The invention relates to an agitator ball mill with a grinding container, wherein an agitator shaft provided with grinding elements is disposed, as result of which a grinding chamber is formed between the grinding container and the agitator shaft, in which grinding chamber the grinding elements extend and in which at least one inlet channel and one outlet channel for grinding stock emerge and a dynamic separating device for auxiliary grinding bodies is provided, wherein the dynamic separating device is provided with recesses for the return of auxiliary grinding bodies. The invention also relates to a method for grinding with an agitator ball mill with the device according to the invention, wherein grinding stock is supplied via a supply opening, said grinding stock being conveyed via the grinding chamber in the direction of the dynamic separating device, wherein auxiliary grinding bodies contained in the grinding stock are transported in the radial direction back into the grinding chamber by means of the separating device.
Agitator ball mills are used for the size-reduction and homogenisation of solid particles, wherein auxiliary grinding bodies are moved intensively by means of an agitator shaft. The solid particles are thereby size-reduced by impact, pressure, shearing and friction. In principle, agitator ball mills can be different with regard to a horizontal or vertical orientation of the grinding chamber. The activation of the auxiliary grinding bodies takes place by means of the agitator shaft, which can be provided with agitator elements such as for example rods or discs. The grinding chamber is usually filled up to seventy to ninety percent with auxiliary grinding bodies in the size range from 0.03-9 mm.
The product to be ground flows continuously in the grinding process from a product inlet axially through the grinding chamber to a product outlet. The separation of the auxiliary grinding bodies from the product flow then takes place in an outlet region by means of a separating system.
The throughput and the size of the grinding bodies are limited by the separating device in closed agitator ball mills. With the aid of the separating device, the auxiliary grinding bodies are intended to be reliably held back in the grinding container and, even in the presence of high throughput rates, must not lead to compression of the grinding bodies or to blockages. The separating devices can be constituted in a known manner as splitting systems, centrifugal systems or as external separating systems. Known splitting systems are for example sieve cartridges or split tubes, which can be disposed at different points of the grinding chamber.
Centrifugal systems are also known from the prior art as dynamic separating devices, wherein the auxiliary grinding bodies are accelerated radially, as a result of which the latter are transported back into the grinding container on account of the acting centrifugal force. Such dynamic separating devices can be constituted for example by a cage rotating around a sieve, the use whereof finds particular application in the case of high throughput rates or when use is made of extremely small grinding bodies.
An agitator ball mill is known for example from DE 102007043670 A1, wherein a part of the drive energy is transmitted to auxiliary grinding bodies by means of an agitator shaft connected to a drive, as result of which penetration of the auxiliary grinding bodies into the grinding stock outlet is prevented.
Another agitator ball mill known from the prior art with a grinding body separating system (DD 256460 A1) comprises a separating sieve, with the aid whereof the auxiliary grinding bodies are intended to be held in the grinding chamber. The grinding body separating system is constituted for this purpose by a rectangular, box-type sieve frame, a lower curved separating sieve with a rectangular shape and a grinding body sieve trap lying beneath the latter at a distance. The actual grinding body separation is brought about by the separating sieve constituted rectangular, which is fastened to the sieve frame by means of holding elements on two opposite sides, which is inserted with both sieves as a closed modular unit into the grinding container.
A further agitator ball mill provided with a dynamic separating system is disclosed in European patent application EP 1468739 A1, wherein the separating device is disposed in front of a stock outlet and is constituted by a separating element and a drive element driving the latter. The separating element comprises two circular discs disposed coaxial with the chamber axis, between which discs a plurality of conveying or wing elements are disposed, being distributed symmetrically about the centre-point of the discs and leading inwards from the edge of the disc, said conveying or wing elements generating a counter-pressure on the stock/grinding body mixture during operation of the agitator ball mill, so that the auxiliary grinding bodies are separated from the product and conveyed back into the interior as a result of the centrifugal force and the different specific density.
The separating devices known from the prior art for agitator ball mills are able to prevent auxiliary grinding bodies from passing into the product outlet, but it has been shown in practice that an increased concentration of auxiliary grinding bodies occurs in the region of the separating device. The actual grinding process does not however take place in this region, but in the grinding chamber in a region before the separating device. The low concentration of auxiliary grinding bodies in the region that is particularly effective for grinding causes a reduced grinding efficiency, which can lead to an unsatisfactory grinding result.
It would therefore be desirable to make available an agitator ball mill with a separating system which enables an improved distribution of the auxiliary grinding bodies in the grinding chamber. The desired uniform distribution of the auxiliary grinding bodies in the grinding chamber should be possible without design modifications, additions or conversions of the grinding chamber. The known devices of the aforementioned type, however, are not entirely suitable for a uniform auxiliary grinding body distribution.
The problem underlying the invention, therefore, is to provide a device of the type mentioned at the outset, which enables an improved distribution of the auxiliary grinding bodies in the grinding chamber.
According to the invention, this problem is solved by the fact that the agitator shaft is provided with at least one recess that extends the dynamic separating device, said recess extending in the axial direction into the grinding chamber.
The invention proceeds from the consideration that, for a uniform distribution of the auxiliary grinding bodies in the grinding chamber, the return of the auxiliary grinding bodies into the grinding chamber can take place through a suitable embodiment and coupling of the separating device and the agitator shaft. The return of the auxiliary grinding bodies should in particular be able to take place, as far as possible, without a costly conversion of the grinding container or through rerouting the auxiliary grinding bodies outside the grinding container.
This is achieved by the fact that the dynamic separating device is coupled with the agitator shaft in such a way that at least one recess of the separating device is extended axially, in such a way that the extended recess extends in the axial direction in a region of the agitator shaft into the grinding chamber. For this purpose, recesses are introduced into the agitator shaft, said recesses being connected to the recesses in the separating device and extending the latter. During operation of the mill, part of the auxiliary grinding bodies can thus be conveyed through the recess in the agitator shaft back into the grinding chamber.
The region of the recesses of the separating device is preferably smaller in the axial direction than the region with the extended recess. As a result of a separating region thus shortened or a lengthened region outside this separating region, the auxiliary grinding bodies are conveyed farther in the axial direction into the grinding chamber, so that the dwell time of the auxiliary grinding bodies in the grinding chamber is effectively increased.
The extended recess preferably runs axis-parallel with the rotary axis of the agitator shaft. It is particularly advantageous here that the production cost for introducing such a recess into the agitator shaft is comparatively low.
It has proved to be advantageous if the extended recess runs at least partially in the axial direction helically or in the form of a helical line around the rotary axis of the agitator shaft. The flow rate, for example, and therefore also an exit point or re-entry point of the auxiliary grinding bodies into the grinding chamber can thus be favourably influenced. If, for example, the helical recess runs against the direction of rotation of the agitator shaft, the flow rate in the axial direction towards the product inlet is increased, as result of which the re-entry point of the auxiliary grinding bodies can be displaced into a front region of the grinding chamber, close to the product inlet.
In a particularly advantageous embodiment, the extended recess essentially extends over the entire length of the agitator shaft. The effect of this is that the auxiliary grinding bodies can also be distributed over the entire length of the agitator shaft in the grinding chamber.
It is also regarded as advantageous if the extended recess is constituted as a flow channel. Through a suitably selected cross-section of the channel for example, the distribution of the auxiliary grinding bodies can thus be influenced in an advantageous way.
The flow channel can be introduced into the agitator shaft at least in sections as a groove or as an axial bore. It is for example also conceivable that the flow channel is introduced into the agitator shaft as a bore in an axial region close to the separating device and is constituted as a groove in a section close to the product inlet. The auxiliary grinding bodies are thus conveyed in the axial direction through a flow channel and only exit again close to the product inlet into the grinding chamber.
According to a preferred development, the number of flow channels corresponds to the number of the recesses of the separating device. The uniform distribution of the auxiliary grinding bodies is further improved by the plurality of flow channels distributed over the circumference of the agitator shaft. In this regard, it is also viewed as advantageous if the flow channels run parallel with one another.
According to the invention, the grinding process in the grinding chamber is improved by the fact that the auxiliary grinding bodies can additionally flow into the grinding chamber through a section of the agitator shaft coupled with the separating device. Without the inventive coupling with the separating device, experience shows that an increased concentration of the auxiliary grinding bodies in the vicinity of the separating device occurs during the grinding process, the effect of which is that the concentration of auxiliary grinding bodies falls in the region of the agitator shaft. The aim, however, is to achieve a distribution of the auxiliary grinding bodies that is as uniform as possible in the grinding chamber so that the grinding process can proceed effectively.
During the operation of the agitator ball mill, a material to the ground, for example in liquid form, is conveyed continuously via an inlet channel into the interior of the grinding chamber and is conveyed in the latter together with the auxiliary grinding bodies to the product outlet. The auxiliary grinding bodies are separated from the grinding stock in the region of the product outlet by means of the separating device and the grinding stock is conveyed out of the grinding container via the outlet channel. In contrast with the known methods, the auxiliary grinding bodies, proceeding from the separating device, flow along the agitator shaft back into the grinding chamber due to the fact that the resistance to the auxiliary grinding bodies, caused by the continuously conveyed grinding stock, is reduced on account of the inventive embodiment of the separating device and the agitator shaft.
The exit point or exit region of the auxiliary grinding bodies is preferably adjusted by adjusting and coordinating the speed of the agitator shaft, the cross-sectional shape of the return channels and/or the orientation of the extending recess in the agitator shaft. The adjustment and coordination can take place manually or in an automated manner by means of a control loop. Since the exit point is also dependent, amongst other things, on the throughput rate and therefore the flow rate, which can change from grinding process to grinding process depending on the given task and requirements on the grinding outcome, said exit point should be adaptable. For example, it has been shown that the exit point with a comparatively high throughput rate can be displaced in a disadvantageous way in the direction of the separating device. By a suitable choice of the speed of the agitator shaft and/or the embodiment of the return channels, the displacement of the exit point can be counteracted.
For the method according to the invention, the agitator shaft comprises at least one recess extending in the axial direction, which is assigned to a dynamic separating device. The recess is preferably constituted as a flow channel and suitably leads auxiliary grinding bodies back into the grinding chamber. In particular, the agitator shaft comprises on the separating-device side an end portion with which a connection of the flow channel with at least one recess of the separating device can be produced.
The dynamic separating device can be driven both by the agitator shaft as well as by means of a separate device. The separating device is constituted such that the mixture constituted by the auxiliary grinding bodies and the ground and/or dispersed stock can flow via the recesses of the separating device to the product outlet. During flowing into the recess, a part of the rotation energy is transmitted to the auxiliary grinding bodies, after which the grinding bodies used for the grinding are separated from the grinding stock on account of the radially acting centrifugal force and the different density and are conveyed back into the interior of the grinding chamber. The grinding stock itself passes through the separating device and leaves the grinding chamber via the outlet channel.
As a result of the rotation of the dynamic separating device, the grinding stock, as it flows through the separating device against the centrifugal force, has to overcome a relative pressure, said pressure being generated by a feed pump which is connected to the inlet channel of the agitator ball mill. On the other hand, the auxiliary grinding bodies have to be transported back in the direction of the grinding chamber against the flow generated by the feed pump, which in the case of the known agitator ball mills usually leads to an accumulation of the auxiliary grinding bodies in the region of the separating device. As a result of the inventive recesses in the agitator shaft running axially into the grinding chamber, the auxiliary grinding bodies can take an evasive route via these recesses. The flow of grinding stock on the one hand and of the auxiliary grinding bodies on the other hand acting radially from both sides leads to a flow of the auxiliary grinding bodies in the extended recesses back into the grinding chamber, preferably into a region of the agitator shaft that is particularly effective for grinding.
The extended recess in the agitator shaft is preferably introduced into the agitator shaft as a flow channel in the form of a groove and/or a bore. This thus makes it possible for the auxiliary grinding bodies to flow in a specific direction and for the auxiliary grinding bodies not to exit out of the agitator shaft until they are at a specific point, for example by a suitable combination of groove and bore.
In a further preferred embodiment, at least one radially running longitudinal wall of the flow channel is angled, in such a way that, in addition to the centrifugal force, a further radial force component created by the angled channel wall acts on the auxiliary grinding bodies in the flow channel. An accumulation of the auxiliary grinding bodies, for example, can thus be prevented by the fact that the auxiliary grinding bodies leave the flow channel again relatively quickly. Due to the increased radial acceleration of the auxiliary grinding bodies resulting therefrom, the latter are conveyed farther into the grinding chamber in the radial direction, which contributes towards an improved distribution of the auxiliary grinding bodies in the cross-section of the grinding chamber. It is however also conceivable for at least one channel wall to run helically in the axial direction in order for example to allow the auxiliary grinding bodies not to exit again until they are at a specific region of the grinding chamber or to do so in an intensified manner.
In an alternative or additional advantageous development, the grinding elements of the agitator shaft are constituted as grinding discs and comprise at least one opening close to the centre, said opening being introduced into the grinding disc as a through-going recess. Distance bushings are disposed between the grinding discs. The grinding discs are axially braced with the distance bushings and form the agitator which is followed by the dynamic separating device. The return channel runs axially through the openings in the grinding discs.
The distance bushings preferably have a polygonal cross-section, in particular a square cross-section. The distance bushings can however also have another cross-section. It should however be noted that the cross-section of the distance bushing is not circular, because otherwise the desired pumping effect in the radial direction is not achieved.
The opening in the grinding discs is introduced close to the centre in such a way that auxiliary grinding bodies flowing through the opening close to the centre are picked up by the distance bushings, accelerated and transported radially outwards. The distance bushings are preferably constituted such that their edges sweep at least partially, particularly preferably completely over the opening area when the agitator shaft is rotating.
In addition, the grinding discs can advantageously comprise radial recesses. The latter serve primarily to activate the auxiliary grinding bodies, but can also enable an additional return flow of the auxiliary grinding bodies in accordance with the invention.
The advantages achieved with the invention lie in particular in the fact that the auxiliary grinding bodies in the region of the separating device can take an evasive route through the return channels, as a result of which a local accumulation of the auxiliary grinding bodies is prevented. The uniform distribution of the auxiliary grinding bodies that is sought for an effective grinding process can be achieved by the recesses running axially into the grinding chamber. In addition, an adaptation of the distribution of the auxiliary grinding bodies to the given grinding task can be made by the described design adaptations of the agitator shaft and/or of the grinding parameters such as speed and through-flow rate. A further advantage results from the fact that the advantageous effect is essentially based on the special embodiment of the agitator shaft. An agitator ball mill can thus also be modified with corresponding design requirements and/or suitable adapter components.
Embodiments of the present invention are described by way of example by reference to the appended drawings. In the figures:
Agitator ball mill 2 according to
A static separating device constituted as a sieve 22 is disposed upstream of a product outlet channel 20. Groove-shaped recesses 18 in agitator shaft 8 run axis-parallel with the rotational axis of agitator shaft 8 and form return channels 18 for the auxiliary grinding bodies. Return channels 18 and recesses 16 in separating device 14 merge into one another, so that the auxiliary grinding bodies can take an evasive route via return channels 18 in the direction of the product inlet during operation of mill 2, arrive back in the grinding chamber and thus become distributed.
Agitator ball mill 2 is designed in such a way that the stock to the ground is conveyed continuously into grinding container 4 via inlet channel 12 by means of a pump not represented here and flows in grinding chamber 10 together with auxiliary grinding bodies axially in the direction of outlet channel 20 and is thereby ground. In the region of separating device 14, the grinding stock flows with the grinding bodies through recess 16 in separating device 14. The grinding stock leaves grinding container 4 via outlet channel 20 and the auxiliary grinding bodies are moved radially outwards on account of the centrifugal forces acting on the auxiliary grinding bodies due to rotating separating device 14. The continuously conveyed grinding stock/auxiliary grinding body mixture, however, flows from outside coming from grinding chamber 10 into recess 16 of separating device 14, for which reason the return flow of the auxiliary grinding bodies is hindered. As a result of this, the auxiliary grinding bodies flow into return channel 18 in agitator shaft 8 and are then further accelerated by likewise rotating agitator shaft 8 and conveyed back into grinding chamber 10.
An agitator ball mill 2 with a separating device 14 as represented in
Agitator ball mill 2 with an agitator shaft 8 with return channels 18 running in a helical manner in the axial direction, said return channels being introduced as a groove into agitator shaft 8, is represented in
Return channel 18 could however also be introduced in a helical form continued over the separating device 14. Such an embodiment is represented in
Grinding discs 38 as grinding elements with at least one opening 40 close to the centre are represented in
Each grinding disc 38 in
It has been shown in practice that, as a result of the arrangement of openings 40 close to the centre, the auxiliary grinding bodies are transported particularly effectively back into the grinding chamber.
A grinding disc 38 with a distance bushing 42 with a square cross-section is represented in
Agitator ball mill 2 is specifically aimed at an effective distribution of the auxiliary grinding bodies in grinding chamber 10. Due to the fact that the auxiliary grinding bodies are conveyed in the axial direction along agitator shaft 8 from separating device 14 back into grinding chamber 10, an increased concentration of auxiliary grinding bodies in the region of separating device 14 is prevented.
Furthermore, unground product that flows close to the centre along agitator shaft 8 from the inlet region of agitator ball mill 2 in the axial direction towards separating device 14 is also conveyed in the radial direction back into grinding chamber 10, into an outer more effective grinding region. In the case of an agitator ball mill 2 with grinding discs 38, this effect becomes particularly marked in the case of grinding discs 38 with a radial recess 48, since unground product can flow back close to the centre in the axial direction in particular through recesses 48 in grinding disc 38. The risk of unground product thus passing into outlet channel 20 is minimised by the pumping effect of distance bushings 42.
Number | Date | Country | Kind |
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102013107190.2 | Jul 2013 | DE | national |
Number | Date | Country | |
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Parent | 14978763 | Dec 2015 | US |
Child | 16534476 | US | |
Parent | PCT/DE2014/000330 | Jun 2014 | US |
Child | 14978763 | US |