This application claims the benefit of priority of Japanese Patent Application Number 2017-094230 filed on May 10, 2017, the entire content of which is hereby incorporated by reference.
The present disclosure relates to a saw wire and a cutting apparatus including the saw wire.
Conventionally, a multi-wire saw for slicing a silicon ingot using wires composed of piano wire, has been known (see reference, for example, to Japanese Unexamined Patent Application Publication. No. 2008-213111).
During the slicing operation of a wire saw, swarf is produced in an amount approximately corresponding to the wire diameter. The aforementioned multiwire saw uses wires composed of piano wire, however, it is difficult to reduce the diameter size of piano wire. More specifically, it is difficult, in the present conditions, to manufacture piano wire having a diameter less than 60 μm. In addition, since piano wire has an elastic modulus of at least 150 GPa and at most 250 GPa, even if the piano wire could be thinned, deflection still occurs during the slicing process. Therefore, thinned piano wire is unsuitable for use in wire-saw slicing.
In view of the above, an object of the present disclosure is to provide a saw wire capable of reducing kerf loss of an object to be cut, and a cutting apparatus including the saw wire.
In order to achieve the above-described object, a saw wire according to an aspect of the present disclosure includes a metal wire containing at least one of tungsten and a tungsten alloy. A surface roughness Ra of the metal wire is at most 0.15 μm, and a diameter of the metal wire is at most 60 μm.
In addition, a cutting apparatus according to an aspect of the present disclosure includes the saw wire.
In addition, a method of slicing an ingot according to an aspect of the present disclosure includes: moving at least one saw wire relative to the ingot, each saw wire including a metal wire containing at least one of tungsten and a tungsten alloy, a surface roughness Ra of the metal wire being at most 0.15 μm, and a diameter of the metal wire being at most 60 μm; and dividing the ingot at least into partly-sliced portions by the at least one saw wire.
In addition, a method of manufacturing a saw wire according to an aspect of the present disclosure includes forming a metal wire containing at least one of tungsten and a tungsten alloy. In the method, a surface roughness Ra of the metal wire is at most 0.15 μm, and a diameter of the metal wire is at most 60 μm.
According to the present disclosure, it is possible to provide a saw wire capable of reducing kerf loss of an object to be cut, and a cutting apparatus including the saw wire.
The figures depict one or more implementations in accordance with the present teaching, by way of examples only, not by way of limitations. In the figures, like reference numerals refer to the same or similar elements.
The following describes in detail a saw wire and a cutting apparatus according to an embodiment of the present disclosure, with reference to the drawings. It should be noted that the embodiment described below indicates one specific example of the present disclosure. The numerical values, shapes, materials, structural components, the disposition and connection of the structural components, etc. described in the following embodiment are mere examples, and do not intend to limit the present disclosure. Furthermore, among the structural components in the following exemplary embodiment, components not recited in the independent claim which indicates the broadest concept of the present invention are described as arbitrary structural components.
In addition, each diagram is a schematic diagram and not necessarily strictly illustrated. Accordingly, for example, scale sizes, etc., are not necessarily exactly represented. In each of the diagrams, substantially the same structural components are assigned with the same reference signs, and redundant descriptions wilt be omitted or simplified.
In addition, a term, such as “parallel” or “equal”, representing a relationship between the components as well as a term, such as “circular”, representing a form, and a numerical range arc used in the present description.. Such terms and range are each not representing only a strict meaning of the term or range, but implying that a substantially same range, e.g., a range that includes even a difference as small as a few percentage points, is connoted in the term or range.
(Cutting Apparatus)
First, an overview of a cutting apparatus including a saw wire according to the present embodiment will be described with reference to
As illustrated in
It should be noted that ingot 20 is a silicon ingot but is not limited to such. For example, an ingot including other substance such as silicon carbide or sapphire may be used. Alternatively, an object to be cut by cutting apparatus 1 may be concrete, glass, etc.
As illustrated in
A single saw wire 10 is looped multiple times over two guide rollers 2. Here, for convenience of explanation, one loop of saw wire 10 is regarded as one saw wire 10, and it is assumed that a plurality of saw wires 10 are looped over two guide rollers 2. Stated differently, in the description below, the plurality of saw wires 10 form a single continuous saw wire 10. It should be noted that the plurality of saw wires 10 may be a plurality of saw wires that are separated from one another.
Each of guide rollers 2 rotates in the state in which saw wire 10 is straightly tightened with a predetermined tension, and thereby causes saw wire 10 to rotate at a predetermined speed. Saw wires 10 are disposed in parallel to one another and are equally spaced. More specifically, each guide roller 2 is provided with grooves positioned at predetermined intervals for saw wires 10 to fit in. The intervals between the grooves are determined according to the thickness of the wafers desired to be sliced off. The width of the groove is substantially the same as diameter φ of saw wire 10.
Tension releasing device 4 is a device that releases tension exerted on saw wire 10. Tension releasing device 4 is, for example, an elastic body such as a coiled or plate spring. As illustrated in
It should be noted that cutting apparatus 1 may include three or more guide rollers 2. Saw wires 10 may be looped over three or more guide rollers 2.
Ingot holder 3 holds ingot 20 which is an object to be cut. Ingot holder 3 pushes ingot 20 through saw wires 10, and thereby ingot 20 is sliced by saw wires 10.
It should be noted that, although not illustrated in the diagram, cutting apparatus 1 may include a feeder that feeds a cutting fluid such as a coolant to saw wires 10.
By pushing ingot 20 through saw wires 10, ingot 20 is simultaneously divided into partly-sliced portions 21 by saw wires 10. Space 22 between neighboring partly-sliced portions 21 is a space made by ingot 20 being scrap off by saw wire 10. In other words, the size of space 22 is equivalent to a kerf loss of ingot 20.
Width d of space 22 depends on diameter φ of saw wire 10. Stated differently, width d increases as diameter φ of saw wire 10 becomes larger, and thereby, the kerf loss of ingot 20 increases. Width d decreases as diameter φ of saw wire 10 becomes smaller, and thereby, the kerf loss of ingot 20 decreases.
More specifically, width d of space 22 becomes greater than diameter φ. The difference between width d and diameter φ depends or the size of abrasive particles 130 fixed to saw wire 10 and the oscillation width of the vibrations caused when saw wire 10 rotates around guide rollers 2.
It should be noted that thickness D of partly-sliced portion 21 depends on the intervals at which saw wires 10 are disposed. Accordingly, wire saws 10 are disposed at intervals each resulting from adding desired thickness D and a predetermined margin. More specifically, a margin is a difference between width d and diameter φ, and is a value determined in accordance with the oscillation width of saw wire 10 and the grain diameter of abrasive particle 130.
Based on what has been described above, diameter φ of saw wire 10 is a significant parameter in order to reduce the kerf loss of ingot 20. More specifically, by decreasing diameter φ of saw wire 10, the kerf loss of ingot 20 can be reduced.
The following describes the structure and manufacturing method of saw wire 10.
(Saw Wire)
As illustrated in
Metal wire 100 is a metal thin wire which includes tungsten (W) and is extremely fine. Metal wire 100 comprises pure tungsten. More specifically, the degree of purity of tungsten is 99.9% or higher.
Metal wire 100 which contains tungsten has a strength per an area of cross-section that increases with a decreasing diameter. Accordingly, use of metal wire 100 which contains tungsten makes it possible to implement saw wire 10 having small diameter and a high strength, and to reduce a kerf loss of ingot 20.
In addition, an elastic modulus of metal wire 100 is at least 350 GPa and at most 450 GPa. It should be noted that the elastic modulus is longitudinal elastic modulus. In other words, metal wire 100 has an elastic modulus approximately twice as high as that of piano wire.
The diameter of metal wire 100 is, for example, at most 60 μm. It should be noted that metal wire 100 which contains tungsten has a strength per an area of cross-section that increases as metal wire 100 becomes thinner; that is, increases with a decreasing diameter. For example, the diameter of metal wire 100 may be less than or equal to 50 μm or less than or equal to 40 μm. For example, the diameter of metal wire 100 is 20 μm, but may be 10 μm. It should be noted that, in the case where abrasive particles 130 are to he included as in the present embodiment, the diameter of metal wire 100 is, for example, greater than or equal to 10 μm.
Metal wire 100 is formed to be uniform in diameter. Note that diameter of metal wire 100 may not be entirely uniform and the size of diameter may slightly differ by approximately a few percentage points, e.g., 1%, depending on the portion of metal wire 100. Since the diameter of metal wire 100 is at most 60 μm, metal wire 100 has elasticity and thus can be bent easily to a satisfactory extent. Accordingly, it is possible to easily loop saw wire 10 over and across guide rollers 2.
As illustrated in
Metal wire 100 has a surface roughness Ra of at most 0.15 μm. It should be noted that the surface roughness Ra may be less than or equal to 0.10 μm. In addition, when the surface roughness Ra is excessively small, the adhesion of nickel plating layer 110 decreases, and thus the surface roughness Ra of metal wire 100 may be greater than 0.05 μm, for example.
Nickel plating layer 110 is a plating layer provided over the surface of metal wire 100. Nickel plating layer 110 is a thin-film layer containing nickel (Ni). Nickel plating layer 110 has a thickness of, for example, 1 μm. However, the thickness of nickel plating layer 110 is not limited to this example.
Nickel plating layer 110 tightly and closely covers at least part of the respective abrasive particles 130, and covers the entirely of the surface of metal wire 100 between the plurality of abrasive particles 130. More specifically, as illustrated in
The plurality of abrasive particles 130 are hard particles, such as diamond, cubic boron nitride (CBN), etc. An average grain diameter of the plurality of abrasive particles 130 is less than, or equal to 10 μm, for example. However, the average grain diameter of the plurality of abrasive particles 130 is not limited to this example. The plurality of abrasive particles 130 are each provided to the surface of saw wire 10 by being at least partially affixed firmly to nickel plating layer 110.
(Method of Manufacturing Saw Wire)
The following describes a method of manufacturing saw wire 10 having the above-described features. The method of manufacturing saw wire 10 includes a process of manufacturing metal wire 100 which has a reduced diameter size, and a process of fixing the plurality of abrasive particles 130 to metal wire 100.
First, the process of manufacturing metal wire 100 will be described with reference to FIG, 4.
First, tungsten powder 101 is prepared, as illustrated in (a) in
Next, by pressing and sintering tungsten powder 101, an ingot containing tungsten is produced. By performing, onto the ingot, a swaging processing of extending an ingot by press-forging the ingot from its periphery, tungsten wire 102 having a wire shape is produced, as illustrated in (b) in
Next, drawing processing using wire drawing dies is carried out, as illustrated in (c) in
To be specific, firstly, tungsten wire 102 is annealed, as illustrated in (c1) in
Next, drawing of tungsten wire 102 using wire drawing die 30, i.e., wire drawing process, is performed, as illustrated in (c2) in
Next, through the electrolytic polishing of tungsten wire 103 after the drawing process, the surface of tungsten wire 103 is rendered smooth, as illustrated in (c3) in
Next, die exchange is performed, as illustrated in (c4) in
The processes from (c1) to (c4) illustrated in
Similarly, in the annealing process illustrated in (c1) in
More specifically, the larger the diameter of the tungsten wire is, at higher temperature the tungsten wire is annealed, and the smaller the diameter of the tungsten wire is, at lower temperature the tungsten wire is annealed. To be more concrete, in the case where the diameter of the tungsten wire is large, for example, the tungsten wire is annealed at the temperature between 1400 degrees Celsius and 1800 degrees Celsius in the annealing process carried out in the first drawing processing. In the final annealing process carried out in the final drawing processing in which the tungsten wire is thinned down to finally have a desired diameter, the tungsten wire is heated at the temperature between 1200 degrees Celsius and 1500 degrees Celsius. It should be noted that, in the final annealing process, electricity need not, be conducted to the tungsten wire.
Moreover, an annealing process may be omitted when a drawing processing is repeated. For example, the final annealing process may be omitted. More specifically, the final annealing process may be omitted and a lubricant as well as the form and hardness of a wire drawing die may be adjusted.
In the drawing process after the final annealing process (i.e., the final drawing process), a single-crystal diamond die containing single-crystal diamond is used as wire drawing die 31. Diamond particles are less likely to be detached in the process using the single-crystal diamond die, and thus a streak is less likely to be formed on the tungsten wire after the drawing process. It is thus possible to reduce the surface roughness Ra of the tungsten wire which has a desired diameter.
In addition, when the drawing process is repeated, drawing is started using the single-crystal diamond die having a pore diameter of 200 μm, when a weight ratio of an amount of oxide included in the tungsten wire having a mass of 50 MG is in a range from 0.2% to 0.5%. In this manner, metal wire 100 having the surface roughness Ra less than or equal to 0.15 μm is manufactured, as illustrated in (d) in
Next, the process of fixing the plurality of abrasive particles 130 to metal wire 100 will be described with reference to
First, nickel plating layer 110 is formed on a surface of metal wire 100, and abrasive particles 130 are electrodeposited. More specifically, as illustrated in (e) in
In this manner, as illustrated in (f) in
With the processes as described above, saw wire 10 is manufactured.
It should be noted that each of
(Advantageous Effects, Etc.)
As described above, saw wire 10 according to the present embodiment includes metal wire 100 which contains tungsten, and a surface roughness Ra of metal wire 100 is at most 0.15 μm and a diameter of metal wire 100 is at most 60 μm.
With this configuration, since metal wire 100 contains tungsten., the strength of metal wire 100 increases and thereby tolerance against breakage is improved, as metal wire 100 is rendered thinner. Furthermore, metal wire 100 which contains tungsten is higher in an elastic modulus than piano wire. Since metal wire 100 is high in the strength and elastic modulus, it is possible to loop saw wire 10 over guide rollers 2 with a strong tension. Accordingly, it is possible to reduce the vibrations of saw wire 10 caused during the process of cutting ingot 20.
As described above, since saw wire 10 has a small diameter and is high in the strength and elastic modulus, it is possible to reduce the amount of swarf produced when ingot 20 is sliced, i.e., the kerf loss of ingot 20. Accordingly, it is possible to increase the number of wafers cut out from a single ingot 20.
Moreover, since the surface roughness Ra of metal wire 100 is small, when abrasive particles 130 are fixed to metal wire 100, stress applied to abrasive particles 130 during the process of slicing ingot 20 is easily and uniformly dispersed. Accordingly, it is possible to inhibit detachment of abrasive particles 130 from metal wire 100, and thus a decrease in sharpness of saw wire 10 can be reduced. In addition, stress applied to ingot 20 via abrasive particles 130 can also be easily and uniformly dispersed. Thus, ingot 20 can be smoothly sliced and vibrations of saw wire 10 are reduced, making it possible to reduce the kerf loss of ingot 20.
Here, a relationship between the surface roughness Ra of metal wire 100, the degree of detachment of abrasive particles 130, and the adhesion of nickel plating layer will be described with reference to
As illustrated in
In contrast, when the surface roughness Ra is excessively small, the adhesion of nickel plating layer 110 decreases. Accordingly, there is a possibility that abrasive particles 130 are detached together with nickel plating layer 110 from metal wire 100. For example, when the surface roughness Ra is 0.05 μm, detachment of nickel plating layer 110 occurs. Accordingly, metal wire 100 may have the surface roughness Ra greater than 0.05 μm and less than or equal to 0.15 μm.
In addition, for example, saw wire 10 further includes a plurality of abrasive particles 130 provided to a surface of metal wire 100.
With this configuration, saw wire 10 can he included in cutting apparatus 1 of a fixed abrasive particle type.
In addition, for example, saw wire 10 further includes nickel plating layer 110 provided to the surface of metal wire 100.
With this configuration, it is possible to enhance the adhesion of a plurality of abrasive particles 130 to metal wire 100.
In addition, cutting apparatus 1 according to the present embodiment includes saw wire 10.
With this configuration, the diameter of saw wire 10 is reduced, and thus it is possible to increase the number of wafers cut out from a single ingot 20. In addition, it is possible to reduce the amount of swarf produced when ingot 20 is sliced.
In addition, for example, cutting apparatus 1 includes tension releasing device 4 which releases tension exerted on saw wire 10.
With this configuration, it is possible to inhibit strong tension from being exerted on saw wire 10. Therefore, it is possible to inhibit breaking off or the like of saw wire 10.
(Variation)
Here, variation examples of the above-described embodiment will be described.
For example, although the case where metal wire 100 contains pure tungsten has been described in the above-described embodiment, the present disclosure is not limited to this example. Metal wire 100 may contain rhenium-tungsten (ReW) alloy.
More specifically, metal wire 100 may contain tungsten as a major component, and a predetermined proportion of rhenium. The rhenium content of metal wire 100 is, for example, at least 0.1 wt % and at most 10 wt % with respect to a total weight of rhenium and tungsten. Although the rhenium content, specifically, is 3 wt %, it may be 1 wt %.
Since metal wire 100 contains rhenium, it is possible to increase the strength of metal wire 100 to be higher than the strength of a pure tungsten wire. With this configuration, metal wire 100 has improved tolerance against breakage even after the thinning process as well as a surface having resistance to scraping. Accordingly, it is possible to easily reduce the surface roughness Ra. In other words, it is possible to easily manufacture metal wire 100 having the surface roughness Ra of at most 0.15 μm.
It should be noted that, although rhenium-tungsten (ReW) alloy is described as the tungsten alloy, the tungsten alloy may be nickel-tungsten (NiW) alloy.
In addition, for example, metal wire 100 of saw wire 10 may be doped with potassium (K).
The metal wire which contains tungsten and is dope with potassium (K) (hereinafter referred to as a potassium-doped tungsten wire) contains tungsten as a major component, and a predetermined proportion of potassium. The potassium content of the potassium-doped tungsten wire is at least 0.005 wt % and at most 0.010 wt % with respect to a total weight of potassium and tungsten.
The potassium-doped tungsten wire has a strength per an area of cross-section that increases with decreasing diameter φ. Accordingly, as with the case of the ReW alloy, use of the potassium-doped tungsten wire allows the surface of metal wire 100 to be resistant to scraping, and it is thus possible to easily reduce the surface roughness Ra. In other words, it is possible to easily manufacture metal wire 100 having the surface roughness Ra of at most 0.15 μm.
The elastic modulus, diameter, etc. of the ReW wire or the potassium-doped tungsten wire are respectively the same as those of metal wire 100 which contains tungsten.
(Others)
Although the saw wire and the cutting apparatus according to the present disclosure have been described based on the above-described embodiment and the variations thereof, the present disclosure is not limited to the above-described embodiment.
For example, although the case where nickel plating layer 110 is provided to the surface of metal wire 100 has been described in the above-described embodiment, the present disclosure is not limited to this example. A plurality of abrasive particles 130 may be fixed directly to metal wire 100.
In addition, for example, although cutting apparatus 1 of a fixed abrasive particle type in which abrasive particles 130 are fixed to metal wire 100 in advance has been described in the above-described embodiment, the present disclosure is not limited to this example. For example, cutting apparatus 1 may be of a free abrasive particle type. In this case, saw wire 10 is quite simply metal wire 100.
The stress applied to ingot 20 is more uniformed, with a decrease in the surface roughness Ra of saw wire 10, i.e., metal wire 100. Accordingly, it is possible to cut ingot 20 smoothly. Thus, when the surface roughness Ra is small, the oscillation width of saw wire 10 can be reduced as well. Accordingly, it is possible to reduce the kerb loss of ingot 20.
Moreover, cutting apparatus 1 is not limited to a multi-wire saw, and may be, for example, a wire sawing apparatus that, cuts out a wafer one by one by slicing ingot 20 using one wire saw 10. In addition, cutting apparatus 1 illustrated in
It should be noted that the present disclosure also includes other forms in which various modifications apparent to those skilled in the art are applied to the embodiment or forms in which structural components and functions in the embodiment are arbitrarily combined within the scope of the present disclosure.
While the foregoing has described one or more embodiments and/or other examples, it is understood that various modifications may be made therein and that the subject matter disclosed herein may be implemented in various forms and examples, and that they may be applied in numerous applications, only some of which have been described herein. It is intended by the following claims to claim any and all modifications and variations that fall within the true scope of the present teachings.
Number | Date | Country | Kind |
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2017-094230 | May 2017 | JP | national |