Patent Grant
9532856
This invention relates to screws, particularly those used in the dental implant field to attach secondary components, such as abutments, to a dental implant.
Dental implants are used to replace individual teeth or for anchoring more complex structures, which generally replace several or even all of the teeth.
Implants are often constructed in two parts, in which case they consist of an anchoring part, often referred to in isolation as the implant, and of a separate abutment. The anchoring part is either embedded completely in the bone, that is to say to the height of the alveolar crest, or protrudes by a few millimeters from the alveolar crest into the soft tissue. The abutment is mounted on the anchoring part and extends into the oral cavity to form a support for a dental prosthesis or denture.
During the lifetime of the prosthesis, which can be over 20 years, the implant system will be subjected to large loads caused by mastication. The abutment must therefore be firmly fastened to the implant in order to prevent loosening and potential loss of the component. This can be achieved in numerous ways, for example, via compression fit or gluing. However, screw fit connections are generally preferred. By applying a sufficiently high torque during attachment a firm connection between the implant and abutment can be achieved.
In many systems therefore the implant comprises an internal threaded bore, while the abutment comprises a corresponding apical thread, thus allowing the abutment to be screwed directly into the implant.
However, this has the disadvantage that the exact angular position of the abutment relative to the implant is not known until final fixation. This can have disadvantages, particularly when the abutment is intended to support a single tooth prosthesis.
Therefore, many implant systems comprise anti-rotation means, which prevent relative rotation between the implant and abutment and which set a finite number of angular positions which the abutment can have relative to the implant.
These anti-rotation means consist of complementary non-circular symmetric portions in the implant and abutment, usually having a polygonal shape such as a hexagon or octagon.
Such systems ensure that the exact angular position of the abutment in relation to the implant is known prior to fixation and can help to prevent loosening of the abutment during the lifetime of the implant.
Of course, when such anti-rotation means are employed it is not possible to rotate the abutment relative to the implant and hence the abutment can no longer be directly screwed into the implant. Therefore a third component, often a screw known as a “basal screw”, is used to connect the abutment to the implant.
When a basal screw is used the abutment typically comprises a screw channel extending through the abutment and having a screw seat. This enables the basal screw to be fed through the abutment until the screw head abuts the screw seat and for a screwdriver to be inserted into the channel to engage the screw and fasten this to the internal threaded bore of the implant, thus clamping the abutment securely to the implant.
An example of such a known implant system can be found for instance in EP1679049, in which the screw seat is conical and WO2006/012273, in which the screw seat is planar.
As well as abutments, basal screws are also used to connect other, temporary secondary components to the implant, for example, healing caps, closure screws and impression posts.
As mentioned above, it is important that the abutment in particular is firmly fastened to the implant in order to prevent loosening over the lifetime of the implant system. In the case of screw fit systems, this is achieved by tightening the screw component, whether this is a third component or the abutment itself, in order to achieve a high pre-load, or clamping force.
In order to achieve the maximum pre-load, it is desirable to tighten the screw as much as possible without reaching the yield strength of the screw. At this point, the tension within the screw body can result in plastic deformation of the threads and in some cases fracturing of the screw. This is highly undesirable as the screw must then be removed and replaced. Removal of a damaged screw is not always easy and furthermore this can result in damage to the internal threads of the implant. In some cases, the damage to the screw may not become apparent until after the final prosthesis has been fixed to the abutment, and hence the replacement of the screw can also result in the need for the creation of a new prosthesis.
Manufacturers of dental implant systems therefore set recommended maximum torque values, which ensure a high pre-loading of the screw without risking over tensioning.
However, given the natural desire to ensure a high pre-loading of the implant system, dental practitioners often apply a fastening torque significantly over the recommended value, which can lead to failure of the screw.
In order to increase the tensional strength of screws to prevent breakage in such situations, one potential solution would be to manufacture the screws from a different, stronger material. However, given the long term use of the screw within the human body any new material must undergo rigorous safety tests, and finding a new material having the necessary high strength together with the required biocompatibility is not a simple matter.
Another option would be to increase the dimensions of the screw. However, in dental implant systems space is restricted as the implant must fit within the available space within the jaw bone whilst removing as little bone mass as possible, to limit trauma at the implant site. Therefore the overall dimensions of the implant system can not be altered, and so any increase in the diameter of the screw would result in an equivalent reduction in the thickness of the implant and/or abutment. Such a modification would simply weaken the system in another area.
It is therefore an object of at least a preferred embodiment of the present invention to provide a screw component having a design which enables this to withstand a higher amount of torque without requiring a change of material or overall dimensions.
In accordance with one aspect the present invention provides a fastening system comprising a screw component and a seating component. The screw component comprises a shaft extending along a longitudinal axis and having a maximum radius R1, said shaft comprising a threaded section, said screw component further comprising, at one end of the screw shaft, a head, the head comprising a bottom end having a larger maximum radius R2 than the screw shaft such that an exposed underside of the screw head extends radially beyond the maximum radius of the screw shaft. The seating component comprises a screw channel comprising a planar screw seat having a minimum radius R3 which is equal to or greater than R1. The bottom end of the screw head comprises an annular contact surface for abutment against said screw seat, the contact surface being formed by the distal end of at least one downwardly extending protrusion on the underside of the screw head, wherein the annular contact surface has a minimum radius greater than the minimum radius of the screw seat.
In the present context the “bottom” of the screw component is considered to be the distal end of the screw shaft, i.e. the opposing end of the screw shaft to the screw head. The bottom end of the head is therefore the end of the head closest to the screw shaft and a downwardly extending protrusion is one that protrudes towards the bottom of the screw.
In accordance with conventional dental terminology, “apical” refers to the direction towards the bone and “coronal” to the direction towards the teeth. Therefore the apical part of a component is the part which, in use, is directed towards the jaw bone and the coronal part is that which is directed towards the oral cavity. When the screw component of the present invention is a dental screw component therefore, the bottom end of the screw head can also be considered as the apical end and the one or more protrusions as apically extending.
According to the present invention, the annular contact surface of the screw head is located at a radial location remote from the outer radius of the screw shaft. In other words, at the axial location of the annular contact surface a gap exists between the minimum radius of the contact surface and the radially inner part of the screw head. This is achieved by providing, on the underside of the screw head, one or more protrusions which extend in the downward direction to create the annular contact surface. The gap created between the inner portion of the screw head and the annular contact surface is great enough that the annular contact surface has a larger minimum radius than the minimum radius of the screw seat.
As the minimum radius of the contact surface is greater than the minimum radius of the screw seat, the innermost area of the screw seat will not be in contact with the screw head during use.
When tightening a screw only some of the applied torque is translated into pre-load. The overall torque which must be applied to the screw is significantly higher, as a large amount of torque is used to overcome the friction acting on the screw head and threads. In general it is estimated that only approximately 10-15% of the applied torque is used to tighten the screw.
In prior art screw systems the underside of the screw head is shaped to complement the screw seat. Therefore, when the screw seat is planar the underside of the screw is also planar. Thus, a large contact surface is formed. In effect, the entire underside of the screw head acts as an annular contact surface. In contrast, in the present invention, the at least one downwardly extending protrusion creates a smaller contact surface as only a part of the underside of the screw head forms the contact surface. The protrusion has the effect that not all of the radially overlapping areas of the screw head and screw seat are in contact with one another. As the annular contact surface has a minimum radius greater than the minimum radius of the screw seat, this has a larger friction radius than is achieved when using a traditional flat screw head, which also contacts the inner part of the screw seat. Consequently, the torque required to overcome the friction on the screw head is increased and hence reduces the percentage of torque translated into pre-loading force.
Therefore, a user who exceeds the recommended maximum torque limit is less likely to damage the screw as more of the applied torque is “absorbed” by the frictional resistance of the screw head.
In most systems, the minimum radius of the screw seat is equal to the maximum radius of the screw shaft, taking into account manufacturing tolerances. This provides the narrowest screw channel possible below the screw seat which can still accommodate the screw shaft. Consequently, traditional flat head screws comprise a planar underside that extends outwards from R1.
Therefore, viewed from another aspect the present invention provides a screw component comprising a shaft extending along a longitudinal axis and having a maximum radius R1, said shaft comprising a threaded section, said screw component further comprising, at one end of the screw shaft, a head, said head comprising a bottom end having a larger maximum radius R2 than the screw shaft such that an exposed underside of the screw head extends radially beyond the maximum radius of the screw shaft, said bottom end comprising an annular contact surface for abutment against a planar screw seat, the contact surface being formed by the distal end of at least one downwardly extending protrusion on the underside of the screw, said contact surface having a minimum radius greater than the maximum radius of the screw shaft.
Preferred features of both aspects of the invention are described below.
The annular contact surface can be formed by a plurality of protrusions, such that the contact surface is discontinuous, or “broken”. When the underside of the screw head comprises multiple protrusions, the distal ends of these may be at different radial locations. For example, the distance from the longitudinal axis to the protrusions may alternate from protrusion to protrusion. In such embodiments the minimum radius of the annular contact surface is set by the distal end of the protrusion(s) closest to the longitudinal axis.
However, preferably the distal ends of the plurality of protrusions are an equal distance from the longitudinal axis. In addition, although the protrusions may have differing shapes, it is preferred that these are identical, or at least that the shape of their distal ends are identical.
Preferably however the annular contact surface is formed by a single protrusion extending 360° about the longitudinal axis. Preferably this annular contact surface has a uniform inner radius, although it is possible for the annular contact surface to have an irregular, e.g. undulating, shape. Preferably the annular contact surface is uniform about the longitudinal axis, i.e. the minimum and maximum radii are both uniform. As the contact surface is intended to abut, in use, the planar screw seat, the annular contact surface lies in a plane perpendicular to the longitudinal axis.
The provision of a contact surface having a uniform inner radius enables the greatest friction radius to be achieved. The “friction radius” is the mean radius of the contact surface. This is the surface which in use contacts the screw seat and hence the greater this radius the greater the torque required to overcome the frictional resistance under the screw head.
Traditional methods of increasing the friction radius include widening the screw head and/or increasing the minimum radius of the screw seat. However, as discussed above, in certain systems, such as dental implant systems, where space is restricted, such increases are not possible or would lead to unacceptable weakening of the components clamped by the screw.
The present invention provides an alternative way of increasing the friction radius which does not require any loss of volume from the surrounding components. Instead, this can be achieved through a relatively minor modification to the underside of the screw head.
In principle it is preferable for the annular contact surface to be as narrow as possible and have a minimum radius that is as large as possible, in order to maximise the friction radius. For this reason it is also preferred that the maximum radius of the annular contact surface is equal to the maximum radius of the bottom end of the screw head. In a preferred embodiment the maximum radius of the annular contact surface is equal to the outer radius of the screw head. However, in practice manufacturing and other concerns must also be taken into account.
For example, the screw seat can be located at the end of the screw channel, such that the screw seat is formed on an exterior surface of the seating component. However, in many cases, the screw seat will be located within the screw channel. In such cases the screw channel is formed of at least two sections, a first section, having a first diameter, and a second section having a second, smaller diameter, wherein the screw seat is formed by the transition between these two diameters. In some components this transition may happen gradually, leading to a conical screw seat. However, this invention is only concerned with planar screw seats, where at least a part of the transition between the first and second diameters happens as a step change. At the transition between the wall of the first screw channel section and the screw seat a small radius is often formed, due to the manufacturing methods used to create this channel. When the screw head has an outer radius which is approximately equal to the diameter of the first screw channel section, an annular contact surface located at the radial edge of the screw head may not sit correctly on the screw seat and may further not be capable of smooth rotation.
In addition, depending on the function of the screw component, the head may taper radially outwards from the bottom end, such that the maximum radius of the screw head is significantly greater than the screw seat radius and hence the contact surface radius.
Therefore, alternatively the location of the contact surface can be defined in relation to the underside of the screw head or the minimum radius of the screw seat.
It is preferable for the annular contact surface to be located in the outer half of the underside of the screw head. More preferably the annular contact surface is located within the outer 75% of the underside of the screw head, and even more preferably in the outer 80%. In the context of the present invention the underside of the screw head is defined as the surface which extends radially beyond the outer boundary of the screw shaft to the maximum radius of the bottom end of the screw (R2−R1).
Preferably the minimum radius of the annular contact surface is at least 20% greater than the minimum radius of the screw seat, more preferably 25% greater. Preferably the contact surface is located within a range of 125-150% of the minimum radius of the screw seat. In a particularly preferred embodiment the contact surface is located within a range of 128-140% of the minimum radius of the screw seat.
Preferably, in use, at least the inner 50% of the surface area of the screw seat is not contacted by the annular contact surface.
The above ratios provide a suitable inner area of uncontacted screw seat in order to provide an effective increase in the friction radius, without requiring any increase in the overall diameter of the screw head or screw seat.
As discussed above, in many embodiments the minimum radius of the screw seat is approximately equal to the maximum radius of the screw shaft.
Consequently, in a preferred embodiment the minimum radius of the annular contact surface is at least 20% greater than the maximum radius of the screw shaft, more preferably 30% greater. Preferably the contact surface is located within a range of 125-150% of the maximum radius of the screw shaft. In a particularly preferred embodiment the contact surface is located within a range of 130-140% of the maximum radius of the screw shaft.
In the field of dental implants, in which the screw component has very small dimensions in order to fit within the implant, the maximum radius of the screw shaft, R1, is preferably between 0.6 and 1 mm and the maximum radius of the bottom end of the screw head R2 is preferably between 1.2 to 1.5 times R1. A particularly preferred range for R2 is 0.8-1.3 mm.
As mentioned above, it is desirable for the annular contact surface to be narrow, and therefore in some embodiments the distal end(s) of the protrusion(s) may be pointed or curved in shape. Upon tightening of the screw head against the screw seat, such a narrow contact surface would be deformed and flattened against the screw seat. This ensures a very close contact between the two surfaces and is particularly beneficial when the surface of the screw seat is rough or uneven. In many cases however it is preferable that the one or more protrusion comprises a flat distal end. This is easier to manufacture and reduces the risk of injury to the user. Preferably the contact surface has a radial width of 10-20% of the maximum screw shaft radius and/or 10-20% of the minimum screw seat radius.
In the field of dental implants, the contact surface has a width of preferably between 0.05-0.15 mm. Preferably the difference between the maximum radius of the screw shaft and the minimum radius of the annular contact surface is between 0.2 and 0.4 mm.
The at least one protrusion can be formed such that this extends downwardly at approximately right angles from the underside of the screw head. However, preferably the one or more protrusion is tapered at least on its radially inner side.
Such a taper brings a further advantage to the present invention. As the screw is tightened against the screw seat the tapered protrusion flexes slightly in the upward, or coronal, direction.
This is particularly beneficial in 3-part systems, such as when a separate screw component is used to attach a dental abutment to an implant. Over time and with use, it is common for the abutment to settle slightly into the implant. In prior art systems this results in the screw seat sinking away from the screw head and hence in a reduction in the friction between the components. This is evidenced by the removal torque necessary to unscrew the screw after use or dynamic testing, which is always significantly less than the initial insertion torque used.
It has been surprisingly found however, that in addition to increasing the maximum torque which can be withstood by the screw during insertion, the screw design of this preferred embodiment also increases the removal torque. This is considered to be due to the above mentioned flexing of the screw head. This enables the screw head to act as a spring and, as the abutment sinks during use, the screw head unflexes and lowers with the abutment such that a greater degree of contact is maintained between the screw seat and screw head. This therefore increases the removal torque required to unscrew the screw and thus increases the security of the connection.
Preferably the radially inner side of the one or more protrusion tapers downwards at an angle of between 15 and 25°, most preferably 20°. Preferably the taper is at least partially, preferably fully, curved over a radius. When the taper is only partially curved this curvature should preferably be located at the proximal end of the protrusion.
The axial location of the bottom end of the screw head is defined by the annular contact surface, which in accordance with the present invention is radially separated from the inner part of the screw head by a gap. The radially inner part of the bottom end of the screw head joins to the screw shaft. This part of the screw head can have a radius equal to R1, or in some cases greater than R1, as long as this is less than the minimum radius of the screw seat.
Preferably the screw comprises an undercut at the transition between the screw shaft and the screw head, such that the taper of the protrusion starts radially inwards of R1. This enables the tapered protrusion to have a longer radial length, which in turn increases the spring effect. When the taper is curved over a radius this curve preferably continues into and forms at least a part of the undercut.
The undercut can be located within the screw shaft or screw head or both. In a preferred embodiment undercut is at least partially located in the screw shaft such that the upper end of the screw shaft has a radius less than R1. This increases the tolerance between the screw shaft and the screw seat edge.
The provision of a tapered protrusion on the screw head is considered inventive in its own right and therefore, viewed from another aspect the present invention provides a fastening system comprising a screw component and a seating component. The screw component comprises a shaft extending along a longitudinal axis and having a maximum radius R1, said shaft comprising a threaded section, said screw component further comprising, at one end of the screw shaft, a head, said head comprising a bottom end having a larger maximum radius R2 than the screw shaft such that an exposed underside of the screw head extends radially beyond the maximum radius of the screw shaft. The seating component comprises a screw channel comprising a planar screw seat having a minimum radius R3 equal to or greater than R1. The bottom end of the screw head comprises an annular contact surface for abutment against this screw seat, the annular contact surface being formed by the distal end of at least one downwardly extending protrusion on the underside of the screw head, wherein said at least one downwardly extending protrusion is tapered at least on its radially inner side.
Preferably the minimum radius of the contact surface is greater than the minimum radius of the screw seat. The screw component in accordance with this aspect may additionally or alternatively have any or all of the preferred features discussed herein.
It has been found that, using a screw component in accordance with the present invention the maximum torque that can be withstood by the screw component can be increased up to 10%.
In accordance with the present invention therefore, the incidence rate of screw failure can be reduced without needing to make external dimensional or material alterations to the system. No alterations to the shape or volume of the clamped components, such as the implant and abutment, are required. Preferably the screw component is integrally formed.
The screw and seating components of the present invention can be used in any technological field in which standard flat head screws are used. The invention is particularly beneficial in systems in which there is limited ability to alter the external dimensions of the clamped components, such as dental implant systems. Therefore, preferably the screw component is a dental screw component. This can be, for example, a secondary dental component, such as a dental abutment, for direct attachment to a dental implant or other dental component. Preferably however the screw component is a dental screw arranged to attach one dental component, e.g. an abutment or other secondary component, to another, e.g. implant. The dental screw could also be used to attach, for example, a prosthesis to an abutment.
For the avoidance of doubt, a dental screw is an element which is used to clamp one component to another. It therefore can be seen as a “third component” of the system. The dental screw does not itself perform any function in the dental implant system other than to attach another component to the system via clamping. In contrast, when the screw component of the present invention is a secondary dental component, this performs an additional function once attached to the implant. For example, an abutment provides a support structure for the prosthesis while a healing cap seals the implant during osseointegration and assists in shaping the gingiva around the implant. A prosthesis provides a temporary or permanent replacement to a natural tooth or teeth.
In one preferred embodiment the screw component comprises a dental secondary component, such as an abutment and the seating component comprises a dental implant. In this embodiment the screw channel is formed by an interior bore in the implant. The planar screw seat may be formed within this bore or may be formed by the coronal end face of the implant, i.e. at the coronal end of the screw channel.
In another preferred embodiment the seating component comprises a dental secondary component and the screw component is a dental screw for securing the secondary component to an implant. In such embodiments the screw seat is usually located within the screw channel, which runs through the secondary component. The secondary component can be, for example, a dental abutment or an impression post.
Preferred embodiments of the invention shall now be described, by way of example only, with reference to the accompanying drawings, in which:
The bottom, or apical, end of head 4 has a larger maximum radius R2 than the maximum radius R1 of the shaft 2. This results in an annular contact surface being formed by the underside 8 of the screw head 4. As the abutment or other component with which the screw engages must comprise a screw channel dimensioned to allow passage of the screw shaft 2 the maximum contact area possible between the screw head 4 and screw seat is π(R22−R12).
It is worth noting that the maximum radius R2 of the bottom end is less than the overall maximum radius of the screw head 4. This is because a bevelled surface 9 links the bottom end to the outer circumference of the screw head 4. This improves the fit of the screw 1 within the screw channel, as will be demonstrated later.
Despite this bevel, underside 8 provides a relatively large surface area with which the head 4 can contact the screw seat of the abutment or other secondary component. Further, this surface area extends from the maximum radius R1 of the screw shaft 2 outwards.
In contrast to the prior art, the underside 18 of screw head 14 is not planar but instead comprises a downwardly extending protrusion 17. This protrusion 17 tapers downwards to a flat distal surface, which defines the bottom, or apical, end 15 of the screw head 14. The taper is formed on the radially outer side by bevelled surface 19 and on the radially inner side by a concave surface.
The shape of the underside 18 results in the creation of an annular contact surface having a width less than R2−R1 and which is located towards the outer radius of the screw head 14. This shape of screw head increases the friction radius of the screw and hence increases the torque required in order to overcome the frictional resistance of the screw head.
This is demonstrated with reference to
Abutment 20 is seated in an internal bore 31 of implant 30. The bore is shaped to snugly accommodate the abutment 20 and comprises a threaded section 33.
In order to connect the abutment 20 to the implant 30 screw 1 is passed through screw channel 21 until the threaded section 3 of the screw 1 can engage with the threaded section 33 of the implant. By tightening screw 1 the head 4 is forced down onto the screw seat 22 and clamps the abutment 20 within the implant 30.
The bevelled edge 9 of screw head 4 prevents any interference with the curved transition area of the screw channel 21. The planar surface of the underside 8 creates a broad contact region C1 between the screw head 4 and screw seat 22. The friction radius of the system shown in
When torque is applied to the screw 1 via the hollow 6 (not shown in
Significantly, no contact between the surfaces exists at the radially innermost area of the screw seat 22 because the contact surface of the screw head has a greater minimum radius than the minimum radius R3 of the screw seat 22. This radius is similar to that of the maximum radius R1 of the screw shaft 12, as the screw shaft 12 must be able to pass through the screw seat 22 into the apical part of the screw channel 21.
The lack of contact at the radially inner area of the screw seat 22 increases the friction radius RF2 of the system and consequently the torque needed to overcome the frictional resistance under the screw head 14. By using a screw in accordance with the present invention therefore a smaller percentage of the applied torque will be used to tension the screw body and hence the screw 10 can withstand more torque before over tensioning occurs.
Protrusion 17 is located as close to the outer radial edge of the screw head 14 as possible, in order to increase the friction radius RF2. In addition the distal surface of protrusion 17 is made as narrow as possible.
The protrusion 17 of the screw 10, shown in
In order to increase the length of this taper, the screw 10 comprises an undercut 11 at the transition from the screw shaft 12 to the screw head 14. This increases the spring effect of the protrusion 17 and in addition increases the tolerance between the screw head 14 and screw seat 22. In this embodiment it is the curve of the taper which continues into and forms a part of the undercut 11.
Comparative tests have been run on screws having the designs shown in
It is also possible for the contact surface to be formed by a plurality of protrusions. This is shown in
The invention has mainly been described above in relation to a separate screw component, which can be used to connect a secondary component such as an abutment to an implant. However, it is also possible for the secondary component itself to form the screw component of the present invention. When it is not necessary to know with certainty the exact angular position of the component with respect to the implant the secondary component is often directly screwed into the implant. This direct connection is common for example, when the implant is intended for supporting a bridge, i.e. a single prosthesis which replaces multiple teeth. In such situations the bridge is attached to two or more implants and the angular orientation of the bridge is thus defined by these multiple connection points. Other secondary components, such as healing caps, which are only used on a temporary basis and do not support a prosthesis, may also be directly screwed to the implant.
The bottom or apical end the head 94 has a larger radius than the shaft 92, such that an underside 98 is created. The underside 98 comprises an apically extending protrusion 97 which extends 360° about the longitudinal axis of the component such that an annular contact surface is formed. The detail circled in
The above described embodiments are for illustrative purposes only and the skilled man will realize that many alternative arrangements are possible which fall within the scope of the claims.
Where technical features mentioned in any claim are followed by reference signs, those reference signs have been included just for the sole purpose of increasing intelligibility of the claims and accordingly, such reference signs do not have any limiting effect on the scope of each element identified by way of example by such reference signs.
| Number | Date | Country | Kind |
|---|---|---|---|
| 10016023 | Dec 2010 | EP | regional |
This application is a division of U.S. Ser. No. 13/304,552, entitled Screw Head, filed 25 Nov. 2011 which claims priority to European Application No. 10 016 023.3, filed 23 Dec. 2010.
| Number | Name | Date | Kind |
|---|---|---|---|
| 4154138 | Melone | May 1979 | A |
| 5527183 | O'Brien | Jun 1996 | A |
| 6332778 | Choung | Dec 2001 | B1 |
| 8226408 | Grant | Jul 2012 | B2 |
| 20040043360 | Obata | Mar 2004 | A1 |
| 20050042573 | Lustig et al. | Feb 2005 | A1 |
| 20060216672 | Dinkelacker | Sep 2006 | A1 |
| 20080039837 | Gambale et al. | Feb 2008 | A1 |
| Number | Date | Country |
|---|---|---|
| 1054409 | May 1979 | CA |
| 102008009547 | Aug 2009 | DE |
| 1679049 | Dec 2006 | EP |
| 2006012273 | Feb 2006 | WO |
| 2008110575 | Sep 2008 | WO |
| Entry |
|---|
| European Search Report in corresponding application EP 10016023. |
| Number | Date | Country | |
|---|---|---|---|
| 20150305837 A1 | Oct 2015 | US |
| Number | Date | Country | |
|---|---|---|---|
| Parent | 13304552 | Nov 2011 | US |
| Child | 14795249 | US |
