The invention relates to an agitator mill according to the preamble of claim 1.
Such an agitator mill is known from EP 0 370 022 B1 (corresponding to U.S. Pat. No. 5,062,577). In this agitator mill, the auxiliary grinding bodies are centrifuged from the flow of grinding stock and auxiliary grinding bodies via the auxiliary-grinding-body return conduits before said flow reaches the protective screen. The basic function of the protective screen is to collect worn-out auxiliary grinding bodies which are too light to be thrown out via the auxiliary-grinding-body return conduits, thus serving as a throttle device for generating a counter-pressure counteracting the flow of grinding stock. The agitator is provided with agitator implements protruding into the exterior grinding chamber. When using extremely small auxiliary grinding bodies, it is not ensured that the auxiliary grinding bodies will not eventually reach the protective screen, thus gradually clogging the latter. In particular when using extremely small auxiliary grinding bodies, it is required to use correspondingly fine protective screens which in turn may be damaged very easily, should they be hit by auxiliary grinding bodies. If, however, relatively viscous grinding stocks are to be treated by using auxiliary grinding bodies of a usual size, a partially clogged protective screen leads to a substantial pressure build-up in the agitator mill, which also results in a disturbance of the grinding process.
An agitator mill is known from EP 0 504 836 B1 which has a cup-shape rotor disposed in a cylindrical housing, said rotor being provided with passage slots along the length thereof. An interior stator comprising a protective screen is disposed within the rotor. The exterior grinding chamber is provided with implements that are fixed to both the rotor and the wall de-limiting the grinding chamber. This agitator mill is not suitable for the use of extremely small auxiliary grinding bodies. Moreover, said mill is subject to the same problems as already described above.
An agitator mill is known from DE 34 37 866 A1 (corresponding to U.S. Pat. No. 5,011,089), said agitator mill having a rotor with paddle-shaped implements disposed on the outside thereof. A protective screen is disposed within the rotor. The rotor is composed of axially parallel bars to which the paddle-shaped implements are fastened. The grinding stock is supplied radially. Owing to the paddle-shaped design of the agitator implements, this agitator mill ensures a concentration of auxiliary grinding bodies to be obtained in the area of the receptacle wall; a defined grinding, in particular by means of extremely small auxiliary grinding bodies as well as a reliable separation of the auxiliary grinding bodies without the risk of operational failures is however not obtainable either. Since the grinding stock flows through the packing of auxiliary grinding bodies in a radial direction, the grinding stock is subject to a grinding process over a very short distance only. Accordingly, if the grinding stock passes through the agitator mill only once, only a moderate grinding progress is obtained.
An agitator mill of the generic type is known from DE 196 38 354 A1 (corresponding to U.S. Pat. No. 5,894,998), said agitator mill having a protective screen fixed to the cup-shaped rotor which is sealed against the interior stator by means of a mechanical seal. The protective screen thus co-rotates with the rotor, thereby ensuring that auxiliary grinding bodies reaching said filter are thrown out even more efficiently.
It is the object of the invention to develop an agitator mill of the generic type in a way as to obtain a grinding and disperging effect with a narrow particle distribution even if the grinding stock passes through the agitator mill only once, in particular when using auxiliary grinding bodies having an extremely small diameter, whilst avoiding the risk of operational failures, caused in particular by auxiliary grinding bodies hitting the protective screen.
This object is attained according to the invention by the features in the characterizing part of claim 1. The crux of the invention is that auxiliary grinding bodies are only located in the grinding chamber between the rotor and the receptacle wall and are concentrated in said grinding chamber. Concentrating the auxiliary grinding bodies in said grinding chamber already ensures that said auxiliary grinding bodies do not enter the grinding-stock discharge conduit. Fastened to the rotor, the implements extend as far as into the vicinity of the receptacle wall, thereby ensuring that the auxiliary grinding bodies are accelerated outward and concentrated together. The grinding stock flows through the close-packed grinding stock in the axial direction so as to obtain a uniform grinding and dispersion. Along with the measures for concentrating auxiliary grinding bodies in the annular exterior grinding chamber, devices are provided for effectively preventing the auxiliary grinding bodies from reaching the protective screen. The grinding-stock discharge conduit, which is located within the rotor and is defined by the rotor and the interior stator, contains no or only very few auxiliary grinding bodies, thereby effectively eliminating the drawbacks described above.
The measures according to claims 2 to 4 contribute to a concentration of the auxiliary grinding bodies in the grinding chamber.
The measures according to claims 5 to 7 further help to prevent the auxiliary grinding bodies from entering the deflection conduit.
The development according to claim 8 prevents the few auxiliary grinding bodies that do reach the grinding-stock discharge conduit from depositing, thereby causing them to remain in the flow towards the auxiliary-grinding-body return conduits where they are re-supplied into the beginning of the grinding chamber. The measures according to claim 9 ensure that the auxiliary grinding bodies are furthermore accelerated in the direction of the auxiliary-grinding-body return conduits.
The development according to claim 10 prevents a layer of grinding stock and auxiliary grinding bodies from forming at the inside of the rotor that no longer takes part in the process.
The development according to claim 11 is particularly advantageous in conjunction with the measures according to claims 8 to 10 owing to the particularly intensive cooling of in particular temperature-sensitive grinding stock in the grinding-stock discharge conduit without requiring any additional supply of energy, said grinding stock thus being subject to high energy only during the actual grinding process in the grinding chamber.
The embodiment according to claim 12 enables auxiliary grinding bodies present in the grinding-stock discharge conduit to be directly thrown outward into the grinding chamber, this effect being promoted by the development according to claim 13.
Appropriate diameter ranges for extremely small auxiliary grinding bodies are stated in claim 14.
Further features, advantages and details will become apparent from the ensuing description of embodiments of the invention, taken in conjunction with the drawing, in which
The agitator mill shown in
As can be seen in particular from
The grinding receptacle 2 has an upper annular flange 14 by means of which it is fastened to the underside of a support housing 15 by means of screws 16, said support housing 15 being fixed to the stand 1 of the agitator mill. The grinding chamber 8 is closed by a lid 17. The support housing 15 has a central bearing and sealing housing 18 which is aligned coaxially with the central longitudinal axis 19 of the grinding receptacle 2. This bearing and sealing housing 18 is penetrated by the drive shaft 6 which also extends coaxially with the axis 19 and is provided with an agitator 20.
A grinding-stock supply line 21 projects into the area of the bearing and sealing housing 18 neighbouring the grinding chamber 8.
An approximately cup-shaped, cylindrical interior stator 22 projecting into the grinding chamber 2 is disposed on the bottom plate 12, said interior stator 22 having an outer wall 23 aligned coaxially with the axis 19 and a cylindrical inner casing 24 within said outer wall 23. Between each other, the outer wall 23 and the inner casing 24 define a cooling chamber 25 of the interior stator 22. The cooling chamber 25 is supplied with cooling water via a cooling-water supply connector 26, said cooling water being discharged via a cooling-water discharge connector 27. The cooling chamber 11 of the grinding receptacle 2 is supplied with cooling water via a cooling-water supply connector 28, said cooling water being discharged via a cooling-water discharge connector 29.
As shown in the drawing, a protective screen 30 is disposed at the upper end of the interior stator 22, said protective screen 30 being connected to a grinding-stock discharge line 31. In the area of the bottom plate 12, the discharge line 31 is provided with a handle 32 which is detachably connected to the bottom plate 12 by means of screws 33.
The protective screen 30 is sealed against the interior stator 22 by means of a seal 34 and may be, together with the discharge line 31, pulled downwards out of the interior stator 22 after loosening the screws 33.
The agitator 20 has a cup-shaped basic structure, thus having a substantially annular cylindrical rotor 35. The agitator 20 has a lid-type closing member 36 of the rotor 35 at the upper end thereof. An auxiliary-grinding-body return device 37 is disposed in the agitator 20, strictly speaking in the transition area between the lid-type closing member 36 and the annular cylindrical, i.e. tubular, rotor 35.
The following applies to the radial width a of the grinding chamber 8: a=(D9−D35)/2, with D9 being the diameter of the receptacle wall 9, i.e. the external diameter of the grinding chamber 8, and with D35 referring to the external diameter of the rotor 35, i.e. the internal diameter of the ding chamber. The following applies:
0.6≦D35/D9≦0.95, and preferably, 0.7≦D35/D9≦0.85.
The inside of the receptacle wall 9 is cylindrically smooth, having no implements projecting into the annular grinding chamber 8. On the other hand, the outside of the equally cylindrical rotor 35 is provided with peg-style implements 38 radially projecting into the grinding chamber 8 with respect to the central longitudinal axis 19. Said implements 38 almost extend as far as the receptacle wall 9, thus only leaving a gap 39 determined by construction and having a gap width b. As can be seen from
In a second area 45 below the first area 40, the implements 38 are disposed along a second helical curve 46 extending in the opposite direction, with the momentum thus imparted to the auxiliary grinding bodies 43 being directed opposite to the direction of flow 44 of the grinding stock when the agitator 20 is driven in the direction of rotation 42. As can be seen from
An annular cylindrical grinding-stock discharge conduit 47 is formed between the rotor 35 and the outer wall 23 of the interior stator 22. The outer wall 23 of the interior stator 22 is provided with peg-style wiper elements 48 radially projecting outwards into the discharge conduit 47. As can be seen from
The following applies to the gap width b of the gap 39 in relation to the diameter c of the auxiliary grinding bodies 43: 4c≦b≦6c, with a minimum marginal condition of 1.0 mm≦b≦2.0 mm being defined for the use of particularly small auxiliary grinding bodies 43. Correspondingly, the following applies to the gap width e of the gap 49 in relation to the diameter c of the auxiliary grinding bodies 43: 4c≦e≦6c, with the minimum marginal condition of 1.0 mm≦e≦2.0 mm equally applying to the use of extremely small auxiliary grinding bodies. This design enables the implements 38 to constantly swirl the packing of auxiliary grinding bodies in the grinding chamber 8. When driven, the rotor 35 is uniformly wiped by the wiper elements 48 owing to the small gap width e. When using auxiliary grinding bodies 43 of an extremely small diameter c, i.e. micro-auxiliary grinding bodies, the following applies to the diameter c thereof: 20 μm≦c≦100 μm.
The discharge conduit 47 has a radial width f to which applies: f=(d35−d23)/2, with d35 referring to the internal diameter of the rotor 35, i.e. the external diameter of the discharge conduit 47, and d23 referring to the external diameter of the interior stator 22, i.e. the internal diameter of the discharge conduit 47. The following applies: 0.8≦d23/d35≦0.98, and preferably 0.9≦d23/d35≦0.98. The grinding chamber 8 is connected to the discharge conduit 47 by means of a deflection conduit 50, the width thereof approximately equalling that of the discharge conduit 47, as can be seen from
As indicated in
As can be seen from
When flowing through the grinding chamber 8 in the direction of flow 44, the grinding stock flows downward from the grinding-stock supply line 21 through a grinding-stock supply chamber 58 disposed between the closing member 36 of the agitator 20 and the lid 17, the first area 40 and the second area 45 of the grinding chamber 8 before flowing radially inward via the deflection conduit 50 and from there, upward into a discharge conduit 59 via the grinding-stock discharge conduit 47, said discharge conduit 59 being formed between the closing member 36 and the interior stator 22 and substantially extending radially inward towards the protective screen 30. Afterwards, the grinding stock passes through the protective screen 30 to enter the grinding-stock discharge line 31 through which it is discharged from the agitator mill.
When passing through the grinding chamber 8, the grinding stock is ground due to the rotating agitator 20 in cooperation with the auxiliary grinding bodies 43. An amount of tangential momentum is imparted to the auxiliary driving bodies by the implements 38, thereby moving them in the direction of the receptacle wall 9. As indicated in the drawing, this causes the auxiliary grinding bodies 43 to be concentrated in the radially outer area of the grinding chamber 8. The small width b of the gap 39 between the implements 38 and the receptacle wall 9 prevents auxiliary grinding bodies 43 from depositing at the receptacle wall 9; even auxiliary grinding bodies 43 that have moved there are activated and entrained over and over again. The already described arrangement of implements 38 along the two helical curves 41 and 46 prevents the auxiliary grinding bodies 43 in the upper first area 40 from flowing back into the grinding-stock supply line 21 via the grinding-stock supply chamber 58. The arrangement of the agitator implements in the second area 45 prevents auxiliary grinding bodies 43, or at least most of them, from entering the discharge conduit 47 via the deflection conduit 50. This gives rise to a turbulent flow in the grinding chamber 8 characterized by strongly interacting vortices within the grinding stock when flowing through the grinding chamber 8, thereby preventing a linear movement thereof. This causes the individual grinding-stock particles to alternately flow from the rotor 35 to the receptacle wall 9 and vice versa. In the direction of flow 44, the throughput of the agitator mill is superimposed on this radially reciprocating flow, with the magnitude of the velocity component in the direction of flow 44 being obtained from the volumetric throughput of grinding stock per unit of time and the free cross-section of the grinding chamber 8, strictly speaking the cross-section of the grinding chamber 8 minus the cross-section of the available auxiliary grinding bodies 43.
If auxiliary grinding bodies 43 do manage to enter the grinding-stock discharge conduit 47 despite the described measures, they are transported through the entire discharge conduit 47 together with the grinding stock by means of the wiper elements 48 before being returned into the first area 40 of the grinding chamber 8 via the return device 37.
The embodiment according to
As can be seen from the true length of the inside of the rotor 35′ shown in
The embodiment according to
The agitator mill according to
The embodiment according to
The closing wall 71 of said protective screen 30″ opens towards the front wall 70 in the shape of a truncated cone, thereby defining an annular gap 73 at the radially outer area thereof facing towards the front wall 70, said annular gap 73 allowing virtually no auxiliary grinding bodies 43 to enter when the agitator mill is in use. Auxiliary grinding bodies 43 that may have entered this area during standstill are thrown outward again through the annular gap 73 so as to enter the auxiliary-grinding-body return conduits 55.
In this embodiment, the protective screen 30″, together with the foil or piece of sheet metal 63 thereof, respectively, is also perfectly aligned with the auxiliary-grinding-body return conduits 55 in the axial direction. In case any auxiliary grinding bodies 43 do manage to enter the area of the protective screen 30″, they are also thrown into the return conduits 55 by the foil or piece of sheet metal 63, respectively, forming the cylindrical circumference thereof.
Although each of the previously described embodiments shows agitator mills having a vertical central longitudinal axis 19, the described embodiments may easily be fitted in a horizontal position or in an intermediate position.
In case of using auxiliary grinding bodies 43 of an extremely small diameter c, i.e. micro-auxiliary grinding bodies, the grinding stock has a very low viscosity in the range of 1 to 100 mPas.
Filing Document | Filing Date | Country | Kind | 371c Date |
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PCT/EP2005/010910 | 10/11/2005 | WO | 00 | 12/9/2008 |