This invention relates in general to variable capacitance measuring devices, and more particularly, to variable capacitance measuring devices used as force or pressure sensors, components within the devices, and process for making them.
Many pressure sensors include a variable capacitor to determine pressure. Some of these pressure sensors include a fixed electrode as one capacitor electrode and a diaphragm as another capacitor electrode. The diaphragm deforms when is a pressure difference across it. This varying gap between the diaphragm and the fixed electrode results in different capacitance values for a capacitor as the pressure changes.
While the principles of a capacitive pressure sensor are relatively simple, external factors can distort the pressure readings. This is particularly true for sensors to measure pressures significantly lower than atmospheric pressure because of its high sensitivity. For example, temperature changes can affect the capacitance values.
One attempt to solve the temperature-induced problem uses a pair of fixed electrodes on one side of the diaphragm. From an electrical standpoint, the pressure sensor includes two capacitors connected in series. A layout of the two fixed electrodes built on an insulator, typically a ceramic disk, has a center electrode surrounded and spaced apart from an annular electrode. Additionally, ruby rollers may be used to support the ceramic disk in order to minimize the frictional forces between the parts in the pressure sensor as the temperature changes. The use of the two capacitors can be used to determine flow rate over a relatively larger range in temperatures by monitoring the difference in capacitance readings between the two capacitors between the diaphragm and each of the fixed electrodes.
The two-capacitor pressure sensor is not without problems. First, a trim operation is typically used to match the two the capacitances by changing the area for at least one of the relatively fixed electrodes. This operation tends to be a manual operation and involves some trial and error. Variations from pressure sensor to pressure sensor may occur. Although the ruby rollers or the like are able to improve temperature-induced hysteresis by minimizing “stick-slip” types of movements inside the sensors, the added complexity in design and manufacturing increases cost. Also, the contacts of ruby rollers and its supporting structures have stress concentrations and may adversely affect the long-term stability of the sensors. Because this pressure sensor uses the difference of the two capacitance readings to measure pressure, it needs a larger size diaphragm in order to gain enough sensitivity. Another problem is a long warm-up time, because the size and mass are relatively large, and the small ruby rollers or the like restrict the heat transfer. For example, it may take the pressure sensor one day to reach a steady-state temperature operating condition. Such a long warm-up is unacceptable to many manufacturing operations.
A variable capacitance measuring device can comprise any one or more features described in various embodiments to allow a reliable, compact device to be achieved. A capacitor electrode, a gettering housing, and pinch-off connector may be aligned along a common axis to reduce width dimensions without a substantial increase in length. By selecting materials that have coefficients of thermal expansion relatively close to one another, temperature-induced variations may be reduced. Substantially varying topologies for ceramic-metal interfaces may reduce the likelihood of external contaminants from reaching the evacuated portion of the device. A tube can be used between the capacitor portion and a gettering housing to isolate heat and stress between the getter housing and the sensor. Note that the present invention does not require all of the features described herein to be present within a single device. Embodiments also include processes for forming the devices or portions of them.
In one set of embodiments, a variable capacitance measuring device can comprise an electrode assembly and an insulating material. The insulating material may laterally surround the electrode assembly. The coefficient of thermal expansion of the insulating material can be within approximately 50% of the coefficient of thermal expansion of the electrode assembly.
In another embodiment, a variable capacitance measuring device can comprise an electrode, a housing adapted to hold a gettering material, and a pinch-off connector. The electrode, the housing, and the pinch-off connector may lie along a common axis.
Still another embodiment may include a component for a variable capacitance measuring device. The component can comprise a conductive portion, an electrode assembly, and an insulator. Each of the conductive portion and the electrode assembly can have a surface with a substantially varying topology. The insulator can contact the surfaces of the conductive portion and electrode assembly and electrically insulate the conductive portion from the electrode assembly.
Yet another embodiment may include a component for a variable capacitance measuring device. The component can comprise a main body portion, a housing adapted to hold a gettering material, and a tube lying between the main portion and the housing. The width of the tube can be less than the width of the housing.
In another set of embodiments, a process for using a variable capacitance measuring device can comprise applying a first signal to an electrode, a gettering housing, and a pinch-off connector; applying a second signal to a diaphragm; and measuring a capacitance of a capacitor that includes the electrode and the diaphragm. The electrode, the getter housing, and the pinch-off connector may lie along a common axis.
In still a further set of embodiments, a process for making a component for a variable capacitance measuring device can comprise holding an electrode assembly and a conductive portion in relatively stationary positions. The electrode assembly lies within a mold, and the conductive portion laterally surrounds and is spaced apart from the electrode assembly to form a spaced-apart region. The method can further comprise molding an insulating material to lie within the spaced-apart region.
The foregoing general description and the following detailed description are exemplary and explanatory only and are not restrictive of the invention, as defined in the appended claims.
The present invention is illustrated by way of example and not limitation in the accompanying figures.
Skilled artisans appreciate that elements in the figures are illustrated for simplicity and clarity and have not necessarily been drawn to scale. For example, the dimensions of some of the elements in the figures may be exaggerated relative to other elements to help to improve understanding of embodiments of the present invention.
Reference is now made in detail to the exemplary embodiments of the invention, examples of which are illustrated in the accompanying drawings. Wherever possible, the same reference numbers will be used throughout the drawings to refer to the same or like parts (elements).
A variable capacitance measuring device can comprise any one or more features described herein to allow a reliable, compact device to be achieved. In some embodiments, aligning a capacitor electrode, a gettering housing, and a pinch-off connector along approximately a common axis may reduce width dimensions without a substantial increase in length. The device is relatively smaller and reaches a steady-state temperature faster than prior capacitance sensors. In another set of embodiments, temperature-induced variations may be reduced by selecting materials for a capacitor portion of the sensor that have coefficients of thermal expansion relatively closer to one another. In still another set of embodiments, substantially varying topologies can be used for ceramic-metal interfaces to reduce the likelihood of air or other external contaminants from reaching the reference side of a diaphragm within the capacitor portion. In a further set of embodiments, a tube can be used between the capacitor portion of the device and the gettering housing to isolate heat and stress between the gettering housing and the sensor. Embodiments also include processes for forming the devices. The present invention is better understood after reading the descriptions of various embodiments that follow.
The electrode assembly 12 can include a housing 122, a tube 124, and a main body portion 126. The housing 122 can be adapted to hold a gettering material 106. The gettering material can be used to absorb or adsorb contaminants or outgassing that may remain on the reference side of the diaphragm 156 after the sensor 10 is sealed. In this specification, the reference side of the diaphragm 156 includes the portions of the pressure sensor 10 on the side of the diaphragm 156 closer to the top of the illustration in
The solids barrier 108 can lie along one side of the gettering material 106 to reduce the likelihood of particles from the gettering material 106 reaching the capacitor portion 14 of the pressure sensor 10. The solids barrier 108 may include a wire mesh screen, a sintered glass, a membrane, or the like. The solids barrier 108 may allow gas to flow through it but does not allow significantly large particles from gettering material 106 to enter the capacitor body 14.
The electrode assembly 12 can further include a tube 124 that lies between the housing 122 and the capacitor portion 14. The capacitor portion 14 may include the insulator 142 and a main body portion 126 of the electrode assembly 12. In addition, the wall of the tube 124 should be as thin as possible. The tube 124 may have a diameter (width) that is narrower than the diameter (width) of the housing 122. This tube 124 and its narrower diameter and thin wall help to reduce the amount of heat transferred to the capacitor portion 14 when the gettering material 106 is being activated at a high temperature. The tube 124 also reduces any external forces applied to the pinch-off connector 102 or the gettering housing 122 being transferred to the capacitor portion 14. When the capacitor portion 14 operates at an elevated temperature, the tube 124 helps to reduce the heat loss and protect electronics connected to the pinch off connector 102. The electrode assembly 12 may further include threads 128 along an inside portion of the main body portion 126. The threads 128 can be used to secure the electrode 154, which has complementary threads, to the electrode assembly 12. Other means for securing the electrode 154 to the electrode assembly 12 can include screws or bolts (separate from the electrode 154), rivets, welds, or the like.
The capacitor portion 14 can include an insulator 142, a reference-side ring 144, a process-side ring 147, weld preps 145, and a shell 146. Weld preps 145 help to retain welding heat to the joint and reduce the overall welding power, thus minimizing distortion to the parts. A capacitor housing 141 can include a combination of the reference-side ring 144 and the shell 146. Although not shown, the electrode 154 has an opening and a hollow shaft to allow for the evacuation of the reference side of the diaphragm 156. An optional shim 152 may lie between the electrode assembly 12 and the electrode 154 and be used to control the position of the electrode 154 relative to the diaphragm 156. The weld joint of rings 144, 147, and diaphragm 156 substantially prevents any fluids from flowing from the process side of the diaphragm 156 to the reference side of the diaphragm 156.
The process side of the diaphragm 156 can include a plasma shield 158 used to prevent potential damage to the sensor 10 if the sensor 10 is connected to a process using a plasma gas. A process tube 148 may be connected to the process side of the capacitor portion 14 and may be part of a flow measuring apparatus or as a stand-alone sensor for measuring force or pressure within a system. In one specific, non-limiting embodiment, the reference-side ring 144, the process-side ring 147, and the diaphragm 156 may be welded to each other as a subassembly. That subassembly may be welded to the shell 146 and using weld preps 145. In this embodiment, all metal-to-metal connections are welded.
The capacitor portion 14 can include a variable capacitor structure for the pressure sensor 10. A combination of the electrode 154, diaphragm 156, and the gap 150 between the electrode 154 and the diaphragm 156 can be the variable capacitor for pressure sensor 10. When the pressures on both sides of the diaphragm 156 are substantially the same, the distance between the electrode 154 and the diaphragm 156 may be in a range of approximately 50 to 250 microns.
In some embodiments, the pressure sensor 10 can be modified to be a differential pressure sensor. For example, the differential pressure sensor can be used in determining how much above or below atmospheric pressure a measured pressure is. The sensor 10 can be modified by removing the pinch-off connector 102, the retainer 104, and the gettering material 106. The solids barrier 108 may remain to substantially prevent particles from entering the capacitor portion 14. The reference side may be at substantially atmospheric pressure and the gas within the process tube 148 may be at a pressure above or below atmospheric pressure. In other embodiments, atmospheric pressure may be on the other side of the diaphragm 156. Electrical connections may be made to the tube 122 to provide a desired potential or other signal to the electrode 154. Another differential pressure sensing application is described later with respect to a mass flow controller.
Some of the physical features of the pressure sensor 10 are pointed out to note some of its advantages. First, the pressure sensor 10 has relatively smaller dimensions compared to a two-capacitor pressure sensor. The following dimensions are exemplary rather than limiting. Typically the width 162 of the pressure sensor 10 may be no greater than approximately 35 mm. The height of the capacitor portion 14, as illustrated by dimension to 164, may be no greater than approximately 20 mm, and the combined height of the housing 122 and the pinch-off connector 102 may be no greater than approximately 20 mm. In one specific embodiment, the width 162 is approximately 25 mm, and a combination of the dimensions 164 and 166 is approximately 30 mm. Therefore, a relatively smaller pressure sensor 10 can be made. The pressure sensor 10 may take less than approximately four hours to reach a steady-state temperature and may be less than approximately two hours in some situations. Compare this to the nearly 24 hours as seen with a conventional two-capacitor sensor. Compare this to the nearly 24 hours as commonly seen with a conventional two-capacitor sensor.
The electrode 154, the electrode assembly 12 (including the main body portion 126, the tube 124, and the housing 122), and the pinch off connector 102 can be centered about a common axis 100 as illustrated in FIG. 1. Aligning at least some of those items along the common axis 100 can allow the width of the pressure sensor 10 to be relatively narrower compared to a sensor where at least one of those items is aligned along a separate, substantially parallel axis.
Other than the flexing of the diaphragm 156, the sensor 10 has no moving parts. The sensor 10 is less likely to have mechanical failure or irreproducible readings due to failure or “stick-slip” movement of moving parts. Also, the sensor 10 does not have any rollers, such as ruby rollers. Therefore, the distortion and manufacturing complications associated with the rollers can be eliminated.
The materials used for the sensor 10 can be selected such that many of the materials within the capacitor portion 14 have coefficients of thermal expansion that are relatively the same. For example, each of the electrode assembly 12, the reference-side ring 144, the shell 146, the process-side ring 147, the process tube 148, the electrode 154, the diaphragm 156, and the plasma shield 158 may be made of the same material. If the pressure sensor 10 is used in a corrosive environment, that material can be iron-nickel alloys, by themselves, or include any one or more of copper, chromium, molybdenum, silicon, tungsten, or the like. Examples may include INCONEL™, INCOLOY™, MONEL™, HASTELLOY™, stainless steel, or the like. In one specific embodiment, INCONEL 718 can be used. Any or all of the electrode assembly 12, the reference-side ring 144, the shell 146, the process-side ring 147, the process tube 148, the electrode 154, the diaphragm 156, and the plasma shield 158 can be examples of electrically conductive portions. Note that different materials may be used for the various conductive portions.
In another embodiment (not shown), the housing 141 may include one or more insulating, resistive, or semiconductor materials. The materials of the housing should comprise a coefficient of thermal expansion that is similar to the coefficient of thermal expansion of the insulator 142. If any or all insulating, resistive, or semiconductor materials are used for the housing 141, a separate electrical connection may be made to control the signal or potential of the diaphragm 146 during operation. A wire or other interconnect (not shown) may be electrically connected to the diaphragm 146 and the process tube 148 or other external conductor. Welds, screws, rivets, conductive adhesives or epoxies may be used to make the electrical connections to the wire or other interconnect.
The insulator 142 should include a principal insulating material having a coefficient of thermal expansion similar to that of the other materials within the capacitor portion 14. This insulator should be stable to withstand stress and heat from the sensor manufacturing process. For sensors with reference side evacuated and sealed, the insulator should not outgas. In another embodiment, a glass-mica composite can be used for the insulating material. In one specific non-limiting example, glass-mica COMPOSITE 561™ made by Mykroy/Mycalex Ceramics, a division of Spaulding Composites Co., of Clifton, N.J. can be used. COMPOSITE 561™ is a molding grade of a glass-mica composite.
In another embodiment, the insulator 142 may comprise a glass-ceramic material. Examples of the glass-ceramic materials include glasses comprising at least one non-silicate oxide compound including alumina (Al2O3), barium oxide (BaO), cobalt monoxide (CoO), boron oxide (B2O3), lithium oxide (Li2O), potassium oxide (K2O), phosphorus pentoxide (P2O5), and the like. In a specific non-limiting embodiment, the glass comprises silicon dioxide (SiO2) in a range of approximately 55-80 weight percent. U.S. Pat. Nos. 4,135,936, 4,414,282, and 5,820,989 include more details on the composition and formation of these glass-ceramic materials and are incorporated herein by reference.
Typically, the materials within the capacitor body 14, such as the electrode assembly 12, insulator 142, reference-side ring 144, process-side ring 147, shell 146, electrode 154, and diaphragm 156, should be selected such that the coefficient of thermal expansion of the insulator 142 (or its principal insulating material) is within approximately 50% of the coefficient(s) of thermal expansion of any or all of the other solid materials within the capacitor portion 14. Often, the coefficient of thermal expansion of the insulator 142 may be within approximately 10 percent of the coefficient(s) of thermal expansion for any or all of the other materials within the capacitor portion 14. Ideally, all the coefficients of thermal expansion should be substantially the same. By selecting materials with similar coefficients of thermal expansion, temperature-induced variations of readings from the sensor 10 should not occur or will be relatively insignificant.
Thermal coefficients of expansions for some exemplary materials are given. INCONEL™718 is approximately 13E−6 cm/cm/degree Celsius or 8E−6 in/in/degree Fahrenheit, MONEL™ is approximately 14E−6 cm/cm/degree Celsius or 7E−6 in/in/degree Fahrenheit, HASTELLOY™ is approximately 11-13E−6 cm/cm /degree Celsius or 6-7E−6 in/in /degree Fahrenheit, stainless steel 300 series (e.g., stainless steel 316 or the like) is approximately 18E−6 cm/cm/degree Celsius or 10E−6 in/in/degree Fahrenheit, stainless steel 400 series is approximately is approximately 11E−6 cm/cm/degree Celsius or 6E−6 in/in/degree Fahrenheit, alumina is approximately 7E−6 cm/cm/degree Celsius or 4E−6 in/in/degree Fahrenheit, fosterite is approximately 10E−6 cm/cm/degree Celsius or 6E−6 in/in/degree Fahrenheit, glass-mica COMPOSITE 561™ is approximately 13E−6 cm/cm/degree Celsius or 7E−6 in/in/degree Fahrenheit, each of glass-mica COMPOSITE 410 ™ and 555™ is approximately 11E−6 cm/cm/degree Celsius or 6E−6 in/in/degree Fahrenheit, and glass-ceramic materials are in a range of approximately 10E−6 to 18E−6 cm/cm/degree Celsius or 6E−6 to 10E−6 in/in/degree Farhenheit. After reading this specification, skilled artisans understand how to select materials to reduce the likelihood of significant adverse effects due to temperature changes.
During operation of the pressure sensor 10 as shown in
Note that the inner surface of the reference-side ring 144 and the outer surface the electrode assembly 12 can have substantially varying topologies. These substantially varying topologies help to seal the reference side of the component from the exterior side of the component that may be exposed to atmospheric pressure. The substantially varying topologies can form a longer and more difficult path for air, water, or other external contaminant to migrate to reach the evacuated region on the reference side of the diaphragm 156. This also strengthens the bonds between the parts. A serpentine, saw-tooth, square-wave, or nearly any other pattern can be used. This substantially varying topology can be achieved by using a router or other cutting tool to obtain the shape desired. Note that the substantially varying topology can have changes in topology that are typically greater than the root mean square surface roughnesses of the materials used for the reference-side ring 144 and the electrode assembly 12 when polished.
An optional glass seal 22 may be formed along the surfaces of the reference-side ring 144 and the electrode assembly 12 as shown in FIG. 2. In one example, a glass paste can be used to improve the metal-ceramic seal between the ring 144 and an insulating material. As an example, GEC-100 ™, made by Aremco Products, Inc. of Valley Cottage, N.Y., is a glass paste that can be used. The glass paste may be cured before or after forming an insulating material within the gap between the electrode assembly 12 and the reference-side ring 144. Next, a moldable insulating material 24, (e.g., glass-mica COMPOSITE 561™ or the like), can be molded to lie between the reference-side ring 144 and the electrode assembly 12. The insulating material 24 may have a coefficient of thermal expansion similar to that of the reference-side ring 144 and the electrode assembly 12. Following the molding operation, an optional anneal may be performed to improve the integrity of the seals between the various materials present within the component 20. In an alternative embodiment, the combination of the glass seal 22 and moldable insulating material 24 used for the insulator 142 may be replaced by a glass-ceramic material previously described.
In some applications, when the gettering material 106 is used and temperature activated, the activation temperature can be as high as approximately 800 degrees Celsius. The selection of the materials for the component 20 is such that it can withstand short-term thermal shock. It is also common that the sensor 10 may operate at an elevated temperature (sometimes above approximately 200 degrees Celsius). The selection of materials for the component 20 is also such that they do not significantly contribute to contamination or outgassing that may occur when evacuating the reference side of the diaphragm or during subsequent processing conditions if the pressure sensor 10 is exposed to an elevated temperature.
Referring to
In the foregoing specification, the invention has been described with reference to specific embodiments. However, one of ordinary skill in the art appreciates that various modifications and changes can be made without departing from the scope of the present invention as set forth in the claims below. Accordingly, the specification and figures are to be regarded in an illustrative rather than a restrictive sense, and all such modifications are intended to be included within the scope of present invention.
Benefits, other advantages, and solutions to problems have been described above with regard to specific embodiments. However, the benefits, advantages, solutions to problems, and any element(s) that may cause any benefit, advantage, or solution to occur or become more pronounced are not to be construed as a critical, required, or essential feature or element of any or all the claims.
As used herein, the terms “comprises,” “comprising,” “includes,” “including,” “has,” “having” or any other variation thereof, are intended to cover a non-exclusive inclusion. For example, a process, process, article, or apparatus that comprises a list of elements is not necessarily limited only those elements but may include other elements not expressly listed or inherent to such process, process, article, or apparatus. Further, unless expressly stated to the contrary, “or” refers to an inclusive or and not to an exclusive or. For example, a condition A or B is satisfied by any one of the following: A is true (or present) and B is false (or not present), A is false (or not present) and B is true (or present), and both A and B are true (or present).
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Number | Date | Country | |
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20030233882 A1 | Dec 2003 | US |