The present invention relates to material processing and more particularly to a process performance control system and method thereof for controlling a process in a material processing system.
One area of material processing in the semiconductor industry which presents formidable challenges is, for example, the manufacture of integrated circuits (ICs). Demands for increasing the speed of ICs in general, and memory devices in particular, force semiconductor manufacturers to make devices smaller and smaller on the substrate surface. Moreover, in order to reduce fabrication costs, it is necessary to reduce the number of steps (e.g., etch steps, deposition steps, etc.) required to produce an IC structure and, hence, reduce the overall complexity of the IC structure and the fabrication methods thereof. These demands are further exacerbated by both the reduction in feature size and the increase of substrate size (i.e., 200 mm to 300 mm and greater), which places greater emphasis on critical dimensions (CD), process rate and process uniformity to maximize the yield of superior devices. through inter-level dielectric layers. Usually, an etch stop layer is placed under a dielectric layer in order to protect the underlying layers (devices) from being damaged during over-etching. An etch stop layer generally includes a material that when exposed to the chemistry utilized for etching the dielectric layer has an etch rate less than the dielectric layer etch rate (i.e., the etch chemistry has a high etch selectivity to the dielectric layer relative to the etch stop layer). Furthermore, the etch stop layer provides a barrier for permitting an over-etch step to assure that all features on the substrate are etched to the same depth.
However, the etch stop layer complicates the process integration, increases manufacturing cost and decreases device performance. Without an etch stop layer, etch depth can vary depending on etch rate (ER) since fixed-time recipes are used. Since, for example, the etch tool is subject to equipment disturbance, the etch rate can change significantly over maintenance cycles. In order to maintain a constant etch rate, frequent tool qualification and maintenance procedures are required. Therefore, in-situ estimation of the etch rate can determine whether the process chamber is in a normal condition and can provide information to control the etch time so that the etch depth is on target.
The present invention provides for a material processing system comprising a process tool and a process performance control system. The process performance control system comprises a process performance controller coupled to the process tool, where the process performance controller comprises a process performance prediction model configured to receive tool data from a plurality of sensors and configured to predict process performance data. The process performance control system further comprises a process recipe correction filter coupled to the process performance prediction model, configured to receive predicted process performance data and configured to generate a process recipe correction, and a process controller coupled to the process recipe correction filter, configured to receive the process recipe correction and update the process recipe using the process recipe correction.
The present invention advantageously provides a process performance control system that further comprises a metrology tool coupled to the process tool and the process performance controller, configured to receive substrates processed within the process tool and configured to measure process performance data. The process performance controller further comprises a process performance model correction algorithm configured to receive measured process performance data and coupled to the process performance prediction model in order to provide an adjustment of the process performance prediction model.
The present invention advantageously provides a method for controlling a process tool of a material processing system. The method comprises the steps of executing a first process in the process tool, recording tool data for the first process, where the tool data comprises a plurality of tool data parameters, and predicting process performance data from the tool data for the first process using a process performance prediction model, where the process performance data comprises one or more process performance data parameters. The method further comprises the steps of determining a process recipe correction from the predicted process performance data using a process recipe correction filter, updating the process recipe by incorporating the process recipe correction using a process controller coupled to the process tool, and executing a second process in the process tool using the updated process recipe.
These and other advantages of the invention will become more apparent and more readily appreciated from the following detailed description of the exemplary embodiments of the invention taken in conjunction with the accompanying drawings, where:
According to an embodiment of the present invention, a material processing system 1 is depicted in
In addition, the process performance control system 100 can further include a metrology tool 140, and the process performance controller 55 can further include a process performance model correction algorithm 150. Metrology tool 140 can be coupled to the process tool 10 and to the process performance controller 55, and metrology tool 140 can be configured to receive substrates processed within the process tool 10 and to measure process performance data. The process performance correction algorithm 150 can be configured to receive measured process performance data from the metrology tool 140, and the process performance correction algorithm 150 can be coupled to process performance prediction model 110 in order to provide an adjustment of the process performance prediction model 110.
In the illustrated embodiment depicted in
As shown in
For example, the substrate 25 can be affixed to the substrate holder 20 via an electrostatic clamping system 28. Furthermore, substrate holder 20 can further include a cooling system including a re-circulating coolant flow that receives heat from substrate holder 20 and transfers heat to a heat exchanger system (not shown), or when heating, transfers heat from the heat exchanger system. Moreover, gas can be delivered to the back-side of the substrate via a backside gas system 26 to improve the gas-gap thermal conductance between substrate 25 and substrate holder 20. Such a system can be utilized when temperature control of the substrate is required at elevated or reduced temperatures. For example, temperature control of the substrate can be useful at temperatures in excess of the steady-state temperature achieved due to a balance of the heat flux delivered to the substrate 25 from the plasma and the heat flux removed from substrate 25 by conduction to the substrate holder 20. In other embodiments, heating elements, such as resistive heating elements, or thermoelectric heaters/coolers can be included.
In the exemplary embodiment shown in
Alternately, RF power can be applied to the substrate holder electrode at multiple frequencies. Furthermore, impedance match network 32 can serve to maximize the transfer of RF power to plasma in processing chamber 10 by minimizing the reflected power. Various match network topologies (e.g., L-type, π-type, T-type, etc.) and automatic control methods can be utilized.
With continuing reference to
Vacuum pump system 58 can, for example, include a turbo-molecular vacuum pump (TMP) capable of a pumping speed up to 5000 liters per second (and greater) and a gate valve for throttling the chamber pressure. In related plasma processing devices utilized for dry plasma etch, a 1000 to 3000 liter per second TMP is generally employed. TMPs are useful for low pressure processing, typically less than 50 mTorr. At higher pressures, the TMP pumping speed falls off dramatically. For high pressure processing (i.e., greater than 100 mTorr), a mechanical booster pump and dry roughing pump can be used. Furthermore, a device for monitoring chamber pressure (not shown) is coupled to the process chamber 16. The pressure measuring device can be, for example, a Type 628B Baratron absolute capacitance manometer commercially available from MKS Instruments, Inc. (Andover, Mass.).
As depicted in
For example, light detection device 34 can include a detector such as a (silicon) photodiode or a photomultiplier tube (PMT) for measuring the total light intensity emitted from the plasma. It can further include an optical filter such as a narrow-band interference filter. In an alternate embodiment, light detection device 34 can include a line CCD (charge coupled device) or CID (charge injection device) array and a light dispersing device such as a grating or a prism. Additionally, light detection device 34 can include a monocbromator (e.g., grating/detector system) for measuring light at a given wavelength, or a spectrometer (e.g., with a rotating grating) for measuring the light spectrum such as, for example, the device described in U.S. Pat. No. 5,888,337.
For example, the light detection device 34 can include a high resolution OES sensor from Peak Sensor Systems. Such an OES sensor has a broad spectrum that spans the ultraviolet (UV), visible (VIS) and near infrared (NIR) light spectrums. The resolution is approximately 1.4 Angstroms, that is, the sensor is capable of collecting 5550 wavelengths from 240 to 1000 nm. The sensor is equipped with high sensitivity miniature fiber optic UV-VIS-NIR spectrometers which are, in turn, integrated with 2048 pixel linear CCD arrays.
The spectrometers receive light transmitted through single and bundled optical fibers, where the light output from the optical fibers is dispersed across the line CCD array using a fixed grating. Similar to the configuration described above, light emitting through an optical vacuum window is focused onto the input end of the optical fibers via a convex spherical lens. Three spectrometers, each specifically tuned for a given spectral range (UV, VIS and NIR), form a sensor for a process chamber. Each spectrometer includes an independent A/D converter. And lastly, depending upon the sensor utilization, a full emission spectrum can be recorded every 0.1 to 1.0 seconds.
The electrical measurement device 36 can include, for example, a current and/or voltage probe for monitoring an electrical property, such as voltage, current, impedance and phase, of the electrical system including the processing region 45, a power meter, or spectrum analyzer. For example, plasma processing systems often employ RF power to form plasma, in which case, an RF transmission line, such as, for instance, a coaxial cable or structure, is employed to couple RE energy to the plasma through an electrical coupling element (i.e., inductive coil, electrode, etc.). Electrical measurements using, for example, a current-voltage probe, can be exercised anywhere within the electrical (RF) circuit, such as within an RE transmission line. Furthermore, the measurement of an electrical signal, such as a time trace of voltage or current, permits the transformation of the signal into frequency space using discrete Fourier series representation (assuming a periodic signal). Thereafter, the Fourier spectrum (or for a time varying signal, the frequency spectrum) can be monitored and analyzed to characterize the state of material processing system 1. A voltage-current probe can be, for example, a device as described in detail in pending U.S. application Ser. No. 60/259,862 filed on Jan. 8, 2001, and U.S. Pat. No. 5,467,013, each of which is incorporated herein by reference in its entirety.
In alternate embodiments, electrical measurement device 36 can comprise a broadband RF antenna useful for measuring a radiated RE field external to material processing system 1. A commercially available broadband RF antenna is a broadband antenna such as Antenna Research Model RAM-220 (0.1 MHz to 300 MHz).
In general, the plurality of sensors can include any number of sensors, intrinsic and extrinsic, and can be coupled to process tool 10 to provide tool data to the process performance controller 55 of the process performance control system 100.
As described above, the process performance control system 100 includes process performance controller 55. The process performance controller 55 can include a microprocessor, memory, and a digital I/O port (potentially including D/A and/or A/D converters) capable of generating control voltages sufficient to communicate and activate inputs to material processing system 1 as well as monitor outputs from material processing system 1. Moreover, process performance controller 55 is coupled to and exchanges information with RF generator 30, impedance match network 32, gas injection system 40, vacuum pump system 58, backside gas delivery system 26, electrostatic clamping system 28, light detection device 34, and electrical measurement device 36. A program stored in the memory is utilized to activate the inputs to the aforementioned components of a material processing system 1 according to a stored process recipe. One example of process performance controller 55 is a DELL PRECISION WORKSTATION 530™, available from Dell Corporation, Austin, Tex. Alternately, process performance controller 55 can comprise a Digital Signal Processor (DSP).
As shown in
As shown in
As shown in
Alternately, the plasma can be formed using electron cyclotron resonance (ECR). In yet another embodiment, the plasma is formed from the launching of a Helicon wave. In yet another embodiment, the plasma is formed from a propagating surface wave.
As discussed above, the process performance prediction model 100 establishes a relationship between tool data and process performance data and, therefore, it enables the prediction of process performance data for a given observation of tool data. The following describes the method of constructing the process performance prediction model 110.
Table 1 presents an exemplary set of tool data, to be correlated with process performance data, including sixty-one tool data parameters.
Moreover, an exemplary set of process performance data pertaining to trench etching as part of a damascene process can include a mean trench etch depth and a trench etch depth range. The mean trench etch depth can, for example, include a spatial average of the trench etch depth at a plurality of locations on a substrate. The trench etch depth range can, for example, include a minimum-maximum range, a variance, a standard deviation, or a root mean square (rms) of the data scatter about the mean value for the etch depth.
The measurement of the trench etch depth and trench etch depth range can be performed directly using a scanning electron microscope (SEM) to view SEM micrographs from cleaved substrates, or indirectly using advanced, in-situ technology such as, for example, DUV spectroscopic ellipsometry (e.g., see “Specular spectroscopic scatterometry”, IEEE Transactions on Semiconductor Manufacturing, Vol. 14, No. 2, May 2001, which is incorporated herein by reference in its entirey). A commercially available product featuring optical digital profilometry (ODP) is that sold and distributed by Timbre Technologies, Inc., A TEL Company (5341 Randall Place, Fremont, Calif. 94538) coupled with the hardware from Therma-Wave, Inc. (1250 Reliance Way, Fremont, Calif. 94539).
Each set of data, including both tool data and corresponding process performance data, includes an observation set, where either a single observation can be made per substrate or a plurality of observations can be performed per substrate. Each observation in an observation set, including both tool data and process performance data, can include an nth order statistic (e.g., time average, rms of time trace, skewness of time trace, etc.). For example, each observation set can correspond to a substrate processed, wherein each tool data parameter is sampled during the length of the process, trimmed (i.e., data at the start and end of the sampled data is trimmed to remove start/end transients), and averaged.
Given a plurality of observations sets, a relationship can be determined between the tool data in the plurality of observation sets and the process performance data in the plurality of observation sets using multivariate analysis (MVA). One exemplary MVA technique for determining such a relationship is partial least squares (PLS) modeling.
Using PLS, observation sets of tool data are received from a plurality of sensors. For each observation set, tool data can be stored as a row in a matrix {overscore (X)} and process performance data can be stored as a row in matrix {overscore (Y)}. Hence, once the matrix {overscore (X)} is assembled, each row represents a different observation and each column represents a different tool data parameter (from Table 1), and, once the matrix {overscore (Y)} is assembled, each row represents a different observation and each column represents a different process performance parameter. Hence, using the set of parameters in Table 1, matrix {overscore (X)} is a rectangular matrix of dimensions M by sixty-one, where M is the number of observation sets. Similarly, matrix {overscore (Y)} is a rectangular matrix of dimensions M by 2. More generally, matrix {overscore (X)} can be an m by n matrix, and matrix {overscore (Y)} can be an m by p matrix. Once all of the data is stored in the matrices, the data can be mean-centered and/or normalized, if desired. The process of mean-centering the data stored in a matrix column involves computing a mean value of the column elements and subtracting the mean value from each element. Moreover, the data residing in a column of the matrix can be normalized by the standard deviation of the data in the column.
In the following discussion, a set of tool data and process performance data is utilized from forty-five substrates in order to present the method by which tool data are optimized and a model is established for relating the tool data and the process performance data (i.e., M=45 in the above discussion.) The forty-five process runs (substrates) includes three sets of substrates processed in an etch chamber, where each set of substrates is preceded by a chamber wet clean. The tool data included in the PLS analysis model is listed in Table 1 and the process performance data includes the mean trench etch depth and the trench etch depth range.
In the PLS analysis, a set of loading (or correlation) coefficients can be defined which relate the tool data ({overscore (X)}) to the process performance data ({overscore (Y)}). In general, for multivariate analysis, the relationship between the tool data and the process performance data can be expressed as follows:
{overscore (XB)}={overscore (Y)}, (1)
where {overscore (X)} represents the m by n matrix described above, {overscore (B)} represents an n by p (p<n) loading (or correlation) matrix and {overscore (Y)} represents the m by p matrix described above.
Once the data matrices {overscore (X)} and {overscore (Y)} are assembled, a relationship designed to best approximate the {overscore (X)} and {overscore (Y)} spaces and to maximize the correlation between {overscore (X)} and {overscore (Y)} is established using PLS analysis.
In the PLS analysis model, the matrices {overscore (X)} and {overscore (Y)} are decomposed as follows:
{overscore (X)}={overscore (TP)}T+{overscore (E)}; (2a)
{overscore (Y)}={overscore (UC)}T+{overscore (F)}; (2b)
and
{overscore (U)}={overscore (T)}+{overscore (H)}; (2c)
where {overscore (T)} is a matrix of scores that summarizes the {overscore (X)} variables, {overscore (P)} is a matrix of loadings for matrix {overscore (X)}, {overscore (U)} is a matrix of scores that summarizes the {overscore (Y)} variables, {overscore (C)} is a matrix of weights expressing the correlation between {overscore (Y)} and {overscore (T)} ({overscore (X)}), and {overscore (E)}, {overscore (F)} and {overscore (H)} are matrices of residuals. Furthermore, in the PLS analysis model, there are additional loadings {overscore (W)} called weights that correlate {overscore (U)} and {overscore (X)}, and are used to calculate {overscore (T)}. In summary, the PLS analysis geometrically corresponds to fitting a line, plane or hyper plane to both the {overscore (X)} and {overscore (Y)} data represented as points in a multidimensional space, with the objective of well approximating the original data tables {overscore (X)} and {overscore (Y)}, and maximizing the covariance between the observation positions on the hyper planes.
In general, SIMCA-P outputs other important information regarding the descriptive power of the model (i.e., the quality of the correlation obtained between {overscore (X)} and {overscore (Y)}), and the predictive power of the model. For example, SIMCA-P iteratively computes one PLS component at a time, that is one vector each of X-scores {overscore (T)}, Y-scores {overscore (U)}, weights {overscore (W)} and {overscore (C)}, and loadings {overscore (P)}. The PLS components are calculated in descending order of importance. After each PLS component, SIMCA-P can display the following: the fraction of the sum of squares (SS) of all Y's and X's explained by the current component (R2X, R2Y); the fraction of variance of all the Y's and X's explained by the current component R2Xadj, R2Yadj); the cumulative SS of all the Y's and X's explained by all extracted components (R2X(cum), R2Y(cum)); and the cumulative variance of all the Y's and X's explained by all extracted components W2Xadj(cum), R2Yadj(cum)).
Furthermore, for every active variable, the fraction of SS R2V) or variance (R2Vadj) explained can be displayed. This value is computed for the current component as well as cumulatively for all PLS components. For response variables {overscore (Y)}, this value corresponds to R2 (the multiple correlation coefficient), the “goodness” of the fit. For example, utilizing the data above,
In general, additional criterion used to determine the model dimensionality (number of significant PLS components), is cross validation. With cross validation, observations are kept out of the model development, then the response values ({overscore (Y)}) for the kept out observations are predicted by the model, and compared with the actual values. This procedure is repeated several times until every observation has been kept out once and only once. The prediction error sum of squares (PRESS) is the squared differences between observed {overscore (Y)} and predicted values when the observations were kept out. For every dimension, the overall PRESS/SS is computed, where SS is the residual sum of squares of the previous dimension, and also (PRESS/SS)m for each {overscore (Y)} variable (m). These values are good measures of the predictive power of the model. For example, SIMCA-P can present this information as follows: the fraction of the total variation of the Y's that can be predicted by a component (Q2=(1.0-PRESS/SS)); the fraction of the variation of a variable Ym that can be predicted by a component (Q2V=(1.0-PRESS/SS)m); the cumulative Q2 for the extracted components (Q2cum=II (1.0-PRESS/SS)a); and the cumulative Q2V of a variable (Q2Vcum=II (1.0-PRESS/SS)a).
Once the PLS analysis is complete and the above output matrices have been computed, the influence on the {overscore (Y)} matrix of every term or column in the {overscore (X)} matrix, namely, the VIP is determined. VIP is the sum over all model dimensions of the contributions variable influence (VIN). For a given PLS dimension, (VIN)ij2 is related to the squared PLS weight (wij)2 of that term. The accumulated (over all PLS dimensions) value,
is used for further analysis. Once the VIPs are computed for each variable in matrix {overscore (X)}, they may be sorted and plotted in descending order against the variable number. Those variables with the largest VIP will have the greatest impact on the process performance data in matrix {overscore (Y)}.
For example,
Using the VIP data of
Using any one of the above-mentioned criteria, those variables that have minimal impact on the process performance data can be discarded. This data reduction or refinement, in turn, reduces the column space of the data matrix {overscore (X)} from p (sixty-one in the above example) to q (e.g., <sixty-one parameters), and forms a “new”, reduced or refined data matrix {overscore (X)}* of dimensions m by q (forty-five by<sixty-one). Once an initial data reduction has taken place, those tool data parameters important for establishing a “good” model between the tool data and the process performance data can be stored. Thereafter, further refinement or reduction of the data matrix {overscore (X)}* can be performed and/or the method can proceed with re-computing the output matrices from the PLS analysis model using the reduced data matrix {overscore (X)}* and determining the correlation matrix {overscore (B)} for establishing the relationship between the tool data and the process performance data.
At this point, the PLS model is repeated following the schematic presented in
{overscore (B)}={overscore (W)}({overscore (P)}T{overscore (W)})−1{overscore (C)}T. (4)
Once the data matrix {overscore (X)}* has been optimized, a final pass through the PLS analysis is generally required to update or re-compute the output matrices necessary for computing the correlation matrix {overscore (B)}. Hereinafter, the evaluation of equation (4) leads to a set of correlation coefficients to be used for extracting the predicted process performance data from the sampled tool data.
Using
Once the correlation matrix {overscore (B)} has been evaluated (or the process performance prediction model formulated), the correlation matrix {overscore (B)} can be used as part of a fault detection algorithm to provide robust determination and prediction of process faults. The fault detection algorithm can, in general, be applied to a variety of processes, however, the specific correlation matrix {overscore (B)} developed as described above will be specific to a particular process in a specific process tool. For example, silicon processing, such as etching, can be performed in a process tool much like that depicted in
In the preceding text, methods of constructing a process performance prediction model 110 and applying the model for fault detection have been described. Using the example from above, the detection of a fault can subsequently be associated with either a fault in the mean trench etch depth or the trench etch depth range (i.e., one of process rate and/or process uniformity).
For example, the occurrence of a fault in mean trench etch depth can arise due to perturbations to the process tool performance (e.g., process drifts, etc.), sensor noise, drift in sensor calibration, etc. There exist a number of variables that are introduced from run-to-run, which can cause variations in process performance. However, with the formulation of a process performance prediction model 110, a prediction of process performance data, using an observation of tool data from a prior run, can be employed to update a process recipe in order to correct for process perturbations.
As described earlier, an element of the process recipe for (damascene structure) trench etch is the trench etch time which requires knowledge of the trench etch rate. According to one embodiment of the present invention, the process performance prediction model 110 can be utilized to predict a mean trench etch depth from an observation of tool data. Dividing the predicted mean trench etch depth dpredicted by the etch time τold during the prior run produces the predicted mean trench etch rate εpredicted (i.e., εpredicted=dpredicted/εold).
Following the prediction of the mean trench etch rate using the process performance prediction model 110 and the known etch time for the prior run, a corrected etch time can be determined using the process recipe correction filter 120. The process recipe correction filter 120 can include an exponentially weighted moving average (EWMA) filter to correct the etch time in the process recipe using the old value for the etch time, the predicted value for the etch time and a filter constant, viz.
τnew=(1−λ)τold+λ(τpredicted−τold), (5)
where λ is the EWMA filter coefficient ( 0≦λ≦1), τold is the (old) process recipe etch time for the prior run, τpredicted is the predicted etch time using the known etch depth d for the (damascene) trench structure and the predicted etch rate εpredicted (i.e., τpredicted=d/εpredicted), and τnew is the process recipe etch time for the upcoming run. Note that when λ=0, the new etch time is equivalent to the old etch time and, when λ=1, the new etch time is equivalent to the predicted etch time.
In general, when using substrate numbers twenty-six through fifty-two for model evaluation, a RMSE of the measured and predicted data was utilized to quantify the process performance prediction model 110 performance, where the RMSE is defined as follows:
In equation (6), the summation over i=1 to n represents the summation over the substrates (twenty-six through fifty-two) used for model evaluation, and {overscore (ε)}measured represents the average measured etch rate. Clearly, by inspection of
The average error can be further improved by implementing periodic updates of the process performance prediction model 110. At pre-determined intervals in substrate processing, a substrate can be transported from the process tool 10 to the metrology tool 140 for measurement of the process performance data. Following the above exemplary process, the process performance data can include the mean trench etch depth and the trench etch range. This data can be measured using conventional techniques in metrology tool 140, as described above.
The measurement of process performance data can be submitted to the process performance model correction algorithm 150. Tool data and the corresponding measured process performance data are inserted with the tool data matrix {overscore (X)} and the process performance data matrix {overscore (Y)}, and the correlation matrix {overscore (B)} is re-evaluated using PLS analysis as described with reference to
In step 750, the process recipe correction filter employs the EWMA filter and model prediction of process performance data to correct the process recipe by determining a process recipe correction. The correction to the process recipe can, for example, include a correction to the etch time. The EWMA filter employs a filter coefficient and, desirably, the selected filter coefficient is the optimal filter coefficient. In step 760, the process recipe is updated using the process controller prior to determining if another process is to be run in step 770.
If step 730 determines that the process performance prediction model is to be updated, then control passes to step 780. In step 780, process performance data is measured using the metrology tool and submitted to the process performance model correction algorithm. In step 790, the process performance model correction algorithm employs PLS analysis according to the procedures set forth above. The PLS analysis uses measured process performance data (from the metrology tool) and corresponding tool data in addition to the tool data and process performance data used for formulation of the current process performance prediction model. When appropriate (as deemed by the length of time to update the process performance prediction model relative to executing substrate runs), the process performance prediction model is updated.
Although only certain exemplary embodiments of this invention have been described in detail above, those skilled in the art will readily appreciate that many modifications are possible in the exemplary embodiments without materially departing from the novel teachings and advantages of this invention. Accordingly, all such modifications are intended to be included within the scope of this invention.
The present application claims priority to previously filed U.S. application Ser. No. 60/391,966, filed on Jun. 28, 2002. This application is related to U.S. application Ser. No. 60/391,965, filed on Jun. 28, 2002. The entire contents of these applications are incorporated herein by reference.
Filing Document | Filing Date | Country | Kind | 371c Date |
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PCT/US03/16239 | 6/27/2003 | WO | 11/15/2004 |
Number | Date | Country | |
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60391966 | Jun 2002 | US |