Chamber cleaning mechanism

Information

  • Patent Grant
  • 6775876
  • Patent Number
    6,775,876
  • Date Filed
    Wednesday, November 13, 2002
    22 years ago
  • Date Issued
    Tuesday, August 17, 2004
    20 years ago
Abstract
An apparatus for cleaning a reaction chamber which has a chamber, a blade apparatus and a reciprocable rotating unit. The chamber has a wall with an interior surface. The blade apparatus has at least one annular mounting member and at least three scraping blades attached peripherally about the annular mounting member and arranged in a parallel relationship to a longitudinal axis of the chamber. The reciprocable movement unit has a reciprocable member pivotally connected at a peripheral position to the blade apparatus. The reciprocable movement unit rotates the scraping blade(s) circumferentially back and forth along the interior surface of the chamber to scrape its interior surface.
Description




1. BACKGROUND OF THE INVENTION




The invention relates to a method and apparatus for cleaning a chamber.




Chemical vapor deposition (CVD) processes, such as organometallic chemical vapor deposition (OMCVD or MOCVD) processes, are commonly employed in the semiconductor, optical, and optoelectronic industries for doping or coating a substrate. Certain chemical vapor deposition processes, particularly those associated with large scale fabrication of epitaxial semiconductor devices, produce highly toxic effluent gases, such as dichlorosilane, trichlorosilane, phosphine, arsine, and hydrogen and nitrogen derivatives which have been generated in the fabrication reactor. These toxic gaseous effluents frequently contain particulate or particle-forming components, e.g., silica particles, which must be removed before the gases can be further processed, diluted mid/or neutralized, prior to ultimate discharge into the ambient environment.




Particulate-containing gaseous effluent is typically introduced into a scrubbing chamber through an inlet. The particulate matter is sticky in character and tends to adhere to the inner surface of the chamber. Various reaction chamber cleaning mechanisms (RCCMs) have been devised to prevent, or at least slow down, the buildup of particulate matter on the inner surfaces of the scrubbing chambers.




In currently available cleaning chambers, a spray jet is commonly employed to spray inside the bottom of the reaction chamber. This spray serves the dual purposes of quenching the hot gas flow and performing a water scrubbing function. A major drawback of such scrubbers is that the water spray can cause corrosion and buildup. There is a need in the art for an RCCM which provides an effective scrubbing mechanism without depending on water spray inside the reaction chamber for cooling. Such an RCCM would avoid the corrosion and buildup problems associated with presently available cleaning chambers.




RCCMs commonly use blade assemblies to scrape particulate matter from the interior surfaces of cleaning chambers. The RCCM blade assemblies of currently available RCCMs often lack sufficient strength to cut through the deposits formed on the reaction chamber wall. Such blade assemblies commonly become bent and/or twisted and thereafter permit buildup to form on the walls of the reaction chamber. There is a need in the art for an RCCM that overcomes these deficiencies in prior art blade assemblies.




Currently available RCCMs employ a push rod assembly drive mechanism to rotate the blade assembly about the inner surface of the cleaning chamber. These push rod assemblies are often not reliable, resulting in a low average service life for the cleaning chamber apparatus. The inventor has discovered that such push rod assemblies fail because the return spring becomes fatigued and fails to bend the push rod enough to engage it with the RCCM gear. The alignment key in the RCCM housing fails and causes the push rod assembly to rotate, thereby forcing the push rod to work at an angle that causes failure of the pivot pin. The alignment key and push rod assembly engagement surfaces are often damaged. The tip of the push rod assembly deforms permanently due to compressive stresses. The fasteners that attach the blade assembly to the drive mechanism often corrode and fail depending on exposure to corrosive gases. The bearings cold flow and loosen up over time, allowing water to leak into the housing. The RCCMs have no means of adjusting for manufacturing tolerance build up. Occasionally, the Teflon bearings are too tight, preventing the RCCM gear from turning. There is no indicator to monitor the functioning of the RCCM.




There is therefore a need in the art for an RCCM apparatus which overcomes all of these difficulties.




2. SUMMARY OF THE INVENTION




The present invention provides a reaction chamber cleaning apparatus comprising a chamber comprising a chamber wall comprising an interior surface; a blade apparatus comprising (i) at least cute annular mounting member and (ii) at least three scraping blades attached peripherally about the annular mounting member and arranged in a parallel relationship to a longitudinal axis of the chamber; and a reciprocal movement unit for rotating said scraping blade(s) circumferentially back and forth along the interior surface of said chamber to scrape the interior surface of said chamber, wherein such reciprocable movement unit comprises a reciprocable member pivotally connected to an extension member, and the extension member is pivotally connected at a peripheral position to the blade apparatus.




The present invention also provides a vortex unit comprising: (i) a top plate comprising a top surface, a bottom surface and a central opening; (ii) a generally conical outer shell attached to and extending downwardly from the top plate, in which the outer shell comprises an inner surface and a central opening that is generally aligned with the central opening of the top plate; (iii) a liquid inlet arranged in relation to the outer shell to tangentially introduce liquid into the outer shell, thereby forming a laminar sheet of fluid on the inner surface of the outer shell; (iv) a baffle attached to the lower surface of the top plate and extending generally vertically downwardly therefrom, in which the baffle comprises an inner surface, an outer surface, a bottom edge, and a central opening generally concentrically aligned with the central opening of the outer shell; (v) a concentric chamber bounded by the outer surface of the baffle, the inner surface of the outer shell, and the bottom surface of the top plate; and (vi) a concentric opening formed between the bottom edge of the baffle and the inner surface of the outer shell.




The reaction chamber cleaning apparatus and the vortex unit are suitably combined into a unitary assembly as a single article of manufacture.




In one aspect, the baffle of the vortex unit is arranged to provide a flow restriction so that during operation of the self-cleaning chamber mechanism, the concentric chamber is completely filled with liquid. The water vortex unit may also comprise a flange that accommodates attachment of the reaction chamber cleaning apparatus.




In one aspect, the liquid inlet is in fluid connection with a source of water.




In another aspect, the reaction chamber cleaning apparatus also comprises an exhaust moisture control system arranged to pass day air through the chamber to a secondary scrubbing tower.




The reaction chamber cleaning apparatus may be incorporated into an effluent abatement system by positioning the apparatus in downstream fluid flow communication with an effluent source such as a chemical vapor deposition apparatus or a semiconductor manufacturing apparatus.




In one aspect of the present invention, the blades of the reactor chamber cleaning apparatus are double-edged. Moreover, the blades preferably have a width and the reciprocating member has a range of movement, which width and range of movement are selected to provide each blade with a rotational path which overlaps with the rotational path of another blade. The blades are preferably from about 0.65 to about 0.75 inches wide, more preferably about 0.70 inches wide, and the rotation range is about 90°.




In another aspect, the reciprocable member of the reactor chamber cleaning apparatus is a piston of an air cylinder. The air cylinder is preferably equipped with a mechanism for indicating whether the cylinder is sufficiently extending and/or retracting to ensure that the apparatus is properly cleaning the chamber. For example, the mechanism may comprise one or more appropriately positioned magnetic reed switches. The mechanism for indicating whether the cylinder is sufficiently extending and retracting is preferably configured to provide an output, such as an electronic signal, indicative of whether the cylinder is sufficiently extending and/or retracting. The electronic signal may be transmitted to a CPU for further processing and/or may trigger an alarm, such as an audible alarm to indicate that the cylinder is not sufficiently extending and/or retracting.




The present invention also provides a method for using the apparatus of the invention for abating an effluent. The method generally comprises the steps of flowing liquid into the inlet so as to fill the concentric chamber with liquid and form a laminar sheet of liquid on the inner surface of the outer shell and flowing effluent into the chamber for abatement.




Other aspects, features and embodiments of the invention will be more fully apparent from the ensuing disclosure and appended claims.











3. BRIEF DESCRIPTION OF THE DRAWINGS





FIG. 1

shows an exploded view of an embodiment of the RCCM/vortex of the present invention.





FIG. 2

shows enlarged view of an embodiment of the vortex of the present invention.





FIG. 3

shows an embodiment of the thrust bearing unit of the present invention.





FIG. 4A

shows an embodiment of the air cylinder component of the invention.





FIG. 4B

shows an exploded section of an embodiment of the drive assembly of the apparatus of the invention.





FIG. 5

shows a top cross-sectional view of the RCCM/vortex apparatus of the present invention.





FIG. 6

shows an enlarged section of

FIG. 5

showing aspects of the drive mechanism of the present invention.





FIG. 7

shows a cut-away view of the thrust bearing in the top plate of the thrust bearing unit.





FIG. 8A

shows plan view of the RCCM/Vortex with the air cylinder in its retracted position.





FIG. 8B

shows the RCCM/Vortex apparatus of the present invention as the cylinder is extending.





FIG. 8C

shows the RCCM/Vortex with the air cylinder in its full-extended position.











4. DETAILED DESCRIPTION OF THE INVENTION




The present invention provides a new and improved RCCM and a new and improved water vortex. The RCCM and vortex aspects of the invention are suitably combined into one unit.

FIG. 1

shows an expanded view of a combined RCCM/vortex apparatus of the present invention, including the water vortex unit


100


and the RCCM unit


200


.




4.1 Water Vortex Unit





FIG. 2

shows an enlarged view of the water vortex unit


100


. The water vortex unit generally comprises a top plate


101


, a generally cone-shaped outer shell


105


and a baffle


112


.




The top plate


101


comprises a top surface


102


, a bottom surface


103


and a central opening


104


.




The outer shell


105


comprises an outer surface


106


, an inner surface


107


, a top edge


108


, a bottom edge


109


and a central opening


110


, which is generally aligned with the central opening


104


of the top plate


101


. The top edge


108


of the outer shell


105


is attached to and extends downwardly front the top plate


101


. The diameter of the central opening


110


of the outer shell


105


narrows as the distance from the top plate


101


increases, thus providing the outer shell


105


with a cone-like shape. The outer shell


105


may be attached to the top plate by any means known in the art, including for example welding, screws, bolts or other mechanical fasteners, compression and/or other means of fixation. Alternatively, the top plate and the outer shell may be molded as a unitary article.




The outer shell


105


comprises a liquid inlet


111


. The liquid inlet


111


is arranged in relation to the outer shell


105


such that as liquid is introduced tangentially into the outer shell


105


a laminar sheet of fluid (not shown) is formed on the inner surface


107


of the outer shell


105


. The liquid inlet


111


is in fluid connection with a fluid source (not shown). The preferred fluid is water. The laminar sheet of water circles around and completely covers the inner surface


107


of the outer shell.




The water vortex unit


100


also comprises a baffle


112


attached to the top plate


101


and extending generally vertically downwardly therefrom. The baffle


112


has an inner surface


113


, an outer surface


114


, a top edge


115


, a bottom edge


116


and a central opening


117


. The baffle


112


is attached such that the central opening


117


is generally concentrically aligned with the central opening


110


of the outer shell


105


and the central opening


104


of the top plate


101


. The baffle


112


may be attached to the top plate


101


inside the diameter of the central opening


104


of the top plate


101


as specifically shown in FIG.


2


. Moreover, the central openings of the top plate


101


and the baffle


112


may be coextensive, essentially forming a single central opening through the top plate


101


and the baffle.




A concentric chamber


118


is bounded by the outer surface


114


of the baffle


112


, the inner surface


107


of the outer shell


105


and the bottom surface


103


of the top plate


101


. The concentric chamber has a concentric opening


119


between the bottom edge


116


of the baffle


112


and the inner surface


107


of the outer shell


105


.




The baffle


112


is arranged to provide a flow restriction which ensures that the concentric chamber


118


is substantially or completely filled with liquid. This arrangement prevents corrosive gases from entering the concentric chamber


118


, prevents splashing, and aids in making the water flow laminar.




The water vortex unit


100


preferably comprises a flange


120


which accommodates the bushing


205


for the RCCM.




4.2 RCCM Unit





FIG. 1

shows an exploded view of the RCCM/vortex apparatus of the present invention, including an exploded view of the RCCM unit


200


.




The RCCM unit


200


is enclosed in the RCCM housing


300


(shown in FIG.


1


). The RCCM unit comprises a blade assembly


201


. The blade assembly


201


comprises 1 or more, preferably 2 to 6, more preferably 3, 4 or 5, and most preferably 4 blades


202


attached by welding or other attachment means known in the art to at least an upper ring


203


and a lower ring


204


. The blades


202


are preferably double-edged blades. The apparatus of the present invention provides greater blade assembly strength. The failure mode of currently available blade assemblies is caused by insufficient torsional strength. Torsional strength is increased in the blade assembly of the present invention by increasing the number of blades.




The blade assembly


201


is suitably arranged to pivot on a bushing


205


, which is attached to the water vortex unit


100


. The blade assembly


201


is preferably designed to press fit into the water vortex unit and is suitably held in place by a spring loaded thrust bearing unit


206


. The liquid flowing through the liquid vortex


100


cools the bushing


205


without allowing water to enter the RCCM housing


300


(shown in FIG.


1


). The spring-loaded thrush bearing accommodates manufacturing tolerance build up.




The thrust bearing unit


206


preferably has a maximum vertical range of motion of about 0.01 to about 0.05 inches, more preferably about 0.02 to about 0.04 inches, and most preferably about 0.03 inches, to account for tolerance build up and to prevent process gas from entering the RCCM housing


300


.




Referring now to

FIG. 3

, the thrust bearing unit


206


comprises a thrust bearing


207


and a top plate


208


. The thrust bearing


207


rides in a circular groove


209


cut into the top plate


208


. The top plate


208


also suitably comprises pins


210


that mate with holes


211


in the thrust bearing


207


to prevent it from rotating. The holes


211


in the thrust bearing


207


are constructed and arranged to receive the pins


210


of the top plate


208


. The thrust bearing


207


is constrained to linear motion to prevent wear on springs


212


that are arranged in a pushing relationship between the top plate


208


and the thrust bearing


207


to force the thrust bearing towards the top surface of the lower ring


204


of the RCCM blade assembly


201


to keep the thrust bearing


207


in contact with the top surface


204


A of the lower ring


204


of the RCCM blade assembly


201


.




Referring now to

FIG. 5

, the RCCM unit is preferably contained in a housing


300


. The housing is preferably manufactured from aluminum for ease of manufacture, weight minimization, ease of maintenance, and heat transfer. The housing also preferably comprises an inlet port


308


and an outlet port


309


to prevent the introduction of fluid components into the interior of the housing


300


. The inlet port and the outlet port are suitably employed for the introduction of clean dry air (CDA) for exhaust moisture suppression. The fitting


307


of the outlet port is shown in FIG.


1


. The introduction of CDA also assists in cooling the drive components and doubles as an air purge to prevent process gases from entering the RCCM drive mechanism.




The RCCM apparatus of the present invention suitably comprises a drive mechanism


400


(see

FIG. 4B

) comprising an air cylinder


401


(see FIG.


4


A). The drive mechanism operates without the necessity of springs, gears, or push rod assembly. This advance over the presently existing cleaning mechanisms is enabled by directly linking the air actuator to the blade assembly.




Referring now to

FIG. 4A

, the air cylinder


401


is preferably capable of generating at least 400 lbs. of force with a source pressure of 80 psi. The air cylinder


401


is suitably equipped with a mechanism for indicating whether the cylinder is making complete strokes. Such mechanism suitably comprises magnetic reed switches


402


.




Referring now to

FIG. 6

, the air cylinder


401


comprises a piston rod


403


connected to a cylinder adapter


404


. The means of attachment may be by any means known in the art; a suitable means is threading the piston rod


403


into the cylinder adapter


404


. The cylinder adapter


404


is preferably attached to a rotating link


405


via pivot pin


406


. The other end of the rotating link is preferably attached to the lower ring


204


of the blade assembly


201


via pivot pin


406


. Unlike currently available RCCMs the apparatus of the present invention avoids the need for using 8-32 fasteners in the drive mechanism. The pivot pin


406


at the adapter


404


is preferably held in place with a snap ring


407


. The pivot pin


406


at the blade assembly


201


is held in place with a retainer plate for ease of disassembly in the field. The air cylinder


401


is threaded into the RCCM housing


300


as shown in

FIG. 5

(in which the top and thrust bushing are removed for clarity).





FIG. 5

also shows a guide plate


304


that is attached to the RCCM housing


300


. The guide plate may be attached to the housing by any means known in the art, for example, the guide plate


304


is suitably attached by two mechanical fasteners


305


(see also FIGS.


1


and


6


). The cylinder adapter


404


is preferably designed to slide along the guide plate


304


when the air cylinder


401


extends against a high load. Accordingly, the guideplate


304


is arranged in relation to the RCCM housing


300


and the cylinder adapter


404


so that the cylinder adapter


404


slides along the guide plate


305


when the air cylinder


401


extends against a high load. When the air cylinder


401


retracts against a high load, the cylinder adapter


404


is designed to slide along the outside diameter


217


of the lower ring


204


of the blade assembly


201


. The air cylinder piston rod


403


is thereby protected from excessive deflection or buckling, and the guide bushing (not shown) in the air cylinder


401


is protected from excessive wear. The guide plate


304


and bushing


205


are preferably designed to be removable rather than integral parts of other components so that they can be replaced with different materials if wear is excessive.




4.3 Operation of the RCCM Apparatus




The blade assembly


201


of the RCCM/Vortex rotates clockwise and counter clockwise with the extension and retraction (or vice versa) of the piston


403


of the air cylinder


401


. The blades


202


are preferably double edged and clean in both the clockwise and counter clockwise directions. The blade width and rotation range are selected to provide overlap in the cleaning passes. For example, in a preferred aspect, the blades


202


are preferably from about 0.65 to 0.75 inches wide, more preferably 0.70 inches wide, and the rotation range is about 90°, thereby providing overlap in the cleaning passes. An air cylinder stroke actuates the cleaning motion; the stroke is suitably about 6 inches in length. The air cylinder


401


is linked to the blade assembly


201


via rotating link.

FIG. 8A

shows a plan view of the RCCM/Vortex with the air cylinder in its retracted position.

FIG. 8B

shows the RCCM/Vortex apparatus of the present invention as the cylinder


401


is extending.

FIG. 8C

shows the RCCM/Vortex with the air cylinder


401


in its full-extended position.




In a preferred embodiment, the cylinder


401


takes approximately 2-3 seconds (unobstructed, with solenoid throttles set to full open) to fully extend or fully retract. The timing circuit is set to apply pressure to extend and retract the air cylinder


401


for a time which is ample to permit the blade assembly


201


to cut through obstructions before changing directions. Thus, for example, the timing circuit is preferably set to apply pressure to extend the air cylinder


401


for about 10 seconds and retract the air cylinder


401


for about 10 seconds, thereby providing ample time for the RCCM blade assembly


201


to cut through obstructions before changing directions. The duration of pressure to extend and retract the air cylinder


401


can easily be altered to accommodate different field conditions by modifying the timing circuit program.




The RCCM blade assembly of the present invention cleans in both the counter-clockwise and clockwise directions, and is thereby more effective than currently available apparatuses at dislodging deposits in the reaction chamber.




Fluid flowing through the fluid vortex will cool the main bushing


205


about which the blade assembly


201


rotates. Air from the exhaust moisture control system will preferably make one pass through the RCCM housing


300


before entering an upper secondary scrubbing tower. This will provide additional RCCM component cooling and act as a purge for the RCCM housing


300


.




The magnetic reed switches


402


located on the air cylinder


401


will indicate if the cylinder


401


is sufficiently extending and retracting, thereby providing a measure of the functioning of the apparatus, since the air cylinder


401


is positively linked to the blade assembly


201


.




The present invention preferably incorporates both a fluid vortex unit


100


and an RCCM unit


200


in a single cleaning apparatus. This apparatus is preferably used in conjunction with a lower spray jet outside of the reaction chamber, thereby preventing lower reaction chamber corrosion and build-up caused by minerals in the water.




It is to be understood that the embodiment described above is merely illustrative of some of the many specific embodiments of the present invention, and that other arrangements will be readily apparent by one of ordinary skill in the art in light of the present disclosure without departing from the scope of the invention.















List of Reference Numerals


























100




Water Vortex Unit







101




Top Plate







102




Top Surface of Top Plate 101







103




Lower Surface of Top Plate 101







104




Opening in Top Plate 101







105




Outer Shell







106




Outer Surface of Outer Shell 105







107




Inner Surface of Outer Shell 105







108




Top Edge of Outer Shell 105







109




Bottom Edge of Outer Shell 105







110




Central Opening of Outer Shell 105







111




Water Inlet of Outer Shell 105







112




Baffle







113




Inner Surface of Baffle 112







114




Outer Surface of Baffle 112







115




Top Edge of Baffle 112







116




Bottom Edge of Baffle 112







117




Central Opening of Baffle 112







118




Concentric Chamber







119




Concentric Opening in Bottom of








Concentric Chamber







120




Flange







121




RCCM/Vortex Assembly Bolts







200




RCCM Unit







201




Blade Assembly







202




Double Edged Blades







203




Upper Ring of Blade Assembly 201







203a




Top Surface of Upper Ring 203







203b




Bottom Surface of Upper Ring 203







204




Lower Ring of Blade Assembly 201







205




Bushing







206




Thrust Bearing Unit







207




Thrust Bearing of Bearing Unit 206







208




Top Plate of Bearing Unit 206







209




Circular Groove Cut in Top Plate 208







210




Pins in Top Plate 208







211




Holes in Thrust Bearing 207







212




Springs of Bearing Unit 206







213




Cylindrical Opening of RCCM Uit







214




Reaction Chamber Gasket







215




Upper Gasket for RCCM Housing 300







216




Opening for Exhaust Moisture Control








CDA Exit







217




Outside Diameter of Lower Ring 204







218




Hole for RCCM/Vortex Assembly Bolts







219




Air Cylinder Boss







220




Opening for Air Cylinder Piston Rod








403 and Air Cylinder Adaptor 404







223




Lower Gasket for RCCM Housung 300







300




RCCM Houstng







301




Cylindrical Wall of RCCM Housing







302




Interior Surface of Cylindrical Wall 301







303




Exterior Surface of Cylindrical Wall 301







304




Guideplate







305




Fasteners for Guideplate 304







306




Exhaust Moisture Control CDA Fitting







307




Exhaust Moisture Control CDA Fitting







308




Exhaust Moisture Control CDA Inlet







309




Exhaust Moisture Control CDA Outlet







400




Drive Mechanism







401




Air Cylinder







402




Reed Switches







403




Piston Rod







404




Air Cylinder Adaptor







405




Rotating Link







406




Pivot Pin







407




Snap Ring







408




Retainer Plate







409




Lower Ring Lug







410




Air Cylinder Fitting







411




Sliding Support of Cylinder Adaptor 404














Claims
  • 1. A reaction chamber cleaning apparatus comprising:(a) a cylindrical chamber comprising a chamber wall comprising an interior surface; (b) a blade apparatus comprising: (i) at least one annular mounting member; (ii) at least three scraping blades attached peripherally about the annular mounting member and arranged in a parallel relationship to a longitudinal axis of the chamber; and (c) a reciprocable movement unit for rotating said scraping blade(s) circumferentially back and forth along the interior surface of said chamber to scrape the interior surface of said chamber, said reciprocable movement unit comprising a reciprocable member pivotally connected to an extension member, said extension member being pivotally connected at a peripheral position to the blade apparatus.
  • 2. The apparatus of claim 1 with four scraping blades.
  • 3. The apparatus of claim 1 with five scraping blades.
  • 4. The apparatus of claim 1 with six scraping blades.
  • 5. The apparatus of claim 1 wherein the blades are double-edged.
  • 6. The apparatus of claim 1 wherein the blades have a width and the reciprocable member has a range of rotational movement, which width and range of rotational movement are selected in conjunction with the number of blades to provide each blade with a rotational path which overlaps with the rotational path of an adjacent blade.
  • 7. The apparatus of claim 6 with four blades, wherein each blade is from about 0.65 to about 0.75 inches wide and wherein The range of rotational movement is about 90°.
  • 8. The apparatus of claim 1 wherein the reciprocable member is a piston of an air cylinder.
  • 9. The apparatus of claim 8 wherein the air cylinder is equipped with at least one detector for indicating whether the cylinder is sufficiently extending and retracting to ensure that the blades have a scraping path which substantially covers the interior surface of the cylindrical way of the chamber.
  • 10. The apparatus of claim 9 wherein the at least one detector is configured to provide an output indicative of whether the cylinder is sufficiently extending and retracting to ensure that the blades have a scraping path which substantially covers the interior surface of the cylindrical way of the chamber.
  • 11. The apparatus of claim 9 wherein the at least one detector comprises one or more magnetic reed switches arranged to indicate if the cylinder is sufficiently extending and retracting to ensure that the blades have a scraping path which substantially covers the interior surface of the cylindrical way of the chamber.
  • 12. The apparatus of claim 8 wherein the piston has a stroke which is about 6 inches.
Parent Case Info

This is a division of U.S. application Ser. No. 09/525,221 filed on Mar. 14, 2000 now U.S. Pat. No. 6,544,482.

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