1. Field of the Invention
The present invention relates to a method of grinding a back-side surface of a wafer such as a semiconductor wafer so as to thin the wafer.
2. Description of the Related Art
In a semiconductor device manufacturing process in which a face-side surface of a wafer composed of a semiconductor such as silicon is provided with a multiplicity of devices and the wafer is divided to obtain the devices as individual chips, a step of grinding the back-side surface of the wafer so as to thin the wafer is conducted at the stage of wafer. The thinning of the wafer corresponds to thinning of device packages, and the wafer is thinned, for example, from an initial thickness of around 700 μm to about 200 μm. In accordance with the marked thinning nowadays, the wafers may in some cases be thinned to a very small thickness of 50 μm or 30 μm.
For grinding the back-side surface of a wafer, infeed grinding is generally used in which the wafer is suction held onto a vacuum chuck type chuck table, and, while revolving the wafer about its center by rotating the chuck table, a grinding tool such as a grindstone is pressed against the back-side surface of the wafer. In the case of grinding the back-side surface of a wafer in this manner, the face-side surface of the wafer is covered with a protective member so that the face-side surface does not make direct contact with the holding surface of the chuck table, in order to prevent electronic circuits of the devices from being damaged (refer to Japanese Patent Laid-open No. 2005-057052).
Examples of the protective member include a protective tape obtained by applying an acrylic pressure sensitive adhesive material to one side of a base sheet made of polyolefin or the like. In such a protective tape, in many cases, at least one of the base sheet and the pressure sensitive adhesive material has unevenness, if slight, in the thickness thereof. If such a protective tape is adhered to the face-side surface of the wafer and the back-side surface of the wafer is ground, the unevenness of thickness of the protective tape would be transferred to the wafer, resulting in unevenness of thickness of the wafer as a single body. If the finished thickness of the wafer is comparatively large and the unevenness of thickness of the protective tape is as tiny as about 3 μm, for example, the ratio of the thickness unevenness to the wafer thickness after grinding is so small as not to matter considerably. If the finished thickness of the wafer is as extremely small as about 30 μm, however, the thickness unevenness of 3 μm is as large as 10% of the wafer thickness and, therefore, it is difficult to make uniform the wafer thickness with high precision.
The above-mentioned patent document discloses a protective film formed by applying a fluid resist to the back-side surface of a wafer by a spin coating process or a printing process. However, even such a protective film has unevenness of thickness, so that the protective film is not superior to the protective tape from the viewpoint of thickness unevenness.
Accordingly, it is an object of the present invention to provide a method of grinding a back-side surface of a wafer by which the unevenness of thickness of a wafer as a single body due to the thickness unevenness of a protective member in the prior art can be suppressed and a wafer with a uniform thickness can be obtained in high precision.
In accordance with an aspect of the present invention, there is provided a method of grinding a back-side surface of a wafer having a face-side surface provided with devices, the method including: a resin film covering step of covering the face-side surface of the wafer with a resin film; and a wafer holding step of holding the wafer, with the face-side surface exposed, by a holding means of a cutting apparatus of which the facing angle relative to a machining plane of a cutting member held by a rotating body can be controlled to be substantially parallel. The method further includes: a wafer angle controlling step of regulating the facing angle of the holding means relative to the cutting member so as to control the face-side surface of the wafer held by the holding means to be substantially parallel to the machining plane of the cutting member; a resin film cutting step of cutting a surface of the resin film to be flat by the cutting member being rotated; and a back-side grinding step of holding the wafer by a holding means of a grinding apparatus with the cut surface of the resin film being directed downward and grinding the exposed back-side surface of the wafer.
The resin film covering the face-side surface of the wafer is provided by applying a liquid resin to the face-side surface of the wafer by a spin coating process, or by adhering a pressure sensitive adhesive tape to the face-side surface of the wafer.
In the present invention, in the wafer angle controlling step the face-side surface of the wafer held by the holding means of the cutting apparatus is controlled to be substantially parallel to the machining plane of the cutting member, whereby it is ensured that when the surface of the resin film is cut in the subsequent resin film cutting step, the cut surface becomes a flat surface parallel to the face-side surface of the wafer. When the resin film has unevenness of thickness, the thickness unevenness is suppressed by cutting the surface of the resin film. When the wafer is held by the holding means of the grinding apparatus with the cut surface of the resin film being directed downward and the back-side surface of the wafer which is exposed in this condition is ground, the ground back-side surface is processed to be a flat surface parallel to the face-side surface of the wafer. In other words, the wafer subjected to back grinding becomes uniform in thickness.
In the back grinding step, the resin film is kept by the holding means of the grinding apparatus, and the face-side surface of the wafer does not make direct contact with the holding surface of the holding means, so that the devices are protected.
According to the present invention, instead of using the protective film in the related art which is accompanied by unevenness of thickness, the face-side surface of the wafer is covered with the resin film, the surface of the resin film is cut to form a reference surface parallel to the face-side surface of the wafer, and the surface of the resin film is kept by the holding means of the grinding apparatus, which ensures that the wafer as a single body after the back grinding is uniform in thickness. The resin film after the cutting is a protective member free of thickness unevenness, and its surface serves as an appropriate reference surface in back grinding. Therefore, with the resin film provided on the face-side surface of the wafer, the thickness unevenness of the wafer after the back grinding can be suppressed.
According to the present invention, the surface of the resin film covering the face-side surface of the wafer is cut to be a flat surface parallel to the face-side surface of the wafer, the surface of the resin film is kept by the holding means of the grinding apparatus, and, in this condition, the back-side surface of the wafer is ground. Therefore, the thickness unevenness of the wafer as a single body due to the thickness unevenness of the protective member in the related art can be suppressed, resulting in that a wafer with a uniform thickness can be obtained in high precision.
The above and other objects, features and advantages of the present invention and the manner of realizing them will become more apparent, and the invention itself will best be understood from a study of the following description and appended claims with reference to the attached drawings showing some preferred embodiments of the invention.
Now, a method of grinding a back-side surface of a wafer according to an embodiment of the present invention will be described below referring to the drawings. Symbol 1 in
The method of grinding a back-side surface of a wafer according to this embodiment includes, as shown in
As above-mentioned, in this embodiment, first, the face-side surface 1a of the wafer 1 is covered with the resin film 5 having a thickness (for example, 5 to 100 μm or more) according to the rugged (projection-and-recess) state of the face-side surface 1a (resin film covering step). The resin film 5 is formed, for example, by using a photo-resist (a film of a photosensitive resin) known in the photolithography technique. For covering the face-side surface 1a of the wafer 1 with the resist, a spin coating process is preferably adopted in which the wafer 1 is mounted and held on a table driven to rotate in such a manner that the face-side surface 1a is exposed and the center of the wafer 1 is located on the rotational axis of the table, the table 1 is rotated, and the resist in a liquid state is dropped onto the center of the wafer 1 being rotated so that the resist is distributed under the centrifugal force to the whole area of the face-side surface 1a. The resin film 5 thus formed is shown on the face-side surface 1a of the wafer 1 in
The wafer 1 having its face-side surface 1a covered with the resin film 5 is then subjected to a process in which the surface 5a of the resin film 5 is cut to be flat. For the cutting, a cutting apparatus 10 shown in
Now, the configuration and operations of the cutting apparatus 10 will be described below. The cutting apparatus 10 has a rectangular parallelopiped base 11, and a plurality of the wafers 1 are stackedly contained in a supply cassette 12 detachably set at a predetermined position on the base 11 so that the face-side surface 1a covered with the resin film 5 of each of the wafers 1 is on the upper side. One of the wafers 1 is drawn out of the supply cassette 12 by a feeding robot 13, and the wafer 1 is put on a positioning table 14 with its face-side surface 1a up, where it is positioned into a predetermined position.
The wafer 1 thus positioned on the positioning table 14 is picked up from the positioning table 14 by a supply arm 15, and is concentrically put on a circular disk-shaped chuck table 20 being in vacuum operation, with its face-side surface 1a up (wafer holding step). As shown in
As shown in
In the cutting unit 30, the cutting tool 37 for actually cutting the resin film 5 is rotated in a horizontal plane, so that the cutting or machining plane formed by the rotational locus of a cutting part at the tip of the cutting tool 37 is also horizontal. The chuck table 20 is so configured that the frame body 21 is swingably supported on the table base 25, whereby the facing angle of the suction surface 22a relative to the cutting or machining plane of the cutting tool 37 can be controlled in the following manner.
As shown in
As shown in
With the first movable shaft 40B and the second movable shaft 40C rotated, the movable shaft attaching parts of the frame body 21 are lifted up or down according to the directions of rotation, whereby the chuck table 20 as a whole is swung, with the pivot 41 of the fixed shaft 40A as a fulcrum. In the chuck table 20, the state with the suction surface 22a kept horizontal is a fundamental posture, and the chuck table 20 is swung by appropriately operating the two movable shafts 45B and 45C, whereby the facing angle of the suction surface 22a relative to the cutting unit 20 can be varied.
The cutting unit 30 is disposed at a front surface of a column 16 erecting at an end part on the depth side of the base 11 so that it can be lifted up and down along the Z direction (vertical direction). More specifically, a guide 51 extending in the Z direction is provided on the front surface of the column 16, and the cutting unit 30 is slidably mounted to the guide 51 through a slider 52. The cutting unit 30 is lifted up and down in the Z direction through the slider 52, by a ball screw type feeding mechanism 54 driven by a servo motor 53.
The cutting unit 30 has a structure in which a spindle shaft 32 shown in
The cutting implement 35 has the cutting tool 37 detachably attached to the lower surface of the annular frame 36 through a shank 38, and the frame 36 is so designed to be coaxially attached to the flange 34. The cutting tool 37 is provided at its lower end with the cutting part which is formed of diamond or the like and operative to actually cut a work. The cutting implement 35 is rotated as one body with the spindle shaft 32, and the outer diameter of cutting of the cutting tool 37 is set to be greater than the diameter of the wafer 1. The cutting or machining plane formed by the rotational locus of the cutting part at the tip of the cutting tool 37 is set to be horizontal, as above-mentioned.
In cutting the resin film 5 by the cutting unit 30, in the loading/unloading position the suction surface 22a of the chuck table 20 is controlled to be horizontal, and the facing angle of the suction surface 22a relative to the cutting or machining plane of the cutting tool 37 is set to be parallel (wafer angle controlling step). Since the wafer 1 is uniform in thickness, the result of controlling the suction surface 22a to be horizontal is that the face-side surface 1a (the surface covered with the resin film 5) of the wafer 1 held on the suction surface 22a is set to be parallel to the cutting or machining plane of the cutting tool 37, i.e., set to be horizontal. In this embodiment, the step of thus setting the face-side surface 1a of the wafer 1 in parallel to the cutting or machining plane of the cutting tool 37 is the wafer angle controlling step.
If the wafer 1 is uniform in thickness, the wafer angle controlling step is achieved by merely setting the suction surface 22a of the chuck table 20 to be horizontal as above-mentioned. However, in the case where the thickness of the wafer 1 varies to the outside of an allowable range of evenness (for example, where a thickness unevenness of not less than 3 μm is present), the face-side surface 1a of the wafer 1 would not become parallel to the cutting or machining plane of the cutting tool 37 even if the suction surface 22a of the chuck table 20 is set to be horizontal. In this case, it suffices to grasp the condition of the thickness unevenness of the wafer 1 at the stage before covering with the resin film 5, and, based on the grasped condition, to properly incline the chuck table 20 so as to make horizontal the face-side surface 1a of the wafer 1 held by the chuck table 20, thereby controlling the above-mentioned facing angle.
Grasping the thickness unevenness condition of the wafer 1 can be achieved by measuring the thickness of the wafer 1 at a plurality of positions (for example, at three positions), with the notch 4 in the wafer 1 as a reference position. To control the facing angle by holding the wafer 1 on the chuck table 20, it suffices to incline the chuck table 20 so that the face-side surface 1a of the wafer 1 becomes horizontal, with the notch 4 as a reference.
After the face-side surface 1a of the wafer 1 is thus set to be horizontal, i.e., set to be parallel to the cutting or machining plane of the cutting tool 37, the surface 5a of the resin film 5 is cut to be flat by the cutting tool 37 of the cutting unit 30 (resin film cutting step). For performing this step, the cutting unit 30 is lowered by the feeding mechanism 54 to such a height that the height of the tip of the cutting part of the cutting tool 37 is set to a height for cutting the resin film 5 by a predetermined amount (for example, about 1 to 10 μm), and, further, the cutting implement 35 is put into rotation. Then, the table base 25 is moved toward the depth side, thereby gradually moving the wafer 1 toward the machining position. Attended with the movement, as shown in
At the time when the wafer 1 has been moved until covered with the frame 36, the whole area of the surface 5a of the resin film 5 has been cut to be flat. When the resin film 5 has been cut by a required amount at this stage, the resin film cutting step is finished. On the other hand, where the required cutting amount has not yet been attained, the table base 25 is reciprocated so that the cutting tool 37 is made to act on the surface 5a of the resin film 5 a plurality of times.
After the whole area of the surface 5a of the resin film 5 is cut by the required amount, the cutting unit 30 is raised to retract from the wafer 1, whereas the table base 25 is returned into the loading/unloading position. At the loading/unloading position, the vacuum operation of the chuck table 20 is stopped. Then, the wafer 1 is fed by a recovery arm 17 to a spinner type cleaning apparatus 18, where it is cleaned and dried. Thereafter, the wafer 1 is fed by the feeding robot 13 to, and contained into, a recovery cassette 19. Besides, the chuck table 20 from which the wafer 1 has been unloaded is cleared of cuttings and the like by air jetted from an air nozzle 27.
After the surface 5a of the resin film 5 is cut and the surface 5a is machined to be parallel to the face-side surface 1a of the wafer 1 in the above-mentioned manner, the back-side surface 1b of the wafer 1 is then ground to thin the wafer 1 to a desired thickness. For the back grinding of the wafer 1, a grinding apparatus 60 for performing infeed grinding shown in
Now, the configuration and operations of the grinding apparatus 60 will be described below. The grinding apparatus 60 has a rectangular parallelopiped base 61, and a plurality of the wafers 1 are stackedly contained in a supply cassette 62 detachably set at a predetermined position on the base 61, with the face-side surface 1a of each of the wafers 1 up. One of the wafers 1 is drawn out of the supply cassette 62 by a feeding robot 63, and the wafer 1 is mounted on a positioning table 64, with its back-side surface 1b up, where it is positioned to a predetermined position.
On the base 61, a turntable 75 driven to rotate in an R direction is provided. At outer peripheral parts of the turntable 75, a plurality of (in this case, three) circular disk-shaped chuck tables 70 are disposed at regular intervals along the circumferential direction. Each of the chuck tables 70 is rotatably supported, and is rotated in one direction or in both directions by a rotational driving mechanism (not shown).
The wafer 1 positioned on the positioning table 64 is picked up from the positioning table 64 by a supply arm 65, and is mounted on one of the chuck tables 70 being in vacuum operation, with its face-side surface 1a up and in a concentric manner. As shown in
With the turntable 75 rotated by a predetermined angle in the R direction, the wafer 1 held by the chuck table 70 is fed into a primary machining position under the grinding unit 80A for rough grinding, where rough grinding of the back-side surface 1b is conducted by the grinding unit 80A. Then, the turntable 75 is again rotated by a predetermined angle in the R direction, whereby the wafer 1 is fed into a secondary machining position under the grinding unit 80B for finish grinding, where finish grinding of the back-side surface 1b is performed by the grinding unit 80B.
At an end part on the depth side of the base 61, two columns 66A and 66B arranged side by side in an X direction are erectly provided, and the grinding units 80A and 80B are disposed at front surfaces of the columns 66A and 66B so that they can be lifted up and down in the Z direction (vertical direction). The lifting mechanisms here are the same as that in the case of the cutting unit 30 described above, and the grinding units 80A and 80B are slidably mounted to guides 91 provided at the front surfaces of the columns 66A and 66B and extending in the Z direction, through sliders 92, respectively. Besides, each of the grinding units 80A and 80B is lifted up and down in the Z direction through the slider 92, by a ball screw type feeding mechanism 94 driven by a servo motor 93.
The grinding units 80A and 80B are the same in basic configuration, and are distinguished from each other in that one of them is equipped with a grindstone for rough grinding whereas the other is equipped with a grindstone for finish grinding. As shown in
The grinding wheel 85 has a plurality of grindstones 87 arrayed on and firmly attached to the lower surface of an annular frame 86. A grinding or machining plane formed by the lower surfaces of the grindstones 87 is set to be horizontal, i.e., to be orthogonal to the axial direction of the spindle shaft 82. Therefore, the grinding or machining plane is parallel to the suction surface 72a of the chuck table 70. As the grindstone 87, for example, a grind stone obtained by mixing diamond abrasive grains into a vitreous bonding material, molding the mixture, and sintering the molded product is used.
As the grindstones 87 attached to the grinding unit 80A for rough grinding, for example, those containing comparatively coarse abrasive grains of about #320 to #400 are used. On the other hand, as the grindstones 87 attached to the grinding unit 80B for finish grinding, for example, those containing comparatively fine abrasive grains of about #2000 to #8000 are used. Each of the grinding units 80A and 80B is provided with a grinding water supply mechanism (not shown) for supplying grinding water for cooling the surface under grinding, for lubrication or for discharging the debris generated upon grinding.
The grinding wheel 85 is rotated as one body with the spindle shaft 82, and the outer diameter of grinding by the grindstones 87 in rotation is set to be greater than the diameter of the wafer 1. In addition, a machining position of the wafer 1 which is determined by rotating the turntable 75 by a predetermined angle is so set that the cutting edges at the lower surfaces of the grindstones 87 pass through the center of rotation of the wafer 1 and that the whole area of the back-side surface 1b of the wafer 1 put into revolution about its center by rotating the chuck table 70 can be ground.
The back-side surface 1b of the wafer 1 is ground by the grinding units 80A and 80B at the machining positions for rough grinding and finish grinding, respectively (back grinding step). The back grinding is performed by a process in which the chuck table 70 is rotated to put the wafer 1 into revolution about its center, the grinding unit 80A (80B) is gradually lowered by the feeding unit 94, and, in this condition, the grindstones 87 of the grinding wheel 85 in rotation are pressed against the exposed back-side surface 1b of the wafer 1. While the wafer 1 is thinned to a desired thickness through the rough grinding and the finish grinding, the measurement of thickness is performed by thickness measuring gauges 100 provided in the vicinity of the machining positions.
The thickness measuring gauge 100 includes a combination of a reference-side height gauge 101 having a probe 101a brought into contact with the surface 71a of the frame body 71 of the chuck table 70, with a movable-side height gauge 102 having a probe 102a brought into contact with the work surface (in this case, the back-side surface 1b of the wafer 1). The thickness of the wafer 1 under back grinding is minutely measured by comparing the height values measured by both the height gauges 101 and 102. The back grinding of the wafer 1 is carried out while measuring the thickness of the wafer 1 by the thickness measuring gauge 100, and the feed amount of the grinding wheel 85 fed by the feeding mechanism 94 is controlled based on the measured value of wafer thickness. Incidentally, the rough grinding is conducted until the wafer is thinned to a thickness value which is greater than the desired thickness upon finish grinding by, for example, 20 to 40 μm, and the residual part of thinning is carried out by the finish grinding. Incidentally, as shown in
After the wafer 1 is thinned to the desired thickness through the rough grinding and the finish grinding, recovery of the wafer 1 is carried out as follows. First, the finish grinding unit 80B is raised to retract from the wafer 1, whereas the turntable 75 is rotated by a predetermined angle in the R direction, whereby the wafer 1 is returned to the loading/unloading position at which the wafer 1 has been put from the supply arm 65 onto the chuck table 70. At the loading/unloading position, the vacuum operation of the chuck table 70 is stopped. Then, the wafer 1 is fed by a recovery arm 67 to a spinner type cleaning apparatus 68, where it is cleaned and dried. Thereafter, the wafer 1 is fed by the feeding robot 63 to, and contained into, a recovery cassette 69. In addition, the chuck table 70 from which the wafer 1 has been unloaded is cleared of debris generated upon grinding and the like by washing water discharged from a nozzle 76.
In the above-described manner, the back-side surface 1b of the wafer 1 is ground, and the wafer 1 is thinned to the desired thickness. The wafer 1 is finally cut and split along the planned dividing lines 2 into a plurality of individual semiconductor chips 3; in this case, the resin film 5 formed on the face-side surface 1a of the wafer 1 is removed, as required, before division into the individual chips, by peeling it off with a highly tacky pressure sensitive adhesive tape or by dissolving it with a solvent or by the like means. In some cases, the resin film 5 is not removed but is left as it is when division into the individual semiconductor chips 3 is carried out. In this case, the resin film 5 is so formed that electrodes of the semiconductor chips 3 formed on the side of the face-side surface 1a of the wafer 1 are not covered with the resin film 5 and that wiring to the electrodes can be performed at the time of mounting of the semiconductor chip 3.
Meanwhile, in this embodiment, in grinding the back-side surface 1b of the wafer 1, the face-side surface 1a is covered with the resin film 5 for protecting the face-side surface 1a. Not only the resin film 5 is merely formed on the face-side surface 1a but also the surface 5a of the resin film 5 is cut. In this case, the wafer angle controlling step is conducted in which the face-side surface 1a of the wafer 1 held onto the suction surface 22a of the chuck table 20 in the cutting apparatus 10 is controlled to be parallel to the cutting or machining plane of the cutting tool 37, and, in the subsequent resin film cutting step, the surface 5a of the resin film 5 is cut. By this process, the surface 5a is formed to be a flat surface parallel to the face-side surface 1a of the wafer 1.
In the case where unevenness is present in the thickness of the resin film 5 formed on the face-side surface 1a of the wafer 1, the thickness unevenness is eliminated by cutting the surface 5a of the resin film 5, or, if present, the thickness unevenness is suppressed to an extremely minute level of about 1 μm, for example. Then, when the wafer 1 is held while putting the thus cut surface 5a of the resin film 5 in contact with the suction surface 72a of the chuck table 70 in the grinding apparatus 60, the face-side surface 1a of the wafer 1 is horizontal, in other words, it is parallel to the grinding or machining plane of the grindstones 87 of the grinding unit 80A (80B). Therefore, when the back-side surface 1b of the wafer 1 is ground starting from this condition, the back-side surface 1b is ground to be a flat surface parallel to the face-side surface 1a. That is, the thickness of the wafer 1 as a single body having undergone the back grinding is uniform in thickness. In the back grinding step, the resin film 5 makes contact with the chuck table 70, whereby the semiconductor chips 3 on the side of the face-side surface 1a are protected.
According to this embodiment, the unevenness in the thickness of the resin film 5 is suppressed, whereby the thickness unevenness of the wafer 1 after back grinding is also suppressed accordingly. As a result, particularly where the desired thickness of the wafer 1 is as extremely small as about 30 to 50 μm, also, the influence of the thickness unevenness on the overall thickness of the wafer 1 can be obviated. Thus, the method according to this embodiment is highly promising as a method of back grinding for a wafer which is as extremely thin as this level.
In the prior art, the surface protective member used at the time of back grinding for a wafer has been a protective tape or the like which has unevenness in thickness. In this embodiment, on the other hand, the face-side surface 1a of the wafer 1 is covered with the resin film 5 used instead of a protective tape, and the surface 5a of the resin film 5 is cut to be parallel to the face-side surface 1a of the wafer 1 and to be used as a reference plane at the time of back grinding. Then, the surface 5a of the resin film 5 is brought into contact with the suction surface 72a of the chuck table 70, which ensures that the wafer 1 subjected to back grinding will be uniform in thickness. Since the resin film 5 covering the face-side surface 1a of the wafer 1 is so cut that its surface 5a is made parallel to the face-side surface 1a of the wafer 1, it is unnecessary to especially control the thickness of the resin film 5 rigorously at the time of applying the resin film 5 to the face-side surface 1a. Therefore, the kind of material of the resin film 5, the method of application, and the like factors can be selected comparatively freely, from the viewpoints of the rugged (projection-and-recess) condition of the face-side surface 1a, ease of application, cost, etc.
Incidentally, while the resin film 5 formed by application of a liquid resist has been used as the surface protective member in the above-described embodiment, a pressure sensitive adhesive tape 6 shown in
In the mode in which the pressure sensitive adhesive tape 6 is adhered to the face-side surface 1a of the wafer 1, the operation of covering the face-side surface 1a with the resin film is comparatively easy to carry out. In addition, removal of the resin film can also be easily carried out by peeling off the pressure sensitive adhesive tape 6 itself. Thus, this mode is advantageous on a workability basis.
The present invention is not limited to the details of the above described preferred embodiments. The scope of the invention is defined by the appended claims and all changes and modifications as fall within the equivalence of the scope of the claims are therefore to be embraced by the invention.
Number | Date | Country | Kind |
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2007-207168 | Aug 2007 | JP | national |
Number | Date | Country |
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A 2005-57052 | Mar 2005 | JP |
Number | Date | Country | |
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20090042488 A1 | Feb 2009 | US |