The present invention generally relates to generating tunable electromagnetic waves using carbon nanotube-based field emitters.
X-ray computed tomography (X-ray CT) refers to a non-destructive inspection technique that generally involves irradiating a target with X-rays to produce three-dimensional representations of the scanned target. Typically, the target is irradiated with the X-rays, and the response (e.g. backscatter or transmission through the target) is detected, characterized, and thereby used in analyzing the structure of the target.
Systems and methods in accordance with embodiments of the invention generate tunable electromagnetic waves using carbon nanotube-based field emitters. In one embodiment, a CNT-based irradiator includes: at least one CNT-based cathode, itself including: a plurality of carbon nanotubes adjoined to a substrate; a plurality of anodic regions; where each anodic region is configured to emit a distinctly different class of photons in a direction away from the at least one cathode in response to a same reception of electrons; where each of the plurality of anodic regions is operable to receive electrons emitted from at least one of said at least one CNT-based cathode; and where each of the at least one CNT-based cathode and the plurality of anodic regions are disposed within a vacuum encasing.
In another embodiment, at least one of the plurality of anodic regions includes one of: Copper, Cobalt, Molybdenum, Tungsten, Palladium, Tantalum, Platinum, and Gold.
In yet another embodiment, each of the plurality of anodic regions is configured to emit a distinctly different class of photons corresponding with the X-ray portion of the electromagnetic spectrum in a direction away from the at least one cathode in response to a same reception of electrons.
In still yet another embodiment, each of the distinctly different classes of photons are distinctly different as measured by the respective characteristic Kα lines.
In a further embodiment, the plurality of carbon nanotubes are in the form of bundles of carbon nanotubes that are between approximately 1 μm and approximately 2 μm in diameter and that are spaced apart at a distance of approximately 5 μm.
In a still further embodiment, the plurality of anodic regions define a contiguous anode.
In a yet further embodiment, the contiguous anode is rotatable such that each of the plurality of anodic regions can be placed within the line of sight of at least one of said at least one CNT-based cathode.
In a still yet further embodiment, the plurality of anodic regions define a contiguous circular anode.
In another embodiment, the plurality of anodic regions define quadrants within the contiguous circular anode.
In yet another embodiment, the plurality of anodic regions define a pyramidal shape.
In still another embodiment, a CNT-based irradiator further includes: a first gate electrode configured to accelerate electrons emitted from at least one of said at least one CNT-based cathode; and a second gate electrode configured to focus electrons emitted from at least one of said at least one CNT-based cathode relative to at least one of the plurality of anodic regions.
In still yet another embodiment, a CNT-based irradiator further includes a beam steering device operable to steer electrons emitted from at least one of said at least one CNT-based cathode towards a selected one of the plurality anodic regions in a first mode and a selected different one of the plurality of anodic regions in a second mode.
In a further embodiment, the beam steering device is in the form of focusing coils.
In a yet further embodiment, the at least one CNT-based cathode is at least two CNT-based cathodes.
In a still further embodiment, each of the CNT-based cathodes is independently operable such that a first CNT-based cathode can be operating to emit electrons while a second CNT-based cathode is not emitting electrons.
In a still yet further embodiment, each of at least two CNT-based cathodes is operable to simultaneously emit electrons towards a different respective one of the plurality of anodic regions.
In another embodiment, the anodic regions are configured such that each of at least two anodic regions can emit a distinctly different class of photons in a same general direction in response to the reception of electrons.
In still another embodiment, at least one anodic region is operable to emit a distinctly different class of photons causing the propagation of electromagnetic waves in a planar manner 360° outside of the vacuum encasing.
In yet another embodiment, a CNT-based irradiator includes: at least one CNT-based cathode, itself including: a plurality of carbon nanotubes adjoined to a substrate; at least one anodic region comprising an alloy and thereby configured to generate multispectral output in response to the reception of electrons; where at least one of the at least one anodic region is operable to receive electrons emitted from at least one of the at least one CNT-based cathode; where the at least one CNT-based cathode and the at least one anodic region are disposed within a vacuum encasing.
In still yet another embodiment, the at least one anodic region is operable to emit distinctly different classes of photons corresponding with the X-ray portion of the electromagnetic spectrum as determined by respective characteristic Kα lines.
Turning now to the drawings, systems and methods for generating tunable electromagnetic waves using carbon nanotube-based field emitters are illustrated. As can be appreciated, X-ray CT techniques have widespread applications. For example, such techniques can find use in: medical imaging, nondestructive materials analyses, and reverse engineering. Importantly, they can also be used in the context of geological exploration and excavation (including in the context of extraterrestrial planetary subsurface geological formation analysis). Such geological survey information can be particularly useful in the oil and gas industry. Indeed, the conventional notion of “Logging While Drilling” references acquiring respective geological formation information while boring into the Earth (e.g. to establish an oil well). For instance, such geological formation information can include: formation density, porosity, permeability, and low-resolution indirect images of the surrounding formation. In some instances, to provide high-resolution information concerning a respective geological formation, Caesium-137 has been used to implement compositional analysis; specifically, Caesium-137 can emit gamma rays and thereby provide compositional analysis. However, Caesium-137 is radioactive, and this generally undesirable characteristic can limit its real-world viability. In many instances, it is desirable to be able to provide tomography and other structural analysis without having to rely on radioactive components.
Carbon nanotubes (CNTs) have many exceptional properties that make them attractive for a variety of applications. For instance, CNTs are amongst the strongest materials, as measured by tensile strength, and amongst the stiffest materials, as measured by elastic modulus. Additionally, CNTs have also been determined to possess outstanding electrical ‘field emission’ properties, with high emission currents at low electric field strengths (e.g., applied field from 1-3 V/μm and an emission current ˜0.1 mA from a single nanotube, as measured in conventional configurations). For context, field electron emission generally regards the emission of electrons, e.g. from a solid surface into a vacuum, based on the influence of an electric field. Field electron emission is relied on in a number of applications including microscopy, spectroscopy, and display technology. In any case, CNTs have demonstrated viability as cold-cathode field emission sources, especially for applications requiring high current densities (e.g. hundreds to thousands of amperes per cm2) and lightweight packages (high frequency vacuum tube sources).
Indeed, in U.S. patent application Ser. No. 11/137,725 (issued as U.S. Pat. No. 7,834,530—the “530 patent”), Manohara et al. disclose particular configurations for a high density carbon nanotube-based field emitter that provide favorable performance characteristics. For example, Manohara et al. disclose that field emitters that include a plurality of bundles of CNTs disposed on a substrate, where the diameter of the bundles is between approximately 1 μm and approximately 2 μm, and where the bundles of CNTs are spaced at a distance of approximately 5 μm from one another, demonstrate particularly advantageous performance characteristics. The '530 patent is hereby incorporated by reference in its entirety, especially as it pertains to the aforementioned configurations.
Nonetheless, even though CNT-based field emitters have been proposed and developed, in many instances, these field emitters have been deficient in some respects. For example, in many previous instances, the CNTs were not sufficiently bonded to the underlying substrate. For instance, in many cases, when the field emitters were subject to an electric field during operation, the electric field would cause at least some of the carbon nanotubes to detach from the substrate. In some instances, it was determined that pressures as light as between approximately 20 kPa and approximately 60 kPa were sufficient to detach CNTs from the underlying substrate. Thus, gently rubbing the surface of the substrate of these field emitters with a Q-tip could have been sufficient to dislodge CNTs from the substrate. This fragility can be problematic. For example, the field emission performance of the field emitter can degrade as a function of the number of detached CNTs. Moreover, detached CNTs can potentially short circuit associated circuitry. In essence, the weak bond between CNTs and associated substrates of these CNT-based field emitters can undermine their potential to serve as robust field emitters that can withstand rigorous operating conditions. To address this issue, in U.S. patent application Ser. No. 14/081,932 (issued as U.S. Pat. No. 9,064,667—“the '667 patent”), Manohara et al. disclose particular methods for better adhering CNTs to a respective underlying substrate. For example, the '667 patent discloses heating the substrate so as to soften it and thereby allow a plurality of the CNTs to become at least partially enveloped by the softened substrate. The disclosure of the '667 patent is hereby incorporated by reference in its entirety, especially as it regards methods enabling the substrate to envelop at least a portion of a plurality of CNTs.
Against this backdrop, many embodiments of the invention utilize CNT-based field emitters to generate tunable electromagnetic waves, e.g. that can be used to implement radiography. In many embodiments, a CNT-based field emitter is implemented in conjunction with a selectable metallic anodic region; the emission of electrons towards a selected anodic region can result in the generation of electromagnetic waves. Importantly, by modulating the potential difference applied to cause CNT field emission and causing electrons to be emitted towards a particular metallic anodic region, electromagnetic waves of a desired frequency range (e.g. X-rays), intensity, and characteristic values can be achieved. As can be appreciated, such ‘irradiators’ can be used in conjunction with detection devices to achieve radiography. In this way, versatile non-radioactive irradiators can be achieved. CNT-based radiography techniques are now described in greater detail below.
In many embodiments of the invention, irradiators that include CNT-based field emitters are implemented; such ‘CNT-based irradiators’ can be implemented in radiography. Within the context of the instant application, an Irradiator′ can generally be understood to be a source of electromagnetic energy, e.g. it can radiate electromagnetic waves. For purposes of context,
Importantly, any suitable CNT-based field emitter can be implemented in accordance with embodiments of the invention. For example, any of the CNT-based field emitters described in the '530 patent and/or the '667 patent can be implemented in accordance with embodiments of the invention. Thus, for instance
Accordingly, the anodic regions 206 can comprise any suitable combination of materials in accordance with embodiments of the invention. In many embodiments, the anodic material that the electrons are ‘aimed’ toward is selectable such that the corresponding electromagnetic spectrum can be adjusted. For instance, in many embodiments, the anode includes portions made from discretely different elements associated with discretely different emission spectra, and the orientation of the CNT-based cathode and the anode can be adjusted such that the electrons can be emitted toward a desired one of the discrete elements. For example, where the anodic regions correspond with the emission of X-ray spectra, the distinctly different emission spectra can be characterized by discretely different characteristic Kα lines. Since the discretely different elements are associated with discretely different emission spectra, the irradiator can be tuned by ‘aiming’ the CNT cathode towards a respective desired element.
Table 1 below lists data relating to X-ray source spectra plots for various metallic anodic regions that can be implemented in accordance with embodiments of the invention.
In particular, Table 1 lists the Kα levels associated with anodes made from various materials, as well as an applied potential difference that can result in the stated Kα level.
Nevertheless, it is seen that CNT-based irradiators that can radiate tunable electromagnetic waves can be implemented. Various structures for such irradiators are now described.
In many embodiments of the invention, tunable CNT-based irradiators are implemented. As can be appreciated from the above discussion, such irradiators can be implemented for the purposes of tomography and/or elemental composition analysis. Importantly, these tunable CNT-based irradiators can be implemented in any of a variety of configurations in accordance with embodiments of the invention. In many embodiments, an irradiator includes a CNT cathode and a plurality of anodic regions that are all disposed within a vacuum sealed enclosure. As mentioned previously, the potential difference applied to cause field emission as well as the anodic region that the electrons are directed towards can be modulated to control the emission spectra. In many embodiments, the irradiator further includes gates that can augment the operation of the irradiator.
The plurality of anodic regions can be realized in any of a variety of ways in accordance with embodiments of the invention. For example, in many embodiments of the invention, the anodic regions are contiguous with one-another, with each anodic region being characterized by discretely different emission spectra. The irradiator is configured such that the electrons emitted from the CNT-based cathode can be targeted towards one of the desired anodic regions; in this way the resulting emission spectra can be controlled. This can be achieved using any of a variety of configurations in accordance with embodiments of the invention. For example, in some embodiments, the anodic regions are contiguous and define a circular face, with each anodic region defining a different surface area—e.g. a quadrant—within the circular face. Moreover, the ‘circular face’ is capable of being rotated such that each quadrant can be positioned within the line of sight of the emitted electrons.
The illustrated gates 608, 610 can be used to facilitate the operation of the irradiator. For example, in many embodiments, the gates embody focusing and accelerating devices to focus and accelerate the emitted electrons toward the respective anodic region. For example, in some embodiments, the first gate 608 defines a focusing grid, while the second gate 610 defines an accelerating grid. In general, gates can be used in any suitable way to facilitate the operation of irradiators in many embodiments of the invention.
As can be appreciated, the circular face can be angled so as to ‘aim’ the direction of the reflected/emitted photons. The irradiator 602 further includes an actuating wheel 606 that can be used to rotate the circular face 605 such that it can be determined which particular quadrant 604 of the circular face 605 is within the line of sight of the CNT-based cathode 612. In this way, the emission spectra can be controlled. Of course, it should be appreciated that while an anode having a circular face 605 divided into four quadrants 604 is depicted, the anodic regions 604 can be arranged in any suitable manner in accordance with embodiments of the invention. For example, the anodic regions 604 can define ‘slices’ of any suitable dimension in accordance with certain embodiments of the invention. Moreover, CNT-based irradiators can include any number of anodic regions in accordance with certain embodiments of the invention. Furthermore, the anodic regions do not necessarily have to define a contiguous shape—they can be arranged in any suitable way.
In many embodiments, electrons are emitted towards particular regions of the anode without relying on the repositioning of the anodic regions. For instance, in many embodiments, magnetic steering of the electrons emitted from the cathode is implemented to direct the emitted electrons toward a particular anodic region. Thus for example,
While certain examples of tunable CNT-based irradiator configurations have been given, it should be clear that tunable CNT-based irradiators can be implemented in any of a variety of ways in accordance with embodiments of the invention. For example, in some embodiments, the anodic regions define a pyramidal shape, with each pyramidal face being characterized by a different emission spectra; the pyramidal shape can be rotated to augment which of its faces is in the line of sight of the emitted electrons. Thus, for example,
While CNT-based irradiators including a single CNT-based cathode have been depicted, in many embodiments, CNT-based irradiators include a plurality of CNT-based cathodes. This can allow for the simultaneous emission of electromagnetic waves defined by distinctly different characteristics. Thus, for example,
In some embodiments, each of a plurality of CNT-based cathodes within an irradiator can be individually powered. In this way, greater control can be exercised over the respective CNT-based irradiator. Thus, for example,
While the above descriptions have regarded CNT-based irradiators that emit electromagnetic spectra defined by different characteristics in different directions, in many embodiments, CNT-based irradiators can be configured to emit electromagnetic spectra having different characteristics in a same direction. Thus, for instance,
For reference,
Of course, it can be understood that the various details of the described CNT-based irradiators can be implemented in any of a variety of ways in accordance with embodiments of the invention. For example, the described structures can adopt any suitable height and diameter. In many embodiments, the irradiators have a height of approximately 2.5 inches. In a number of embodiments, the irradiators can have a diameter of approximately 1 inch. However, it should be appreciated that the disclosed irradiators can conform to any suitable length scale in accordance with embodiments of the invention. Similarly, the described irradiators can be made from any suitable materials. For instance, in some embodiments, the housing is made from stainless steel and Vespel® (a high dielectric plastic). In general, any suitable configuration that allows electrons emitted from a CNT-based cathode to be controllably directed toward a specific anodic region (each of a plurality of anodic regions corresponding with a different emission spectrum) can be implemented in accordance with embodiments of the invention.
Although the present invention has been described in certain specific aspects, many additional modifications and variations would be apparent to those skilled in the art. It is therefore to be understood that the present invention may be practiced otherwise than specifically described without departing from the scope and spirit of the present invention. Thus, embodiments of the present invention should be considered in all respects as illustrative and not restrictive. Accordingly, the scope of the invention should be determined not by the embodiments illustrated, but by the appended claims and their equivalents.
The current application claims priority to U.S. Provisional Application No. 62/181,894, filed Jun. 19, 2015, the disclosure of which is hereby incorporated by reference in its entirety.
The invention described herein was made in the performance of work under a NASA contract NNN12AA01C, and is subject to the provisions of Public Law 96-517 (35 USC 202) in which the Contractor has elected to retain title.
Number | Date | Country | |
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62181894 | Jun 2015 | US |