Claims
- 1. A process for the production of a finely dispersed crystal suspension of an organic compound comprising the steps of
- a) spraying a melt of the organic compound into an aqueous phase having a temperature below the crystallization point of the molten organic compound, in such a manner that the mixing ratio of melt to aqueous phase results in a mixture, the temperature of the mixture being lower than the solidification or crystallization temperature of the melt to form a preliminary emulsion, and
- b) feeding the preliminary emulsion within a residence time of 0.005 s to 0.15 s through a homogenizing nozzle to form a finely dispersed emulsion, thereby solidifying the finely dispersed emulsion to form a final crystal suspension.
- 2. A process according to claim 1, wherein the residence time is from about 0.01 s to 0.1 s.
- 3. A process according to claim 1, wherein the melt is sprayed into the aqueous phase immediately before the homogenizing nozzle.
- 4. A process according to claim 1, wherein a jet disperser comprising one or more capillary bores is used as the homogenizing nozzle.
- 5. A process according to claim 1, wherein the particle size is specifically adjusted by varying the pressure under which the melt is sprayed into the aqueous phase.
- 6. A process according to claim 1, wherein the crystal suspension is partly recirculated and cooled and then passed through the emulsification zone.
Priority Claims (1)
Number |
Date |
Country |
Kind |
3916465 |
May 1989 |
DEX |
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Parent Case Info
This application is a continuation of application Ser. No. 525,414, filed May 18, 1990, now abandoned.
US Referenced Citations (9)
Foreign Referenced Citations (3)
Number |
Date |
Country |
0101007 |
Feb 1984 |
EPX |
0289422 |
Nov 1988 |
EPX |
1569288 |
Jun 1980 |
GBX |
Continuations (1)
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Number |
Date |
Country |
Parent |
525414 |
May 1990 |
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