 20° C.]:
0.0960



CCP-3-1
8.00%
Δε [1 kHz, 20° C.]:
−2.6



CY-3-O2
15.00%
ε|| [1 kHz, 20° C.]:
3.4



CCY-3-O1
7.00%
ε [1 kHz, 20° C.]:
6.0



CCY-3-O2
9.50%
γ1 [mPa · s, 20° C.]:
79



CPY-3-O2
8.50%
K1 [pN, 20° C.]:
13.0



PCH-302
5.50%
K3 [pN, 20° C.]:
16.0



PY-V-O2
8.00%
V0 [20° C., V]:
2.6










Example 125




















BCH-32
1.00%
Clearing point [° C.]:
75



CC-3-V
41.00%
Δn [589 nm, 20° C.]:
0.0948



CCP-3-1
8.50%
Δε [1 kHz, 20° C.]:
−2.3



CY-3-O2
13.00%
ε|| [1 kHz, 20° C.]:
3.2



CCY-3-O1
6.50%
ε [1 kHz, 20° C.]:
5.5



CCY-3-O2
8.50%
γ1 [mPa · s, 20° C.]:
70



CPY-3-O2
6.00%
K1 [pN, 20° C.]:
13.4



PCH-302
7.00%
K3 [pN, 20° C.]:
16.5



PY-1V-O2
8.50%
V0 [20° C., V]:
2.84










Example 126




















PY-3-O2
7.50%
Clearing point [° C.]:
74



PY-1V-O2
4.00%
Δn [589 nm, 20° C.]:
0.1094



CY-3-O2
14.50%
Δε [1 kHz, 20° C.]:
−3.0



CCY-3-O1
3.00%
ε|| [1 kHz, 20° C.]:
3.6



CCY-3-O2
9.00%
ε [1 kHz, 20° C.]:
6.6



CPY-2-O2
7.50%
γ1 [mPa · s, 20° C.]:
85



CPY-3-O2
9.00%
K1 [pN, 20° C.]:
12.9



CC-3-V
37.00%
K3 [pN, 20° C.]:
14.6



BCH-32
8.00%
V0 [20° C., V]:
2.34



PPGU-3-F
0.50%










Example 127




















PY-3-O2
8.00%
Clearing point [° C.]:
74.5



PY-3V-O2
5.00%
Δn [589 nm, 20° C.]:
0.1086



CY-3-O2
11.50%
Δε [1 kHz, 20° C.]:
−3.0



CCY-3-O1
10.00%
ε|| [1 kHz, 20° C.]:
3.6



CCY-3-O2
4.00%
ε [1 kHz, 20° C.]:
6.6



CPY-2-O2
10.00%
γ1 [mPa · s, 20° C.]:
87



CPY-3-O2
7.00%
K1 [pN, 20° C.]:
12.9



CC-3-V
37.50%
K3 [pN, 20° C.]:
14.1



BCH-32
6.50%
V0 [20° C., V]:
2.30



PPGU-3-F
0.50%










Example 128




















PY-V2-O2
12.00%
Clearing point [° C.]:
76



CY-V-O2
9.00%
Δn [589 nm, 20° C.]:
0.1087



CCY-3-O1
9.00%
Δε [1 kHz, 20° C.]:
−3.1



CCY-V2-O2
8.00%
ε|| [1 kHz, 20° C.]:
3.7



CPY-2-O2
8.00%
ε [1 kHz, 20° C.]:
6.9



CPY-V-O2
10.50%
γ1 [mPa · s, 20° C.]:
83



CC-3-V
36.50%
K1 [pN, 20° C.]:
12.4



BCH-32
6.50%
K3 [pN, 20° C.]:
14.7



PPGU-3-F
0.50%
V0 [20° C., V]:
2.28










Example 129




















PY-V2-O2
11.50%
Clearing point [° C.]:
75.5



CY-3-O2
11.00%
Δn [589 nm, 20° C.]:
0.1074



CCY-3-O1
9.00%
Δε [1 kHz, 20° C.]:
−3.1



CCY-3-O2
4.00%
ε|| [1 kHz, 20° C.]:
3.7



CPY-2-O2
12.00%
ε [1 kHz, 20° C.]:
6.8



CPY-3-O2
9.00%
γ1 [mPa · s, 20° C.]:
87



CC-3-V
37.00%
K1 [pN, 20° C.]:
13.0



BCH-32
6.00%
K3 [pN, 20° C.]:
14.7



PPGU-3-F
0.50%
V0 [20° C., V]:
2.29










Example 130




















PY-1V-O2
10.50%
Clearing point [° C.]:
72



CY-3-O2
18.00%
Δn [589 nm, 20° C.]:
0.1068



CCY-3-O1
7.00%
Δε [1 kHz, 20° C.]:
−3.1



CCY-3-O2
5.00%
ε|| [1 kHz, 20° C.]:
3.6



CPY-2-O2
7.00%
ε [1 kHz, 20° C.]:
6.7



CPY-3-O2
8.00%
γ1 [mPa · s, 20° C.]:
78



CC-3-V
41.00%
K1 [pN, 20° C.]:
12.6



BCH-32
3.00%
K3 [pN, 20° C.]:
14.6



PPGU-3-F
0.50%
V0 [20° C., V]:
2.30










Example 131




















PY-V2-O2
10.50%
Clearing point [° C.]:
75



CY-3-O2
10.00%
Δn [589 nm, 20° C.]:
0.1070



CCY-3-O1
6.00%
Δε [1 kHz, 20° C.]:
−3.3



CCY-3-O2
9.00%
ε|| [1 kHz, 20° C.]:
3.7



CPY-2-O2
8.00%
ε [1 kHz, 20° C.]:
7.0



CPY-3-O2
12.00%
γ1 [mPa · s, 20° C.]:
90



CC-3-V
35.00%
K1 [pN, 20° C.]:
12.7



BCH-32
6.50%
K3 [pN, 20° C.]:
14.5



PPGU-3-F
0.50%
V0 [20° C., V]:
2.23



Y-4O-O4
2.50%
LTS (bulk) [−20° C.]:
>1000 h





LTS (bulk) [−30° C.]:
>1000 h










Example 132




















PY-1V-O2
10.00%
Clearing point [° C.]:
73.5



CY-3-O2
18.00%
Δn [589 nm, 20° C.]:
0.1084



CCY-3-O1
6.00%
Δε [1 kHz, 20° C.]:
−3.2



CCY-3-O2
6.00%
ε|| [1 kHz, 20° C.]:
3.6



CPY-2-O2
7.00%
ε [1 kHz, 20° C.]:
6.8



CPY-3-O2
9.00%
γ1 [mPa · s, 20° C.]:
82



CC-3-V
40.00%
K1 [pN, 20° C.]:
12.8



BCH-32
3.50%
K3 [pN, 20° C.]:
14.9



PPGU-3-F
0.50%
V0 [20° C., V]:
2.3










Example 133




















PY-V2-O2
11.50%
Clearing point [° C.]:
74.5



CY-3-O2
10.00%
Δn [589 nm, 20° C.]:
0.1071



CCY-3-O1
4.50%
Δε [1 kHz, 20° C.]:
−3.4



CCY-3-O2
11.00%
ε|| [1 kHz, 20° C.]:
3.8



CPY-2-O2
7.00%
ε [1 kHz, 20° C.]:
7.1



CPY-3-O2
12.50%
γ1 [mPa · s, 20° C.]:
91



CC-3-V
34.50%
K1 [pN, 20° C.]:
12.7



BCH-32
6.00%
K3 [pN, 20° C.]:
14.6



PPGU-3-F
0.50%
V0 [20° C., V]:
2.2



Y-4O-O4
2.50%










Example 134




















PY-V2-O2
14.00%
Clearing point [° C.]:
74.5



CY-3-O2
10.50%
Δn [589 nm, 20° C.]:
0.1075



CCY-3-O1
5.00%
Δε [1 kHz, 20° C.]:
−3.2



CCY-3-O2
10.00%
ε|| [1 kHz, 20° C.]:
3.6



CPY-2-O2
9.00%
ε [1 kHz, 20° C.]:
6.8



CPY-3-O2
12.00%
γ1 [mPa · s, 20° C.]:
90



CC-3-V
36.50%
K1 [pN, 20° C.]:
11.7



BCH-32
2.50%
K3 [pN, 20° C.]:
14.1



PPGU-3-F
0.50%
V0 [20° C., V]:
2.21










Example 135




















PY-3V-O2
10.50%
Clearing point [° C.]:
74.5



CY-3-O2
15.00%
Δn [589 nm, 20° C.]:
0.1073



CCY-3-O1
7.50%
Δε [1 kHz, 20° C.]:
−3.0



CCY-3-O2
4.00%
ε|| [1 kHz, 20° C.]:
3.6



CPY-2-O2
11.00%
ε [1 kHz, 20° C.]:
6.6



CPY-3-O2
8.00%
γ1 [mPa · s, 20° C.]:
84



CC-3-V
40.50%
K1 [pN, 20° C.]:
12.8



BCH-32
3.00%
K3 [pN, 20° C.]:
14.1



PPGU-3-F
0.50%
V0 [20° C., V]:
2.29










Example 136




















CC-3-V
36.50%
Clearing point [° C.]:
73



CY-3-O2
10.00%
Δn [589 nm, 20° C.]:
0.1081



CCY-3-O1
6.50%
Δε [1 kHz, 20° C.]:
−3.3



CCY-3-O2
11.00%
ε|| [1 kHz, 20° C.]:
3.5



CCY-4-O2
6.00%
ε [1 kHz, 20° C.]:
6.8



CPY-3-O2
8.50%
γ1 [mPa · s, 20° C.]:
90



PY-3-O2
4.00%
K1 [pN, 20° C.]:
13.2



PY-3V-O2
6.50%
K3 [pN, 20° C.]:
15.0



PY-1-O4
4.50%
V0 [20° C., V]:
2.25



PYP-2-3
3.00%



PP-1-2V1
3.50%










Example 137




















PY-V2-O2
7.00%
Clearing point [° C.]:
75.5



CY-3-O2
10.00%
Δn [589 nm, 20° C.]:
0.1086



CY-1V2-O2
6.00%
Δε [1 kHz, 20° C.]:
−2.7



CCY-3-O1
5.00%
ε|| [1 kHz, 20° C.]:
3.5



CCY-3-O2
2.00%
ε [1 kHz, 20° C.]:
6.2



CPY-2-O2
12.00%
γ1 [mPa · s, 20° C.]:
85



CPY-3-O2
10.00%
K1 [pN, 20° C.]:
12.8



CC-3-V
37.00%
K3 [pN, 20° C.]:
14.5



BCH-32
10.50%
V0 [20° C., V]:
2.45



PPGU-3-F
0.50%
LTS (bulk) [−20° C.]:
>1000 h










Example 138




















PY-V-O2
5.00%
Clearing point [° C.]:
75



PY-V2-O2
5.00%
Δn [589 nm, 20° C.]:
0.1087



PY-3-O2
3.00%
Δε [1 kHz, 20° C.]:
−3.1



CY-V-O2
4.00%
ε|| [1 kHz, 20° C.]:
3.7



CY-3-O2
3.00%
ε [1 kHz, 20° C.]:
6.8



CCY-3-O1
3.50%
γ1 [mPa · s, 20° C.]:
83



CCY-3-O2
7.00%
K1 [pN, 20° C.]:
12.6



CCY-4-O2
5.00%
K3 [pN, 20° C.]:
14.2



CPY-2-O2
8.00%
V0 [20° C., V]:
2.28



CPY-3-O2
10.00%
LTS (bulk) [−20° C.]:
>1000 h



CC-3-V
38.00%



BCH-32
6.00%



PPGU-3-F
0.50%



Y-4O-O4
2.00%










Example 139




















PY-V2-O2
5.50%
Clearing point [° C.]:
75.5



PY-3-O2
8.00%
Δn [589 nm, 20° C.]:
0.1075



CY-V-O2
6.00%
Δε [1 kHz, 20° C.]:
−3.1



CCY-3-O1
5.50%
ε|| [1 kHz, 20° C.]:
3.7



CCY-3-O2
5.00%
ε [1 kHz, 20° C.]:
6.8



CCY-4-O2
4.00%
γ1 [mPa · s, 20° C.]:
88



CPY-2-O2
8.00%
K1 [pN, 20° C.]:
12.6



CPY-3-O2
9.00%
K3 [pN, 20° C.]:
14.0



CC-3-V
35.00%
V0 [20° C., V]:
2.26



BCH-32
8.00%
LTS (bulk) [−20° C.]:
>1000 h



PPGU-3-F
0.50%
LTS (bulk) [−30° C.]:
>1000 h



Y-4O-O4
2.00%










Example 140




















PY-V-O2
5.50%
Clearing point [° C.]:
74.5



PY-3-O2
4.50%
Δn [589 nm, 20° C.]:
0.1098



CY-3-O2
11.00%
Δε [1 kHz, 20° C.]:
−3.0



CCY-3-O2
10.50%
ε|| [1 kHz, 20° C.]:
3.7



CPY-2-O2
10.00%
ε [1 kHz, 20° C.]:
6.7



CPY-3-O2
11.00%
γ1 [mPa · s, 20° C.]:
85



CC-3-V
37.00%
K1 [pN, 20° C.]:
12.9



BCH-32
8.00%
K3 [pN, 20° C.]:
14.5



PPGU-3-F
0.50%
V0 [20° C., V]:
2.31



Y-4O-O4
2.00%
LTS (bulk) [−20° C.]:
>1000 h





LTS (bulk) [−30° C.]:
>1000 h










Example 141




















PY-3-O2
6.00%
Clearing point [° C.]:
75



PY-V2-O2
6.00%
Δn [589 nm, 20° C.]:
0.1079



CY-3-O2
12.00%
Δε [1 kHz, 20° C.]:
−3.2



CCY-3-O1
4.00%
ε|| [1 kHz, 20° C.]:
3.7



CCY-3-O2
9.50%
ε [1 kHz, 20° C.]:
6.9



CPY-2-O2
9.50%
γ1 [mPa · s, 20° C.]:
91



CPY-3-O2
10.00%
K1 [pN, 20° C.]:
13.1



CC-3-V
35.50%
K3 [pN, 20° C.]:
14.9



BCH-32
7.00%
V0 [20° C., V]:
2.29



PPGU-3-F
0.50%
LTS (bulk) [−20° C.]:
>1000 h





LTS (bulk) [−30° C.]:
>1000 h










Example 142




















PY-3-O2
6.00%
Clearing point [° C.]:
75



PY-1V2-O2
6.50%
Δn [589 nm, 20° C.]:
0.1088



CY-3-O2
13.00%
Δε [1 kHz, 20° C.]:
−3.3



CCY-3-O2
12.00%
ε|| [1 kHz, 20° C.]:
3.7



CPY-2-O2
8.00%
ε [1 kHz, 20° C.]:
6.9



CPY-3-O2
12.00%
γ1 [mPa · s, 20° C.]:
93



CC-3-V
36.00%
K1 [pN, 20° C.]:
13.5



BCH-32
6.00%
K3 [pN, 20° C.]:
15.6



PPGU-3-F
0.50%
V0 [20° C., V]:
2.32










Example 143




















PY-3-O2
4.50%
Clearing point [° C.]:
75



PY-V2-O2
6.00%
Δn [589 nm, 20° C.]:
0.1078



CY-3-O2
10.00%
Δε [1 kHz, 20° C.]:
−3.1



CCY-3-O1
2.00%
ε|| [1 kHz, 20° C.]:
3.7



CCY-3-O2
11.00%
ε [1 kHz, 20° C.]:
6.8



CPY-2-O2
8.00%
γ1 [mPa · s, 20° C.]:
88



CPY-3-O2
12.00%
K1 [pN, 20° C.]:
13.0



CC-3-V
36.00%
K3 [pN, 20° C.]:
14.8



BCH-32
8.00%
V0 [20° C., V]:
2.31



PPGU-3-F
0.50%
LTS (bulk) [−30° C.]
>1000 h



Y-4O-O4
2.00%










Example 143a

The mixture according to Example 143 additionally comprises 0.01% of




embedded image


Example 144




















BCH-32
6.00%
Clearing point [° C.]:
77



CCH-23
16.00%
Δn [589 nm, 20° C.]:
0.0953



CCH-301
3.50%
Δε [1 kHz, 20° C.]:
−2.5



CCH-34
6.00%
ε|| [1 kHz, 20° C.]:
3.3



CCH-35
6.00%
ε [1 kHz, 20° C.]:
5.8



CCP-3-1
12.00%
γ1 [mPa · s, 20° C.]:
96



CY-3-O2
15.00%
K1 [pN, 20° C.]:
14.6



CCY-3-O1
5.00%
K3 [pN, 20° C.]:
15.6



CCY-3-O2
7.00%
V0 [20° C., V]:
2.66



CPY-3-O2
8.50%
LTS (bulk) [−20° C.]
>1000 h



PCH-302
6.00%
LTS (bulk) [−30° C.]
>1000 h



PY-V2-O2
9.00%










Example 145




















BCH-32
4.00%
Clearing point [° C.]:
76



CC-3-V
34.50%
Δn [589 nm, 20° C.]:
0.0955



CCP-3-1
10.00%
Δε [1 kHz, 20° C.]:
−2.5



CY-3-O2
14.00%
ε|| [1 kHz, 20° C.]:
3.4



CCY-3-O1
6.00%
ε [1 kHz, 20° C.]:
5.9



CCY-3-O2
9.00%
γ1 [mPa · s, 20° C.]:
82



CPY-3-O2
9.00%
K1 [pN, 20° C.]:
13.4



PCH-302
4.50%
K3 [pN, 20° C.]:
16.2



PY-V2-O2
9.00%
V0 [20° C., V]:
2.66





LTS (bulk) [−20° C.]:
>1000 h





LTS (bulk) [−30° C.]:
>1000 h










Example 146




















BCH-32
6.50%
Clearing point [° C.]:
76.5



CCH-23
16.00%
Δn [589 nm, 20° C.]:
0.0933



CCH-301
4.50%
Δε [1 kHz, 20° C.]:
−2.5



CCH-34
8.00%
ε [1 kHz, 20° C.]:
3.3



CCH-35
6.00%
ε [1 kHz, 20° C.]:
5.8



CCP-3-1
8.50%
γ1 [mPa · s, 20° C.]:
96



CY-3-O2
15.00%
K1 [pN, 20° C.]:
14.3



CCY-3-O1
5.50%
K3 [pN, 20° C.]:
15.0



CCY-3-O2
8.00%
V0 [20° C., V]:
2.57



CPY-3-O2
9.00%



PCH-302
4.50%



PY-V2-O2
8.50%










Example 147




















Y-4O-O4
7.00%
Clearing point [° C.]:
75.5



PY-1-O4
2.00%
Δn [589 nm, 20° C.]:
0.1062



CCY-3-O1
2.50%
Δε [1 kHz, 20° C.]:
−2.2



CCY-3-O2
8.00%
ε [1 kHz, 20° C.]:
3.4



CPY-3-O2
10.00%
ε [1 kHz, 20° C.]:
5.5



PYP-2-3
8.50%
γ1 [mPa · s, 20° C.]:
90



CCH-23
19.00%
K1 [pN, 20° C.]:
14.5



CCH-34
6.00%
K3 [pN, 20° C.]:
14.2



CCH-35
6.00%
V0 [20° C., V]:
2.70



PCH-302
8.00%



BCH-32
7.00%



CCP-3-1
10.00%



PY-V2-O2
6.00%










Example 148




















BCH-32
7.00%
Clearing point [° C.]:
75



CCH-23
16.00%
Δn [589 nm, 20° C.]:
0.0930



CCH-301
3.50%
Δε [1 kHz, 20° C.]:
−2.5



CCH-34
6.50%
ε [1 kHz, 20° C.]:
3.3



CCH-35
6.50%
ε [1 kHz, 20° C.]:
5.8



CCP-3-1
9.50%
γ1 [mPa · s, 20° C.]:
93



CY-3-O2
7.50%
K1 [pN, 20° C.]:
13.7



CY-V1-O2
7.00%
K3 [pN, 20° C.]:
14.1



CCY-3-O1
6.00%
V0 [20° C., V]:
2.52



CCY-3-O2
9.00%
LTS (bulk) [−20° C.]
>1000 h



CPY-3-O2
7.00%



PCH-302
5.00%



PY-V2-O2
9.50%










Example 149




















BCH-32
7.00%
Clearing point [° C.]:
74



CCH-23
15.00%
Δn [589 nm, 20° C.]:
0.0921



CCH-301
4.00%
Δε [1 kHz, 20° C.]:
−2.5



CCH-34
8.00%
ε [1 kHz, 20° C.]:
3.4



CCH-35
7.00%
ε [1 kHz, 20° C.]:
5.9



CCP-3-1
8.00%
γ1 [mPa · s, 20° C.]:
95



CY-3-O2
9.00%
K1 [pN, 20° C.]:
13.4



CY-V1-O2
7.00%
K3 [pN, 20° C.]:
14.1



CCY-3-O1
9.00%
V0 [20° C., V]:
2.49



CCY-3-O2
7.00%



CPY-1V-O1
7.00%



PCH-302
4.00%



PY-V2-O2
8.00%










Example 150




















BCH-32
7.00%
Clearing point [° C.]:
77



CCH-23
13.00%
Δn [589 nm, 20° C.]:
0.0935



CCH-301
3.00%
Δε [1 kHz, 20° C.]:
−2.4



CCH-34
10.00%
ε [1 kHz, 20° C.]:
3.3



CCH-35
6.00%
ε [1 kHz, 20° C.]:
5.7



CCP-3-1
10.50%
γ1 [mPa · s, 20° C.]:
97



CY-3-O2
8.50%
K1 [pN, 20° C.]:
14.1



CY-V1-O2
5.50%
K3 [pN, 20° C.]:
14.6



CCY-3-O1
10.00%
V0 [20° C., V]:
2.62



CCY-3-O2
6.00%



CPY-1V-O1
5.50%



PCH-302
6.00%



PY-V2-O2
9.00%










Example 151




















CY-3-O2
9.50%
Clearing point [° C.]:
75



PY-V-O2
9.50%
Δn [589 nm, 20° C.]:
0.1101



CCY-3-O2
9.00%
Δε [1 kHz, 20° C.]:
−3.0



CCY-4-O2
6.00%
ε [1 kHz, 20° C.]:
3.5



CPY-2-O2
5.00%
ε [1 kHz, 20° C.]:
6.5



CPY-3-O2
9.50%
γ1 [mPa · s, 20° C.]:
100



CCH-34
10.00%
K1 [pN, 20° C.]:
13.4



CCH-23
21.00%
K3 [pN, 20° C.]:
14.3



PYP-2-3
7.00%
V0 [20° C., V]:
2.31



CCP-3-1
3.00%



PCH-301
10.50%










Example 152




















PY-3-O2
11.00%
Clearing point [° C.]:
75



PY-1V-O2
8.00%
Δn [589 nm, 20° C.]:
0.1100



CY-3-O2
5.00%
Δε [1 kHz, 20° C.]:
−3.4



CCY-3-O2
9.00%
ε [1 kHz, 20° C.]:
3.5



CCY-3-O1
6.00%
ε [1 kHz, 20° C.]:
6.9



CPY-2-O2
7.00%
γ1 [mPa · s, 20° C.]:
107



CPY-3-O2
10.00%
K1 [pN, 20° C.]:
14.3



CCH-34
10.00%
K3 [pN, 20° C.]:
15.2



CCH-23
21.00%
V0 [20° C., V]:
2.24



CCP-3-1
4.00%



PCH-301
9.00%










Example 153




















CY-3-O2
10.00%
Clearing point [° C.]:
75



PY-V-O2
9.00%
Δn [589 nm, 20° C.]:
0.1099



CCY-3-O2
9.00%
Δε [1 kHz, 20° C.]:
−3.2



CCY-4-O2
7.00%
ε [1 kHz, 20° C.]:
3.5



CPY-2-O2
7.00%
ε [1 kHz, 20° C.]:
6.7



CPY-3-O2
9.00%
γ1 [mPa · s, 20° C.]:
104



CCH-34
11.00%
K1 [pN, 20° C.]:
13.2



CCH-23
20.00%
K3 [pN, 20° C.]:
14.1



PYP-2-3
7.00%
V0 [20° C., V]:
2.24



CCP-3-1
1.00%



PCH-301
10.00%










Example 154




















CY-3-O2
12.50%
Clearing point [° C.]:
74



PY-3-O2
4.00%
Δn [589 nm, 20° C.]:
0.1026



PY-V-O2
5.00%
Δε [1 kHz, 20° C.]:
−3.2



CCY-3-O2
9.00%
ε [1 kHz, 20° C.]:
3.5



CCY-3-O1
6.00%
ε [1 kHz, 20° C.]:
6.7



CCY-4-O2
2.00%
γ1 [mPa · s, 20° C.]:
102



CPY-2-O2
7.00%
K1 [pN, 20° C.]:
13.5



CPY-3-O2
9.00%
K3 [pN, 20° C.]:
14.1



CCH-34
10.00%
V0 [20° C., V]:
2.22



CCH-23
21.00%
LTS (bulk) [−20° C.]:
>1000 h



BCH-32
5.50%



PCH-301
8.00%



PYP-2-3
1.00%










Example 155




















PY-3-O2
12.00%
Clearing point [° C.]:
75



PY-V-O2
5.00%
Δn [589 nm, 20° C.]:
0.1112



CCY-3-O2
10.00%
Δε [1 kHz, 20° C.]:
−3.1



CCY-4-O2
9.50%
ε [1 kHz, 20° C.]:
3.5



CPY-2-O2
6.00%
ε [1 kHz, 20° C.]:
6.6



CPY-3-O2
9.00%
γ1 [mPa · s, 20° C.]:
107



CCH-34
5.50%
K1 [pN, 20° C.]:
13.7



CCH-23
21.00%
K3 [pN, 20° C.]:
14.4



PYP-2-3
4.50%
V0 [20° C., V]:
2.29



CCH-35
4.00%



PCH-301
12.00%



BCH-32
1.50%










Example 156




















PY-V-O2
8.00%
Clearing point [° C.]:
74.8



CY-3-O2
5.50%
Δn [589 nm, 20° C.]:
0.1073



CY-V-O2
11.00%
Δε [1 kHz, 20° C.]:
−3.1



CCY-3-O1
4.00%
ε [1 kHz, 20° C.]:
3.7



CCY-3-O2
10.00%
ε [1 kHz, 20° C.]:
6.8



CPY-3-O2
10.00%
γ1 [mPa · s, 20° C.]:
82



CPY-V-O4
7.00%
K1 [pN, 20° C.]:
12.1



CC-3-V
37.00%
K3 [pN, 20° C.]:
14.6



BCH-32
7.00%
V0 [20° C., V]:
2.30



PPGU-3-F
0.50%










Example 157




















PY-3-O2
5.00%
Clearing point [° C.]:
76



PY-V2-O2
6.50%
Δn [589 nm, 20° C.]:
0.1082



CY-3-O2
12.00%
Δε [1 kHz, 20° C.]:
−3.2



CCY-3-O1
5.00%
ε [1 kHz, 20° C.]:
3.7



CCY-3-O2
10.00%
ε [1 kHz, 20° C.]:
6.9



CPY-V-O2
9.00%
γ1 [mPa · s, 20° C.]:
89



CPY-V-O4
10.00%
K1 [pN, 20° C.]:
12.6



CC-3-V
35.00%
K3 [pN, 20° C.]:
14.6



BCH-32
7.00%
V0 [20° C., V]:
2.26



PPGU-3-F
0.50%










Example 157a

The mixture according to Example 157 additionally comprises 0.01% of




embedded image


Example 157b

The mixture according to Example 157 additionally comprises 0.01% of




embedded image


Example 158




















PY-V-O2
5.00%
Clearing point [° C.]:
73.5



PY-V2-O2
5.00%
Δn [589 nm, 20° C.]:
0.1074



PY-3-O2
3.00%
Δε [1 kHz, 20° C.]:
−2.9



CY-V-O2
4.00%
ε [1 kHz, 20° C.]:
3.7



CY-3-O2
3.00%
ε [1 kHz, 20° C.]:
6.6



CCY-3-O1
3.00%
γ1 [mPa · s, 20° C.]:
78



CCY-3-O2
6.00%
K1 [pN, 20° C.]:
12.5



CCY-4-O2
5.00%
K3 [pN, 20° C.]:
14.0



CPY-2-O2
7.50%
V0 [20° C., V]:
2.33



CPY-3-O2
10.00%



CC-3-V
39.00%



BCH-32
7.00%



PPGU-3-F
0.50%



Y-4O-O4
2.00%










Example 159




















PY-V-O2
5.00%
Clearing point [° C.]:
75



CY-3-O2
8.00%
Δn [589 nm, 20° C.]:
0.1078



CY-V-O2
11.00%
Δε [1 kHz, 20° C.]:
−3.0



CCY-3-O1
4.00%
ε [1 kHz, 20° C.]:
3.7



CCY-3-O2
7.00%
ε [1 kHz, 20° C.]:
6.7



CPY-3-O2
8.00%
γ1 [mPa · s, 20° C.]:
84



CPY-V-O4
5.00%
K1 [pN, 20° C.]:
11.9



CPY-V-O2
7.00%
K3 [pN, 20° C.]:
14.4



CC-3-V
35.50%
V0 [20° C., V]:
2.30



BCH-32
9.00%



PPGU-3-F
0.50%










Example 160




















APUQU-2-F
9.00%
Clearing point [° C.]:
77.5



APUQU-3-F
8.50%
Δn [589 nm, 20° C.]:
0.1087



CC-3-V
43.50%
Δε [1 kHz, 20° C.]:
9.9



CCP-30CF3
7.50%
ε [1 kHz, 20° C.]:
13.7



CCP-V-1
7.00%
ε [1 kHz, 20° C.]:
3.8



DPGU-4-F
3.50%
γ1 [mPa · s, 20° C.]:
68



PGP-2-2V
4.00%
K1 [pN, 20° C.]:
12.4



PGUQU-4-F
4.50%
K3 [pN, 20° C.]:
13.1



PUQU-3-F
8.50%
V0 [20° C., V]:
1.18



PY-3V-O2
4.00%
LTS (bulk) [−20° C.]:
>1000 h





LTS (bulk) [−30° C.]:
>1000 h










Example 161




















PY-1V-O2
4.50%
Clearing point [° C.]:
73.5



PY-V2-O2
5.00%
Δn [589 nm, 20° C.]:
0.1074



CY-3-O2
10.00%
Δε [1 kHz, 20° C.]:
−2.8



CY-V-O2
4.50%
ε|| [1 kHz, 20° C.]:
3.6



CCY-3-O1
6.00%
ε [1 kHz, 20° C.]:
6.4



CCY-3-O2
3.00%
γ1 [mPa · s, 20° C.]:
78



CPY-2-O2
9.00%
K1 [pN, 20° C.]:
12.5



CPY-3-O2
10.00%
K3 [pN, 20° C.]:
14.3



CC-3-V
39.50%
V0 [20° C., V]:
2.40



BCH-32
8.00%



PPGU-3-F
0.50%










Example 162




















PY-V2-O2
5.50%
Clearing point [° C.]:
74



PY-3-O2
6.00%
Δn [589 nm, 20° C.]:
0.1074



CY-V2-O2
5.00%
Δε [1 kHz, 20° C.]:
−2.9



CY-3-O2
4.00%
ε|| [1 kHz, 20° C.]:
3.7



CCY-3-O1
3.00%
ε [1 kHz, 20° C.]:
6.6



CCY-3-O2
3.00%
γ1 [mPa · s, 20° C.]:
85



CCY-4-O2
6.00%
K1 [pN, 20° C.]:
12.6



CPY-2-O2
8.00%
K3 [pN, 20° C.]:
13.9



CPY-3-O2
12.00%
V0 [20° C., V]:
2.30



CC-3-V
36.50%



BCH-32
8.50%



PPGU-3-F
0.50%



Y-4O-O4
2.00%










Example 163




















PY-V2-O2
6.00%
Clearing point [° C.]:
74.5



PY-3-O2
6.00%
Δn [589 nm, 20° C.]:
0.1086



CY-1V2-O2
4.50%
Δε [1 kHz, 20° C.]:
−2.9



CY-3-O2
4.00%
ε|| [1 kHz, 20° C.]:
3.6



CCY-3-O1
3.00%
ε [1 kHz, 20° C.]:
6.5



CCY-3-O2
3.00%
γ1 [mPa · s, 20° C.]:
86



CCY-4-O2
6.00%
K1 [pN, 20° C.]:
12.8



CPY-2-O2
8.00%
K3 [pN, 20° C.]:
14.2



CPY-3-O2
12.00%
V0 [20° C., V]:
2.33



CC-3-V
37.00%



BCH-32
8.00%



PPGU-3-F
0.50%



Y-4O-O4
2.00%










Example 164




















PY-V2-O2
6.50%
Clearing point [° C.]:
74



CY-3-O2
11.00%
Δn [589 nm, 20° C.]:
0.1068



CY-V2-O2
6.50%
Δε [1 kHz, 20° C.]:
−2.8



CCY-3-O1
6.00%
ε|| [1 kHz, 20° C.]:
3.6



CCY-3-O2
2.00%
ε [1 kHz, 20° C.]:
6.4



CPY-2-O2
10.00%
γ1 [mPa · s, 20° C.]:
85



CPY-3-O2
12.00%
K1 [pN, 20° C.]:
12.3



CC-3-V
36.00%
K3 [pN, 20° C.]:
14.1



BCH-32
9.50%
V0 [20° C., V]:
2.35



PPGU-3-F
0.50%










Example 165




















PCH-504FF
10.00%
Clearing point [° C.]:
72



PCH-502FF
8.00%
Δn [589 nm, 20° C.]:
0.1216



PCH-304FF
4.00%
Δε [1 kHz, 20° C.]:
−4.0



CCP-V2-1
6.00%
ε|| [1 kHz, 20° C.]:
3.9



BCH-32
7.00%
ε [1 kHz, 20° C.]:
7.9



CCH-35
5.00%
γ1 [mPa · s, 20° C.]:
125



CC-5-V
7.00%
K1 [pN, 20° C.]:
14.6



CC-3-V1
10.00%
K3 [pN, 20° C.]:
14.7



CPY-2-O2
10.00%
V0 [20° C., V]:
2.03



CPY-3-O2
13.00%



PY-V2-O2
20.00%










Example 166




















CY-3-O2
24.00%
Clearing point [° C.]:
81



PY-1V2-O2
7.00%
Δn [589 nm, 20° C.]:
0.1019



CCY-3-O3
4.00%
Δε [1 kHz, 20° C.]:
−3.1



CCY-3-O2
5.00%
ε|| [1 kHz, 20° C.]:
3.5



CPY-2-O2
7.00%
ε [1 kHz, 20° C.]:
6.6



CPY-3-O2
5.00%
γ1 [mPa · s, 20° C.]:
126



CCP-3-3
9.00%
K1 [pN, 20° C.]:
14.9



CCP-3-1
9.00%
K3 [pN, 20° C.]:
16.0



BCH-32
5.00%
V0 [20° C., V]:
2.39



CCH-34
10.00%
LTS (bulk) [−20° C.]:
>1000 h



CCH-25
10.00%



PCH-301
5.00%










Example 167




















CY-3-O2
18.00%
Clearing point [° C.]:
80.5



PY-1V2-O2
6.00%
Δn [589 nm, 20° C.]:
0.0949



CCY-3-O2
8.00%
Δε [1 kHz, 20° C.]:
−3.1



CCY-4-O2
4.00%
ε|| [1 kHz, 20° C.]:
3.4



CPY-2-O2
7.00%
ε [1 kHz, 20° C.]:
6.4



CPY-3-O2
10.00%
γ1 [mPa · s, 20° C.]:
113



CCH-34
8.00%
K1 [pN, 20° C.]:
14.9



CCH-23
22.00%
K3 [pN, 20° C.]:
16.0



CCP-3-3
7.00%
V0 [20° C., V]:
2.41



CCP-3-1
7.00%
LTS (bulk) [−20° C.]:
>1000 h



PCH-301
3.00%










Example 168




















CY-1V-O1V
20.00%
Clearing point [° C.]:
82.5



PY-1V2-O2
7.00%
Δn [589 nm, 20° C.]:
0.0987



CY-3-O2
5.00%
Δε [1 kHz, 20° C.]:
−3.0



CCY-3-O2
5.00%
ε|| [1 kHz, 20° C.]:
3.4



CCY-4-O2
5.00%
ε [1 kHz, 20° C.]:
6.4



CPY-3-O2
10.00%
γ1 [mPa · s, 20° C.]:
109



CCH-34
10.00%
K1 [pN, 20° C.]:
14.9



CC-3-V1
11.00%
K3 [pN, 20° C.]:
18.9



CC-2-V1
11.00%
V0 [20° C., V]:
2.66



CCP-3-1
8.00%
LTS (bulk) [−20° C.]:
>1000 h



PCH-301
2.00%



CCVC-3-V
6.00%










Example 169




















CY-1V-O1V
20.00%
Clearing point [° C.]:
81



PY-1V2-O2
5.00%
Δn [589 nm, 20° C.]:
0.0953



CY-3-O2
7.00%
Δε [1 kHz, 20° C.]:
−3.0



CCY-3-O2
6.00%
ε|| [1 kHz, 20° C.]:
3.4



CCY-3-O1
6.00%
ε [1 kHz, 20° C.]:
6.4



CPY-3-O2
8.00%
γ1 [mPa · s, 20° C.]:
106



CCH-34
10.00%
K1 [pN, 20° C.]:
14.5



CC-3-V1
11.00%
K3 [pN, 20° C.]:
18.6



CC-2-V1
11.00%
V0 [20° C., V]:
2.63



CCP-3-1
8.00%
LTS (bulk) [−20° C.]:
>1000 h



PCH-301
2.00%



CCVC-3-V
6.00%










Example 170




















CY-1V-O1V
20.00%
Clearing point [° C.]:
81.5



PY-1V2-O2
6.00%
Δn [589 nm, 20° C.]:
0.0947



CY-3-O2
6.00%
Δε [1 kHz, 20° C.]:
−3.0



CCY-3-O2
7.00%
ε|| [1 kHz, 20° C.]:
3.4



CCY-3-O1
7.00%
ε [1 kHz, 20° C.]:
6.4



CPY-3-O2
6.00%
γ1 [mPa · s, 20° C.]:
104



CCH-34
10.00%
K1 [pN, 20° C.]:
14.6



CC-3-V1
12.00%
K3 [pN, 20° C.]:
18.6



CC-2-V1
12.00%
V0 [20° C., V]:
2.64



CCP-V2-1
4.00%



CCP-V-1
4.00%



CCVC-3-V
6.00%










Example 171




















CY-1V-O1V
20.00%
Clearing point [° C.]:
80.5



PY-1V2-O2
5.00%
Δn [589 nm, 20° C.]:
0.0962



CY-3-O2
12.00%
Δε [1 kHz, 20° C.]:
−3.4



CCY-3-O2
6.00%
ε|| [1 kHz, 20° C.]:
3.5



CCY-4-O2
6.00%
ε [1 kHz, 20° C.]:
6.9



CPY-3-O2
8.00%
γ1 [mPa · s, 20° C.]:
112



CCH-34
7.00%
K1 [pN, 20° C.]:
14.3



CC-3-V1
11.00%
K3 [pN, 20° C.]:
18.5



CC-2-V1
11.00%
V0 [20° C., V]:
2.45



CCP-3-1
6.00%



CCVC-3-V
8.00%










Example 172




















CY-1V-O1V
20.00%
Clearing point [° C.]:
81.5



PY-1V2-O2
7.00%
Δn [589 nm, 20° C.]:
0.0932



CY-3-O2
7.50%
Δε [1 kHz, 20° C.]:
−3.3



CCY-3-O2
10.50%
ε|| [1 kHz, 20° C.]:
3.4



CCY-4-O2
10.00%
ε [1 kHz, 20° C.]:
6.7



CC-3-V2
11.00%
γ1 [mPa · s, 20° C.]:
104



CC-3-V1
11.00%
K1 [pN, 20° C.]:
14.9



CC-2-V1
11.00%
K3 [pN, 20° C.]:
19.0



CCP-3-1
6.00%
V0 [20° C., V]:
2.55



CCVC-3-V
6.00%
LTS (bulk) [−20° C.]
>1000 h










Example 173




















CY-3-O2
12.00%
Clearing point [° C.]:
80.0



PY-1V2-O2
11.00%
Δn [589 nm, 20° C.]:
0.0950



CCY-3-O2
10.00%
Δε [1 kHz, 20° C.]:
−3.1



CCY-4-O2
10.00%
ε|| [1 kHz, 20° C.]:
3.3



CPY-3-O2
10.00%
ε [1 kHz, 20° C.]:
6.4



CCH-34
8.00%
γ1 [mPa · s, 20° C.]:
111



CCH-23
22.00%
K1 [pN, 20° C.]:
15.1



CCP-3-3
3.00%
K3 [pN, 20° C.]:
16.6



CCP-3-1
7.00%
V0 [20° C., V]:
2.46



PCH-301
7.00%
LTS (bulk) [−20° C.]
>1000 h










Example 174




















CY-1V-O1V
18.00%
Clearing point [° C.]:
80.5



PY-1V2-O2
4.00%
Δn [589 nm, 20° C.]:
0.0943



CY-3-O2
15.00%
Δε [1 kHz, 20° C.]:
−3.6



CCY-3-O2
8.00%
ε|| [1 kHz, 20° C.]:
3.5



CCY-4-O2
7.00%
ε [1 kHz, 20° C.]:
7.2



CPY-3-O2
7.00%
γ1 [mPa · s, 20° C.]:
112



CCH-34
7.00%
K1 [pN, 20° C.]:
14.2



CC-3-V1
11.00%
K3 [pN, 20° C.]:
18.2



CC-2-V1
11.00%
V0 [20° C., V]:
2.37



CCP-3-1
3.00%



CCVC-3-V
9.00%










Example 175




















CY-1V-O1V
18.00%
Clearing point [° C.]:
80.5



PY-1V2-O2
3.00%
Δn [589 nm, 20° C.]:
0.0946



CY-3-O2
16.00%
Δε [1 kHz, 20° C.]:
−3.7



CCY-3-O2
10.00%
ε|| [1 kHz, 20° C.]:
3.5



CCY-4-O2
5.00%
ε [1 kHz, 20° C.]:
7.2



CPY-3-O2
7.00%
γ1 [mPa · s, 20° C.]:
113



CC-3-V2
7.00%
K1 [pN, 20° C.]:
14.2



CC-3-V1
11.00%
K3 [pN, 20° C.]:
18.7



CC-2-V1
11.00%
V0 [20° C., V]:
2.39



CCP-3-1
3.00%



CCVC-3-V
9.00%










Example 176




















PY-3-O2
11.00%
Clearing point [° C.]:
75



PY-V2-O2
6.50%
Δn [589 nm, 20° C.]:
0.1105



CCY-3-O2
9.00%
Δε [1 kHz, 20° C.]:
−3.1



CCY-4-O2
3.00%
ε|| [1 kHz, 20° C.]:
3.5



CCY-3-O1
5.00%
ε [1 kHz, 20° C.]:
6.6



CPY-2-O2
6.50%
γ1 [mPa · s, 20° C.]:
105



CPY-3-O2
10.00%
K1 [pN, 20° C.]:
13.9



CCH-34
10.00%
K3 [pN, 20° C.]:
14.3



CCH-23
21.00%
V0 [20° C., V]:
2.28



PYP-2-3
6.00%
LTS (bulk) [−20° C.]
>1000 h



CCP-3-1
3.00%



PCH-301
9.00%










Example 177




















PY-3-O2
11.00%
Clearing point [° C.]:
74



PY-1V2-O2
7.50%
Δn [589 nm, 20° C.]:
0.1107



CCY-3-O2
9.00%
Δε [1 kHz, 20° C.]:
−3.0



CCY-3-O1
5.50%
ε|| [1 kHz, 20° C.]:
3.4



CPY-2-O2
6.50%
ε [1 kHz, 20° C.]:
6.4



CPY-3-O2
10.00%
γ1 [mPa · s, 20° C.]:
104



CCH-34
10.00%
K1 [pN, 20° C.]:
14.0



CCH-23
21.00%
K3 [pN, 20° C.]:
14.8



PYP-2-3
5.50%
V0 [20° C., V]:
2.37



CCP-3-1
4.00%
LTS (bulk) [−20° C.]
>1000 h



PCH-301
10.00%










Example 178




















PY-3-O2
11.00%
Clearing point [° C.]:
74



PY-1V2-O2
8.00%
Δn [589 nm, 20° C.]:
0.1119



CY-3-O2
3.00%
Δε [1 kHz, 20° C.]:
−3.3



CCY-3-O2
9.00%
ε|| [1 kHz, 20° C.]:
3.5



CCY-3-O1
6.00%
ε [1 kHz, 20° C.]:
6.8



CPY-2-O2
6.50%
γ1 [mPa · s, 20° C.]:
108



CPY-3-O2
10.00%
K1 [pN, 20° C.]:
14.3



CCH-34
10.00%
K3 [pN, 20° C.]:
15.0



CCH-23
21.00%
V0 [20° C., V]:
2.26



PYP-2-3
5.00%
LTS (bulk) [−20° C.]
>1000 h



CCP-3-1
4.00%



PCH-301
6.50%










Example 179




















CC-3-V
39.00%
Clearing point [° C.]:
74.5



CC-3-V1
3.00%
Δn [589 nm, 20° C.]:
0.1017



CCP-V-1
8.00%
Δε [1 kHz, 20° C.]:
3.2



CCP-V2-1
12.00%
γ1 [mPa · s, 20° C.]:
64



PGP-2-2V
3.50%
K1 [pN, 20° C.]:
13



PP-1-2V1
9.00%
K3 [pN, 20° C.]:
15.4



PPGU-3-F
1.00%
V0 [20° C., V]:
2.13



PUQU-3-F
15.50%



CCY-3-O2
9.00%










Example 180




















BCH-32
5.00%
Clearing point [° C.]:
75.3



CC-3-V
41.50%
Δn [589 nm, 20° C.]:
0.0989



CC-3-V1
8.50%
Δε [1 kHz, 20° C.]:
−1.9



CCH-35
2.00%
ε|| [1 kHz, 20° C.]:
3.2



CCP-3-1
3.00%
ε [1 kHz, 20° C.]:
5.0



CCY-3-O2
7.00%
γ1 [mPa · s, 20° C.]:
69



CPY-2-O2
5.50%
K1 [pN, 20° C.]:
14.2



CPY-3-O2
12.50%
K3 [pN, 20° C.]:
15.5



PY-3-O2
15.00%
V0 [20° C., V]:
3.02










Example 180a

The mixture according to Example 180 additionally comprises 0.001% of Irganox® 1076 (octadecyl 3-(3,5-di-tert-butyl-4-hydroxyphenyl)propionate, BASF) and 0.3% of RM-1.


Example 181




















CCY-3-O1
8.00%
Clearing point [° C.]:
74.9



CCY-4-O2
7.50%
Δn [589 nm, 20° C.]:
0.1123



CPY-2-O2
10.00%
Δε [1 kHz, 20° C.]:
−3.7



CPY-3-O2
10.00%
ε|| [1 kHz, 20° C.]:
3.7



CC-3-V
15.00%
ε [1 kHz, 20° C.]:
7.5



PY-1-O4
5.00%
γ1 [mPa · s, 20° C.]:
121



PY-3-O2
9.00%
K1 [pN, 20° C.]:
13.2



PY-4-O2
5.00%
K3 [pN, 20° C.]:
15.5



CC-3-V1
9.00%
V0 [20° C., V]:
2.15



CCY-3-O2
6.50%



PCH-301
15.00%










Example 181a

The mixture according to Example 181 additionally comprises 0.01% of




embedded image


Example 182




















CY-3-O2
10.00%
Clearing point [° C.]:
100



CY-3-O4
20.00%
Δn [589 nm, 20° C.]:
0.0865



CY-5-O4
20.00%
Δε [1 kHz, 20° C.]:
−5.4



CCY-3-O2
6.00%
ε|| [1 kHz, 20° C.]:
3.9



CCY-3-O3
6.00%
ε [1 kHz, 20° C.]:
9.3



CCY-4-O2
6.00%
γ1 [mPa · s, 20° C.]:
347



CCY-5-O2
6.00%
K1 [pN, 20° C.]:
15.6



CH-33
3.00%
K3 [pN, 20° C.]:
16.6



CH-35
3.50%
V0 [20° C., V]:
1.84



CH-43
3.50%



CH-45
3.50%



CCPC-33
4.00%



CCPC-34
4.50%



CCPC-35
4.00%










Example 183




















CY-3-O2
15.00%
Clearing point [° C.]:
91



CY-5-O2
12.00%
Δn [589 nm, 20° C.]:
0.105



CCY-3-O1
4.00%
Δε [1 kHz, 20° C.]:
−4.5



CCY-3-O2
4.00%
γ1 [mPa · s, 20° C.]:
106



CCY-3-O3
4.00%
V0 [20° C., V]:
1.32



CCY-4-O2
4.00%



CLY-3-O2
10.00%



CLY-3-O3
2.00%



CPY-2-O2
8.00%



CC-3-V
24.00%



PGP-2-5
5.00%










Example 184




















CY-3-O2
14.00%
Clearing point [° C.]:
84.7



CY-3-O4
4.00%
Δn [589 nm, 20° C.]:
0.1068



CY-5-O2
7.00%
Δε [1 kHz, 20° C.]:
−4.0



CCY-3-O1
4.00%
γ1 [mPa · s, 20° C.]:
138



CCY-3-O2
5.00%
K1 [pN, 20° C.]:
14.1



CCY-4-O2
8.00%
K3 [pN, 20° C.]:
16.2



CCY-5-O2
3.00%
V0 [20° C., V]:
2.13



CPY-2-O2
9.00%



CPY-3-O2
9.00%



PYP-2-3
6.00%



CC-3-V
22.00%



CC-3-V1
3.50%



CCP-V-1
5.00%



PPGU-3-F
0.50%










Example 185




















CY-3-O2
15.00%
Clearing point [° C.]:
80.4



CY-5-O2
12.50%
Δn [589 nm, 20° C.]:
0.1038



CCY-3-O1
2.50%
Δε [1 kHz, 20° C.]:
−3.3



CCY-4-O2
5.00%
ε|| [1 kHz, 20° C.]:
3.5



CPY-2-O2
8.00%
ε [1 kHz, 20° C.]:
6.8



CPY-3-O2
8.00%
γ1 [mPa · s, 20° C.]:
137



CCY-2-1
6.00%
K1 [pN, 20° C.]:
14.2



CCY-3-1
6.00%
K3 [pN, 20° C.]:
14.2



CCH-23
15.00%
V0 [20° C., V]:
2.18



CCH-34
5.00%



CCH-301
1.50%



BCH-32
15.50%










Example 185a

The mixture according to Example 185 additionally comprises 0.25% of RM-35




embedded image


and 0.025% of




embedded image


Example 186




















CC-3-V
34.00%
Clearing point [° C.]:
100



CC-3-V1
2.50%
Δn [589 nm, 20° C.]:
0.1003



CCP-V-1
10.00%
Δε [1 kHz, 20° C.]:
9.1



PUQU-3-F
7.00%
ε|| [1 kHz, 20° C.]:
12.3



PGUQU-3-F
4.00%
ε [1 kHz, 20° C.]:
3.2



CPGU-3-OT
6.00%
γ1 [mPa · s, 20° C.]:
99



CCGU-3-F
4.00%
K1 [pN, 20° C.]:
14.2



APUQU-3-F
8.00%
K3 [pN, 20° C.]:
17.3



CCP-3F.F.F
4.50%



CCP-30CF3
4.00%



CCP-50CF3
3.00%



CCQU-3-F
10.00%



CBC-33
3.00%










Example 186a

The mixture according to Example 186 additionally comprises 0.03% of




embedded image


Example 186b

The mixture according to Example 186 additionally comprises 0.03% of




embedded image


Example 187




















Y-4O-O4
4.50%
Clearing point [° C.]:
100



PYP-2-3
2.00%
Δn [589 nm, 20° C.]:
0.1716



CC-3-V
25.00%
Δε [1 kHz, 20° C.]:
−1.5



CC-4-V
10.00%
ε|| [1 kHz, 20° C.]:
3.4



CCP-V-1
14.00%
ε [1 kHz, 20° C.]:
4.9



PTP-302FF
10.00%
γ1 [mPa · s, 20° C.]:
114



CPTP-302FF
10.00%
K1 [pN, 20° C.]:
15.2



CPTP-302FF
10.00%
K3 [pN, 20° C.]:
18.5



PPTUI-3-2
14.50%
V0 [20° C., V]:
3.76










Example 188




















CCH-23
25.00%
Clearing point [° C.]:
70.3



CC-3-V
4.50%
Δn [589 nm, 20° C.]:
0.0737



PCH-53
25.00%
Δε [1 kHz, 20° C.]:
−1.1



CCY-2-1
12.00%
ε|| [1 kHz, 20° C.]:
2.8



CCY-3-1
12.00%
ε [1 kHz, 20° C.]:
3.9



CCY-3-O2
12.00%
K1 [pN, 20° C.]:
11.7



CCY-3-O3
5.00%
K3 [pN, 20° C.]:
13.1



CBC-33F
4.50%










Example 189




















CC-3-V1
10.25%
Clearing point [° C.]:
74.7



CCH-23
18.50%
Δn [589 nm, 20° C.]:
0.1027



CCH-35
6.75%
Δε [1 kHz, 20° C.]:
−3.1



CCP-3-1
6.00%
ε|| [1 kHz, 20° C.]:
3.4



CCY-3-1
2.50%
ε [1 kHz, 20° C.]:
6.5



CCY-3-O2
12.00%
γ1 [mPa · s, 20° C.]:
104



CPY-2-O2
6.00%
K1 [pN, 20° C.]:
15.4



CPY-3-O2
9.75%
K3 [pN, 20° C.]:
16.8



CY-3-O2
11.50%
V0 [20° C., V]:
2.46



PP-1-2V1
3.75%



PY-3-O2
13.00%










Example 189a

The mixture according to Example 189 additionally comprises 0.01% of Irganox® 1076 (octadecyl 3-(3,5-di-tert-butyl-4-hydroxyphenyl)propionate, BASF) and 0.3% of RM-1.


Example 190




















BCH-3F.F
10.00%
Clearing point [° C.]:
99.6



BCH-3F.F.F
12.00%
Δn [589 nm, 20° C.]:
0.1122



CBC-33
3.00%
Δε [1 kHz, 20° C.]:
10.1



CBC-33F
3.00%
ε|| [1 kHz, 20° C.]:
13.8



CCGU-3-F
8.00%
ε [1 kHz, 20° C.]:
3.6



CCH-34
10.00%
γ1 [mPa · s, 20° C.]:
164



CCH-35
6.50%
K1 [pN, 20° C.]:
11.8



CCP-1F.F.F
10.00%
K3 [pN, 20° C.]:
15.9



CCP-2F.F.F
10.00%
V0 [20° C., V]:
1.14



CCP-3-1
2.50%



CCP-3F.F.F
8.00%



CPGP-4-3
3.00%



CPGP-5-2
2.00%



CPGP-5-3
1.00%



PUQU-2-F
1.00%



PUQU-3-F
10.00%










Example 191

















CBC-53F
3.00%
Clearing point [° C.]:
115.5


CC-3-2V1
1.00%
Δn [589 nm, 20° C.]:
0.1106


CC-3-V
25.00%
Δε [1 kHz, 20° C.]:
7.0


CC-3-V1
5.00%
ε [1 kHz, 20° C.]:
9.9


CCGU-3-F
5.50%
ε [1 kHz, 20° C.]:
2.9


CCP-30CF3
4.00%
γ1 [mPa · s, 20° C.]:
118


CCP-30CF3.F
8.00%
K1 [pN, 20° C.]:
17.4


CCP-40CF3
3.00%
K3 [pN, 20° C.]:
20.4


CCP-50CF3
3.00%
V0 [20° C., V]:
1.66


CCP-V-1
8.00%


CCP-V2-1
12.00%


CPGU-3-OT
5.00%


PGUQU-3-F
4.00%


PGUQU-4-F
4.00%


PGUQU-5-F
2.00%


PP-1-2V1
3.00%


PPGU-3-F
0.50%


PUQU-2-F
1.00%


PUQU-3-F
3.00%









Example 192




















APUQU-2-F
2.50%
Clearing point [° C.]:
85.8



APUQU-3-F
5.00%
Δn [589 nm, 20° C.]:
0.1106



PUQU-3-F
10.00%
Δε [1 kHz, 20° C.]:
8.6



PGUQU-3-F
5.00%
ε [1 kHz, 20° C.]:
12.6



PGUQU-4-F
3.00%
ε [1 kHz, 20° C.]:
4.0



PGUQU-5-F
2.00%
γ1 [mPa · s, 20° C.]:
92



DPGU-4-F
4.00%
K1 [pN, 20° C.]:
13.0



PPGU-3-F
0.50%
K3 [pN, 20° C.]:
15.3



CDUQU-3-F
0.05%
V0 [20° C., V]:
1.30



CC-3-V
39.95%



CCP-V-1
9.00%



CCP-V2-1
8.00%



CCP-3-1
2.00%



PGP-2-3
3.00%



CY-3-O2
5.00%



CCY-3-O2
5.00%










Example 193




















APUQU-2-F
2.50%
Clearing point [° C.]:
85.8



APUQU-3-F
5.00%
Δn [589 nm, 20° C.]:
0.1105



PUQU-3-F
12.50%
Δε [1 kHz, 20° C.]:
10.6



PGUQU-3-F
5.00%
ε [1 kHz, 20° C.]:
14.8



PGUQU-4-F
4.00%
ε [1 kHz, 20° C.]:
4.2



PGUQU-5-F
4.00%
γ1 [mPa · s, 20° C.]:
98



DPGU-4-F
4.00%
K1 [pN, 20° C.]:
12.7



PPGU-3-F
0.50%
K3 [pN, 20° C.]:
15.1



CDUQU-3-F
0.05%



CC-3-V
34.95%



CCP-V-1
7.00%



CCP-V2-1
6.00%



CCP-3-1
2.50%



CCPC-33
2.00%



CY-3-O2
5.00%



CCY-3-O2
5.00%










Example 194




















APUQU-2-F
3.00%
Clearing point [° C.]:
85.7



APUQU-3-F
5.00%
Δn [589 nm, 20° C.]:
0.1097



PUQU-3-F
12.00%
Δε [1 kHz, 20° C.]:
8.7



PGUQU-3-F
5.00%
ε [1 kHz, 20° C.]:
12.4



PGUQU-4-F
4.00%
ε [1 kHz, 20° C.]:
3.7



PGUQU-5-F
3.00%
γ1 [mPa · s, 20° C.]:
82



PPGU-3-F
0.50%
K1 [pN, 20° C.]:
12.9



CDUQU-3-F
0.05%
K3 [pN, 20° C.]:
15.7



CC-3-V
38.95%
V0 [20° C., V]:
1.29



CCP-V-1
10.50%



CCP-V2-1
9.00%



PGP-2-3
2.00%



CCY-3-O2
3.50%



CPY-3-O2
3.50%










Example 195




















APUQU-2-F
3.00%
Clearing point [° C.]:
85.7



APUQU-3-F
5.00%
Δn [589 nm, 20° C.]:
0.1097



PUQU-3-F
12.00%
Δε [1 kHz, 20° C.]:
8.7



PGUQU-3-F
5.00%
ε [1 kHz, 20° C.]:
12.4



PGUQU-4-F
4.00%
ε [1 kHz, 20° C.]:
3.7



PGUQU-5-F
3.00%
γ1 [mPa · s, 20° C.]:
82



PPGU-3-F
0.50%
K1 [pN, 20° C.]:
12.9



CDUQU-3-F
0.05%
K3 [pN, 20° C.]:
15.7



CC-3-V
38.95%
V0 [20° C., V]:
1.29



CCP-V-1
10.50%



CCP-V2-1
9.00%



PGP-2-3
2.00%



CCY-3-O2
3.50%



CPY-3-O2
3.50%










Example 196




















CC-3-V
35.00%
Clearing point [° C.]:
84.6



CCY-3-O1
9.00%
Δn [589 nm, 20° C.]:
0.1010



CCY-3-O2
8.00%
Δε [1 kHz, 20° C.]:
−4.0



CCY-4-O2
5.00%
ε [1 kHz, 20° C.]:
3.6



CLY-3-O3
11.00%
ε [1 kHz, 20° C.]:
7.6



CPY-2-O2
9.50%
γ1 [mPa · s, 20° C.]:
114



CPY-3-O2
4.00%
K1 [pN, 20° C.]:
14.5



CY-3-O2
6.50%



PY-3-O2
12.00%










Example 196a

The mixture according to Example 196 additionally comprises 0.04% of




embedded image


and 0.015% of




embedded image


Example 197




















CC-3-V
33.00%
Clearing point [° C.]:
84



CCY-3-O1
7.00%
Δn [589 nm, 20° C.]:
0.1111



CCY-3-O2
7.00%
Δε [1 kHz, 20° C.]:
−4.0



CCY-4-O2
5.00%
ε [1 kHz, 20° C.]:
3.7



CLY-3-O3
11.00%
ε [1 kHz, 20° C.]:
7.6



CPY-2-O2
9.00%
γ1 [mPa · s, 20° C.]:
119



CPY-3-O2
8.00%
K1 [pN, 20° C.]:
14.8



PP-1-2V1
1.50%



PY-1-O4
8.50%



PY-3-O2
10.00%










Example 197a

The mixture according to Example 197 additionally comprises 0.04% of




embedded image


and 0.015% of




embedded image


Example 198




















APUQU-2-F
4.00%
Clearing point [° C.]:
85.6



APUQU-3-F
7.00%
Δn [589 nm, 20° C.]:
0.1021



PUQU-3-F
5.00%
Δε [1 kHz, 20° C.]:
6.9



PGUQU-3-F
4.00%
ε [1 kHz, 20° C.]:
10.0



PGUQU-4-F
3.00%
ε [1 kHz, 20° C.]:
3.1



PGUQU-5-F
3.00%
γ1 [mPa · s, 20° C.]:
71



CCP-V-1
16.00%
K1 [pN, 20° C.]:
13.1



CC-3-V
40.00%
K3 [pN, 20° C.]:
15.3



CC-3-V1
4.00%
V0 [20° C., V]:
1.45



CC-4-V
3.00%



PGP-2-3
4.00%



PGP-2-4
1.00%



PPGU-3-F
1.00%



CCOC-4-3
5.00%










Example 198a

The mixture according to Example 198 additionally comprises 0.25% of RM-41




embedded image


Example 198b

The mixture according to Example 198 additionally comprises 0.3% of RM-17




embedded image


Example 199




















Y-4O-O4
12.00%
Clearing point [° C.]:
101



CY-3-O2
14.00%
Δn [589 nm, 20° C.]:
0.1504



CCY-3-O1
5.00%
Δε [1 kHz, 20° C.]:
−6.2



CCY-3-O2
6.00%
ε [1 kHz, 20° C.]:
4.5



CCY-3-O3
6.00%
ε [1 kHz, 20° C.]:
10.7



CCY-4-O2
6.00%
γ1 [mPa · s, 20° C.]:
281



CPY-2-O2
2.50%
K1 [pN, 20° C.]:
15.7



PTP-302FF
10.00%
K3 [pN, 20° C.]:
19.9



CPTP-302FF
10.00%
V0 [20° C., V]:
1.90



CPTP-502FF
10.00%



CC-4-V
2.50%



CCP-V-1
11.50%



CCPC-33
4.50%










Example 200




















Y-4O-O4
12.00%
Clearing point [° C.]:
100



CCY-3-O1
5.00%
Δn [589 nm, 20° C.]:
0.1496



CCY-3-O2
6.00%
Δε [1 kHz, 20° C.]:
−4.1



CCY-3-O3
6.00%
ε [1 kHz, 20° C.]:
4.0



CCY-4-O2
2.00%
ε [1 kHz, 20° C.]:
8.1



CC-4-V
15.00%
γ1 [mPa · s, 20° C.]:
180



CCP-V-1
11.00%
K1 [pN, 20° C.]:
16.1



CCP-V2-1
5.00%
K3 [pN, 20° C.]:
18.5



BCH-32
5.00%
V0 [20° C., V]:
2.25



PTP-302FF
10.00%



PTP-502FF
3.00%



CPTP-302FF
10.00%



CPTP-502FF
10.00%










Example 201




















Y-4O-O4
10.00%
Clearing point [° C.]:
100



CCY-3-O1
2.50%
Δn [589 nm, 20° C.]:
0.1515



PTP-302FF
10.00%
Δε [1 kHz, 20° C.]:
−2.1



PTP-502FF
3.50%
ε [1 kHz, 20° C.]:
3.5



CPTP-302FF
10.00%
ε [1 kHz, 20° C.]:
5.6



CPTP-502FF
3.50%
γ1 [mPa · s, 20° C.]:
125



CC-4-V
15.00%
K1 [pN, 20° C.]:
16.6



CC-3-V1
8.00%
K3 [pN, 20° C.]:
18.7



CCP-V-1
12.00%
V0 [20° C., V]:
3.13



CCP-V2-1
12.00%



BCH-32
5.00%



CPTP-3-1
5.00%



CPTP-3-2
3.50%










Example 202




















Y-4O-O4
12.00%
Clearing point [° C.]:
101



CY-3-O2
6.00%
Δn [589 nm, 20° C.]:
0.1218



CY-3-O4
15.00%
Δε [1 kHz, 20° C.]:
−6.2



CCY-3-O2
6.00%
ε [1 kHz, 20° C.]:
4.5



CCY-3-O3
6.00%
ε [1 kHz, 20° C.]:
10.7



CCY-4-O2
6.00%
γ1 [mPa · s, 20° C.]:
302



CLY-3-O2
5.00%
K1 [pN, 20° C.]:
15.7



CPY-2-O2
8.00%
K3 [pN, 20° C.]:
18.9



CPY-3-O2
8.00%
V0 [20° C., V]:
1.83



CPTP-302FF
4.00%



CPTP-502FF
4.00%



CCP-V-1
11.00%



CCPC-33
4.50%



CCPC-34
4.50%










Example 203




















Y-4O-O4
15.00%
Clearing point [° C.]:
101



CCY-3-O2
5.00%
Δn [589 nm, 20° C.]:
0.1216



CCY-3-O3
5.00%
Δε [1 kHz, 20° C.]:
−4.0



CCY-4-O2
5.00%
ε [1 kHz, 20° C.]:
4.0



CLY-3-O2
4.00%
ε [1 kHz, 20° C.]:
8.0



CPY-2-O2
8.00%
γ1 [mPa · s, 20° C.]:
167



CPY-3-02
8.00%
K1 [pN, 20° C.]:
16.1



CPTP-302FF
5.00%
K3 [pN, 20° C.]:
17.3



CPTP-502FF
5.00%
V0 [20° C., V]:
2.19



CC-4-V
13.50%



CCP-V-1
11.50%



CCP-V2-1
10.00%



BCH-32
5.00%










Example 204




















Y-4O-O4
10.00%
Clearing point [° C.]:
100



CCY-3-O2
5.00%
Δn [589 nm, 20° C.]:
0.1203



CCY-3-O3
3.50%
Δε [1 kHz, 20° C.]:
−2.0



CPY-3-O2
5.50%
ε [1 kHz, 20° C.]:
3.4



PTP-302FF
3.50%
ε [1 kHz, 20° C.]:
5.4



CPTP-302FF
5.00%
γ1 [mPa · s, 20° C.]:
117



CPTP-502FF
5.00%
K1 [pN, 20° C.]:
15.6



CCH-301
5.00%
K3 [pN, 20° C.]:
18.5



CC-4-V
15.00%
V0 [20° C., V]:
3.17



CC-3-V1
8.00%



CCP-V-1
13.00%



CCP-V2-1
13.00%



BCH-32
5.00%



CPTP-3-1
3.50%










Example 205




















BCH-32
16.00%
Clearing point [° C.]:
105



BCH-52
6.50%
Δn [589 nm, 20° C.]:
0.1503



CCY-3-O1
5.00%
Δε [1 kHz, 20° C.]:
−4.2



CCY-3-O2
8.00%
ε [1 kHz, 20° C.]:
3.8



CCY-3-O3
6.00%
ε [1 kHz, 20° C.]:
8.0



CCY-4-O2
8.00%
γ1 [mPa · s, 20° C.]:
297



CCY-5-O2
7.00%
K1 [pN, 20° C.]:
18.3



CY-3-O4
13.00%
K3 [pN, 20° C.]:
17.3



PY-3-O2
5.50%
V0 [20° C., V]:
2.13



PY-4-O2
9.00%



PYP-2-3
8.00%



PYP-2-4
8.00%










Example 205a

The mixture according to Example 205 additionally comprises 0.015% of




embedded image


and 0.015% of




embedded image


Example 206




















CC-3-V
35.50%
Clearing point [° C.]:
79.8



CCY-3-O2
6.00%
Δn [589 nm, 20° C.]:
0.0962



CCY-3-O3
6.00%
Δε [1 kHz, 20° C.]:
−3.4



CCY-4-O2
6.00%
ε|| [1 kHz, 20° C.]:
3.6



CCY-5-O2
3.50%
ε [1 kHz, 20° C.]:
7.0



CPY-2-O2
10.00%
γ1 [mPa · s, 20° C.]:
111



CPY-3-O2
9.00%
K1 [pN, 20° C.]:
13.3



CY-3-O4
10.00%
K3 [pN, 20° C.]:
15.2



CY-5-O2
9.00%
V0 [20° C., V]:
2.23



PGIGI-3-F
5.00%










Example 207




















CC-3-V
31.50%
Clearing point [° C.]:
79.6



CCP-V-1
5.00%
Δn [589 nm, 20° C.]:
0.1044



CCY-3-O2
6.00%
Δε [1 kHz, 20° C.]:
−3.4



CCY-3-O3
6.00%
ε|| [1 kHz, 20° C.]:
3.6



CCY-4-O2
5.50%
ε [1 kHz, 20° C.]:
7.0



CPY-2-O2
10.00%
γ1 [mPa · s, 20° C.]:
115



CPY-3-O2
10.00%
K1 [pN, 20° C.]:
13.3



CY-3-O4
7.00%
K3 [pN, 20° C.]:
15.2



CY-5-O2
7.00%
V0 [20° C., V]:
2.24



PGIGI-3-F
5.00%



PY-3-O2
7.00%










Example 208




















CC-3-V
36.50%
Clearing point [° C.]:
84.9



CCP-V-1
3.00%
Δn [589 nm, 20° C.]:
0.1054



CCY-3-O1
6.50%
Δε [1 kHz, 20° C.]:
−3.5



CCY-3-O2
3.50%
ε|| [1 kHz, 20° C.]:
3.5



CCY-4-O2
5.00%
ε [1 kHz, 20° C.]:
7.0



CLY-3-O3
9.00%
γ1 [mPa · s, 20° C.]:
108



CPY-2-O2
11.00%
K1 [pN, 20° C.]:
14.4



CPY-3-O2
9.00%
K3 [pN, 20° C.]:
15.7



CY-3-O2
3.00%
V0 [20° C., V]:
2.24



PY-3-O2
13.50%










Example 209




















CC-3-V
39.00%
Clearing point [° C.]:
75.2



BCH-3F.F.F
8.00%
Δn [589 nm, 20° C.]:
0.1298



PGU-2-F
6.00%
Δε [1 kHz, 20° C.]:
18.3



PGU-3-F
6.00%
ε|| [1 kHz, 20° C.]:
22.6



APUQU-2-F
6.00%
ε [1 kHz, 20° C.]:
4.3



APUQU-3-F
8.00%
γ1 [mPa · s, 20° C.]:
99



PGUQU-3-F
6.00%
K1 [pN, 20° C.]:
10.9



PGUQU-4-F
6.00%
K3 [pN, 20° C.]:
11.1



PGUQU-5-F
6.00%
V0 [20° C., V]:
0.81



DPGU-4-F
9.00%










Example 210




















CC-3-V
38.50%
Clearing point [° C.]:
74.9



CCY-3-O1
4.50%
Δn [589 nm, 20° C.]:
0.1012



CCY-3-O2
4.00%
Δε [1 kHz, 20° C.]:
−3.7



CCY-4-O2
8.00%
ε|| [1 kHz, 20° C.]:
3.7



CLY-3-O2
8.00%
ε [1 kHz, 20° C.]:
7.4



CPY-2-O2
10.00%
γ1 [mPa · s, 20° C.]:
94



CPY-3-O2
9.00%
K1 [pN, 20° C.]:
13.4



PY-1-O4
7.50%
K3 [pN, 20° C.]:
14.4



PY-3-O2
6.00%
V0 [20° C., V]:
2.08



Y-4O-O4
4.50%
LTS (bulk) [−20° C.]
>1000 h










Example 210a

The mixture according to Example 210 additionally comprises 0.25% of




embedded image


and 0.25% of




embedded image


Example 211




















CC-3-V
40.50%
Clearing point [° C.]:
74.8



CC-3-V1
5.00%
Δn [589 nm, 20° C.]:
0.1073



CCPC-33
3.00%
Δε [1 kHz, 20° C.]:
−1.9



CCY-3-O2
9.00%
ε|| [1 kHz, 20° C.]:
3.2



CPY-2-O2
9.00%
ε [1 kHz, 20° C.]:
5.2



CPY-3-O2
9.50%
γ1 [mPa · s, 20° C.]:
63



PP-1-2V1
6.00%
K1 [pN, 20° C.]:
12.6



PY-3-O2
7.00%
K3 [pN, 20° C.]:
14.1



PYP-2-3
8.00%
V0 [20° C., V]:
2.86



Y-4O-O4
3.00%










Example 211a

The mixture according to Example 211 additionally comprises 0.04% of




embedded image


and 0.02% of




embedded image


Example 212




















APUQU-2-F
2.50%
Clearing point [° C.]:
97.5



APUQU-3-F
7.00%
Δn [589 nm, 20° C.]:
0.1000



PGUQU-3-F
4.00%
Δε [1 kHz, 20° C.]:
8.0



PGUQU-4-F
4.00%
ε|| [1 kHz, 20° C.]:
11.1



PUQU-3-F
4.00%
ε [1 kHz, 20° C.]:
3.1



CCP-V-1
6.00%
γ1 [mPa · s, 20° C.]:
93



CCP-V2-1
14.00%
K1 [pN, 20° C.]:
15.3



CCGU-3-F
3.50%
K3 [pN, 20° C.]:
17.6



CCQU-3-F
10.00%
V0 [20° C., V]:
1.45



PCH-302
6.50%



CC-3-V
25.00%



CC-3-V1
8.00%



CCP-30CF3
5.00%



PPGU-3-F
0.50%










Example 212a

The mixture according to Example 212 additionally comprises 0.25% of




embedded image


Example 213




















CY-3-O2
18.50%
Clearing point [° C.]:
80



CCY-3-O2
11.00%
Δn [589 nm, 20° C.]:
0.0896



CCY-4-O2
9.00%
Δε [1 kHz, 20° C.]:
−3.4



CPY-2-O2
7.50%
ε|| [1 kHz, 20° C.]:
3.5



CPY-3-O2
9.00%
ε [1 kHz, 20° C.]:
6.9



CCH-34
9.00%
γ1 [mPa · s, 20° C.]:
117



CCH-35
9.00%
K1 [pN, 20° C.]:
14.4



CC-3-V
10.00%
K3 [pN, 20° C.]:
15.1



CCH-301
9.00%
V0 [20° C., V]:
2.23



CCH-303
5.00%



PYP-2-3
3.00%










Example 213a

The mixture according to Example 213 additionally comprises 0.2% of




embedded image


Example 214




















CY-3-O2
10.50%
Clearing point [° C.]:
79.7



PY-1-O4
5.00%
Δn [589 nm, 20° C.]:
0.1113



PY-3-O2
7.50%
Δε [1 kHz, 20° C.]:
−4.4



PY-4-O2
4.00%
K1 [pN, 20° C.]:
14.5



CCY-3-O1
5.50%
K3 [pN, 20° C.]:
16.7



CCY-3-O2
5.00%
V0 [20° C., V]:
2.05



CCY-4-O2
4.00%



CLY-3-O2
9.00%



CPY-2-O2
9.00%



CPY-3-O2
9.00%



CC-3-V
23.50%



CC-3-V1
7.00%



CBC-33F
1.00%










Example 215




















APUQU-3-F
3.00%
Clearing point [° C.]:
90.5



CC-3-V1
7.75%
Δn [589 nm, 20° C.]:
0.1057



CC-4-V
10.00%
Δε [1 kHz, 20° C.]:
7.4



CC-5-V
9.25%
γ1 [mPa · s, 20° C.]:
91



CCGU-3-F
7.00%
K1 [pN, 20° C.]:
13.6



CCH-34
3.00%
K3 [pN, 20° C.]:
15.5



CCP-30CF3
2.50%
V0 [20° C., V]:
1.43



CCP-V-1
14.00%



CCP-V2-1
9.50%



PCH-301
11.00%



PGP-2-2V
2.00%



PGUQU-3-F
5.00%



PPGU-3-F
0.50%



PUQU-3-F
12.00%



APUQU-2-F
3.50%










Example 216




















CC-3-V
27.00%
Clearing point [° C.]:
74.9



CCY-3-1
9.50%
Δn [589 nm, 20° C.]:
0.1093



CCP-3-1
8.00%
Δε [1 kHz, 20° C.]:
−3.8



CLY-3-O2
6.00%
ε|| [1 kHz, 20° C.]:
3.7



CPY-2-O2
10.50%
ε [1 kHz, 20° C.]:
7.5



CPY-3-O2
10.50%
γ1 [mPa · s, 20° C.]:
108



CY-3-O2
15.00%
K1 [pN, 20° C.]:
14.1



PY-3-O2
13.50%
K3 [pN, 20° C.]:
15.8





V0 [20° C., V]:
2.16










Example 217




















CC-3-V
16.00%
Clearing point [° C.]:
85.4



CC-3-V1
5.00%
Δn [589 nm, 20° C.]:
0.1060



CCH-34
7.00%
Δε [1 kHz, 20° C.]:
−3.7



CCP-3-1
1.00%
ε|| [1 kHz, 20° C.]:
3.6



CCY-3-O1
6.00%
ε [1 kHz, 20° C.]:
7.4



CCY-3-O2
7.50%
γ1 [mPa · s, 20° C.]:
114



CCY-3-O3
2.00%
K1 [pN, 20° C.]:
13.4



CCY-4-O2
5.00%
K3 [pN, 20° C.]:
14.5



CPY-2-O2
10.00%
V0 [20° C., V]:
2.09



CPY-3-O2
9.00%



CY-3-O2
10.00%



CY-3-O4
6.50%



CY-5-O4
6.00%



PYP-2-3
5.50%



PYP-2-4
3.50%










Example 217a

The mixture according to Example 217 additionally comprises 0.04% of




embedded image


Example 218




















CCH-23
12.00%
Clearing point [° C.]:
110.7



CCH-34
10.00%
Δn [589 nm, 20° C.]:
0.1002



CCP-3-1
7.00%
Δε [1 kHz, 20° C.]:
−2.9



CCY-3-1
10.00%
ε|| [1 kHz, 20° C.]:
3.2



CCY-3-O1
1.50%
ε [1 kHz, 20° C.]:
6.1



CCY-3-O2
9.00%
γ1 [mPa · s, 20° C.]:
147



CCY-3-O3
7.50%
K1 [pN, 20° C.]:
17.3



CCY-4-O2
9.00%
K3 [pN, 20° C.]:
18.3



CPGP-4-3
2.00%
V0 [20° C., V]:
2.65



CPY-2-O2
8.00%



CPY-3-O2
8.00%



CY-3-O2
1.50%



CY-3-O4
3.00%



PCH-301
10.00%



PYP-2-3
1.50%










Example 218a

The mixture according to Example 218 additionally comprises 0.04% of




embedded image


Example 219




















BCH-32
1.50%
Clearing point [° C.]:
74.3



CC-3-V
19.50%
Δn [589 nm, 20° C.]:
0.1089



CC-3-V1
5.50%
Δε [1 kHz, 20° C.]:
−3.8



CCP-3-1
8.00%
ε|| [1 kHz, 20° C.]:
3.7



CCP-3-3
4.50%
ε [1 kHz, 20° C.]:
7.5



CLY-3-O2
6.00%
γ1 [mPa · s, 20° C.]:
115



CPY-2-O2
10.50%
K1 [pN, 20° C.]:
13.7



CPY-3-O2
10.50%
K3 [pN, 20° C.]:
16.1



CY-3-O2
15.00%
V0 [20° C., V]:
2.18



CY-5-O2
9.00%



PY-3-O2
10.00%










Example 220




















CY-3-O2
15.00%
Clearing point [° C.]:
74.7



CY-5-O2
6.50%
Δn [589 nm, 20° C.]:
0.1082



CCY-3-O2
11.00%
Δε [1 kHz, 20° C.]:
−3.0



CPY-2-O2
5.50%
ε|| [1 kHz, 20° C.]:
3.6



CPY-3-O2
10.50%
ε [1 kHz, 20° C.]:
6.6



CC-3-V
28.50%
γ1 [mPa · s, 20° C.]:
97



CC-3-V1
10.00%
K1 [pN, 20° C.]:
12.9



PYP-2-3
12.50%
K3 [pN, 20° C.]:
15.7



PPGU-3-F
0.50%
V0 [20° C., V]:
2.42










Example 221




















PGUQU-3-F
5.00%
Clearing point [° C.]:
84.8



CCQU-3-F
8.00%
Δn [589 nm, 20° C.]:
0.1035



CCQU-5-F
4.00%
Δε [1 kHz, 20° C.]:
10.1



PUQU-3-F
13.50%
ε|| [1 kHz, 20° C.]:
13.5



APUQU-2-F
3.00%
ε [1 kHz, 20° C.]:
3.4



APUQU-3-F
6.00%
γ1 [mPa · s, 20° C.]:
86



CC-3-V
25.50%
K1 [pN, 20° C.]:
12.3



CC-3-V1
6.00%
K3 [pN, 20° C.]:
15.0



CCP-V-1
13.00%
V0 [20° C., V]:
1.17



CCP-V2-1
6.00%



PPGU-3-F
0.50%



BCH-3F.F
7.50%



BCH-2F.F
2.00%










Example 221a

The mixture according to Example 221 additionally comprises 0.25% of




embedded image


Example 222




















CY-3-O2
12.00%
Clearing point [° C.]:
85.4



CY-5-O2
12.00%
Δn [589 nm, 20° C.]:
0.1039



CCY-3-O3
5.00%



CCY-4-O2
5.00%



CPY-2-O2
10.00%



CPY-3-O2
10.00%



CCY-2-1
4.00%



CC-3-V
16.00%



CCH-23
10.00%



CCH-34
4.00%



CCP-V-1
4.00%



PGP-2-5
2.00%



CPGP-5-2
3.00%



CPGP-5-3
3.00%










Example 223




















CC-3-V
41.50%
Clearing point [° C.]:
74.5



CCY-3-O1
2.50%
Δn [589 nm, 20° C.]:
0.0984



CCY-3-O2
11.50%
Δε [1 kHz, 20° C.]:
−3.3



CCY-3-O3
5.00%
ε|| [1 kHz, 20° C.]:
3.5



CPY-2-O2
5.00%
ε [1 kHz, 20° C.]:
6.7



CPY-3-O2
12.00%
γ1 [mPa · s, 20° C.]:
89



CY-3-O2
9.50%
K1 [pN, 20° C.]:
13.2



PY-3-O2
7.00%
K3 [pN, 20° C.]:
15.2



PY-4-O2
3.00%
V0 [20° C., V]:
2.29



PYP-2-3
3.00%










Example 223a

The mixture according to Example 223 additionally comprises 0.001% of Irganox® 1076 (octadecyl 3-(3,5-di-tert-butyl-4-hydroxyphenyl)propionate, BASF) and 0.4% of




embedded image


Example 224




















CC-3-V
30.50%
Clearing point [° C.]:
80.1



CC-3-V1
4.50%
Δn [589 nm, 20° C.]:
0.1033



CCY-3-O1
6.00%
Δε [1 kHz, 20° C.]:
−4.0



CCY-3-O2
8.00%
ε|| [1 kHz, 20° C.]:
3.6



CLY-3-O2
8.00%
ε [1 kHz, 20° C.]:
7.6



CPY-2-O2
8.00%
γ1 [mPa · s, 20° C.]:
113



CPY-3-O2
12.00%
K1 [pN, 20° C.]:
14.4



CY-3-O2
15.00%
K3 [pN, 20° C.]:
17.0



PY-3-O2
8.00%
V0 [20° C., V]:
2.16










Example 225




















CC-3-V
41.50%
Clearing point [° C.]:
74.5



CCY-3-O1
2.50%
Δε [1 kHz, 20° C.]:
−3.3



CCY-3-O2
11.50%
K1 [pN, 20° C.]:
13.2



CCY-3-O3
5.00%
K3 [pN, 20° C.]:
15.2



CPY-2-O2
5.00%
V0 [20° C., V]:
2.29



CPY-3-O2
12.00%



CY-3-O2
9.50%



PY-3-O2
7.00%



PY-4-O2
3.00%



PYP-2-3
3.00%










Example 226




















CC-3-V
26.00%
Clearing point [° C.]:
80.5



CCY-3-O2
6.00%
Δn [589 nm, 20° C.]:
0.1040



CCY-3-O3
6.00%
Δε [1 kHz, 20° C.]:
−4.0



CCY-4-O2
6.00%
ε|| [1 kHz, 20° C.]:
3.7



CCY-5-O2
6.00%
ε [1 kHz, 20° C.]:
7.7



CPY-2-O2
6.00%
γ1 [mPa · s, 20° C.]:
133



CPY-3-O2
6.00%
K1 [pN, 20° C.]:
13.6



PYP-2-3
7.00%
K3 [pN, 20° C.]:
15.4



CY-3-O2
15.00%
V0 [20° C., V]:
2.07



CY-5-O2
12.00%
LTS (bulk) [−20° C.]
>1000 h



BCH-32
4.00%










Example 226a

The mixture according to Example 226 additionally comprises 0.3% of




embedded image


Example 227




















CC-3-V
26.50%
Clearing point [° C.]:
84.6



CC-3-V1
2.00%
Δn [589 nm, 20° C.]:
0.1076



CCH-34
2.00%
Δε [1 kHz, 20° C.]:
−4.0



CCY-3-O2
10.00%
ε|| [1 kHz, 20° C.]:
3.7



CCY-3-O3
5.00%
ε [1 kHz, 20° C.]:
7.7



CCY-4-O2
10.00%
γ1 [mPa · s, 20° C.]:
129



CPY-2-O2
10.00%
K1 [pN, 20° C.]:
13.9



CPY-3-O2
10.00%
K3 [pN, 20° C.]:
15.4



CY-3-O2
10.50%
V0 [20° C., V]:
2.06



PYP-2-3
9.00%



Y-4O-O4
5.00%










Example 227a

The mixture according to Example 227 additionally comprises 0.04% of




embedded image


and 0.015% of




embedded image


Example 228




















APUQU-3-F
1.50%
Clearing point [° C.]:
110.1



CC-3-V
34.00%
Δn [589 nm, 20° C.]:
0.1208



CC-3-V1
5.00%
Δε [1 kHz, 20° C.]:
6.2



CCP-30CF3
4.50%
ε|| [1 kHz, 20° C.]:
9.2



CCP-V-1
10.50%
ε [1 kHz, 20° C.]:
3.0



CCP-V2-1
6.00%
γ1 [mPa · s, 20° C.]:
104



CCVC-3-V
3.50%
K1 [pN, 20° C.]:
16.3



CPGP-5-2
4.50%
K3 [pN, 20° C.]:
18.9



CPGP-5-3
4.50%
V0 [20° C., V]:
1.70



DGUQU-4-F
3.00%



PGP-2-3
4.00%



PGP-2-4
2.00%



PGUQU-3-F
5.00%



PGUQU-4-F
3.50%



PGUQU-5-F
3.00%



PPGU-3-F
0.50%



PUQU-3-F
5.00%










Example 229




















APUQU-3-F
1.50%
Clearing point [° C.]:
110



CC-3-V
35.50%
Δn [589 nm, 20° C.]:
0.1257



CCP-30CF3
4.00%
Δε [1 kHz, 20° C.]:
6.3



CCP-V-1
12.00%
ε|| [1 kHz, 20° C.]:
9.3



CCP-V2-1
4.50%
ε [1 kHz, 20° C.]:
3.0



CCVC-3-V
4.00%
γ1 [mPa · s, 20° C.]:
104



CPGP-5-2
5.00%
K1 [pN, 20° C.]:
16.1



CPGP-5-3
5.00%
K3 [pN, 20° C.]:
18.7



DGUQU-4-F
3.00%
V0 [20° C., V]:
1.69



PGP-2-3
4.00%



PGP-2-4
2.00%



PGUQU-3-F
5.00%



PGUQU-4-F
3.50%



PGUQU-5-F
3.00%



PPGU-3-F
0.50%



PUQU-3-F
5.00%



PP-1-2V1
2.50%










Example 230




















CY-3-O2
5.00%
Clearing point [° C.]:
102



CY-3-O4
15.00%
Δn [589 nm, 20° C.]:
0.2503



CCY-3-O2
6.00%
Δε [1 kHz, 20° C.]:
−4.0



CCY-3-O3
6.00%
ε|| [1 kHz, 20° C.]:
4.3



CPY-2-O2
3.00%
ε [1 kHz, 20° C.]:
8.3



PTP-102
5.00%
γ1 [mPa · s, 20° C.]:
392



PPTUI-3-2
15.00%
K1 [pN, 20° C.]:
19.5



PPTUI-3-4
11.00%
K3 [pN, 20° C.]:
24.0



PTP-302FF
12.00%
V0 [20° C., V]:
2.57



PTP-502FF
12.00%



CPTP-302FF
5.00%



CPTP-502FF
5.00%










Example 231




















CC-3-V
35.00%
Clearing point [° C.]:
79.6



CCP-3-1
7.50%
Δn [589 nm, 20° C.]:
0.1095



CCPC-33
2.00%
Δε [1 kHz, 20° C.]:
−2.6



CCY-3-O2
7.00%
ε|| [1 kHz, 20° C.]:
3.5



CCY-4-O2
7.50%
ε [1 kHz, 20° C.]:
6.1



CPY-2-O2
8.50%
γ1 [mPa · s, 20° C.]:
92



CPY-3-O2
9.00%
K1 [pN, 20° C.]:
14.5



PP-1-2V1
5.50%



PY-3-O2
8.00%



PYP-2-3
5.00%



Y-4O-O4
5.00%










Example 231a

The mixture according to Example 231 additionally comprises 0.04% of




embedded image


and 0.02% of




embedded image


Example 232




















CY-3-O4
25.00%
Clearing point [° C.]:
81.2



CY-5-O2
9.00%
Δn [589 nm, 20° C.]:
0.1531



CCY-3-O2
7.00%
Δε [1 kHz, 20° C.]:
−5.0



CCY-3-O3
4.50%
ε|| [1 kHz, 20° C.]:
4.1



CPY-2-O2
10.00%
ε [1 kHz, 20° C.]:
9.1



CPY-3-O2
10.00%
γ1 [mPa · s, 20° C.]:
298



PYP-2-3
14.00%
K1 [pN, 20° C.]:
13.1



PYP-2-4
10.00%
K3 [pN, 20° C.]:
15.9



CCP-V-1
3.00%
V0 [20° C., V]:
1.89



BCH-32
2.00%



PP-1-2V1
3.50%



PGP-2-3
2.00%










Example 232a

The mixture according to Example 232 additionally comprises 10% of




embedded image


Example 233




















CC-3-V
29.00%
Clearing point [° C.]:
80.1



CCY-3-O1
8.00%
Δn [589 nm, 20° C.]:
0.1033



CCY-3-O2
6.00%
Δε [1 kHz, 20° C.]:
−4.5



CCY-4-O2
2.00%
ε|| [1 kHz, 20° C.]:
4.0



CLY-3-O2
8.50%
ε [1 kHz, 20° C.]:
8.4



CLY-3-O3
7.50%
γ1 [mPa · s, 20° C.]:
98



CPY-2-O2
10.00%
K1 [pN, 20° C.]:
13.2



CPY-3-O2
7.50%
K3 [pN, 20° C.]:
14.6



CY-3-O2
6.50%
V0 [20° C., V]:
1.91



PY-3-O2
10.00%



Y-4O-O4
5.00%










Example 233a

The mixture according to Example 233 additionally comprises 0.04% of




embedded image


and 0.02% of




embedded image


Example 234




















CC-3-V
34.00%
Clearing point [° C.]:
79.7



CCPC-33
1.00%
Δn [589 nm, 20° C.]:
0.1095



CCY-3-1
4.00%
Δε [1 kHz, 20° C.]:
−3.5



CCY-3-O2
10.00%
ε|| [1 kHz, 20° C.]:
3.7



CCY-4-O2
9.50%
ε [1 kHz, 20° C.]:
7.2



CPY-2-O2
9.00%
γ1 [mPa · s, 20° C.]:
105



CPY-3-O2
10.00%
K1 [pN, 20° C.]:
14.0



PP-1-2V1
1.50%



PY-3-O2
10.00%



PYP-2-3
6.00%



Y-4O-O4
5.00%










Example 234a

The mixture according to Example 234 additionally comprises 0.04% of




embedded image


and 0.02% of




embedded image


Example 235




















CC-3-V
19.00%
Clearing point [° C.]:
80.2



CCY-3-O1
5.00%
Δn [589 nm, 20° C.]:
0.1104



CCY-3-O2
7.00%
Δε [1 kHz, 20° C.]:
−3.7



CCY-3-O3
12.00%
ε|| [1 kHz, 20° C.]:
3.6



CCY-4-O2
8.00%
ε [1 kHz, 20° C.]:
7.3



CPY-2-O2
9.50%
γ1 [mPa · s, 20° C.]:
143



CPY-3-O2
10.00%
K1 [pN, 20° C.]:
12.9



CY-3-O2
12.00%
K3 [pN, 20° C.]:
14.5



CY-3-O4
3.50%
V0 [20° C., V]:
2.09



PP-1-3
7.00%



PP-1-4
7.00%










Example 236




















CY-3-O2
15.00%
Clearing point [° C.]:
79.1



CY-5-O2
9.50%
Δn [589 nm, 20° C.]:
0.0944



CCY-3-O1
4.00%
Δε [1 kHz, 20° C.]:
−4.0



CCY-3-O2
6.00%
ε [1 kHz, 20° C.]:
3.7



CCY-3-O3
4.50%
ε [1 kHz, 20° C.]:
7.7



CCY-4-O2
6.00%
γ1 [mPa · s, 20° C.]:
120



CCY-5-O2
4.00%
K1 [pN, 20° C.]:
13.4



CPY-2-O2
8.00%
K3 [pN, 20° C.]:
15.4



CPY-3-O2
9.00%
V0 [20° C., V]:
2.06



PYP-2-4
2.00%



CC-3-V
32.00%










Example 236a

The mixture according to Example 236 additionally comprises 0.015% of




embedded image


Example 237




















CY-3-O2
15.00%
Clearing point [° C.]:
79.1



CY-5-O2
9.50%
Δn [589 nm, 20° C.]:
0.0944



CCY-3-O1
4.00%
Δε [1 kHz, 20° C.]:
−4.0



CCY-3-O2
6.00%
ε [1 kHz, 20° C.]:
3.7



CCY-3-O3
4.50%
ε [1 kHz, 20° C.]:
7.7



CCY-4-O2
6.00%
γ1 [mPa · s, 20° C.]:
120



CCY-5-O2
4.00%
K1 [pN, 20° C.]:
13.4



CPY-2-O2
8.00%
K3 [pN, 20° C.]:
15.4



CPY-3-O2
9.00%
V0 [20° C., V]:
2.06



PYP-2-4
2.00%



CC-3-V
32.00%










Example 237a

The mixture according to Example 237 additionally comprises 0.015% of




embedded image


Example 238




















APUQU-3-F
4.00%
Clearing point [° C.]:
85.7



CC-3-V
41.00%
Δn [589 nm, 20° C.]:
0.1004



CC-3-V1
6.50%
Δε [1 kHz, 20° C.]:
6.8



CCP-V-1
12.00%
ε [1 kHz, 20° C.]:
9.8



CCP-V2-1
11.00%
ε [1 kHz, 20° C.]:
3.0



CPGP-5-3
2.50%
γ1 [mPa · s, 20° C.]:
69



PGUQU-3-F
5.00%
K1 [pN, 20° C.]:
13.0



PGUQU-4-F
4.00%
K3 [pN, 20° C.]:
16.6



PGUQU-5-F
3.50%
V0 [20° C., V]:
1.47



PUQU-3-F
10.50%










Example 239




















CC-3-V
32.50%
Clearing point [° C.]:
74.7



CC-3-V1
1.50%
Δn [589 nm, 20° C.]:
0.1090



CCY-3-O1
8.50%
Δε [1 kHz, 20° C.]:
−3.8



CCY-3-O2
5.50%
ε [1 kHz, 20° C.]:
3.7



CLY-3-O2
10.00%
ε [1 kHz, 20° C.]:
7.5



CPY-3-O2
9.50%
γ1 [mPa · s, 20° C.]:
102



PY-3-O2
10.50%
K1 [pN, 20° C.]:
13.8



CY-3-O2
14.00%
K3 [pN, 20° C.]:
15.7



PYP-2-3
8.00%
V0 [20° C., V]:
2.15










Example 240




















CC-3-V
33.00%
Clearing point [° C.]:
80.2



CCY-3-O1
6.00%
Δn [589 nm, 20° C.]:
0.1116



CCY-3-O2
8.00%
Δε [1 kHz, 20° C.]:
−4.1



CCY-4-O2
2.50%
ε [1 kHz, 20° C.]:
3.7



CPY-2-O2
8.00%
ε [1 kHz, 20° C.]:
7.8



CPY-3-O2
12.00%
γ1 [mPa · s, 20° C.]:
119



CLY-3-O2
8.00%
K1 [pN, 20° C.]:
14.5



PY-1-O4
1.50%
K3 [pN, 20° C.]:
16.1



PY-3-O2
10.00%
V0 [20° C., V]:
2.09



PY-4-O2
8.00%



CY-3-O2
3.00%










Example 240a

The mixture according to Example 240 additionally comprises 0.008% of




embedded image


Example 241




















BCH-3F.F
5.00%
Clearing point [° C.]:
101



BCH-3F.F.F
8.50%
Δn [589 nm, 20° C.]:
0.0925



CC-3-V1
10.00%
Δε [1 kHz, 20° C.]:
5.3



CC-4-V
12.50%
ε [1 kHz, 20° C.]:
8.3



CCG-V-F
9.00%
γ1 [mPa · s, 20° C.]:
119



CCP-2F.F.F
3.50%
K1 [pN, 20° C.]:
14.2



CCP-3-1
4.50%
K3 [pN, 20° C.]:
19.9



CCP-3F.F.F
10.00%
V0 [20° C., V]:
1.73



CCP-V-1
12.00%



CCP-V2-1
7.00%



ECCP-5F.F
13.00%



PUQU-3-F
5.00%










Example 242




















APUQU-2-F
4.00%
Clearing point [° C.]:
86.4



APUQU-3-F
6.00%
Δn [589 nm, 20° C.]:
0.1030



PUQU-3-F
10.00%
Δε [1 kHz, 20° C.]:
7.0



CCQU-3-F
2.00%
ε [1 kHz, 20° C.]:
10.1



CCP-V-1
13.00%
γ1 [mPa · s, 20° C.]:
71



CCP-V2-1
7.00%
K1 [pN, 20° C.]:
13.2



PGUQU-3-F
6.00%
K3 [pN, 20° C.]:
15.8



CC-3-V
40.00%
V0 [20° C., V]:
1.45



CC-3-V1
5.50%



PGP-2-3
3.00%



CPGP-5-2
3.00%



PPGU-3-F
0.50%










Example 242a

The mixture according to Example 242 additionally comprises 0.25% of RM-41




embedded image


Example 243




















Y-4O-O4
9.00%
Clearing point [° C.]:
96



CY-3-O4
12.00%
Δn [589 nm, 20° C.]:
0.0796



CCY-3-O1
5.00%
Δε [1 kHz, 20° C.]:
−2.3



CCY-3-O2
5.50%
ε [1 kHz, 20° C.]:
3.4



CCY-3-O3
5.50%
ε[1 kHz, 20° C.]:
5.7



CC-4-V
15.00%
K1 [pN, 20° C.]:
14.8



CC-5-V
5.50%
K3 [pN, 20° C.]:
16.6



CC-3-V1
6.50%
V0 [20° C., V]:
2.85



CCP-V-1
11.00%



CCP-V2-1
10.00%



CH-33
3.00%



CH-35
3.00%



CCPC-33
4.50%



CCPC-34
4.50%










Example 244




















Y-4O-O4
11.50%
Clearing point [° C.]:
95



CCY-3-O1
4.00%
Δn [589 nm, 20° C.]:
0.1697



CCY-3-O2
5.00%
Δε [1 kHz, 20° C.]:
−4.4



CCY-3-O3
2.50%
ε [1 kHz, 20° C.]:
4.1



CPY-3-O2
4.00%
ε [1 kHz, 20° C.]:
8.5



CC-4-V
10.00%
γ1 [mPa · s, 20° C.]:
193



CCP-V-1
6.00%
K1 [pN, 20° C.]:
16.8



CCP-V2-1
12.00%
K3 [pN, 20° C.]:
19.5



BCH-32
5.00%
V0 [20° C., V]:
2.23



PTP-302FF
12.00%



PTP-502FF
12.00%



CPTP-302FF
8.00%



CPTP-502FF
8.00%










Example 245




















CY-3-O2
10.00%
Clearing point [° C.]:
80.7



PY-1-O4
5.00%
Δn [589 nm, 20° C.]:
0.1123



PY-3-O2
6.50%
Δε [1 kHz, 20° C.]:
−4.2



PY-4-O2
3.00%
ε [1 kHz, 20° C.]:
3.8



CCY-3-O1
5.00%
ε [1 kHz, 20° C.]:
8.0



CCY-3-O2
5.00%
γ1 [mPa · s, 20° C.]:
150



CCY-4-O2
3.00%
K1 [pN, 20° C.]:
14.6



CLY-3-O2
8.00%
K3 [pN, 20° C.]:
15.2



CPY-2-O2
10.00%
V0 [20° C., V]:
2.01



CPY-3-O2
10.00%



CCH-301
8.50%



CCH-23
12.00%



CCH-34
4.50%



CCH-35
3.00%



BCH-32
6.50%










Example 246




















PCH-3N.F.F
7.00%
Clearing point [° C.]:
91



CP-1V-N
18.00%
Δn [589 nm, 20° C.]:
0.2003



CP-V2-N
16.00%
Δε [1 kHz, 20° C.]:
10.3



CC-4-V
12.00%
ε [1 kHz, 20° C.]:
14.3



CCP-V-1
9.00%
ε [1 kHz, 20° C.]:
4.0



PPTUI-3-2
18.00%



PPTUI-3-4
20.00%










Example 247




















BCH-32
8.00%
Clearing point [° C.]:
96



CC-3-V
24.50%
Δn [589 nm, 20° C.]:
0.1195



CCP-V-1
8.00%
Δε [1 kHz, 20° C.]:
−2.7



CCY-2-1
2.00%
ε [1 kHz, 20° C.]:
3.3



CCY-3-O1
6.00%



CCY-3-O3
2.00%



CLY-3-O2
5.00%



CLY-3-O3
5.00%



CPY-2-O2
6.50%



CPY-3-O2
6.00%



CY-3-O2
6.00%



CY-3-O4
3.00%



CY-5-O2
5.00%



PYP-2-3
6.50%



PYP-2-4
6.50%










Example 247a

The mixture according to Example 247 additionally comprises 0.03% of




embedded image


and 0.4% of




embedded image


Example 248




















BCH-32
2.00%
Clearing point [° C.]:
80



CC-3-V
31.00%
Δn [589 nm, 20° C.]:
0.1083



CCY-3-O1
4.50%
Δε [1 kHz, 20° C.]:
−3.9



CCY-3-O2
6.00%
ε [1 kHz, 20° C.]:
3.7



CCY-4-O2
7.00%
γ1 [mPa · s, 20° C.]:
120



CLY-3-O2
8.00%
K1 [pN, 20° C.]:
12.7



CPY-2-O2
7.50%
K3 [pN, 20° C.]:
15.1



CPY-3-O2
10.00%
V0 [20° C., V]:
2.07



CY-3-O2
6.25%



PY-3-O2
5.75%



PY-1-O4
6.00%



PY-4-O2
6.00%










Example 248a

The mixture according to Example 248 additionally comprises 0.005% of




embedded image


Example 249




















CC-3-V
37.00%
Clearing point [° C.]:
75.2



CCY-3-O1
5.00%
Δn [589 nm, 20° C.]:
0.1016



CCY-3-O2
5.00%
Δε [1 kHz, 20° C.]:
−3.7



CCY-4-O2
4.00%
ε [1 kHz, 20° C.]:
3.7



CLY-3-O2
7.00%
γ1 [mPa · s, 20° C.]:
99



CPY-2-O2
9.00%
V0 [20° C., V]:
2.13



CPY-3-O2
10.00%



CY-3-O2
11.50%



PY-3-O2
11.50%










Example 249a

The mixture according to Example 249 additionally comprises 0.015% of




embedded image


Example 249b

The mixture according to Example 249 additionally comprises 0.005% of




embedded image


Example 250




















PUQU-3-F
8.00%
Clearing point [° C.]:
96.3



APUQU-2-F
6.00%
Δn [589 nm, 20° C.]:
0.0994



APUQU-3-F
6.00%
Δε [1 kHz, 20° C.]:
9.6



CDUQU-3-F
6.00%
γ1 [mPa · s, 20° C.]:
87



DPGU-4-F
6.00%
K1 [pN, 20° C.]:
14.5



CCGU-3-F
4.00%
K3 [pN, 20° C.]:
16.6



CC-3-V
36.00%
V0 [20° C., V]:
1.29



CC-3-V1
8.00%



CCP-V-1
12.00%



CCP-V2-1
6.00%



CBC-33F
1.50%



PPGU-3-F
0.50%









Claims
  • 1. Process for the purification of a liquid-crystal mixture (7) in which the liquid-crystal mixture (7) is passed through a first electrodialysis cell (2), a concentrate solution (14) is passed through a second electrodialysis cell (8) which is adjacent to the first electrodialysis cell (2) and is separated by an ion-exchanger membrane (9), and, with the aid of an anode/cathode arrangement (15, 16) arranged outside the electrodialysis cells (2, 8), an electric field transverse to a direction of passage of the liquid-crystal mixture (7) through the first electrodialysis cell (2) is generated so that ionised constituents of the liquid-crystal mixture (7) are discharged at the ion-exchanger membrane (9) and removed from the liquid-crystal mixture (7).
  • 2. Process according to claim 1, characterised in that the liquid-crystal mixture (7) is passed through the first electrodialysis cell (2) a number of times.
  • 3. Process according to claim 1, characterised in that the liquid-crystal mixture (7) is passed successively through a plurality of electrodialysis cells having an arrangement, comparable to the first electrodialysis cell (2), of an ion-exchanger membrane (9) and an adjacent second electrodialysis cell (8) and an electric field.
  • 4. Process according to claim 1, characterised in that the liquid-crystal mixture (7) is passed through the first electrodialysis cell (2) over a period of more than one hour, preferably more than four hours.
  • 5. Process according to claim 1, characterised in that the concentrate solution (14) used is deionised water.
  • 6. Process according to claim 1, characterised in that the ion-exchanger membrane (9) used is a membrane having a breakdown voltage of greater than 10 volts, preferably greater than 80 volts and particularly preferably 400 volts or more, and an electric potential difference which effects the greatest possible drop in voltage at the ion-exchanger membrane (9), but which is below the breakdown voltage, is pre-specified with the aid of the anode/cathode arrangement (15, 16).
  • 7. Process according to claim 1, characterised in that the anode (15) and the cathode (16) are flushed with transformer oil (19) while the process is being carried out.
  • 8. Process according to claim 1, characterised in that low-pulsation pumps are used to convey the liquid-crystal mixture (7) and the concentrate solution (14).
  • 9. Process according to claim 1, characterised in that the liquid-crystal mixture (7) is thoroughly mixed and homogenised before introduction into the first electrodialysis cell (2).
Priority Claims (1)
Number Date Country Kind
10 2013 021 279.0 Dec 2013 DE national
PCT Information
Filing Document Filing Date Country Kind
PCT/EP2014/003376 12/16/2014 WO 00