HEAT INTEGRATION

Abstract

A heat integration system for removing heat of reaction from an EC-1 Reactor and generating Chilled liquid for use by one or more Consumer Units, in a catalytic process for producing EC from EO for conversion into MEG wherein the system comprises an EC-1 Reactor Cooler suitable for removing heat from an EC-1 Reactor, an Intermediate Loop which is in communication with the Reactor Cooler and with an absorption Refrigeration Unit, and which is suitable for conducting Intermediate liquid therebetween, the absorption Refrigeration Unit being suitable for generating Chilled liquid,

Description

DESCRIPTION OF FIGURES

Embodiments of the invention are now illustrated in non limiting manner with respect to the following Examples and Figures wherein:

FIG. 1 illustrates a prior art EC/MEG unit.

FIGS. 2 to 5 illustrate embodiments of the heat integration system and control system of the invention.

FIG. 6 illustrates a separator for use in the systems of the invention.

FIGS. 7-10 are schematic flow diagrams of temperature control systems of the invention.

Claims

1. A heat integration system for removing heat of reaction from an EC-1 Reactor and generating Chilled liquid for use by one or more Consumer Units, in a catalytic process for producing EC from EO for conversion into MEG wherein the system comprises an EC-1 Reactor Cooler suitable for removing heat from an EC-1 Reactor, an Intermediate Loop which is in communication with the Reactor Cooler and with an absorption Refrigeration Unit, and which is suitable for conducting Intermediate liquid therebetween, the absorption Refrigeration Unit being suitable for generating Chilled liquid, and a Chilled liquid loop suitable for conducting Chilled liquid generated in the absorption Refrigeration Unit for use by one or more Consumer Units,the system being such that the absorption Refrigeration Unit uses heat generated in the EC-1 Reactor to generate Chilled liquid for the Chilled liquid loop and Consumer Unit(s),wherein the system additionally comprises a Shutdown Cooler having an independent cooling source which is suitable, alternatively or in addition to the absorption Refrigeration Unit, for removing heat from the EC-1 Reactor,and wherein the system additionally comprises an independent stand-by source of Chilled liquid which is suitable, alternatively or in addition to the absorption Refrigeration Unit, for generating chilled liquid, to serve the one or more Consumer Units.

2. A heat integration system according to claim 1, wherein the Intermediate Loop includes a bypass of the absorption Refrigeration Unit whereby Intermediate cooling liquid may be conducted to the absorption Refrigeration Unit for heat removal or may bypass the absorption Refrigeration Unit.

3. A heat integration system according to claim 1, wherein the EC-1 Reactor Cooler is located in an EC-1 Reactor liquid recycle which comprises a side draw and liquid recycle from the EC-1 Reactor.

4. A heat integration system according to claim 1, which comprises a plurality of controllers, a plurality of control valves and one or more Control Units wherein the controllers provide signals relating to EC-1 Reactor loading and Consumer Unit(s) demand, to controllers or Control Units or a combination thereof.

5. A heat integration system according to claim 1, which comprises a plurality of controllers, a plurality of control valves and one or more Control Units wherein the controllers provide signals relating to EC-1 Reactor loading and Consumer Unit(s) demand to control valves regulating operation of the Shutdown Cooler and of the absorption Refrigeration Unit.

6. A heat integration system according to claim 1, which additionally comprises an EC-1 Reactor Trim Cooler for regulating the temperature of the EC-1 Reactor, located downstream of the EC-1 Reactor Cooler and upstream of the EC-1 Reactor in the EC-1 Reactor liquid recycle.

7. A heat integration system according to claim 6, wherein the Trim Cooler is under control of an EC-1 Reactor liquid recycle controller which in turn receives signals from an EC-1 Reactor controller, and sends a signal to a control valve for the Trim Cooler CW supply to control EC-1 Reactor liquid recycle temperature within a preferred recycle temperature range.

8. A heat integration system according to claim 6, wherein there is a bypass around the Trim Cooler and a control valve is located in the bypass, wherein the control valve located in the bypass is controlled by a flow controller upstream of the EC-1 Reactor cooler; and a control valve is located at the inlet to the Trim Cooler and the control valve at the Trim Cooler inlet is controlled by a temperature controller located downstream of the Trim Cooler and downstream of the point where the by-pass rejoins the EC-1 Reactor liquid recycle stream.

9. A heat integration system according to claim 1, additionally comprising a two phase separator for separating two phase flow in a side draw from the EC-1 Reactor in a first compartment providing liquid recycle to EC-1 and a second compartment providing a two phase flow to a second EC Reactor EC-2, such that the two phase flow to EC-2 Reactor is stable; wherein preferably the separator operates without a liquid level in the second compartment to drive the two phase flow to EC-2 Reactor, thereby avoiding the risk of a liquid level building up and flooding the separation vessel, and upsetting the removal of gas from the liquid recycle.

10. A separator for separating two phase flow in a side draw from the EC-1 Reactor in a first compartment providing liquid recycle to EC-1 and a second compartment providing a two phase flow to a second EC Reactor EC-2, such that the two phase flow to EC-2 Reactor is stable.

11. A control system for controlling a heat integration system as hereinbefore defined in claim 1, comprising a plurality of controllers, Control Units and/or control valves wherein the controllers provide signals relating to EC-1 Reactor loading and Consumer Unit(s) demand, to controllers or Control Units or a combination thereof, and to control valves regulating operation of the Shutdown Cooler and the absorption Refrigeration Unit.