The inventive concept described herein generally relates to electron impact X-ray sources, and to liquid targets for use in such X-ray sources.
Systems for generating X-rays by irradiating a liquid target are described in the applicant's International Applications PCT/EP2012/061352 and PCT/EP2009/000481. In these systems, an electron gun comprising a high-voltage cathode is utilized to produce an electron beam that impinges on a liquid jet. The target is preferably formed by a liquid metal with low melting point, such as indium, tin, gallium lead or bismuth, or an alloy thereof, provided inside a vacuum chamber. Means for providing the liquid jet may include a heater and/or cooler, a pressurizing means (such as a mechanical pump or a source of chemically inert propellant gas), a nozzle and a receptacle to collect liquid at the end of the jet. The X-ray radiation generated by the interaction between the electron beam and the liquid jet may leave the vacuum chamber through a window separating the vacuum chamber from the ambient atmosphere.
However, there is still a need for improved X-ray sources.
It is an object of the present inventive concept to provide an improved X-ray source.
According to a first aspect of the inventive concept, an X-ray source is provided comprising: a liquid target source configured to provide a liquid target moving along a flow axis; an electron source configured to provide an electron beam; and a liquid target shaper configured to shape the liquid target to comprise a non-circular cross section with respect to the flow axis, wherein the non-circular cross section has a first width along a first axis and a second width along a second axis, wherein the first width is shorter than the second width, and wherein the liquid target comprises an impact portion being intersected by the first axis; wherein the x-ray source is configured to direct the electron beam towards the impact portion such that the electron beam interacts with the liquid target within the impact portion to generate X-ray radiation; and wherein the X-ray source further comprises an arrangement configured to move a location, within the impact portion, in which the electron beam interacts with the liquid target.
The present inventive concept is based on the realization that by providing the liquid target with a non-circular cross section, a wider impact surface for the electron beam may be achieved without having to increase e.g. the flow rate of the liquid target. A wider, or less curved, impact surface may also allow for multiple electron beams to simultaneously impact the liquid target, preferably along a direction perpendicular to the flow axis, and for larger or wider electron beam spots to be used without substantially impairing the focus of the X-ray spot. It will be appreciated that such an impact surface also may be used with electron beam spots being oval or even line shaped.
Further, a liquid target having a non-circular cross section may provide improved thermal properties compared to a corresponding liquid target having a circular cross section with similar width and flow rate. In particular, by reducing the width along one of the axes defining the cross section of the liquid target, a velocity of the liquid target may be increased, which hence may improve the thermal properties of the liquid target. In other words, the ability to thermally load the liquid target varies with the velocity of the liquid target. To preserve the velocity while increasing the width implies increasing the mass flow which in turn may put harder requirements on the pump system.
It is also desirable to be able to adjust the position of an impact portion relative to a position of the electron source and/or an X-ray window, through which the X-ray radiation may exit the X-ray source. Preferably, the impact portion and the electron source may be aligned such that the electron beam may impinge on the largest surface portion of the liquid target, i.e., the portion of the liquid target having the smallest degree of curvature. Furthermore, it may be desirable to increase the width of the target at the impact portion to provide a larger surface for the electron beam to impinge upon.
Further, it has been realized that the angle of incidence with which the electron beam impinges the liquid target may be of importance for e.g. the spatial distribution of the generated X-ray radiation. In particular, an angle of incidence with which the electron beam impinges the liquid target, and/or a location in which the electron beam impinges the liquid target, may be selectively adjusted by turning the first axis of the cross section with respect to a direction of the electron beam, or vice versa, and/or by adjusting a location in which the electron beam impinges the liquid target.
The term ‘width’ may, in the context of the present application, refer to a diameter or extent from side to side of the liquid target. In particular, the first width may be the largest width of the non-circular cross section along the first axis, and the second width may be the largest width of the non-circular cross section along the second axis. The first and second axis may be perpendicular to each other, and may intersect the flow axis. The second width may be in of the order of 100 μm, such as within the range 10 μm to 1000 μm, such as 100 μm to 500 μm, such as 150 μm to 250 μm. The ratio between the second width and the first width may in some examples be at least 1.05, such as at least 1.1, such as at least 1.5, such as at least 2, such as at least 5.
The term ‘liquid target’ may, in the context of the present application, refer to a stream or flow of liquid being forced through e.g. a nozzle and propagating through a system for generating X-rays. Even though the liquid target in general may be formed of an essentially continuous flow or stream of liquid, it will be appreciated that the liquid target additionally, or alternatively, may comprise or even be formed of a plurality of droplets. In particular, droplets may be generated upon interaction with the electron beam. Such examples of groups or clusters of droplets may also be encompassed by the term ‘liquid target’.
The liquid target may have a non-circular cross section, which may conform to an oval, elliptic or otherwise elongated shape. By making the cross section more elongated, the curvature of the surface at the impact portion may be reduced. Eventually, the curvature may be sufficiently low to allow the surface at the impact portion to be approximated with a flat, two-dimensional surface. Such as target may also be referred to as a ‘flat jet’. Put differently, the location of the impact portion may be selected as the part of the liquid target which bears the closest resemblance to a flat surface. A liquid curtain is an extreme example of such a jet, exhibiting a substantially flat surface which can be used as impact portion for the electron beam.
The liquid target may be formed of a liquid jet that, at least in the location of the impact region, propagates freely relative the surrounding environment. The material of the liquid jet may hence be exposed to the environment in the chamber of the X-ray source.
Typically, the liquid target material is a metal which preferably has a relatively low melting point. Examples of such metals include indium, gallium, tin, lead, bismuth and alloys thereof.
As will be described further in the following disclosure, an electron beam spot of the electron beam may have a round shape, or an elongated shape. In some examples, the elongated shape may also be realized as a line shape or line focus. For a line focus an aspect ratio may be defined, i.e. the ratio between focus width to focus height. A typical value of the aspect ratio attainable on a liquid target with circular cross section is 4. A liquid target with a non-circular cross section may enable larger aspect ratios; e.g. at least 6. The shape of electron beam spot may be chosen depending on the preferred flux and/or brightness of the generated X-ray radiation.
In order to fully appreciate the following disclosure, it may be noted that for large enough Weber numbers, a phenomenon called axis switching may be observed for a liquid target emanating from a nozzle having a non-circular opening. Axis switching is a phenomenon in which the cross section for e.g. a non-circular, such as e.g. elliptical, liquid target, evolves in such a manner that the major and minor axis periodically switch places along the flow direction of the liquid target. The wavelength of the switching increases with increased liquid target velocity. Further, the axis switching is dampened by viscosity, meaning that the amplitude of the axis switching approaches zero as the viscosity increases.
Consequently, it is to be understood that the impact portion may extend along the flow axis. Further, the impact portion may be described as a portion within a sector of the non-circular cross section. The portion may e.g. span sector having an angle of 180 degrees or less, such as e.g. 120 degrees or less, such as 90 degrees or less, such as 60 degrees or less, and may preferably be centered around the first axis.
The X-ray source may be further configured to direct the electron beam towards a specific region within the impact portion. Such a region may also be referred to as an interaction region. The impact portion may thus be understood as the portion, such as a surface portion or volume, that is intersected by the first axis, whereas the interaction region may be understood as the particular portion or region of the impact portion that is hit by the electron beam, and in which the X-ray radiation may be generated. The interaction region may be a volume extending a distance towards a center of the non-circular cross section, i.e. towards the flow axis. Likewise, the impact portion may be a volume, and may extend a distance towards the center of the non-circular cross section, i.e. towards the flow axis.
As is readily understood from the present disclosure, the arrangement may be configured to adjust the position in which the electron beam impinges the liquid target, or in other words, the location of the interaction region. This may be necessary in order to assure that the full size of the electron beam spot is allowed to interact with the liquid target, and in particular that the electron beam spot is allowed to interact with the liquid target within the impact portion.
The arrangement may for example comprise an electron optics arrangement for moving the electron beam relative to the liquid target. Alternatively, or additionally, the arrangement may be configured to cooperate with the liquid target shaper to move or adjust a location in which the electron beam interacts with the target. In an example, the arrangement may comprise a motor or actuator coupled to the liquid target shaper and arranged to move the target shaper in a manner that allows for the position or orientation of the liquid target to be adjusted. The arrangement may for example be configured to rotate the liquid target shaper around the flow axis, resulting in a corresponding rotation of the impact portion around the flow axis, such that an orientation and/or position of the impact portion in relation to the electron source may be varied. In further examples, the arrangement may be configured to translate the liquid target shaper in a direction orthogonal to the flow axis and/or the trajectory of the electron beam, and/or tilt the liquid target shaper relative to the flow axis.
In one example, the arrangement may be configured to control a magnetic field generator configured to generate a magnetic field in order to shape the liquid target to comprise the non-circular cross section. The magnetic field generator will be described in more detail in the following.
The above disclosure provides several examples of how the arrangement can be employed to adjust a relative position between the electron beam and the liquid target. Moving the interaction region and/or the impact portion may result in an adjustment of the angle of incidence of the electron beam. A purpose of such an amendment may be to increase the total X-ray flux along a viewing direction or at a sample position, to increase the brightness of the X-ray source, or to align the position of the X-ray source with other parts (e.g. optics) of an X-ray system. In an example, the adjustment of the angle of incidence and/or the location of the interaction region is based on a measured X-ray output.
The electron beam may interact with the impact portion at an angle of incidence which may be greater than 0 degrees. The angle of incidence may be defined as an angle of incidence with respect to a normal to the non-circular cross section.
An advantage with having the electron beam interacting with the impact portion at an angle of incidence greater than 0 degrees is that less X-rays may be absorbed in the liquid target. In particular, more X-rays can be transmitted via an X-ray window located at an angle, such as substantially perpendicular, to the direction of the electron beam. Consequently, the present arrangement may provide for increased total X-ray flux, and/or an increased X-ray brightness.
Below will follow, among other things, possible modifications of the X-ray source in order to provide for an adjustment of the angle of incidence and/or the location of the interaction region in which the electron beam impinges the liquid target. As will be understood from the following paragraphs, modifications may be directed to the liquid target, the electron beam, or a combination of the two.
The electron source may be configured to be rotated around the flow axis in order to adjust the angle of incidence of the electron beam and/or the location of the interaction region in which the electron beam impinges the target.
The liquid target shaper may comprise a nozzle having a non-circular opening in order to shape the liquid target to comprise the non-circular cross section. The opening may e.g. have a shape selected from the group comprising elliptic, rectangular, square, hexagonal, oval, stadium, and rectangular with rounded corners.
It will be appreciated that the X-ray source according to some embodiments may be configured to move the liquid target relative the electron beam so as to change the location in which the electron beam interacts with the liquid target. The movement may for example be realised in a direction perpendicular to the flow axis of the liquid jet and/or perpendicular to the propagation direction of the electron beam, resulting in a lateral shift of the location of the interaction region. The movement, or shift in position, of the interaction region may for example be achieved by means of the liquid target source.
In one example, the nozzle of the liquid target source may be configured to be moved along the flow axis in order to adjust the angle of incidence and/or the location of the interaction region.
In one example, the nozzle may be configured to be rotated around the flow axis in order to adjust the angle of incidence and/or the location of the interaction region.
In one example, the liquid target source may be configured to be moved in a direction perpendicular to the flow axis in order to adjust the angle of incidence and/or the location of the interaction region.
The liquid target shaper may comprise a magnetic field generator configured to generate a magnetic field in order to shape the liquid target to comprise the non-circular cross section. The magnetic field may be substantially perpendicular to the flow axis. The magnitude of the magnetic field may be non-uniform in the direction of the flow axis so that the liquid target experiences a field gradient as it travels along the flow axis. In other words, the magnetic field may comprise a magnetic field gradient. The mechanism for shaping the liquid target may be based on induced eddy currents within the liquid target, which hence may be electrically conductive. The magnetic field may be an alternating magnetic field.
An example may include a time varying component of the magnetic field directed along the flow axis. This field component may impart acceleration to the liquid target thus increase the thermal load that can be applied to the liquid target before vaporization or similar problems occur.
A maximum relative change of liquid target radius by the application of a magnetic field gradient can be written as:
Na as defined above is called the Stuart number, We is the Weber number, α is the nozzle radius, B0is the magnitude of the magnetic field, Lm is the length scale of the magnetic field gradient, and δe is the electrical conductivity of the liquid target.
In one example, the liquid target consists of liquid gallium, and the following values are input into the formula above:
ρ=6100 kg/m3,
δ=0.7 N/m,
α=100 μm,
ν=100 m/s,
δe=4 MS/m,
B0=1.7 T, and
Lm=1 mm,
which may give a maximum change in liquid target radius of a few percent.
Similar to the case with an elliptic nozzle the shape of the liquid target may oscillate along the flow axis. The values used above gives a wavelength of about 250 nozzle radiuses, i.e. 25 mm. If the exit velocity of the liquid target is increased to 1000 m/s (i.e. the Weber number goes up a factor of 100) the amplitude is about the same, but the wavelength is increased a factor of 10. One way of increasing the magnitude of the relative radius change may be to increase the magnetic field, since the magnitude scales with the Stuart number, i.e. with the square of the magnetic field. Another way to increase the effect may be to increase the Weber number. This can be done without affecting the Stuart number by decreasing the surface tension. This may in turn be achieved by increasing the temperature. As an example, by increasing the magnetic field to 4 T the magnitude of the effect is about 10% in relative change of the radius. As a side note, the magnitude may also increase with increasing nozzle diameter. This may however be counterproductive as discussed above, since just increasing the diameter may result in a lower speed, provided the mass flow is preserved. A lower speed may in turn imply a lower allowed thermal load on the liquid target.
The magnetic field generator may be configured to adjust the magnetic field in order to adjust the angle of incidence and/or the location of the interaction region.
The magnetic field may be non-uniform. In particular, the magnetic field generator may be configured to adjust a direction of a non-uniform magnetic field in order to adjust the angle of incidence and/or the location of the interaction region.
In one example, the magnetic field generator may be configured to generate a magnetic field that moves the liquid target such that the position of the interaction region is moved relative the electron beam.
The liquid target source may be configured to provide an adjustable flow rate of the liquid target in order to adjust the first and second width.
The liquid target may be a metal.
The X-ray source may be configured to turn the impact region with respect to a direction of the electron beam. In other words, the X-ray source may be configured to turn the first axis of the non-circular cross section with respect to a direction of the electron beam.
It is to be understood that a nozzle and a magnetic field generator as described above may both be present in the X-ray source according to the inventive concept.
According to a second aspect of the inventive concept a method for generating X-ray radiation is provided. The method comprises: providing an electron beam; providing a liquid target moving along a flow axis, the liquid target comprising a non-circular cross section with respect to the flow axis, wherein the non-circular cross section has a first width along a first axis and a second width along a second axis, wherein the first width is shorter than the second width, and wherein the liquid target comprises an impact portion being intersected by the first axis; directing the electron beam towards the impact portion such that the electron beam interacts with the liquid target within the impact portion to generate X-ray radiation.
The method may further comprise moving the electron beam along the flow axis and/or in a direction perpendicular to the flow axis in order to move the location in which the electron beam interacts with the liquid target, i.e., the interaction region.
The method may further comprise rotating the electron source around the flow axis in order to adjust the angle of incidence and/or the location of the interaction region.
The method may further comprise moving the nozzle along the flow axis in order to adjust the angle of incidence and/or the location of the interaction region.
The method may further comprise rotating the nozzle around the flow axis in order to adjust the angle of incidence and/or the location of the interaction region.
The step of providing the liquid target may comprise providing a magnetic field for shaping the non-circular cross section of the liquid target.
The method may further comprise adjusting the magnetic field in order to adjust the angle of incidence and/or the location of the interaction region.
The method may further comprise adjusting a flow rate of the liquid target in order to adjust the first and second width.
The method may further comprise turning the impact region with respect to a direction of the electron beam.
The method may further include a step of scanning the electron beam between the liquid target and an unobscured portion of a sensor area in order to determined e.g. a width of the electron beam, preferably at the impact portion. The sensor area, which may form part of the X-ray source according to the first aspect, may be arranged behind the liquid target as seen from the electron source, such that the liquid target at least partly obscures the sensor area. This arrangement allows for the electron beam to be scanned into and/or out of the liquid target and to impinge on the unobscured portion(s) of the sensor area. The output signal from the sensor may then be analyzed to determine the width of the liquid target, preferably in the scanning direction or a direction perpendicular to the flow axis.
The determined width of the liquid target may be used as feedback, or an adjustment parameter, for the operation of the liquid target source, the liquid target shaper and/or the electron beam. The aim of such feedback or adjustments may be to control the width of the liquid target, preferably at the impact portion. Thus, the width may be varied by adjusting a flow rate of the liquid target, by rotating the impact portion around the flow axis, by moving the location in which the electron beam interacts with the liquid target, and/or by adjusting an angle of incidence between the electron beam and a surface of the impact portion.
In one example, the method according to the second aspect may include measurement of the X-ray output, such as e.g. X-ray flux and/or X-ray brightness. The measurements may be performed by sensor means for characterizing or quantifying the generated X-ray radiation. Similar to the feedback mechanism described above, the measured X-ray output may be used for controlling the interaction between the electron beam and the liquid target to achieve a desired output, e.g. in terms of flux or brightness. The interaction may e.g. be controlled by rotating the impact portion around the flow axis, moving the location in which the electron beam interacts with the liquid target, or by adjusting an angle of incidence between the electron beam and a surface of the impact portion.
A feature described in relation to a first one of the above aspects may also be incorporated in the other one of the above aspects, and the advantage of the feature is applicable to all aspects in which it is incorporated.
Other objectives, features and advantages of the present inventive concept will appear from the following detailed disclosure, from the attached claims as well as from the drawings.
Generally, all terms used in the claims are to be interpreted according to their ordinary meaning in the technical field, unless explicitly defined otherwise herein. Further, the use of terms “first”, “second”, and “third”, and the like, herein do not denote any order, quantity, or importance, but rather are used to distinguish one element from another. All references to “a/an/the [element, device, component, means, step, etc]” are to be interpreted openly as referring to at least one instance of said element, device, component, means, step, etc., unless explicitly stated otherwise. The steps of any method disclosed herein do not have to be performed in the exact order disclosed, unless explicitly stated.
The above, as well as additional objects, features and advantages of the present inventive concept, will be better understood through the following illustrative and non-limiting detailed description of different embodiments of the present inventive concept, with reference to the appended drawings, wherein:
The figures are not necessarily to scale, and generally only show parts that are necessary in order to elucidate the inventive concept, wherein other parts may be omitted or merely suggested.
An X-ray source according to the inventive concept will now be described with reference to
The liquid target 104, i.e. the anode, may be formed by the liquid target source 106 comprising a nozzle through which a fluid, such as e.g. liquid metal or liquid alloy, may be ejected to form the liquid target 104. It should be noted that it is to be understood that an X-ray source comprising multiple liquid targets, and/or multiple electron beams, is possible within the scope of the inventive concept.
Still referring to
Referring now to
Referring now to
An electron beam 200 is directed towards the impact portion 216, such that the electron beam 200 interacts with the liquid target 206 and X-ray radiation is generated. In particular, the electron beam 200 is directed to an interaction region 218 located within the impact region 216. The interaction region may be defined as a region wherein X-rays are generated when hit by the electron beam.
Depending on the properties of the liquid target 204, as discussed earlier in the present disclosure, axis switching may be observed. In
Referring now to
Referring now to
Referring now to
Referring now to
Referring now to
Referring now to
Further, although not illustrated, it may be possible to move the nozzle of the liquid target shaper along the flow axis, and/or adjusting a magnetic field generated by a magnetic field generator, in order to adjust the angle of incidence and/or the location of the interaction region. The resulting adjustment of the angle of incidence and/or the location of the interaction region is similar to what has been disclosed above in conjunction to
Further, it is to be understood that any of combination of the adjustments disclosed above in conjunction with
By providing suitable sensor means and a controller (not shown) the adjustments disclosed above in conjunction with
As previously mentioned in connection with
A method for generating X-ray radiation according to the inventive concept will now be described with reference to
In step 724, a liquid target moving along a flow axis is provided. In step 726, an electron beam is provided. In step 728, the liquid target is shaped to comprise a non-circular cross section with respect to the flow axis, wherein the non-circular cross section comprises a first diameter that is shorter than a second diameter, and wherein the liquid target comprises an impact portion being intersected by the first axis. In step 730 the electron beam is directed towards the impact portion such that the electron beam interacts with the liquid target within the impact portion to generate X-ray radiation.
The method may further include steps for adjusting the impact portion to provide a wider impact portion for the electron beam to interact with. The width of the liquid target may be measured by scanning 732 the electron beam across the liquid target and measuring a current absorbed in an e-dump (not shown) located downstream of the liquid target in the direction of the electron beam. Steps for controlling 734 the width towards a desired value may further be included.
Alternatively, or additionally the method may include steps for measuring 736 an X-ray output, such as e.g. X-ray flux or X-ray brightness, and controlling 738 the generation of the X-ray radiation based on the measured X-ray output.
The person skilled in the art by no means is limited to the example embodiments described above. On the contrary, many modifications and variations are possible within the scope of the appended claims. In particular, X-ray sources and systems comprising more than one liquid target are conceivable within the scope of the present inventive concept. Furthermore, X-ray sources of the type described herein may advantageously be combined with X-ray optics and/or detectors tailored to specific applications exemplified by but not limited to medical diagnosis, non-destructive testing, lithography, crystal analysis, microscopy, materials science, microscopy surface physics, protein structure determination by X-ray diffraction, X-ray photo spectroscopy (XPS), critical dimension small angle X-ray scattering (CD-SAXS), and X-ray fluorescence (XRF). Additionally, variation to the disclosed examples can be understood and effected by the skilled person in practising the claimed invention, from a study of the drawings, the disclosure, and the appended claims. The mere fact that certain measures are recited in mutually different dependent claims does not indicate that a combination of these measures cannot be used to advantage.
100 Electron beam
102 Electron source
103 Magnetic field generator
104 Liquid target
106 Liquid target source
108 X-ray radiation
110 Pump
200 Electron beam
204 Liquid target
206 Liquid target source
212 Nozzle
214 Non-circular cross section
216 Impact portion
218 Interaction region
300 Electron beam
314 Liquid target
316 Impact portion
318 Interaction region
320 Second width
322 First width
400 First electron beam
401 Second electron beam
404 Liquid target
408 X-ray radiation
409 X-ray radiation
416 Impact portion
418 First interaction region
419 Second interaction region
421 First X-ray window
423 Second X-ray window
500 Electron beam
504 Liquid target
516 Impact portion
518 Interaction region
600 Electron beam
604 Liquid target
616 Impact portion
618 Interaction region
724 Step of providing a liquid target
726 Step of providing an electron beam
728 Step of shaping the liquid target
730 Step of directing the electron beam
732 Step of scanning the electron beam
734 Step of controlling a width
736 Step of measuring an X-ray output
738 Step of controlling the X-ray output
Number | Date | Country | Kind |
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17204949.6 | Dec 2017 | EP | regional |
Filing Document | Filing Date | Country | Kind |
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PCT/EP2018/083138 | 11/30/2018 | WO | 00 |