Claims
- 1. A method for sintering a powdered metal preform, comprising:
sintering the preform within a first sintering temperature range for a predetermined time period, wherein the preform shrinks; and sintering the preform within a second sintering temperature range for a predetermined time period, wherein the maximum desired density of the preform is obtained at the second sintering temperature range.
- 2. The method of claim 1 wherein the preform has a weight greater than about 250 grams.
- 3. The method of claim 1 wherein the preform has a weight greater than about 300 grams.
- 4. The method of claim 1, wherein the preform has a weight greater than about 1000 grams.
- 5. The method of claim 1, wherein the bore has a diameter greater than about 8 cm.
- 6. The method of claim 1, wherein the bore has a diameter greater than about 5 cm.
- 7. The method of claim 1, wherein the bore has a diameter greater than about 3.8 cm.
- 8. The method of claim 1, wherein the preform has at least two cylindrical bores.
- 9. The method of claim 1, wherein one of the at least two cylindrical bores is larger than another of the at least two cylindrical bores.
- 10. The method of claim 1 wherein the preform is an Inconel 718 powdered metal preform.
- 11. The method of claim 10 wherein the first sintering temperature range is about 1100° C. to about 1240° C.
- 12. The method of claim 11 wherein the second sintering temperature range is about 1280° C.±5° C.
- 13. The method of claim 1, wherein sintering within the first temperature range continues until interparticulate melting of the preform occurs to fix the shape of the preform.
- 14. The method of claim 1 wherein the preform achieves about 60% to about 80% of its maximum density at the first sintering temperature range.
- 15. A sintering tool assembly for supporting a metal injection molded preform with a surface defining an internal passage, the tool assembly comprising:
a support structure: a rod structure having a first end and a second end, the ends of the rod structure mounted on the support structure; wherein the rod structure is located in the passage and supports the preform.
- 16. A sintering tool assembly for supporting a metal injection molded preform with a surface defining an internal passage, the tool assembly comprising:
an insert located in the passage, the insert having at least one surface of predetermined shape; a support structure; a rod structure having a first end and a second end, the ends of the rod structure mounted on the support structure; wherein the rod structure supports the insert; and wherein at least a portion of the surface of predetermined shape of the insert contacts at least a portion of the surface defining the internal passage of the preform to support the preform.
- 17. The sintering tool assembly of claim 16, wherein the rod structure and insert are made of aluminum oxide ceramic.
- 18. The sintering tool assembly of claim 16, wherein the insert is a cylinder having a diameter greater than about 8 cm.
- 19. The sintering tool assembly of claim 16, wherein the insert is a cylinder having a diameter greater than about 5 cm.
- 20. The sintering tool assembly of claim 16, wherein the insert is a cylinder having a diameter greater than about 3.8 cm.
- 21. The sintering tools of claim 16, wherein the support structure includes a pair of blocks and the insert is supported between the pair of blocks.
- 22. The sintering tools of claim 21, wherein each of the pair of blocks has a V-notch and the ends of the rod structure are mounted in the V-notch on respective ones of the pair of blocks.
- 23. The sintering tools of claim 21, wherein each of the pair of blocks is made of firebrick.
- 24. The sintering tools of claim 16, wherein the surface of predetermined shape is a circular circumferential surface.
- 25. The sintering tools of claim 16, wherein the rod structure is a rod that extends through a bore in the insert.
- 26. The method for sintering a powdered metal flowbody, comprising:
providing a flowbody having one or more small cylindrical features and one or more large cylindrical features; sintering the flowbody within a first sintering temperature range for a predetermined time period, wherein the flowbody shrinks; and sintering the flowbody within a second sintering temperature range for a predetermined time period, wherein the maximum desired density of the flowbody is obtained at the second sintering temperature range.
- 27. The method of claim 26, further comprising:
providing a first set of generally cylindrical sintering tools for maintaining the geometry of the small cylindrical features of the flowbody during sintering at the first sintering temperature; providing a second set of generally cylindrical sintering tools for maintaining the geometry of the large cylindrical features of the flowbody during sintering at the second sintering temperature;
- 28. The method of claim 27, wherein the first set of sintering tools comprises a rod and one or more cylinders, wherein the cylinders have a throughbore for slidable receipt of the rod.
- 29. The method of claim 28, wherein the second set of sintering tools comprises a rod and one or more cylinders, wherein the cylinders have a throughbore for slidable receipt of the rod.
- 30. The method of claim 29, wherein the diameter of each cylinder in the second set of one or more cylinders is greater than the diameter of any cylinder in the first set of one or more cylinders.
- 31. The method of claim 26, wherein the sintering tools are made from aluminum oxide ceramic.
- 32. The method of claim 26, wherein the flowbody has a weight greater than about 250 grams.
- 33. The method of claim 26, wherein the flowbody has a weight greater than about 300 grams.
- 34. The method of claim 26 wherein the flowbody has a weight greater than about 1000 grams.
- 35. The method of claim 26, wherein the flowbody is a cylinder having a diameter greater than about 8 cm.
- 36. The method of claim 26, wherein the flowbody is a cylinder having a diameter greater than about 5 cm.
- 37. The method of claim 26, wherein the flowbody is a cylinder having a diameter greater than about 3.8 cm.
- 38. A method for drying a metal preform in preparation for sintering, where the preform is made from a composition comprising powdered metal and a binder, the method comprising the steps of:
drying the preform in a sealed container; drying the preform in a vented container; vaporizing water from the preform by heating the preform at predetermined temperature for a predetermined period of time; and vaporizing binder from the preform by heating the preform to a predetermined temperature for a predetermined period of time.
- 39. The method of claim 38, wherein the preform is dried in the sealed container for a period of about two to three days.
- 40. The method of claim 38, wherein the preform is dried in the vented container for a period of about two to three days.
- 41. The method of claim 38, wherein water is vaporized from the preform by heating the preform at a temperature of 60° C.±5° C. for a period of 24 hours.
- 42. The method of claim 38, wherein binder is vaporized from the preform by heating the preform at a temperature of 275° C.±5° C. for a period of two hours.
- 43. The method of claim 38 further comprising the steps of:
sintering the preform at a first predetermined temperature for a predetermined time period; and sintering the preform at a second predetermined temperature for a predetermined time period.
- 44. A method for processing an Inconel 718 preform where the preform is made from a composition comprising powder metal, water and a binder, the method comprising the steps of:
drying the preform in a sealed container; drying the preform in a vented container; vaporizing water from the preform by baking the preform at predetermined temperature for a predetermined period of time; vaporizing binder from the preform by heating the preform to a predetermined temperature for a predetermined period of time; sintering the preform at a first sintering temperature within a range of about 1100° C. to about 1240° C. for a predetermined time period, wherein inter-particulate melting occurs on the surface of the preform to fix the shape of the preform; and sintering the preform at a second sintering temperature within a range of about 1280° C.±5° C. for a predetermined time period, wherein the preform achieves 98-99% of its maximum desired density at the second sintering temperature.
- 45. The method of claim 44, wherein the preform has a weight greater than about 1000 grams.
- 46. The method of claim 44, wherein the preform is a cylinder having a diameter greater than about 8 cm.
- 47. A sintered flowbody having at least one cylindrical bore, wherein the flowbody has a weight greater than about 250 grams.
- 48. The flowbody of claim 47, wherein the flowbody is made of Inconel 718.
- 49. The flowbody of claim 47, wherein the flowbody has a weight greater than about 300 grams.
- 50. The flowbody of claim 47, wherein the flowbody has a weight greater than about 1000 grams.
- 51. The flowbody of claim 47, wherein the bore has a diameter greater than about 8 cm.
- 52. The flowbody of claim 47, wherein the bore has a diameter greater than about 5 cm.
- 53. The flowbody of claim 47, wherein the bore has a diameter greater than about 3.8 cm.
- 54. The flowbody of claim 47, wherein the flowbody has at least two cylindrical bores.
- 55. The flowbody of claim 54, wherein one of the at least two cylindrical bores is larger than another of the at least two cylindrical bores.
- 56. The flowbody of claim 47, wherein the flowbody has a surface roughness of less than about 30 micro inches.
- 57. An Inconel 718 flowbody having a first pair of cylindrical bores and a second pair of cylindrical bores, wherein the second pair of cylindrical bores is larger in diameter than the first pair of bores, and wherein the density of the flowbody is at least 98% of the density of wrought Inconel 718 alloy.
CROSS-REFERENCE TO RELATED APPLICATION(S)
[0001] This application claims priority to provisional application No. 60/291,054, filed May 14, 2001 and to provisional application No. 60/290,853, filed May 14, 2001.
Provisional Applications (2)
|
Number |
Date |
Country |
|
60291054 |
May 2001 |
US |
|
60290853 |
May 2001 |
US |