This application claims the benefit of priority to Japanese Patent Application Number 2022-116971 filed on Jul. 22, 2022. The entire contents of the above-identified application are hereby incorporated by reference.
The techniques disclosed in the present specification relate to a detector.
A radio frequency (RF) generator applied to a detector using a field asymmetric ion mobility spectrometry (FAIMS) system is known, as described in JP 2015-524164 T. The radio frequency generator described in JP 2015-524164 T includes an active device that drives a series resonant circuit. The series resonant circuit includes a self-resonant dual inductor. The radio frequency generator may be used to drive a capacitive load.
Output of the series resonant circuit of the radio frequency generator described in JP 2015-524164 T is directly connected to the capacitive load of the detector using the field asymmetric ion mobility spectrometry. Thus, when load fluctuations occur in the detector, potential fluctuations occur in the series resonant circuit, making stable detection difficult.
The techniques described in this specification have been created based on the above-described circumstances, and achieve stable detection.
(1) A detector related to the techniques described in this specification includes a first electrode, a second electrode facing the first electrode with a space and forming a flow path for charged particles as objects to be detected between the first electrode and the second electrode, a third electrode arranged side by side with the second electrode on a downstream side in the flow path with respect to the second electrode and configured to collect the charged particles, and a potential supply circuit configured to supply a potential to at least one of the first electrode and the second electrode, in which the potential supply circuit includes a first inductor including a first input portion and a first output portion, and a second inductor including a second input portion and a second output portion, the first input portion of the first inductor is connected to a DC power supply, and the second input portion of the second inductor is connected to the first electrode or the second electrode.
(2) In addition to (1), in the detector, the potential supply circuit may include a transistor and a resonant circuit, the transistor may include a gate electrode, a source electrode, and a drain electrode, the gate electrode may be connected to a PWM signal supply section configured to generate a PWM signal, and the drain electrode and the resonant circuit may be connected in parallel with respect to the first output portion.
(3) In addition to (2), in the detector, the second input portion of the second inductor may be connected to the first electrode.
(4) In addition to (3), in the detector, the second input portion and the first electrode may be connected in parallel with respect to a first compensation potential supply section configured to generate a first compensation potential.
(5) In addition to (2), the detector may include a third inductor including a third input portion and a third output portion, and a core having an annular shape around which the first inductor, the second inductor, and the third inductor are wound, in which a winding direction of the second inductor with respect to the core from the second input portion to the second output portion may be the same as a winding direction of the third inductor with respect to the core from the third output portion to the third input portion, the second input portion of the second inductor may be connected to the first electrode, and the third input portion of the third inductor may be connected to the second electrode.
(6) In addition to (5), in the detector, the second input portion and the first electrode may be connected in parallel with respect to a second compensation potential supply section configured to generate a second compensation potential, and the third input portion and the second electrode may be connected in parallel with respect to a third compensation potential supply section configured to generate a third compensation potential.
(7) In addition to (2), in the detector, the second input portion of the second inductor may be connected to the first electrode, and the second electrode may be connected in parallel to the drain electrode and the resonant circuit with respect to the first output portion.
(8) In addition to (7), in the detector, the second input portion and the first electrode may be connected in parallel with respect to a fourth compensation potential supply section configured to generate a fourth compensation potential, and the second electrode may be connected to a fifth compensation potential supply section configured to generate a fifth compensation potential.
The techniques described in the present specification achieve stable detection.
The disclosure will be described with reference to the accompanying drawings, wherein like numbers reference like elements.
A first embodiment will be described with reference to
As illustrated in
The ionization source 10 is a device that ionizes atoms and molecules of a compound (sample) to be analyzed. When the compound is ionized by the ionization source 10, the ionized compound becomes a charged particle (sample ion) detectable in the detection cell 20. The charged particle is an object to be detected by the detector 50. An ionization method employed by the ionization source 10 is not limited, and any of various existing ionization sources can be used. To be specific, the ionization methods include, for example, an electron impact (EI) method, a chemical ionization method, a gas discharge method, a photoionization method, a desorption ionization method, an electrospray ionization (ESI) method, a thermal ionization method, an ambient ionization method, and a combination thereof. An ionization source capable of ionizing a component to be detected may be appropriately selected. In this example, although not specifically illustrated, a needle electrode is provided as the ionization source 10. The needle electrode generates a corona discharge under atmospheric pressure to generate reactive ions. The reactive ions indirectly generate charged particles by reacting with sample atoms and sample molecules. The charged particles are not limited to ions to be analyzed, but may be reactant ions, ion clusters, or the like.
Examples of the ionization source 10 include, in addition to the needle electrode described above, an ionization unit that includes a radioactive ion source containing a nickel isotope (63Ni), an americium isotope (241Am), or the like and ionizes a sample generated from the radioactive ion source, and an ionization unit that includes an ultraviolet pulsed laser oscillator and irradiates an ultraviolet pulsed laser beam to directly ablate and ionize a sample. The charged particles generated by the ionization source 10 are carried into the detection cell 20 by an air flow generated by supplying an atmospheric gas (neutral buffer gas), such as air or a carrier gas, by the pump 30, which will be described later.
The pump 30 is a component for moving the atmospheric gas containing the charged particles into the detection cell 20 along a flow direction. The pump 30 of the present embodiment is installed downstream of the detection cell 20 in the flow direction. As the pump 30, any of various air supply devices that can supply the charged particles generated by the ionization source 10 into the detection cell 20, which will be described later, at a predetermined speed can be used. An air supply mechanism of the pump 30 is not limited, and may be a diaphragm type, an impeller type, a piston type, a rotary vane type, another air supply device, or the like. Depending on a size or the like of the detection cell 20, as the pump 30, for example, a micro-blower with a maximum discharge pressure of about 0.03 MPa or less and an air supply rate of about 1 L/min or less can be used. For example, a micro-blower in which a diaphragm is fluctuated due to high frequency vibration (e.g., ultrasonic vibration) generated by piezoelectric ceramics is preferable as the pump 30 used in the present embodiment because it can supply air while suppressing pulsation.
The detection cell 20 is a component that separates (filters) charged particles generated by the ionization source 10 based on a difference in mobility, thereby detecting charged particles for each predetermined mobility. The detection cell 20 includes a first electrode 21, a second electrode 22, a first substrate 23 (an example of a support body), a second substrate 24 (an example of a support body), a detection electrode 26, and a deflection electrode 27. All of these elements of the detection cell 20 may be disposed in a chamber.
The first electrode 21 and the second electrode 22 are disposed to face each other to form a pair of parallel plate filter electrodes. Main surfaces of the first electrode 21 and the second electrode 22 facing each other are parallel. A predetermined distance is kept between the first electrode 21 and the second electrode 22. A flow path 25 for charged particles is formed between the first electrode 21 and the second electrode 22. Hereinafter, a direction (main direction) in which charged particles flow in the flow path 25 is referred to as “flow direction”. The flow path 25 includes an ion separation space (drift space). The first electrode 21 and the second electrode 22 of this example are respectively provided on surfaces of the first substrate 23 and the second substrate 24, which will be described later, facing each other.
Shapes, sizes, and the like of the first electrode 21 and the second electrode 22 are not limited. The first electrode 21 and the second electrode 22 of this example each have rectangular shapes that are slightly long in the flow direction. Dimensions of the first electrode 21 and second electrode 22 along the flow direction of the charged particles are not limited to this, but may be, for example, about 0.1 cm or more (such as 1 cm or more) and about 50 cm or less (such as 10 cm or less). Thicknesses of the first electrode 21 and the second electrode 22 are not limited, and may be independently set as appropriate in a range of about 50 nm or more and 1 μm or less, for example. The thicknesses of the first electrode 21 and the second electrode 22 may be typically 600 nm or less, such as 400 nm or less, and typically 100 nm or more, such as 200 nm or more.
A distance (filter gap) between the first electrode 21 and the second electrode 22 is not strictly limited. Narrowing the filter gap is preferable because field intensity formed in the ion separation space (corresponding to a dispersion voltage described later) can be effectively increased. For example,
A material for the first electrode 21 and the second electrode 22 is not limited. The material for the first electrode 21 and the second electrode 22 may be any of various conductive materials capable of generating an electrical field, which will be described later, between the electrodes 21 and 22, and may be a metal material, an inorganic conductive material, or an organic conductive material. When a sample to be detected and ions thereof are considered to be metal corrosive, either the inorganic conductive material or the organic conductive material may be used as the conductive material for surfaces of the first electrode 21 and the second electrode 22. The metal material for the first electrode 21 and the second electrode 22 is not limited. For example, when the first electrode 21 and the second electrode 22 are fabricated by a lithography technique using an ArF excimer laser, the first electrode 21 and the second electrode 22 may be made of one metal selected from highly conductive metals such as gold (Au), copper (Cu), titanium (Ti), aluminum (Al), chromium (Cr), molybdenum (Mo), tantalum (Ta), tungsten (W), and alloys of these metals, alloys containing two or more of these metals, and the like. Among these metal materials, for example, W/Ta, Ti/Al, Ti/Al/Ti, Cu/Ti, or the like may be layered in order from an upper layer side, thereby enhancing physical properties such as adhesion to underlayers (typically, the first substrate 23 and the second substrate 24). Examples of inorganic conductive materials include indium tin oxide (ITO), indium zinc oxide (IZO), indium gallium zinc oxide (IGZO), and ZnO. Examples of organic conductive materials include polyacetylene and polythiophenes. The first electrode 21 and the second electrode 22 may have layered structures of two or more of a metal material, an inorganic conductive material, and an organic conductive material.
The first substrate 23 is a component that supports the first electrode 21. In the present embodiment, as illustrated in
The first substrate 23 and the second substrate 24 of the present embodiment can be made of any of various insulating materials having electrical insulating properties. Examples of insulating materials include materials having a volume resistivity of 107 Ωcm or more (e.g., 1010 Ωcm or more, 1012 Ωcm or more, or 1015 Ωcm or more) at room temperature (e.g., 25° C.), such as organic materials and inorganic materials having the above volume resistivity. Although not limited thereto, in the present embodiment, flat glass substrates are used as the first substrate 23 and the second substrate 24 from the viewpoint that the electrodes can be suitably formed by a lithography technique. Thicknesses of the first substrate 23 and the second substrate 24 are not limited, but may be, for example, about 0.1 to 1 mm (such as 0.5 mm or 0.7 mm).
The detection electrode 26 is a component that receives charges of charged particles introduced into the detection cell 20 when the charged particles come into contact with the detection electrode 26. The detection electrode 26 is a third electrode arranged side by side with the second electrode 22 on the downstream side in the flow path 25. The detection electrode 26 has a collecting surface 26A that receives charged particles. The detection electrode 26 is connected to the control unit 40. With such a configuration, the control unit 40 can count the number of charged particles that the detection electrode 26 has received on the collecting surface 26A.
The deflection electrode 27 is a component for deflecting the charged particles introduced into the detection cell 20 toward the detection electrode 26 so that the detection electrode 26 collects the charged particles. The deflection electrode 27 is a fourth electrode arranged side by side with the first electrode 21 on the downstream side in the flow path 25. The deflection electrode 27 is placed so as to face the detection electrode 26. The deflection electrode 27 is connected to a second potential adjustment unit 42, which will be described later. The deflection electrode 27 can form an electrical field between the detection electrode 26 and the deflection electrode 27 that deflects charged particles to the detection electrode 26 by applying a voltage by the second potential adjustment unit 42. A space between the detection electrode 26 and the deflection electrode 27 is a detection space for detecting charged particles that have passed through the ion separation space.
Shapes of the detection electrode 26 and the deflection electrode 27 are not limited. Thicknesses of the detection electrode 26 and the deflection electrode 27 may be, for example, about 1 μm or less, typically 600 nm or less, such as 500 nm or less, 400 nm or less, or 200 nm or less. The thicknesses of the detection electrode 26 and the deflection electrode 27 may each independently be about 10 nm or more, typically 50 nm or more, such as 100 nm or more. A material and structure of the detection electrode 26 and the deflection electrode 27 may be the same as those of the first electrode 21 and the second electrode 22 described above.
The control unit 40 is a component that controls drive of the analyzer 1. As illustrated in
The control unit 40 is a microcomputer including an interface (I/F) that transmits and receives various kinds of information and the like, a central processing unit (CPU) that executes commands of a control program, a read only memory (ROM) that stores the program that is executed by the CPU, a random access memory (RAM) that is used as a working area for developing the program, a storage unit M that stores various kinds of information, a timer T that has a clocking function, and the like. Although not limited thereto, the ROM may store, for example, computer programs, databases, and data tables used for applying voltages to a first potential adjustment unit 41 and the second potential adjustment unit 42, respectively as well as a computer program, a database, and a table for executing various analysis processes based on the number of detected charged particles. The storage unit M can store, for example, ID information about an analyte to be analyzed, information related to the number of detected charged particles, information used for various analysis processes, information related to analysis results, and the like.
The control unit 40 includes the first potential adjustment unit 41, the second potential adjustment unit 42, a measurement unit 43, an ionization source control unit 44, and a flow rate adjustment unit 45. Each of these units may be independently configured by hardware, or may be functionally implemented by execution of a program by the CPU.
The first potential adjustment unit 41 is an element that adjusts a potential difference that occurs between the first electrode 21 and the second electrode 22. The first potential adjustment unit 41 generates a potential difference (filter voltage) between the first electrode 21 and the second electrode 22, which forms an electrical field between the first electrode 21 and the second electrode 22. Here, ion mobility is constant in a low electrical field regardless of field intensity, but a value of the ion mobility changes depending on the field intensity in a high electrical field. Thus, the first potential adjustment unit 41 typically includes a variable voltage generator such as a pulse voltage generator, and can apply, for example, a dispersion voltage (DV) with a rectangular waveform illustrated in
In the ion separation space between the first electrode 21 and the second electrode 22, a flow of a carrier gas (typically neutral) containing charged particles is formed at a constant flow rate by driving the pump 30 with the flow rate adjustment unit 45, which will be described later. Here, when the voltage of the high voltage level VH is applied by the first potential adjustment unit 41, a high electrical field is formed in the ion separation space. When the voltage of the low voltage level VL is applied by the first potential adjustment unit 41, a low electrical field is formed in the ion separation space. The high electrical field has a polarity different from that of the low electrical field. When charged particles are sent into an environment in which such mutually asymmetrical electrical fields are alternately generated, the charged particles zigzag so as to be alternately attracted by the first electrode 21 and the second electrode 22. At this time, the charged particles largely deflected by the first electrode 21 or the second electrode 22 hit the first electrode 21 or the second electrode 22 and cannot pass through the flow path 25. Only charged particles balanced between the first electrode 21 and the second electrode 22 pass through the flow path 25 and are sent to the detection electrode 26 located downstream. Ion species passing through the flow path 25 can be changed as follows. That is, the first potential adjustment unit 41 applies, for example, a compensation voltage (CV) illustrated in
The second potential adjustment unit 42 is an element that applies a predetermined potential difference between the detection electrode 26 and the deflection electrode 27. The second potential adjustment unit 42 in the present embodiment is connected to the deflection electrode 27, and applies a potential to the deflection electrode 27. When charged particles introduced into the detection cell 20 are positive ions, the second potential adjustment unit 42 adjusts the potential of the deflection electrode 27 such that the potential of the deflection electrode 27 is higher than that of the detection electrode 26. When charged particles introduced into the detection cell 20 are negative ions, the second potential adjustment unit 42 adjusts the potential of the deflection electrode 27 such that the potential of the deflection electrode 27 is lower than that of the detection electrode 26. Thus, the charged particles that have passed through the ion separation space can be deflected toward the detection electrode 26.
The measurement unit 43 is an element that detects the number of charged particles that have reached the detection electrode 26. The measurement unit 43 is connected to the detection electrode 26, and converts a current value based on the number of charged particles that have reached the detection electrode 26 into a voltage value using a transimpedance circuit to acquire the number of ions. The measurement unit 43 may be configured not only to measure the number of charged particles but also to qualify and quantify the charged particles in cooperation with the first potential adjustment unit 41, for example. Information related to the number of charged particles and the like measured by the measurement unit 43 is stored in the storage unit M, for example.
The ionization source control unit 44 is connected to the ionization source 10 and is configured to control an operation of the ionization source 10. The ionization source control unit 44 can switch charged particles to be generated between positive ions and negative ions, for example, by switching a polarity of the voltage applied to the needle electrode in the ionization source 10 between positive and negative. Although not limited thereto, when the ionization source control unit 44 causes the ionization source 10 to generate negative charged particles, the first potential adjustment unit 41 and the second potential adjustment unit 42 adjust the voltages applied to the first electrode 21 and the deflection electrode 27, respectively, so that the negative charged particles can pass through the flow path 25. When the ionization source control unit 44 causes the ionization source 10 to generate positive charged particles, the first potential adjustment unit 41 and the second potential adjustment unit 42 adjust the voltages applied to the first electrode 21 and the deflection electrode 27, respectively, so that the positive charged particles can pass through the flow path 25.
The flow rate adjustment unit 45 is connected to the pump 30 and is configured to control an operation of the pump 30. The flow rate adjustment unit 45 can adjust a flow rate of gas in the detection cell 20 by controlling, for example, timings of driving and stopping the pump 30 and a rotational speed of a fan of the pump 30.
Next, a detailed configuration of the detector 50 will be described. The detector 50 includes at least the first electrode 21, the second electrode 22, and the detection electrode 26, which are constituent elements of the detection cell 20, and the first potential adjustment unit 41, which is a constituent element of the control unit 40. The first electrode 21, the second electrode 22, and the detection electrode 26 are as described above, and the first potential adjustment unit 41 will be described in detail below with reference to
As illustrated in
As illustrated in
The dual inductor 64 includes the first inductor 64A and a second inductor 64B. The first inductor 64A is formed of a winding, and one end portion thereof is a first input portion 64A1 and the other end portion thereof is a first output portion 64A2. The first input portion 64A1 is connected in series to the DC power supply 61. The first output portion 64A2 is connected in parallel to the transistor 65 and the resonant circuit 66. An inductance of the first inductor 64A is, for example, about 40 pH.
The second inductor 64B is formed of a winding, and one end portion thereof is a second input portion 64B1 and the other end portion thereof is a second output portion 64B2. The second input portion 64B1 is connected in parallel to the first compensation potential supply section 63 and the first electrode 21. The first compensation potential supplied from the first compensation potential supply section 63 to the first electrode 21 is the compensation voltage CV illustrated in
As illustrated in
The transistor 65 is, for example, an N-channel metal-oxide-semiconductor field-effect transistor (MOSFET). To be specific, the transistor 65 may be, for example, a transistor with a model number “STW14NM50” manufactured by STMicroelectronics. As illustrated in
The resonant circuit 66 includes two inductors L1 and L2, three capacitor C2, C3, and C4, one resistor R3, and one diode D1. The inductor L1 and the capacitor C2 are connected in series. An inductance of the inductor L1 is, for example, about 1.72 pH. An electrostatic capacitance of the capacitor C2 is, for example, about 2.7 nF. The inductor L1, the capacitor C3, and the diode D1 are connected in parallel with respect to the first output portion 64A2 of the first inductor 64A. Of a pair of electrodes constituting the capacitor C3, the electrode on an opposite side of the electrode connected to the first output portion 64A2 is grounded. An electrostatic capacitance of the capacitor C3 is, for example, about 450 pF. An anode of the diode D1 is grounded. The diode D1 is a fast recovery diode suitable for rectifying high frequencies. The diode D1 may be, for example, a diode with a model number “RF305BM6S” manufactured by ROHM Co., Ltd. Of a pair of electrodes constituting the capacitor C2, to the electrode on an opposite side of the electrode connected to the inductor L1, the inductor L2 and the resistor R3 are connected in parallel. An inductance of the inductor L2 is, for example, about 265 nH. The capacitor C4 is connected in series to the inductor L2. An electrostatic capacitance of the capacitor C4 is, for example, about 1.18 nF. Of a pair of electrodes of the capacitor C4, the electrode on an opposite side of the electrode connected to the inductor L2 is grounded. A resistance value of the resistor R3 is, for example, about 50Ω. The resistor R3 is grounded.
A return current flows through the resonant circuit 66 having such a configuration in accordance with a drive state of the transistor 65. To be specific, when the transistor 65 is in the ON state, in the resonant circuit 66, the return current flows from a capacitor C2 side to an inductor L1 side. At this time, the drain current flowing through the transistor 65 is the sum of the current flowing from the DC power supply 61 and the return current. Thus, when the transistor 65 is in the ON state, no current flows through the capacitor C3, and the potential thereof is maintained at 0. The potential of the capacitor C3 matches a drain voltage. On the other hand, when the transistor 65 is in the OFF state, the return current flows from the inductor L1 side to the capacitor C2 side in the resonant circuit 66. That is, the return current flowing through the resonant circuit 66 when the transistor 65 is in the OFF state is opposite to the return current flowing through the resonant circuit 66 when the transistor 65 is in the ON state. When the transistor 65 is in the OFF state, the current from the DC power supply 61 is divided into a current flowing through the capacitor C2 and a current flowing through the capacitor C3. At this time, a current obtained by subtracting the return current from the current flowing from the DC power supply 61 flows through the capacitor C3. In accordance with this, the capacitor C3 is charged, and the potential of the capacitor C3, that is, the drain voltage is increased. By appropriately setting the capacitors C2 and C3, the drain voltage can be set to 0 V at a timing when the transistor 65 is switched from the OFF state to the ON state and at a timing when the transistor 65 is switched from the ON state to the OFF state (a timing of switching from the ON period of the PWM signal to the OFF period and a timing of switching from the OFF period of the PWM signal to the ON period). Thus, the transistor 65 can be driven in a zero voltage switching (ZVS) state.
An induced electromotive force is generated in the second inductor 64B in synchronization with the timing when the transistor 65 is switched from the OFF state to the ON state and at the timing when the transistor 65 is switched from the ON state to the OFF state. When the power supply voltage of the DC power supply 61 is “V1” and the drain voltage of the transistor 65 is “Vd”, the induced electromotive force generated in the second inductor 64B is “Vd−V1”. In other words, the induced electromotive force is generated in the second inductor 64B in which the power supply voltage of the DC power supply 61 is offset from the drain voltage. The induced electromotive force generated in the second inductor 64B is then applied to the first electrode 21. Voltages with opposite polarities are applied to the first electrode 21 in synchronization with the timing at which the transistor 65 is switched from the OFF state to the ON state and the timing at which the transistor 65 is switched from the ON state to the OFF state. To be specific, during an ON period in which the transistor 65 is in the ON state, a voltage having a positive polarity is applied to the first electrode 21, and during an OFF period in which the transistor 65 is in the OFF state, a voltage having a negative polarity is applied to the first electrode 21. As described above, the dispersion voltage DV with a rectangular waveform (see
As described above, the first electrode 21 is connected to the second input portion 64B1 of the second inductor 64B included in the potential supply circuit 60, but is not directly connected to the first inductor 64A. Thus, even when load fluctuations occur, for example, when variations occur in the space between the first electrode 21 and the second electrode 22, potential fluctuations, due to the load fluctuations, in the first inductor 64A connected to the DC power supply 61 at the first input portion 64A1 are avoided. This stabilizes the induced electromotive force generated in the second inductor 64B, thus stabilizing detection of charged particles.
Next, specific various voltage waveforms and the like when operating the potential supply circuit 60 of the detector having the above-described configuration will be described with reference to
According to
Next, waveforms of a voltage Vfup applied to the first electrode 21 are shown in the graph in
According to
As described above, the detector 50 of the present embodiment includes the first electrode 21, the second electrode 22 facing the first electrode 21 with a space and forming the flow path 25 for charged particles as the objects to be detected between the first electrode 21 and the second electrode 22, the detection electrode (third electrode) 26 arranged side by side with the second electrode 22 on the downstream side in the flow path 25 with respect to the second electrode 22 and configured to collect the charged particles, and the potential supply circuit 60 configured to supply a potential to at least one of the first electrode 21 and the second electrode 22. The potential supply circuit 60 includes the first inductor 64A including the first input portion 64A1 and the first output portion 64A2, and the second inductor 64B including the second input portion 64B1 and the second output portion 64B2. The first input portion 64A1 of the first inductor 64A is connected to the DC power supply 61, and the second input portion 64B1 of the second inductor 64B is connected to the first electrode 21 or the second electrode 22.
When a potential is supplied to at least one of the first electrode 21 and the second electrode 22 by the potential supply circuit 60, an electrical field is generated between the first electrode 21 and the second electrode 22. This electrical field controls whether or not charged particles pass through the flow path 25 formed between the first electrode 21 and the second electrode 22. The charged particles passing through the flow path 25 are collected and detected by the detection electrode 26. The first electrode 21 or the second electrode 22 is connected to the second input portion 64B1 of the second inductor 64B included in the potential supply circuit 60, but is not directly connected to the first inductor 64A. Thus, even when load fluctuations occur, for example, when variations occur in the space between the first electrode 21 and the second electrode 22, potential fluctuations, due to the load fluctuations, in the first inductor 64A connected to the DC power supply 61 at the first input portion 64A1 are avoided. This stabilizes the induced electromotive force generated in the second inductor 64B, thus stabilizing detection of charged particles.
The potential supply circuit 60 includes the transistor and the resonant circuit 66. The transistor 65 includes the gate electrode 65A, the source electrode 65B, and the drain electrode 65C. The gate electrode 65A is connected to the PWM signal supply section 62 that generates the PWM signal, and the drain electrode 65C and the resonant circuit 66 are connected in parallel with respect to the first output portion 64A2. When the PWM signal generated from the PWM signal supply section 62 is supplied to the gate electrode 65A, during the ON period of the PWM signal, the drain current flows between the source electrode and the drain electrode 65C and the return current flows through the resonant circuit 66, and during the OFF period of the PWM signal, the return current flows through the resonant circuit 66 in the direction opposite to that during the ON period. At the timing of switching from the ON period to the OFF period and at the timing of switching from the OFF period to the ON period, the potential of the drain electrode 65C is substantially 0 V. That is, the transistor 65 is driven in the zero voltage switching (ZVS) state. Thus, power consumption can be reduced. The induced electromotive force synchronized with the PWM signal is generated in the second inductor 64B. To be specific, the potential is generated periodically such that the polarity (positive or negative) of the potential generated in the second inductor 64B is reversed between the ON period and the OFF period of the PWM signal. Thus, since the positive and negative potentials are periodically applied to at least one of the first electrode 21 and the second electrode 22, whether or not the charged particles pass through the flow path 25 between the first electrode 21 and the second electrode 22 is controlled favorably.
The second input portion 64B1 of the second inductor 64B is connected to the first electrode 21. When the induced electromotive force synchronized with the PWM signal is generated in the second inductor 64B, positive and negative potentials are periodically applied to the first electrode 21 connected to the second input portion 64B1 of the second inductor 64B. To be specific, during the ON period of the PWM signal, a potential having a negative polarity or a positive polarity is applied to the first electrode 21, and during the OFF period of the PWM signal, a potential having a positive polarity or a negative polarity is applied to the first electrode 21. Thus, between the first electrode 21 and the second electrode 22, a potential difference synchronized with the PWM signal is periodically generated. Since the first electrode 21 and the second electrode 22 are electrically separated from the transistor 65 and the resonant circuit 66 that are the constituent elements of the potential supply circuit 60, even when load fluctuations occur due to the first electrode 21 and the second electrode 22, potential fluctuations due to the load fluctuations can be avoided in the transistor 65 and the resonant circuit 66.
The second input portion 64B1 and the first electrode 21 are connected in parallel with respect to the first compensation potential supply section 63 that generates the first compensation potential. The potential obtained by superimposing the first compensation potential generated from the first compensation potential supply section 63 on the potential based on the induced electromotive force generated in the second inductor 64B is applied to the first electrode 21. Whether or not charged particles pass through the flow path 25 is controlled according to the first compensation potential.
A second embodiment will be described with reference to
As illustrated in
As illustrated in
As illustrated in
In the potential supply circuit 160 having such a configuration, when a transistor 165 is switched from an OFF state to an ON state and from the ON state to the OFF state based on a PWM signal supplied from a PWM signal supply section 162, induced electromotive forces are generated in the second inductor 164B and the third inductor 64D in synchronization with the switching. When the induced electromotive force synchronized with the PWM signal is generated in the second inductor 164B, positive and negative potentials are periodically applied to the first electrode 121 connected to the second input portion 164B1 of the second inductor 164B. To be specific, during an ON period of the PWM signal, a potential having a negative polarity is applied to the first electrode 121, and during an OFF period of the PWM signal, a potential having a positive polarity is applied to the first electrode 121. When the induced electromotive force synchronized with the PWM signal is generated in the third inductor 64D, positive and negative potentials are periodically applied to the second electrode 122 connected to the third input portion 64D1 of the third inductor 64D. To be specific, during the ON period of the PWM signal, a potential having a positive polarity is applied to the second electrode 122, and during the OFF period of the PWM signal, a potential having a negative polarity is applied to the second electrode 122. Thus, potentials applied to the first electrode 121 and the second electrode 122 always have opposite polarities during both the ON period and the OFF period. Therefore, a potential difference generated between the first electrode 121 and the second electrode 122 is about twice as large as that in the first embodiment. Thus, field intensity of an electrical field generated between the first electrode 121 and the second electrode 122 can be increased. The potential difference generated between the first electrode 121 and the second electrode 122 is a dispersion voltage DV. Moreover, a potential obtained by superimposing the second compensation potential generated from the second compensation potential supply section 67 on the potential based on the induced electromotive force of the second inductor 164B is applied to the first electrode 121. Similarly, a potential obtained by superimposing the third compensation potential generated from the third compensation potential supply section 68 on the potential based on the induced electromotive force of the third inductors 64D is applied to the second electrode 122.
Next, specific various voltage waveforms and the like when operating the potential supply circuit 160 having the above-described configuration will be described with reference to
According to
Next, waveforms of the potential difference between the first electrode 121 and the second electrode 122 (Vfup−Vfdown) are shown in a graph in
First, the voltage Vfup is applied to the first electrode 121. The voltage Vfup is obtained by superimposing the second compensation potential supplied from the second compensation potential supply section 67 on the potential obtained by offsetting the power supply voltage V1 of the DC power supply 161 from the drain voltage Vd of the transistor 165. The voltage Vfdown is applied to the second electrode 122. The voltage Vfdown is obtained by superimposing the third compensation potential supplied from the third compensation potential supply section 68 on the potential obtained by reversing the polarity of the potential obtained by offsetting the power supply voltage V1 of the DC power supply 161 from the drain voltage Vd of the transistor 165. Thus, as shown in
As described above, according to the present embodiment, the detector 50 includes the third inductor 64D including the third input portion 64D1 and the third output portion 64D2, and the core 164C having an annular shape around which the first inductor 164A, the second inductor 164B, and the third inductor 64D are wound together. The winding direction of the second inductor 164B with respect to the core 164C from the second input portion 164B1 to the second output portion 164B2 is the same as the winding direction of the third inductor 64D with respect to the core 164C from the third output portion 64D2 to the third input portion 64D1. The second input portion 164B1 of the second inductor 164B is connected to the first electrode 121, and the third input portion 64D1 of the third inductor 64D is connected to the second electrode 122. When the induced electromotive force synchronized with the PWM signal is generated in the second inductor 164B, positive and negative potentials are periodically applied to the first electrode 121 connected to the second input portion 164B1 of the second inductor 164B. To be specific, during the ON period of the PWM signal, a potential having a negative polarity or a positive polarity is applied to the first electrode 121, and during the OFF period of the PWM signal, a potential having a positive polarity or a negative polarity is applied to the first electrode 121. When the induced electromotive force synchronized with the PWM signal is generated in the third inductor 64D, positive and negative potentials are periodically applied to the second electrode 122 connected to the third input portion 64D1 of the third inductor 64D. To be specific, during the ON period of the PWM signal, a potential having a positive polarity or a negative polarity is applied to the second electrode 122, and during the OFF period of the PWM signal, a potential having a positive polarity or a negative polarity is applied to the second electrode 122. Thus, since the potentials of opposite polarities are applied to the first electrode 121 and the second electrode 122, the potential difference between the first electrode 121 and the second electrode 122 is large. Thus, the field intensity of the electrical field generated between the first electrode 121 and the second electrode 122 can be increased. Since the first electrode 121 and the second electrode 122 are electrically separated from the transistor 165 and the resonant circuit 166 that are the constituent elements of the potential supply circuit 160, even when load fluctuations occur due to the first electrode 121 and the second electrode 122, potential fluctuations can be avoided in the transistor 165 and the resonant circuit 166 due to the load fluctuations.
The second input portion 164B1 and the first electrode 121 are connected in parallel with respect to the second compensation potential supply section 67 that generates the second compensation potential, and the third input portion 64D1 and the second electrode 122 are connected in parallel with respect to the third compensation potential supply section 68 that generates the third compensation potential. The potential obtained by superimposing the second compensation potential generated from the second compensation potential supply section 67 on the potential based on the induced electromotive force generated in the second inductor 164B is applied to the first electrode 121. The potential obtained by superimposing the third compensation potential generated from the third compensation potential supply section 68 on the potential based on the induced electromotive force generated in the third inductor 64D is applied to the second electrode 122. Whether or not charged particles pass through the flow path is controlled according to the second compensation potential and the third compensation potential.
A third embodiment will be described with reference to
As illustrated in
As illustrated in
As illustrated in
In the potential supply circuit 260 having such a configuration, when a transistor 265 is switched from an OFF state to an ON state and from the ON state to the OFF state based on a PWM signal supplied from a PWM signal supply section 262, an induced electromotive force is generated in the second inductor 264B in synchronization with the switching. When the induced electromotive force synchronized with the PWM signal is generated in the second inductor 264B, positive and negative potentials are periodically applied to the first electrode 221 connected to the second input portion 264B1 of the second inductor 264B. To be specific, during an ON period of the PWM signal, a potential having a positive polarity is applied to the first electrode 221, and during an OFF period of the PWM signal, a potential having a negative polarity is applied to the first electrode 221. That is, positive and negative potentials are periodically applied to the first electrode 221 of the present embodiment in a phase opposite to that of the first and second embodiments. On the other hand, negative and positive potentials are applied to the second electrode 222 via the capacitor C6 in the same period as the drain voltage Vd in synchronization with switching from an OFF state to an ON state and from the ON state to the OFF state in the transistor 265. To be specific, during the ON period of the PWM signal, a potential having a negative polarity is applied to the second electrode 222, and during the OFF period of the PWM signal, a potential having a positive polarity is applied to the second electrode 222. Thus, potentials applied to the first electrode 221 and the second electrode 222 always have opposite polarities during both the ON period and the OFF period. Therefore, a potential difference generated between the first electrode 221 and the second electrode 222 is about twice as large as that in the first embodiment. Thus, field intensity of an electrical field generated between the first electrode 221 and the second electrode 222 can be increased. The potential difference generated between the first electrode 221 and the second electrode 222 is a dispersion voltage DV. Moreover, a potential obtained by superimposing the fourth compensation potential generated from the fourth compensation potential supply section 69 on the potential based on the induced electromotive force of the second inductor 264B is applied to the first electrode 221. Similarly, a potential obtained by superimposing the fifth compensation potential generated from the fifth compensation potential supply section 70 on the potential based on the drain voltage Vd is applied to the second electrode 222.
Next, specific various voltage waveforms and the like when operating the potential supply circuit 260 having the above-described configuration will be described with reference to
According to
Next, waveforms of the potential difference (Vfup−Vfdown) between the first electrode 221 and the second electrode 222 are shown in a graph in
First, the voltage Vfup is applied to the first electrode 221. The voltage Vfup is obtained by superimposing the fourth compensation potential supplied from the fourth compensation potential supply section 69 on the potential obtained by reversing the polarity of the potential obtained by offsetting the power supply voltage V1 of the DC power supply 261 from the drain voltage Vd of the transistor 265. The voltage Vfdown is applied to the second electrode 222. The voltage Vfdown is obtained by superimposing the fifth compensation potential supplied from the fifth compensation potential supply section 70 on the potential obtained by offsetting the power supply voltage V1 of the DC power supply 261 from the drain voltage Vd of the transistor 265. Thus, as shown in
As described above, according to the present embodiment, the second input portion 264B1 of the second inductor 264B is connected to the first electrode 221, and the second electrode 222 is connected in parallel to the drain electrode 265C and the resonant circuit 266 with respect to the first output portion 264A2. When the induced electromotive force synchronized with the PWM signal is generated in the second inductor 264B, positive and negative potentials are periodically applied to the first electrode 221 connected to the second input portion 264B1 of the second inductor 264B. To be specific, during the ON period of the PWM signal, a potential having a positive polarity or a negative polarity is applied to the first electrode 221, and during the OFF period of the PWM signal, a potential having a negative polarity or a positive polarity is applied to the first electrode 221. the second electrode 222 is connected in parallel to the drain electrode 265C and the resonant circuit 266 with respect to the first output portion 264A2. Thus, positive and negative potentials are periodically applied to the second electrode 222 based on the drain voltage that fluctuates in synchronization with the PWM signal. To be specific, during the ON period of the PWM signal, a potential having a negative polarity or a positive polarity is applied to the second electrode 222, and during the OFF period of the PWM signal, a potential having a negative polarity or a positive polarity is applied to the second electrode 222. Thus, since the potentials having opposite polarities are applied to the first electrode 221 and the second electrode 222, the potential difference between the first electrode 221 and the second electrode 222 is large. Thus, the field intensity of the electrical field generated between the first electrode 221 and the second electrode 222 can be increased.
The second input portion 264B1 and the first electrode 221 are connected in parallel with respect to the fourth compensation potential supply section 69 that generates the fourth compensation potential, and the second electrode 222 is connected to the fifth compensation potential supply section 70 that generates the fifth compensation potential. The potential obtained by superimposing the fourth compensation potential generated from the fourth compensation potential supply section 69 on the potential based on the induced electromotive force generated in the second inductor 264B is applied to the first electrode 221. The potential obtained by superimposing the fifth compensation potential generated from the fifth compensation potential supply section 70 on the potential based on the return current flowing through the resonant circuit 266 is applied to the second electrode 222. Whether or not charged particles pass through the flow path is controlled according to the fourth compensation potential and the fifth compensation potential.
The techniques disclosed in the present specification are not limited to the embodiments described above and illustrated in the drawings, and the following embodiments, for example, are also included within the technical scope.
(1) Specific circuit configurations of the potential supply circuits 60, 160, and 260 can be appropriately changed from the contents illustrated in the drawings. Circuit elements other than those illustrated in the drawings can be added to the potential supply circuits 60, 160, and 260. The circuit elements included in the potential supply circuits 60, 160, and 260 illustrated in the drawings can be changed to other circuit elements. The circuit elements included in the potential supply circuits 60, 160, and 260 illustrated in the drawings can be eliminated.
(2) In the configuration described in the first embodiment, the second input portion 64B1 of the second inductor 64B and the first compensation potential supply section 63 may be connected in parallel to the second electrode 22.
(3) In the configuration described in the first embodiment, the second input portion 64B1 of the second inductor 64B may be connected to the first electrode 21, and the first compensation potential supply section 63 may be connected to the second electrode 22.
(4) In the configuration described in the first embodiment, the second input portion 64B1 of the second inductor 64B may be connected to the second electrode 22, and the first compensation potential supply section 63 may be connected to the first electrode 21.
(5) In the configuration described in the second embodiment, the third input portion 64D1 of the third inductor 64D and the third compensation potential supply section 68 may be connected in parallel to the first electrode 121, and the second input portion 164B1 of the second inductor 164B and the second compensation potential supply section 67 may be connected in parallel to the second electrode 122.
(6) In the configuration described in the third embodiment, the first output portion 264A2, the drain electrode 265C, and the resonant circuit 266 may be coupled to the first electrode 221 via the capacitor C6, and the second input portion 264B1 of the second inductor 264B and the fourth compensation potential supply section 69 may be connected in parallel to the second electrode 222.
(7) In the configuration described in the first embodiment, the specific manner in which the windings of the inductors 64A and 64B are wound around the core 64C can be appropriately changed other than as illustrated in the drawing. Also, in the configuration described in the third embodiment, the specific manner in which the windings of the inductors 264A and 264B are wound around the core 264C can be appropriately changed other than as illustrated in the drawing. For example, the windings of the first inductors 64A and 264A and the windings of the second inductors 64B and 264B may be wound around the cores 64C and 264C so as to overlap each other.
(8) In the configuration described in the second embodiment, the specific manner in which the windings of the inductors 64D, 164A, and 164B are wound around the core 164C can be appropriately changed other than as illustrated in the drawing. For example, the winding of the first inductor 164A, the winding of the second inductor 164B, and the winding of the third inductor 64D may be wound around the core 164C so as to overlap each other.
(9) The dispersion voltage DV may be supplied to each of the first electrode 21, 121, and 221, and the compensation voltage CV may be supplied to each of the second electrode 22, 122, and 222. To be specific, the voltage Vfup applied to each of the first electrode 21, 121, and 221 is the dispersion voltage DV calculated by offsetting the power supply voltage V1 of each of the DC power supply 61, 161, and 261 from the drain voltage Vd. On the other hand, the voltage applied to each of the second electrode 22, 122, and 222 is the compensation voltage CV.
(10) Contrary to (9) above, the dispersion voltage DV may be supplied to each of the second electrode 22, 122, and 222 and the compensation voltage CV may be supplied to each of the first electrode 21, 121, and 221.
(11) In the configuration described in the first embodiment, both the first inductor 64A and the second inductor 64B may be wound clockwise around the core 64C.
(12) In the configuration described in the first embodiment, the winding direction of the first inductor 64A around the core 64C may be opposite to the winding direction of the second inductor 64B around the core 64C. To be specific, when the first inductor 64A is wound counterclockwise around the core 64C, the second inductor 64B may be wound clockwise around the core 64C. When the first inductor 64A is wound clockwise around the core 64C, the second inductor 64B may be wound counterclockwise around the core 64C.
(13) In the configuration described in the second embodiment, all of the first inductor 164A, the second inductor 164B, and the third inductor 64D may be wound clockwise around the core 164C.
(14) In the configuration described in the second embodiment, the winding direction of the first inductor 164A around the core 164C may be opposite to the winding direction of the second inductor 164B around the core 164C and the winding direction of the third inductor 64D around the core 164C. To be specific, when the first inductor 164A is wound counterclockwise around the core 164C, the second inductor 164B and the third inductor 64D may be wound clockwise around the core 164C. When the first inductor 164A is wound clockwise around the core 164C, the second inductor 164B and the third inductor 64D may be wound counterclockwise around the core 164C.
(15) In the configuration described in the third embodiment, the first inductor 264A may be wound clockwise around the core 264C, and the second inductor 264B may be wound counterclockwise around the core 264C.
(16) In the configuration described in the third embodiment, the winding direction of the first inductor 264A around the core 264C may be the same as the winding direction of the second inductor 264B around the core 264C. To be specific, both the first inductor 264A and the second inductor 264B may be wound counterclockwise around the core 264C. Alternatively, both the first inductor 264A and the second inductor 264B may be wound clockwise around the core 264C.
(17) In the configurations described in the first and third embodiments, the number of turns of each of the first inductors 64A and 264A around the cores 64C and 264C may be different from the number of turns of each of the second inductors 64B and 264B around the cores 64C and 264C. The voltage Vfup can be further amplified by adjusting a ratio between the number of turns of each of the first inductors 64A and 264A and the number of turns of each of the second inductors 64B and 264B.
(18) In the configuration described in the second embodiment, some or all of the number of turns of the first inductor 164A around the core 164C, the number of turns of the second inductor 164B around the core 164C, and the number of turns of the third inductor 64D around the core 164C may be different. The voltage Vfup can be further amplified by adjusting the number of turns of the first inductor 164A, the number of turns of the second inductor 164B, and the number of turns of the third inductor 64D.
While preferred embodiments of the disclosure have been described above, it is to be understood that variations and modifications will be apparent to those skilled in the art without departing from the scope and spirit of the disclosure. The scope of the disclosure, therefore, is to be determined solely by the following claims.
Number | Date | Country | Kind |
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2022-116971 | Jul 2022 | JP | national |