The present invention is applicable to the field of tunable lasers and is more specifically applicable to a tunable laser for use in telecommunications.
Introduction
In telecommunications networks that utilize wavelength division multiplexing (WDM), widely tunable lasers enable transmission of information at different wavelengths. Many proposed network configurations require transmitters that can be tuned to transmit at any of N distinct wavelengths. Even in networks where the individual transmitter wavelengths are held fixed, tunable sources are desirable for maintaining stability of the wavelength. Also, because the same part can be used for any channel, a tunable transmitter is useful from an inventory control perspective.
One prior art tunable laser design uses an external optical cavity, which is illustrated in U.S. Pat. No. 5,771,252. A basic configuration from U.S. Pat. No. 5,771,252 is shown in
The grating-based external cavity tunable laser (ECLs) of 5,771,252 is a relatively large, expensive device that is not suitable for use as a transmitter in a large-scale WDM network. Because of the size and distance between components, assembly and alignment of the prior art ECL above is difficult to achieve. Known prior art ECLs use stepper motors for coarse positioning and piezoelectric actuators for fine positioning of wavelength selective components. Because piezoelectric actuators exhibit hysteresis, precise temperature control is needed. In addition, prior art ECL lasers are not robust in the presence of shock and vibration.
Another prior art tunable laser design utilizes a Vertical-Cavity Surface-Emitting Laser (VCSEL). In one embodiment of this device, a MEMS (micro-electro-mechanical-system) mirror device is incorporated into the structure of the VCSEL and is used to tune the wavelength of the laser. Wide tuning range has been demonstrated in such devices for operation around 830 nm, but so far, the development of a reliable, high performance VCSEL at 1550 nm has proved elusive. This device is very difficult to build because the MEMS device must be physically incorporated into the structure of the VCSEL. Furthermore, development of the MEMS actuators in InP-based materials is a formidable challenge.
In other prior art, angular motors have been used in angular gyroscopes and as fine tracking servo actuators for magnetic heads for disk drives. In “Angular Micropositioner for Disk Drives,” D. A. Horsley, A. Singh, A. P. Pisano, and R. Horowitz, Proceedings of the 10th Int. Workshop on Micro Electro Mechanical Systems, 1997, p. 454-458, a deep polysilicon device is described with radial flexures extending from a central fixed column, and radial, parallel plate electrodes that effect rotation of less than 0.5 degree. Batch Fabricated Area Efficient Milli-Actuators, L.-S. Fan, et. al., Proceedings 1994 Solid State Sensor and Actuator Workshop, Hilton Head, p. 38-42 shows a rotary flexural actuator with what appears to be 2 central flexures from central supports; the rotational range is not given but appears to be small. Dual Axis Operation of a Micromachined Rate Gyroscope, T. Juneau, A. P. Pisano, and J. H. Smith, Proceedings 1997 Int. Conf. On Solid State Sensors and Actuators, V. 2, pp. 883-890 describes a polysilicon, surface micromachined gyro, which has 4 radial springs supporting a central circular mass. The springs are supported on the outside, and have a small strain relief feature. The angular drive range is not specified, but appears to be small. All of these prior art devices provide limited angular range. These prior art devices completely fill a circular area in a plan view, thus making it difficult or impossible to arrange such an actuator to provide a remote pivot location, as is required by ECLs.
Tunable Distributed Bragg Reflector (DBR) lasers are currently commercially available, however, these lasers have a limited tuning range. Total tuning of about 15 nm and continuous tuning without mode hops over about 5 nm range is typical.
A tunable laser based on sampled grating DBR technology is presently available. The DBR device is tunable over about 50 nm, but the fabrication is difficult and the control electronics are complex, requiring four different control currents.
Another prior art approach to making a tunable laser is to fabricate multiple Distributed Feedback (DFB) lasers on a single chip and couple them together with an arrayed waveguide structure. Each DFB is fabricated with a slightly different grating pitch so that each lases at a slightly different wavelength. Wavelength tuning is accomplished by activating the laser that matches the particular wavelength of interest. The main problems with this approach are cost and insertion loss. Furthermore, fabrication of multiple lasers on the same chip with different operating wavelengths may require direct e-beam writing of the gratings. Also, if one wants to cover a very wide tuning range, the number of lasers required is prohibitively large. Additionally, the multiple laser approach is lossy because coupling N lasers together into one output waveguide results in an efficiency proportional to 1/N.
What is needed, therefore, is a tunable laser that provides advantages over the prior art.
The present invention comprises a tunable laser assembly. Advantages derived from the present invention include: the ability to use commonly available inexpensive Fabry-Perot (FP) laser diodes; high operating frequencies; reduced size and mass, thermal and mechanical stability; precise alignment of optical components made simple by use of photolithographically-defined features in silicon, high production yields; and simple output frequency control schemes.
The present invention may comprise a tunable laser, including: a source means for providing a light along an optical path with any wavelength selected from a continuous bandwidth of wavelengths; a diffractive element positioned in the optical path and from the source by a first distance to redirect the light; a reflective element positioned in the optical path and from the diffractive element by a second distance to receive the redirected light from the diffractive element, and the reflective element positioned in the optical path and from the diffractive element by the second distance to redirect the light towards the diffractive element; the diffractive element positioned in the optical path and from the source by the first distance to re-direct the light towards the source; and a micro-actuator means for selecting the wavelength from the continuous range of wavelengths by altering the optical path of the light.
The present invention may comprise a laser assembly that includes a source for providing a light along an optical path with any wavelength from a continuous range of wavelengths; a diffractive element positioned in the optical path and from the source by a first distance to redirect the light; a reflective element positioned in the optical path and from the diffractive element by a second distance to receive the redirected light from the diffractive element, and the reflective element positioned in the optical path and from the diffractive element by the second distance to redirect the light towards the diffractive element; the diffractive element positioned in the optical path and from the source by the first distance to re-direct the light towards the source; and a micro-actuator for selecting the wavelength from the continuous range of wavelengths by altering the optical path of the light.
The first distance and the second distance may define an optical path length between the source and the reflective element measured in wavelengths, and wherein the optical path length remains constant over the continuous range of wavelengths.
The micro-actuator may be coupled to the reflective element to displace the reflective element. The displacement may comprise an angular displacement. The angular displacement may occur about a virtual pivot point. The displacement may comprise a translation and a rotation. The micro-actuator may comprise a micro-machined actuator. The micro-machined actuator may be coupled to the reflective element. The reflective element may comprise a retro-reflector. The continuous range of wavelengths may comprise from about 1520 nm to about 1560 nm. The wavelength may be about 1540 nm. The source may comprise a Fabry-Perot laser.
The present invention may also comprise a tunable laser, including: a source means for providing a light along an optical path with any wavelength selected from a continuous bandwidth of wavelengths; a diffractive element positioned in the optical path and from the source by a first distance to redirect the light; a reflective element positioned in the optical path and from the diffractive element by a second distance to receive the redirected light from the diffractive element, and the reflective element positioned in the optical path and from the diffractive element by the second distance to redirect the light towards the diffractive element; the diffractive element positioned in the optical path and from the source by the first distance to re-direct the light towards the source; and a micro-actuator means for selecting the wavelength from the continuous range of wavelengths by altering the optical path of the light.
The present invention may also comprise a method for providing light with any wavelength selected from a continuous range of wavelengths, including the following steps: providing the light along an optical path; providing a diffractive element in optical path to diffract the light; providing reflective element in the optical path to reflect the light; and selecting a particular wavelength of light from the continuous range of wavelengths by altering the optical path through displacement of a micro-actuator.
The method may also include the step of displacing the reflective element with the micro-actuator to alter the optical path.
The method may also include the step of displacing the reflective element by a translation and a rotation.
The method may also include the step of displacing the micro-actuator about a virtual pivot point.
The method may also include the step of selecting the particular wavelength from a continuous range of wavelengths comprising the range from about 1520 nm to 1560 nm.
Referring now to
In the preferred embodiment, a widely-tunable laser (ECL) 100 of the present invention includes a laser 101, a collimating lens 102, a diffraction grating 103, a reflector 104, and a MEMS based actuator 105. In the preferred embodiment, the actuator 105 is a rotary actuator, the laser 101 is a Fabry-Perot laser diode, and the reflector 104 is a retro-reflector. The reflector 104 utilizes a high reflectivity coating on its surface, and the laser 101 utilizes a high-reflectivity coating on its rear facet and an anti-reflection coating on its front facet. In the preferred embodiment, the grating 103 is replicated in glass. The present invention utilizes because the provide several advantages compared to traditional polymer gratings, including: thermal stability; replication and stability using thin substrates; and the ability to be handled, diced, cleaned, etc.
In the present invention, light from the laser 101 is directed through the lens 102 towards the grating 103, by the grating 103 towards the reflector 104, by the reflector 104 back towards the grating 103, and by the grating 103 back towards the laser 101. The optical path traversed by the light from the laser 101 forms an external cavity, which causes an output beam 150 of the laser 101 to lase at a particular wavelength that is a function of the rotation angle of the reflector 104. In the exemplary embodiment, the ECL 100 can be tuned over +/−26 nm with +/−2 degrees of motion of the actuator 105. For optimum performance of the ECL 100, it is desired that the wavelength of the output beam 150 be continuously tunable (i.e., no mode hops occur as the laser 101 is tuned over a range of wavelengths). This condition can be satisfied by selecting a virtual pivot point 108 about which the reflector 104 rotates and/or translates, such that an optical path length of the cavity formed between a rear facet of the laser 101 and the reflector 104 measured in wavelengths remains constant over the desired tuning range. U.S. Pat. Nos. 5,319,668 and 5,771,252 disclose methods for calculating a pivot point and are incorporated herein by reference. The two calculations made in these two prior art patents result in pivot point locations that differ by 40 nm. The calculations used in both of these patents are applicable to the present invention because the component and manufacturing tolerances of the present invention are greater than 40 nm. In fact, adequate performance of the present invention may be obtained by choosing a pivot point such that the cavity phase error and only the first derivative go to zero at the center wavelength. This condition gives an approximate location for the pivot point. During assembly, the tuning performance of the present invention can be measured, and the pivot point 108 adjusted in a manner described in further detail below. The virtual pivot point of the present invention allows for a compact geometry and results in a lower-cost device with better optical performance than if a real pivot point was used. Better optical performance is achieved because the compact geometry results in greater spacing of the external optical cavity modes and greater side-mode suppression.
In an exemplary embodiment, the optical path length of the external cavity (a sum of the optical distance between the front facet of the laser 101, the grating 103, and the front of the reflector 104) is approximately 5 mm; and the center wavelength, grating pitch, angle of incidence, and diffraction angle of the grating 103 are 1540 nm, 1050 lines/mm, 85 degrees, and 38 degrees, respectively. Although the overall tuning range of the ECL 100 is a function of the width of the gain curve of the laser 101, which in the preferred embodiment of the present invention can be tuned over a range on the order of 40 nm, it is understood that a much broader gain profile may be achievable using, for example, a Fabry-Perot strongly-pumped quantum-well laser design, referenced in Electronics Letters, Vol. 26, No. 11, pp. 742-743, “External Grating Laser With Wide Tuning Range of 240 nm,” by Epler et al. In the present invention, single-mode operation occurs when the spacing of the external cavity modes are greater than the linewidth of the grating 103. The linewidth of the grating 103 is determined by the angle of incidence and by the beam size. In an exemplary embodiment, the grating 103 linewidth is about 21 GHz and the external cavity modes are spaced by about 30 GHz. The ultimate linewidth is determined by the external cavity mode spacing and by the quality of the external cavity. In the exemplary embodiment, with high reflectivity coatings on the reflector 104 and on the rear facet of the laser 101, the linewidth is less than 1 Mhz.
Referring now to
In another alternative embodiment, a Fabry-Perot laser 101 with as high a relaxation oscillation frequency as possible could be used to achieve high data transfer rates. In this embodiment, the laser should preferably maximize the differential gain, maximize the internal photon density, and minimize the photon lifetime. Multiple-Quantum-Well (MQW) lasers provide these characteristics and have been demonstrated to operate with modulation bandwidths well in excess of 10 GHz. See for example IEEE Photonics Technology Letters, Vol. 9, No. 3, pp. 306-308, “24-GHz Modulation Bandwidth and Passive Alignment of Flip-Chip Mounted DFB Laser Diodes”, by Lindgren, et al. With this approach, direct modulation of the ECL 100 as high as 2.5 Gb/sec should be possible.
In yet another alternative embodiment, the ECL 100 could be designed to operate at frequencies corresponding to multiples of longitudinal mode spacing (i.e., multiples grater than the relaxation oscillation frequency). This approach would have the drawback of decreasing the mode spacing and increasing the overall size of the ECL 100.
Referring now to
Referring now to FIG. 5 and preceding figures and descriptions as needed, there is seen an embodiment in which a position sensing detector (PSD) is used for servo-control of the actuator. In the embodiment of
Referring now to FIG. 6 and preceding figures and descriptions as needed, there is seen a third embodiment in which a PSD is used for servo control. In the embodiment of
Referring now to
In an alternative embodiment to those of
In yet another alternative embodiment to those of
Referring now to FIG. 8 and preceding figures and descriptions as needed, there is seen an embodiment of a wavelength locker as used with the present invention. The present invention identifies that in an alternative approach to that of
Referring now to
Referring now to
Referring now to
In the preferred embodiment, the actuator 105 is manufactured from the mask shown in
In the preferred embodiment, a potential applied to bond pads 131 and 133 causes an electro-static potential to be created between the respective fixed and movable teeth of the comb drive elements 111, which causes the trusses 125 to rotate clockwise about the virtual pivot point 108. A potential applied to bond pads 130 and 132 causes the trusses 125 to rotate counter-clockwise. In the preferred embodiment, when the lever 122 is moved (for example, manually or by other movement means such as micro-machined actuator or the like) the coupler 123 that is attached to the lever 122 rotates around a point near its center. The opposite coupler 123 that is not connected to the lever 122 causes the small rotation of the first coupler to be converted into a translational motion along an axis extending through the two couplers. By arranging the couplers 123 to be generally parallel to the optical axis of the external optical cavity, motion of the lever 122 can be used to adjust the external optical cavity length independent of the rotation of the actuator 105. The adjustments can be made as required to compensate for changes in temperature or variations in the optical cavity length, or to compensate for small offsets in the virtual pivot point 108.
The present invention takes into consideration that the comb drive elements 111 may become unstable and “snapover” in the radial direction if the radial stiffness of the suspension beams 110 falls below a value equal to the derivative of the electrostatic force between the comb drive elements 111 with respect to radial motion, and that this instability becomes more severe with large, static angular deflection. Although folded beam suspension designs are known by those skilled in the art to provide large rotational range, they do so with a penalty of reduced out-of-plane and radial stiffness, which would work against the desired goal of maintaining mechanical stability. The present invention identifies a novel and new design that takes into consideration the limitations of folded beam designs and instead utilizes the “straight-beam” suspension beams 110 described above. As described above, the basic structure for the actuator 105 is to use 2 or more suspensions 110 that are radially disposed around the axis of rotation of the actuator 105. In the preferred embodiment, 2 or 3 beams are used and are spaced 20-30° apart with respect to the rotation axis. It is understood that if larger angles of rotation are desired, the size of the actuator 105 would be increased. In the preferred embodiment, the rotary comb drive elements 111 are arranged around the suspension beams 110, and can either be contained between the suspension beams, or connected outside the beams. If the comb drive elements 111 are arranged over an arc of about 120°, it may be advantageous to have three suspension beams 110 arranged at 60° spacing.
In the preferred embodiment, the actuator 105 is fabricated from a high aspect ratio process, which can also include plated metal processes, for example, Lithographie, Gavanometrie and Abformung (LIGA) process well known in the art. LIGA processing techniques result in structures that comprise vertical dimensions substantially greater than the horizontal width of the smallest features of the actuator 105. With these processes, the resulting stiffness of the actuator 105, the motion of the actuator may be constrained to be substantially in the plane of the actuator.
Referring now to
Referring now to
Referring now to
Because the laser 101 and actuator 105 of the present invention can be made separately, the wafer fabrication processes for their manufacture can be made simpler, which can provide higher manufacturing yields than the prior art.
The present invention identifies that, other than in the embodiment described above in which capacitance sensing is used for servo control, the ECL 100 exhibits sufficient thermal stability such that a thermo-electric cooler need not be used. This is an advantage because TE coolers can be relatively unreliable and are prone to fail.
Because the rotation angle of the MEMS actuator 105, and hence the reflector 104, can be held steady under simple closed loop control, the wavelength of the output beam 150 may also be held steady. Furthermore, unlike prior art tunable VCSELs, in which wavelength vs. actuator voltage must be re-calibrated as the laser ages, the stable dispersive properties of the diffraction grating 103 of the present invention do not change with age, such that after an initial calibration step, further calibration of the module 106 is not necessarily required. Even if in some embodiments the wavelength of the output beam 150 can not be held stable over the lifetime of the module 106, the wavelength stability of the present invention is good enough such that only intermittent re-calibration is envisioned.
Although, the foregoing discussion has presented particular embodiments of the present invention, it is to be understood that the above description is not to be limited to only the described telecommunications application and embodiments. For example, other applications include: remote sensing or spectroscopy applications. It will also be appreciated by those skilled in the art that it would be possible to modify the size, shape, appearance and methods of manufacture of various elements of the invention, or to include or exclude various elements and stay within the scope and spirit of the present invention. Thus, the invention should be limited only by the scope of the claims as set forth below.
This application claims benefit of U.S. provisional patent application Ser. No. 60/154,899 filed Sep. 20, 1999, claims benefit of U.S. provisional patent application Ser. No. 60/167,951 filed Nov. 29, 1999 and claims benefit of U.S. provisional patent application Ser. No. 60/167,937 filed Nov. 29, 1999.
Number | Name | Date | Kind |
---|---|---|---|
625971 | Gardner et al. | May 1899 | A |
4460977 | Shimada et al. | Jul 1984 | A |
4504950 | AuYeung | Mar 1985 | A |
4560246 | Cotter | Dec 1985 | A |
4583227 | Kirkby | Apr 1986 | A |
4770047 | Arditty et al. | Sep 1988 | A |
4839614 | Hill et al. | Jun 1989 | A |
4843233 | Jeunhomme | Jun 1989 | A |
4847854 | Van Dijk | Jul 1989 | A |
4870269 | Jeunhomme et al. | Sep 1989 | A |
4932782 | Graindorge et al. | Jun 1990 | A |
4994677 | Graindorge | Feb 1991 | A |
5028395 | Sebille et al. | Jul 1991 | A |
5050179 | Mooradian | Sep 1991 | A |
5058124 | Cameron et al. | Oct 1991 | A |
5103457 | Wallace et al. | Apr 1992 | A |
5115677 | Martin et al. | May 1992 | A |
5124993 | Braunlich et al. | Jun 1992 | A |
5141316 | Lefevre et al. | Aug 1992 | A |
5163063 | Yoshikawa et al. | Nov 1992 | A |
5172185 | Leuchs et al. | Dec 1992 | A |
5181078 | Lefevre et al. | Jan 1993 | A |
5181214 | Berger et al. | Jan 1993 | A |
5181717 | Donntag et al. | Jan 1993 | A |
5185643 | Vry et al. | Feb 1993 | A |
5218610 | Dixon | Jun 1993 | A |
5225930 | Land et al. | Jul 1993 | A |
5263037 | Trutna, Jr. et al. | Nov 1993 | A |
5270791 | Lefevre et al. | Dec 1993 | A |
5305330 | Rieder et al. | Apr 1994 | A |
5319257 | McIntyre | Jun 1994 | A |
5319668 | Luecke | Jun 1994 | A |
5321717 | Adachi et al. | Jun 1994 | A |
5327447 | Mooradian | Jul 1994 | A |
5331651 | Becker et al. | Jul 1994 | A |
5347527 | Favre et al. | Sep 1994 | A |
5349440 | DeGroot | Sep 1994 | A |
5373515 | Wakabayashi et al. | Dec 1994 | A |
5387974 | Nakatani | Feb 1995 | A |
5412474 | Reasenberg et al. | May 1995 | A |
5414280 | Girmay | May 1995 | A |
5418800 | Prior et al. | May 1995 | A |
5420687 | Kachanov | May 1995 | A |
5428700 | Hall | Jun 1995 | A |
5434874 | Fouquet et al. | Jul 1995 | A |
5438579 | Eda et al. | Aug 1995 | A |
5444724 | Goto | Aug 1995 | A |
5450202 | Tisue | Sep 1995 | A |
5473625 | Hansen et al. | Dec 1995 | A |
5543916 | Kachanov | Aug 1996 | A |
5583638 | Cutler | Dec 1996 | A |
5594744 | Lefevre et al. | Jan 1997 | A |
5606439 | Wu | Feb 1997 | A |
5631736 | Thiel et al. | May 1997 | A |
5651018 | Mehuys et al. | Jul 1997 | A |
5673129 | Mizrahi | Sep 1997 | A |
5712704 | Martin et al. | Jan 1998 | A |
5719674 | Martin et al. | Feb 1998 | A |
5737109 | Goodwin | Apr 1998 | A |
5751750 | Friede et al. | May 1998 | A |
5760391 | Narendran | Jun 1998 | A |
5771252 | Lang et al. | Jun 1998 | A |
5777773 | Epworth et al. | Jul 1998 | A |
5802085 | Lefevre et al. | Sep 1998 | A |
5812716 | Ohishi | Sep 1998 | A |
5825792 | Villeneuve et al. | Oct 1998 | A |
5848092 | Mitsumoto et al. | Dec 1998 | A |
5862162 | Maeda | Jan 1999 | A |
5867512 | Sacher | Feb 1999 | A |
5872881 | Rossi et al. | Feb 1999 | A |
5886785 | Lefevre et al. | Mar 1999 | A |
5917188 | Atkinson et al. | Jun 1999 | A |
5929542 | Ohnstein et al. | Jul 1999 | A |
5943352 | Fee | Aug 1999 | A |
5946331 | Amersfoort et al. | Aug 1999 | A |
5991061 | Adams et al. | Nov 1999 | A |
5998906 | Jerman et al. | Dec 1999 | A |
6018535 | Maeda | Jan 2000 | A |
6026100 | Maeda | Feb 2000 | A |
6034799 | Hansen | Mar 2000 | A |
6040950 | Broome | Mar 2000 | A |
6043883 | Leckel et al. | Mar 2000 | A |
6044095 | Asano et al. | Mar 2000 | A |
6061369 | Conradi | May 2000 | A |
6064501 | Roberts et al. | May 2000 | A |
6081539 | Mattori et al. | Jun 2000 | A |
6084695 | Martin et al. | Jul 2000 | A |
6108355 | Zorabedian | Aug 2000 | A |
6115121 | Erskine | Sep 2000 | A |
6115401 | Scobey et al. | Sep 2000 | A |
RE37044 | Wu | Feb 2001 | E |
6192058 | Abeles | Feb 2001 | B1 |
6205159 | Sesko et al. | Mar 2001 | B1 |
6215802 | Lunt | Apr 2001 | B1 |
6229835 | Tomaru et al. | May 2001 | B1 |
6243517 | Deacon | Jun 2001 | B1 |
6246480 | O'Brien | Jun 2001 | B1 |
6249364 | Martin et al. | Jun 2001 | B1 |
6249365 | Mizrahi et al. | Jun 2001 | B1 |
6252718 | Lefevre | Jun 2001 | B1 |
6282215 | Zorabedian et al. | Aug 2001 | B1 |
6301274 | Tayebati et al. | Oct 2001 | B1 |
6301280 | Broutin et al. | Oct 2001 | B1 |
6304586 | Pease et al. | Oct 2001 | B1 |
6314115 | Delfyett et al. | Nov 2001 | B1 |
6321011 | Deacon | Nov 2001 | B2 |
6324204 | Deacon | Nov 2001 | B1 |
6329737 | Jerman et al. | Dec 2001 | B1 |
6330253 | Tuganov et al. | Dec 2001 | B1 |
6331892 | Green | Dec 2001 | B1 |
6337660 | Esman et al. | Jan 2002 | B1 |
6366689 | Rao et al. | Apr 2002 | B1 |
6404538 | Chen et al. | Jun 2002 | B1 |
6404798 | Leckel et al. | Jun 2002 | B1 |
6428173 | Dhuler et al. | Aug 2002 | B1 |
6441933 | Jang | Aug 2002 | B1 |
6463085 | Tayebati | Oct 2002 | B1 |
6493365 | Wu et al. | Dec 2002 | B1 |
6532091 | Miyazaki et al. | Mar 2003 | B1 |
20010036206 | Jerman et al. | Nov 2001 | A1 |
20020048297 | Irie et al. | Apr 2002 | A1 |
20020126345 | Green et al. | Sep 2002 | A1 |
20020136104 | Daiber | Sep 2002 | A1 |
Number | Date | Country |
---|---|---|
0 924 821 | Jun 1999 | EP |
0 952 643 | Oct 1999 | EP |
WO 9937013 | Jul 1999 | WO |
Number | Date | Country | |
---|---|---|---|
60167951 | Nov 1999 | US | |
60167937 | Nov 1999 | US | |
60154899 | Sep 1999 | US |