Patent Application
20230141016
The present disclosure relates generally to directed energy deposition, a class of additive manufacturing technology, and, more specifically, to a system and method of directed energy deposition using a sound field.
In the field of advanced manufacturing, and in particular additive manufacturing, the building and repair of components or parts is a well-known process. One method that is used in the building/repairing of parts is via directed energy deposition. In this approach, the part is made or repaired by depositing material on the surface of the part being built/repaired. The material being deposited can be in the form of a powder or wire. As the material is being deposited, energy is added locally to the newly deposited material to melt it and attach it to the part being built/repaired.
There have been different directed energy deposition approaches that have been used in the past. U.S. Pat. No. 9,908,288B2 describes a part being fabricated by an additive manufacturing process while levitating in space. The features of the part are formed by additive manufacturing. The part levitation system allows the spatial orientation of the part to be manipulated relative to one or more material deposition subsystems (print heads). US Patent Publication No. 2016/0228991A1 describes a method and system of generating at least one ultrasonic standing wave between at least one set of opposing ultrasonic transducers. Metal-containing particles are deposited on a node located within the ultrasonic standing wave such that the particles are trapped in the node, positioning a surface of a substrate close to the node, melting the particles with an energy beam to form a melt pool in contact with the surface, and allowing the melt pool to cool and solidify into a metal deposit bound to the surface. US Patent Publication No. 2016/0318129A1 describes a system and method for the additive manufacturing of an object using multiple lasers. The system includes a first laser generating a first focused laser beam having a first surface area where the first focused laser beam is directed onto a first quantity of a powder material on a substrate to fuse particles of the powder material in a first layer of the substrate. A second laser generating a second focused laser beam having a second surface area where the second laser beam is directed onto a second quantity of the powder material on the substrate to fuse particles of the powder material in the first layer of the substrate. The first surface area of the first focused laser beam is greater than the second surface area of the second focused laser beam. However, each of these prior art solutions has disadvantages.
Therefore, herein is provided a novel method and system for directed energy deposition.
The disclosure is directed at a system and method of directed energy deposition using a sound field. In one embodiment, the sound field changes the characteristics of a particle stream as it passes through the sound field. Characteristics include, but are not limited to, the cross-sectional size (spatial focusing) of the particle stream, the shape of the particle stream, and the path of the particle, or powder, stream.
In one aspect of the disclosure, there is provided a method of directed energy deposition including generating a sound field; passing a particle stream through or by the sound field towards a part being fabricated; and melting the particle stream as it contacts the part being fabricated; wherein the sound field controls at least one characteristic of the particle stream as it passes through the sound field and contacts the part being fabricated.
In another aspect, the method further includes, before generating a sound field, generating the particle stream. In a further aspect, generating the particle stream includes transporting material from a material feed system to a material nozzle; and directing the material into the particle stream towards the part being fabricated. In yet another aspect, transporting material from the material feed system to the material nozzle is via a pressurized gas system.
In yet another aspect, generating a sound field includes determining desired characteristics of the particle stream; calculating the sound field required to achieve the desired characteristics; and transmitting signals to sound sources to generate the sound field. In an aspect, calculating the sound field includes calculating the sound field using an iterative backpropagation methodology, analytic phase hologram solutions, or numerical optimization of signal amplitude and/or phases of sound sources. In a further aspect, calculating the sound field using an iterative backpropagation methodology includes calculating the sound field using a Gor′kov methodology.
In another aspect, generating the sound field includes generating at least one sound period averaged pressure intensity isosurface. In a further aspect, the method further includes coating the particle stream with a gaseous or liquid medium before passing the particle stream through of by the sound field. In yet another aspect, the at least one characteristic includes a particle stream cross-sectional particle concentration distribution; a cross-sectional size of the particle stream; a shape of the particle stream or a path of the particle stream.
In another aspect of the disclosure, there is provided a system for directed energy deposition including at least one nozzle for directing a particle stream at a part; at least one energy source for melting the particle stream; and at least one sound source for generating a sound field which the particle stream passes through, the sound field controlling characteristics of the particle stream before it contacts the part.
In a further aspect, the system further includes a processor for calculating and generating the sound field. In yet another aspect, the system further includes at least one sound field modification component for generating the sound field. In another aspect, the system further includes a material feed system for supplying material, in the form of the particle stream, to and through the at least one nozzle. In another aspect, the material may be one of a metal, a metal alloy, a metal filler, a metal-containing flux material, a dopant, a ceramic, a composite, a polymer or any combination thereof.
In yet a further aspect, generating a sound field includes generating isosurfaces for controlling the particle stream as the particle stream passes through or by the isosurfaces.
Embodiments of the present disclosure will now be described, by way of example only, with reference to the attached Figures.
The disclosure is directed at a method and system for directed energy deposition. In one embodiment, the system of the disclosure includes at least one nozzle for directing material (such as in the form of a particle stream) towards a part and at least one energy source for melting the material to form a melt pool. In one embodiment, energy source melts the particle stream as it comes into contact with the part. The system further includes a set of sound generating components that generate a sound field which the particle stream passes through, the sound field affecting certain characteristics of the particle stream to control the certain characteristics of the particle stream.
In a directed energy deposition process, as material and energy are added to the part or component, certain characteristics of the part, such as, but not limited to, the part geometry, surface roughness and material properties such as mechanical properties and microstructure, may be affected or controlled by the melt pool. The part geometry and roughness may be determined by the resolution of the directed energy deposition system, which depends on the size of the melt pool. The mechanical properties and microstructure of the part depend on the changes in cooling rates between the material being deposited and the rest of the part which is partially affected by the shape of the melt pool.
Turning to
The at least one nozzle 102 is connected to a material feed system 110, which provides the particles or material that is directed at the part 106 by the nozzle 102. In other words, the material feed system supplies the material needed to fabricate or repair the part 106. In one embodiment, the material may be in the form of a powder, wire or material particles. The powder may be a polymer, metal, metal alloy, metal filler, metal-containing flux material, dopant, ceramic, or composite material or any suitable element or any combination thereof.
In one embodiment, the material particles are accelerated by the material feed system 110 to and through the nozzle 102 using a gas flow and/or gravitational force, although other methods of transmitting or transporting the material from the material feed system 110 to the nozzle 102 are contemplated. In this embodiment, the part resolution and surface roughness may be controlled or determined by the nozzle design and dimensions. The material feed system 110 may further provide a shielding gas that surrounds the particle stream to assist in particle or particle stream focusing and to reduce the likelihood or prevent chemical reactions between the particle stream (or powder) and atmosphere. In one embodiment, this produces a particle stream with a fixed distance and direction from the nozzle to a location of low, or minimum particle stream cross-section width (particle focus point) and a fixed particle stream cross-section shape. The cross-sectional size and shape of the particle stream refer to a cross-sectional shape of the particle stream, normal to the particle stream path. In some embodiments, the cross-sectional shape may be defined with respect to the powder concentration distribution which may be described by a Gaussian function that has an infinite extent whereby the cross-section may be defined the radius of the particle stream where a threshold value is chosen to drop the edges of the powder concentration distribution function. As discussed below, due to interaction with a sound field, the cross-sectional particle concentration distribution and its corresponding cross-sectional size and shape at some particular particle concentration threshold value can be adjusted.
The system 100 further includes energy sources 112 that supply energy beams 114 to melt the material when it contacts the part 106, in the form of melt pools 116. The term ‘energy beam’ used in this disclosure is used in a general sense to describe a narrow, propagating stream of energy particles and/or packets of energy which may include a light beam, a laser beam, an electron beam, a particle beam, a charged-particle beam, a molecular beam, etc., which upon contact with a material imparts kinetic (thermal) energy to the material. These melt pools 116, at different times within the part build, or directed energy deposition process, may be stationary or moving with respect to the part 106.
As can be seen in
As the particle stream 104 (or streams such as in
The use herein of the term ‘sound period averaged pressure intensity isosurface,’ or any reference to isosurface or isosurfaces refers to the three-dimensional (3D) surface or surfaces formed by points of a constant value within a volume of space, where the value being considered herein is the averaged instantaneous acoustic pressure of the sound field over a period of time equal to the sound wave's period in the sound field. Acoustic pressure may be seen as the local pressure deviation from the ambient (average or equilibrium) atmospheric pressure caused by a sound field. The amount of time used to calculate this averaging may be different than the sound wave's period, for example when using two or more sound fields in a sequence that are then repeated in time, in which case the time used for the averaging will be the repetition time. The description of the sound fields in terms of these isosurfaces aids in the understanding and design of the directed energy deposition system described herein. In some embodiments, the sound period averaged pressure intensity isosurfaces may have values that may range from 2 to 20 kPa (kilopascals).
As taught below, along with controlling the characteristics of the particle stream, right before it contacts the part 106, a path of the particle streams 104 from the nozzle 102 to the melt pools 116 may also be modified or controlled by the sound field.
Although only a single particle stream (and nozzle) is shown with respect to
The sound sources 118 and energy sources 112 (resulting in motion of the energy beams 114) may move and rotate in space while manufacturing the part 106 in order to more accurately control or shape the particle stream.
As is understood, different laser and nozzle/powder stream arrangements produce different particle stream/sound force field interactions, and therefore, different positioning of the sound sources, the energy sources, and particle stream nozzles are contemplated that are not all disclosed or shown in the disclosure.
Turning to
In this embodiment, by strategically positioning the sound sources, the sound field may be focused. When the sound field is focused, the intensity of the sound field changes and the amplitude increases. The time averaged sound intensity (amplitude value) pressure, when it is focused at one point, generates the isosurface and as the particle stream passes by or through the isosurface (depending on the shape of the isosurface), the particles repel from the isosurface. This property of the relationship between the particle stream and the sound field allows a changing of the isosurface shape, in real-time, to change or control the characteristics of the particle stream as it passes through the sound field, which contains isosurfaces. For example, by generating an “isosurface wall” in the path between the nozzle and the part, the particle stream may be re-directed in another direction. Alternatively, a hollow cylinder isosurface may be generated that causes the particle stream to narrow as is passes through the isosurface.
As can be seen in
Another example embodiment of a directed energy deposition system is shown in
In use, the particle streams pass through the sound field (and through or by sound period averaged pressure intensity isosurfaces 124) and contact the part 106 at the same melt pool location whereby the energy beam 114 from a single energy source 112 creates a melt pool 116 between the two particle streams and the part 106 to add the material from the two particle streams to the part 106.
Another embodiment of a directed energy deposition system is shown in
As seen from the above embodiments, the number of energy sources and energy beams, the number of nozzles producing particle streams and the number of sound sources can vary in the directed energy deposition system and may be selected based on the desired application of the directed energy deposition system or a desired number of melt pools or based on the characteristics of the particle stream that are desired to be controlled.
Turning to
In operation, the robot arm 500 may control the position of the components of the end effector 502 of the directed energy deposition system. This may be done as a single control where all of the components of the end effector move together or the components (seen as the material nozzle or nozzles, the sound sources, the build plate, the energy sources and the like) may be individually controlled by the robot arm 500.
For
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In
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As schematically shown in
In one embodiment, to determine the input signals needed to be applied to the sound sources to achieve the required sound field, the calculations may be performed by numerically minimizing the weighted period averaged sound intensity at a desired spatial point minus the axis component weighted Laplacian of the Gor′kov potential of a sound field that will give different sound fields that may produce a sound radiation field pointing towards the desired spatial point from any direction. The negative of gradient of the Gor′kov potential yields the sound radiation force. The variables that are required for this optimization problem are the phases of the sound sources, which are used to compute the Gor′kov potential via a numerical and/or analytic model of the sound fields for each sound source which depends on the sound source phases. By adjusting the weights of each component of the Laplacian and the weight in front of the period averaged sound intensity, one can obtain different useful sound fields such as a vortex sound field which for acoustic levitation is referred to as a vortex trap.
In another embodiment, some analytic solutions for signals for the sound sources to generate a required sound field may be used, such as, but not limited to, vortex sound fields with different topological charges. This sound field may be required to have wider vortex sound field isosurface, for example, the isosurface 124 shown in
In another embodiment, another method of calculating the input signals for the sound sources to generate the desired sound field or sound fields may be performed by using an iterative backpropagation methodology or algorithm to find the phases of the sound sources. This methodology may be used to find the required sound source phases when designing holographic acoustic tweezers. This methodology uses a modified version of the iterative angular spectrum approach, which is based on the Gerchberg-Saxton algorithm used to generate holographic optical tweezers. An example of this iterative backpropagation algorithm being applied to levitate multiple particles is disclosed in A. Marzo and B. W. Drinkwater, “Holographic acoustic tweezers,” PNAS, vol. 116, no. 1, pp. 84-89, January 2019, doi: 10.1073/pnas.1813047115.
Turning to
In the current embodiment, this may be achieved by using the sound sources to generate a pair of disconnected sound period averaged pressure intensity isosurfaces 800 and 802 with two different sound focus points along an axis 804 of a particle stream 806 (
When using this switching method, similar to pulse width modulation in electric motor control, the sound fields can have different or equal sound focus point locations. Sound fields that could be used are a vortex and a twin sound field, for example. The twin sound field produces approximately two cylindrical isosurfaces of sound period averaged pressure intensity 800 and 802 that focus particles along only one direction perpendicular to the particle stream axis. Any combination thereof of the previously described techniques applicable to the sound sources may be combined to focus, move sideways and change the particle focus cross-sectional size and shape or any combination thereof at the same time.
Another embodiment of a directed energy deposition system is shown in
In the current embodiment, the set of material nozzles 902 are stationary with respect to the part 106 while the energy sources 904 may be moving or may be stationary with respect to the part 106. Other components may be used to then direct the energy beams if the energy sources are also stationary. In one embodiment, if the energy sources are lasers, movement of the laser beam energy sources may be accomplished by, but not limited to, a galvanometer or a moving reflector. As with previous embodiments, as the particle stream passes through the sound field, characteristics of the particle stream are controlled by the sound field to, for example, spatially modify the particle stream to have a desired cross-sectional area and/or shape before reaching the melt pools 116.
In one application of the current embodiment, the sound field may be designed so that the particle stream follows a specific path from the material nozzle 902 to the part 106.
In another application of the current embodiment, the sound field may be designed such that the material nozzles 902 can have different powder sources with different material compositions, and the powder streams can be quickly changed to switch the material going to one of the melt pools 116, to allow for the fabrication of functionally graded materials.
Turning to
One embodiment of generating a sound field is shown in
Turning back to
During experiments, a relationship to determine or calculate a particle stream deflection angle was derived using the following assumptions: (1) the force towards the sound field axis crossing the sound focus point decreases linearly to zero; which is an appropriate assumption if a vortex sound field is being used and the approximate cross-sectional radius of the particle stream is less than a quarter of the sound wavelength; and (2) the carrier gas and the particles have a low relative velocity, i.e. negligible particle gas drag.
The derived relationship indicates that the degree of deflection and focusing is higher if the particles in the particle stream are moving slower and/or are less dense. Also, the approximate particle displacement for equally dense particles and for a wide particle size range is independent of particle size, meaning a high degree of focusing is possible even if using a powder with a wide particle size distribution. Other methods such as electromagnetic particle deflection have a dependence on the particle size. Another relation that was realized was the focal length of the particle stream, i.e. at what distance do the particles reach the particle stream axis. From this relation it was found that the focal length is very weakly dependent on the particle's initial normal offset from the particle stream axis (if assumption one is applicable), meaning all the particles have approximately a common focal point such as in an optical or electron lens.
In an alternative embodiment, where the energy source is a laser, the laser energy beam should provide a local addition of power to the material being added to the part being fabricated. In order to control this additional power, the laser beam may be moved and rotated in space using a galvanometer or by moving the energy source via the robotic arm such as schematically shown in
In one embodiment, although the system is able to operate by using sound source input signals ignoring reflections and/or refractions from the part and/or system enclosure, a fewer number of sound sources and/or a reduction of their power consumption might be achievable if the signals going to the sound sources i.e. the required phases are calculated taking into account these reflections and/or refractions. This may be calculated (when the desired sound field is calculated) for reflections either taking one sound reflection instance into account or taking into account an infinite number of sound reflections. An infinite amount of reflections does not happen physically but this assumption simplifies the calculation while being able to more accurately approximate a large number of reflections which is closer to what is happening physically.
A calculation method to find the required signals taking one sound reflection into account can be carried out by combining a modified matrix method with the Gor′kov potential equation to simulate the pressure and potential field generated by all the sound sources. In the traditional matrix method, the radiation surface of each transducer is discretized in small surface elements. For this calculation method an analytical expression for the acoustic pressure generated by the sound sources using the far-field approximation may be used. This modified matrix method may be used to calculate more than one reflection however it may be very computationally expensive. An example of the calculation taking into account one reflection being used for transporting and merging liquid dropplets in mid-air is described in M. A. B. Andrade, T. S. A. Camargo, and A. Marzo, “Automatic contactless injection, transportation, merging, and ejection of droplets with a multifocal point acoustic levitator,” Review of Scientific Instruments, vol. 89, no. 12, p. 125105, December 2018, doi: 10.1063/1.5063715.
A calculation method to find the required signals taking an infinite amount of reflections into account can be carried out by simulating the sound field using the boundary element method for solving the Helmholtz equation and directly solving a constrained optimization problem to obtain the required phases. This can be shown to reduce to an eigendecomposition. An example of the calculation taking into account an infinite number of reflections for ultrasound directed self-assembly to organize particles dispersed in a fluid medium into a desired three-dimensional user-specified pattern is described in M. Prisbrey, J. Greenhall, F. Guevara Vasquez, and B. Raeymaekers, “Ultrasound directed self-assembly of three-dimensional user-specified patterns of particles in a fluid medium,” Journal of Applied Physics, vol. 121, no. 1, p. 014302, January 2017, doi: 10.1063/1.4973190.
Although the latter method is more accurate, it may be more computationally expensive. An even fewer number of sound sources or sound source power consumption may be achieved if this calculation is done taking into account the varying shape of the part while being manufactured and taking into account sound field modification components.
The operation of the system at very high sound intensities may produce observable distortions in the sound field due to non-linear sound propagation. These effects might be reduced either by using a certain gas at some temperature and pressure surrounding the directed energy deposition process and/or taking into account the physics of non-linear sound propagation when calculating the signals going to the sound sources.
The greater degree of freedom due to changing the degree of particle focusing independent of distance from the nozzle to the part allows for the possibility of a better cross-sectional particle concentration distribution at the particle stream for different melt pool sizes. This may be used together with the use of multiple energy beams that can rotate independently and/or have variable power output and focal lengths to produce a directed energy deposition system that can print at different resolutions while the part is being fabricated or repaired. By printing at finer voxel resolutions at the surface of the part and coarser voxel resolutions otherwise may also increase the system's part throughput. This print speed increase for the same surface resolution has been observed when the same variable voxel resolution is available in the two-photon polymerization additive manufacturing process. One example of this is shown in Y. Tan et al., “High-throughput multi-resolution three dimensional laser printing,” Phys. Scr., vol. 94, no. 1, p. 015501, November 2018, doi: 10.1088/1402-4896/aaec99.
In one embodiment, for the gas system that transports the material from the material feed system to and through the nozzle towards the part, the gas may be an Ar—He gas mix that can closely match air's acoustic impedance. Alternatively, the gas may be neon or any other gases whereby the gas or gas mixture closely matches the acoustic impedance of air. In another embodiment, the gas may be nitrogen. In a further embodiment, the system may include a transducer that can interact with the gas system to improve power transfer based on the gas and a required wavelength to better affect the particle stream. The presence of the transducers may facilitate calculation of the sound field to be generated based on parameters such as, but not limited to, orientation of transducers, location of transducers, density of gas, density of metal, speed of sound in both, frequency of sound and sound pressure field around transducer for a specific applied voltage.
Affecting the path of the particle stream in either of the systems shown in
In a further embodiment, the particle stream gas and shielding gas may be accelerated and/or directed via acoustic streaming phenomenon, where the sound field used to affect the particles in the particle stream, another sound field, or rapidly switching between the sound field used to affect the particles in the particle stream and another sound field may be used to also move a gas. A sound field that may be used for this may be an acoustic Bessel beam. An example where an acoustic Bessel beam generated from a phased array (multiple sound sources) is used to produce an electronically steerable long narrow air stream is described in K. Hasegawa, L. Qiu, A. Noda, S. Inoue, and H. Shinoda, “Electronically steerable ultrasound-driven long narrow air stream,” Appl. Phys. Lett., vol. 111, no. 6, p. 064104, August 2017, doi: 10.1063/1.4985159. Other sound fields besides an acoustic Bessel beam for more complex gas stream paths may also be used.
Thus, through experiments and/or simulations, it was shown that that the use of a sound field can be used to change the powder stream cross-sectional size and shape (spatial focusing) in order to produce a metal component at a faster rate and a higher resolution.
Faster part manufacture may be possible by quickly changing the powder stream cross-sectional size (degree of powder focusing) for many possible feature sizes and surface resolutions. The degree of focusing may be higher than a typical directed energy deposition nozzle for a wider range of particle mass feed rates. Fast changes in the degree of focusing may also allow for a more accurate material deposition when using different materials in the same part, which might produce different particle stream shapes when going through the same nozzle in a typical directed energy deposition machine. Switching materials while producing the same part is required to produce parts with functionally graded materials for example.
Doing this in a typical directed energy machine would require stopping the fabrication process many times while making a single component and switching between many different nozzles. The method herein may be considered solid-state, which may allow for higher reliability as well as faster part manufacture. Both the change of the powder stream cross-sectional size and shape may allow for the real-time feedback needed to control melt pool track geometry, microstructure properties such as metal grain morphology and phase formation, as well as controlling against porosity formation for example.
The method herein uses sound fields to affect the particle stream and does not use sound fields to affect the spatial location and orientation of the part being built. Using sound fields to move and rotate the part while it is being built would require a continuous accurate simulation and modification of the required sound field to account for the changing shape of the part and the recoil from the impacting particles for accurate material deposition.
Another advantage of the current disclosure is that the method and system of the disclosure uses sound to deflect the particle streams and does not require a given amount of particles to reach and/or levitate at the node at a particular spatial location in a standing wave field. This increases the density range of particles that may be used with this method i.e. full metal particles may be used instead of only metal-containing particles. Also, the sound field may or may not be a standing wave-field between at least one set of opposing sound sources (transducers). The method herein also may use a sound field with the highest sound period averaged pressure intensity volume away from the part being built, with the final smallest particle stream cross-sectional area being produced downstream of this volume. This is due to the particles being deflected and then focusing further due to their own inertia as illustrated for example in
In an alternative embodiment, the directed energy deposition system and method of the disclosure may be able to produce parts with functionally graded materials, by gradually changing from one material source to another while the nozzle is depositing material during the manufacture of a single part. This may be very useful in the aircraft and aerospace industries as well as the computer circuit industries, which require parts to withstand high-temperature gradients. An effective way of achieving this is with a functionally graded material composed of a ceramic and a metal for example.
In a further embodiment, the system and method of the disclosure may benefit from additional build control mechanisms to achieve particle focusing independently of the gas moving the particles from the feed system to and through the nozzle and the shielding gas, to control the distance and direction of the produced particle focus point and to change the cross-sectional size and shape of the particle stream at the particle focus point while the component is being manufactured.
In another embodiment, the system may be able to perform variable resolution printing. In this embodiment, the energy source may be a laser where the laser focus is adjustable so that the laser spot diameter can be changed, such as via, but not limited to, a liquid crystal lens. Other mechanical methods of manipulating the laser spot diameter are also contemplated.
In a further embodiment, the system may include a vision system, such as a camera vision system for more accurately aligning the energy beam and the powder stream, using the sound field to affect the powder or particle stream. The camera vision system may also be used to monitor the powder stream to provide feedback to the system whereby the sound focus point can be dynamically changed/updated by the system to adjust for unexpected variances.
In another embodiment, the system may optimize, or improve, both phase and voltage for vortex like fields with a force function normal to the particle stream axis, producing a different effective ‘lens’ diameters (similar to a vortex field) regardless of transducer produced sound wavelength. Furthermore, with a pulse width modulation (motor control) type of system, as described in
The above-described embodiments of the disclosure are intended to be examples of the present disclosure and alterations and modifications may be effected thereto, by those of skill in the art, without departing from the scope of the disclosure.
In this description, for purposes of explanation, numerous details are set forth in order to provide a thorough understanding of the embodiments. However, it will be apparent to one skilled in the art that these specific details may not be required. In other instances, well-known structures may be shown in block diagram form in order not to obscure the understanding. Further, elements of an embodiment may be used with other embodiments and/or substituted with elements from another embodiment as would be understood by one of skill in the art.
Applicants reserve the right to pursue any embodiments or sub-embodiments disclosed in this application; to claim any part, portion, element and/or combination thereof of the disclosed embodiments, including the right to disclaim any part, portion, element and/or combination thereof of the disclosed embodiments; or to replace any part, portion, element and/or combination thereof of the disclosed embodiments.
The above-described embodiments are intended to be examples only. Alterations, modifications and variations can be effected to the particular embodiments by those of skill in the art without departing from the scope, which is defined solely by the claims appended hereto.
The disclosure claims priority from U.S. Provisional Application No. 62/991,299 filed Mar. 18, 2020, the contents of which are hereby incorporated by reference.
| Filing Document | Filing Date | Country | Kind |
|---|---|---|---|
| PCT/CA2021/050358 | 3/18/2021 | WO |
| Number | Date | Country | |
|---|---|---|---|
| 62991299 | Mar 2020 | US |
