SBIR Phase I: Nonporous Zirconia for Ultrafast Analytical Chromatography

Information

  • NSF Award
  • 9761543
Owner
  • Award Id
    9761543
  • Award Effective Date
    1/1/1998 - 27 years ago
  • Award Expiration Date
    6/30/1998 - 26 years ago
  • Award Amount
    $ 100,000.00
  • Award Instrument
    Standard Grant

SBIR Phase I: Nonporous Zirconia for Ultrafast Analytical Chromatography

*** 9761543 McNeff This Small Business Innovation Research Phase I project will test the feasibility of synthesizing monodisperse, nonporous zirconia microspheres for use as high performance liquid chromatography (HPLC) supports for the analysis of environmentally-impactive substances. Current HPLC supports limit speed and resolution in the analysis of herbicides and pesticides, and require large amounts of solvent, because they are porous and cannot tolerate high temperature. Nonporous zirconia, coated by CVD with carbon, will overcome these problems. These zirconia microspheres (ca. 1 micrometer in diameter) will be synthesized using zirconium alkoxides and zirconium salts. The primary objective is to provide nonporous monodisperse spherical zirconia particles to produce ultrafast chromatography columns, but the particle synthesis work will also benefit other industries e.g. ceramic synthesis and catalysis. The primary commercial benefit of this research will be the reduction of organic solvent used in reversed-phase chromatographic separations of environmentally impactive substances. ***

  • Program Officer
    Joseph E. Hennessey
  • Min Amd Letter Date
    12/11/1997 - 27 years ago
  • Max Amd Letter Date
    12/11/1997 - 27 years ago
  • ARRA Amount

Institutions

  • Name
    ZirChrom Separations, Inc.
  • City
    Anoka
  • State
    MN
  • Country
    United States
  • Address
    617 Pierce Street
  • Postal Code
    553031601
  • Phone Number
    7634215264

Investigators

  • First Name
    Clayton
  • Last Name
    McNeff
  • Email Address
    mcnef002@tc.umn.edu
  • Start Date
    12/11/1997 12:00:00 AM