The present invention relates to a magnetization measurement device and a magnetization measurement method.
As a conventional art, Patent Document 1 discloses a magnetization measurement method using a longitudinal Kerr effect. In the magnetization measurement method, a sample configured with a magnetic material film, etc., is irradiated with linearly polarized light emitted from a laser light source, and a light quantity of reflected light proportional to a rotational angle of a polarized surface corresponding to a magnitude of magnetization due to the Kerr effect is detected by a light quantity detector, to thereby measure the magnetization of the sample.
By the way, in the case where a current that periodically changes, such as a pulse current, is supplied to a sample which has uniaxial magnetic anisotropy and to which a predetermined bias magnetic field is applied, the magnetization of the sample sometimes changes over time corresponding to the supply of the current.
An object of the present invention is to enable to measure change in magnetization of a sample over time, which corresponds to supply of a periodically changing current.
A magnetization measurement device to which the present invention is applied includes: a current supply part supplying a periodically changing current to a sample made of a soft magnetic material with uniaxial magnetic anisotropy in a predetermined first direction and a bias magnetic field applied in a second direction crossing the first direction; a light irradiation part irradiating a surface of the sample with linearly polarized pulse light having a predetermined delay time with respect to the current and having a predetermined polarized surface; and a measurement part measuring magnetization of the sample at the delay time based on reflected light of the pulse light reflected by the surface of the sample.
Here, the current supply part supplies a pulse current having a predetermined repetition period to the sample.
Moreover, the light irradiation part emits the pulse light to cause an advancing direction of the pulse light that is to enter the sample and an advancing direction of the reflected light reflected by the surface of the sample to be in parallel with the first direction or the second direction.
From another standpoint, a magnetization measurement method to which the present invention is applied includes: supplying a periodically changing current to a sample made of a soft magnetic material with uniaxial magnetic anisotropy in a predetermined first direction and a bias magnetic field applied in a second direction crossing the first direction; irradiating a surface of the sample with linearly polarized pulse light having a predetermined delay time with respect to the current and having a predetermined polarized surface; and measuring magnetization of the sample at the delay time based on reflected light of the pulse light reflected by the surface of the sample.
According to the present invention, it is possible to measure the change in the magnetization of the sample over time, which corresponds to supply of the periodically changing current.
Hereinafter, an exemplary embodiment according to the present invention will be described with reference to attached drawings.
The magnetization measurement device 1 includes: a pulse laser 2 that emits the pulse light toward the magnetic sensor 100; and a polarizer 3 that linearly polarizes the pulse light emitted from the pulse laser 2 to have a predetermined polarized surface. The magnetization measurement device 1 also includes: a detection device 4 that detects reflected light, which is light emitted from the pulse laser 2 and reflected by a surface of the magnetic sensor 100; and an analyzer 5 that transmits the reflected light with a predetermined polarized surface toward the detection device 4. The magnetization measurement device 1 further includes a current supply part 7 that supplies the pulse current to the magnetic sensor 100.
Though details will be described later, in the magnetization measurement device 1, the surface of the magnetic sensor 100 (more specifically, the sensitive element 31) is irradiated with the pulse light emitted from the pulse laser 2 via the polarizer 3. The polarized surface of the reflected light of the pulse light reflected on the surface of the sensitive element 31 is rotated by the magneto-optical Kerr effect in accordance with the state of the magnetization on the surface of the sensitive element 31, and the reflected light is incident on the detection device 4 via the analyzer 5. The detection device 4 measures the magnetization on the surface of the magnetic sensor 100 (the sensitive element 31) based on the result of detection of the reflected light.
The pulse laser 2 emits the pulse light with a predetermined pulse width and wavelength toward the surface of the sensitive element 31 at a predetermined period.
The oscillation period of the pulse light by the pulse laser 2 is equal to the period of the pulse current supplied to the magnetic sensor 100 by the current supply part 7. To additionally describe, the pulse light from the pulse laser 2 is synchronized with the rise in the pulse current supplied by the current supply part 7 to have a predetermined delay time T (refer to
Moreover, it is preferable that the pulse width of the pulse light by the pulse laser 2 is sufficiently small as compared to the pulse width of the pulse current supplied to the magnetic sensor 100 by the current supply part 7. The pulse width of the pulse light from the pulse laser 2 can be set within the range of, for example, 0.5 ns to 20 ns though it may differ depending on the pulse width of the pulse current by the current supply part 7. The pulse laser 2 is not particularly limited, and a solid-state laser capable of pulse oscillation (for example, an Nd-YAG laser), a gas laser (for example, a CO2 laser), a semiconductor laser, or other lasers can be used.
The polarizer 3 linearly polarizes the pulse light emitted from the pulse laser 2 to have a predetermined polarized surface. Note that, in the case where a laser emitting linearly polarized light is used as the pulse laser 2, the magnetization measurement device 1 does not have to include the polarizer 3.
In the exemplary embodiment, the pulse laser 2 and the polarizer 3 constitute a light irradiation part that irradiates the surface of the magnetic sensor 100 (the sensitive element 31) with the pulse light having a predetermined polarized surface.
The analyzer 5 passes light having a specific polarized surface, from among the reflected light of the pulse light emitted from the pulse laser 2 and reflected on the surface of the sensitive element 31, toward the detection device 4. The polarized surface of the light passing through the analyzer 5 can be, for example, in a direction perpendicular to the polarized surface of light passing through the polarizer 3. In this case, the intensity of the light (the light quantity) passing through the analyzer 5 corresponds to the rotation angle of the polarized surface rotated on the surface of the sensitive element 31 by the magneto-optical Kerr effect.
The detection device 4 is an example of a measurement part and detects the light quantity of the reflected light passed through the analyzer 5 and measures the magnetization on the surface of the sensitive element 31 based on the detection results. As the detection device 4, for example, a charge coupled device (CCD) camera detecting the light quantity of the reflected light can be used. In addition, the detection device 4 may detect the angle of the polarized surface of the reflected light, to thereby measure the magnetization on the surface of the sensitive element 31 based on the detection results. In this case, the magnetization measurement device 1 does not have to include the analyzer 5.
Note that the method of measuring the magnetization on the surface of the sensitive element 31 by the detection device 4 will be described in detail later.
The current supply part 7 is configured with a circuit with a power supply and a pulse generator, etc., for example, and is connected to terminal parts 33 (refer to
The pulse width of the pulse current supplied by the current supply part 7 can be set at, for example, 20 ns to 200 ns. In addition, the repetition period of the pulse current supplied by the current supply part 7 can be set at, for example, 1 MHz to 50 MHz.
Note that, other than the components shown in
Subsequently, the magnetic sensor 100, which is a sample for measuring change in the magnetization by the magnetization measurement device 1 of the exemplary embodiment, will be described.
As shown in
Here, the hard magnetic material has a large, so-called coercive force, the hard magnetic material being once magnetized by an external magnetic field, even upon removal of the external magnetic field, maintaining the magnetized state. On the other hand, the soft magnetic material has a small, so-called coercive force, the soft magnetic material being easily magnetized by an external magnetic field, but, upon removal of the external magnetic field, quickly returning to a state with no magnetization or a little magnetization.
Note that, in the present specification, an element constituting the magnetic sensor 100 is indicated by a two-digit number, and a layer processed into an element (the hard magnetic material layer 103 or the like) is indicated by a number of one hundreds. Then, for a figure indicating an element, a figure indicating a layer processed into the element is written in parentheses. For example, the case of the thin film magnet 20 is written as thin film magnet 20 (hard magnetic material layer 103). In the figure, the case is written as 20 (103). The same is true in other cases.
Description will be given of a planar structure of the magnetic sensor 100 by
The connection part 32 is provided between end portions of the adjacent sensitive elements 31 and windingly performs serial connection of the adjacent sensitive elements 31. In the magnetic sensor 100 shown in
The terminal parts 33 are provided to the (two) respective end portions of the sensitive parts 31, the end portions not being connected to the connection parts 32. The terminal part 33 may have a size capable of connecting the electric wires. In the exemplary embodiment, in the case where the magnetization of the sensitive element 31 is measured by the magnetization measurement device 1 (refer to
Then, the sensitive elements 31, the connection parts 32 and the terminal parts 33 of the sensitive part 30 are integrally constituted by a single layer of the soft magnetic material layer 105. The soft magnetic material layer 105 has conductivity, and therefore, when the pulse current is supplied from the current supply part 7, the pulse current flows from one terminal part 33 to the other terminal part 33.
Further, the magnetic sensor 100 includes two yokes 40a and 40b, each of which is provided to face each of both end portions of the sensitive elements 31 in the longitudinal direction thereof. Note that, in the case where the yokes 40a and 40b are not distinguished, the yokes are referred to as yokes 40. The yoke 40 guides magnetic force lines to the end portion of the sensitive element 31 in the longitudinal direction thereof. Therefore, the yokes 40 are constituted by a soft magnetic material (the soft magnetic material layer 105) through which the magnetic force lines are likely to pass. In other words, the sensitive part 30 and the yokes 40 are formed of a single layer of the soft magnetic material layer 105.
Next, with reference to
The substrate 10 is composed of a non-magnetic material; for example, an oxide substrate, such as glass or sapphire, a semiconductor substrate, such as silicon, or a metal substrate, such as aluminum, stainless steel, or a nickel-phosphorus-plated metal, can be provided.
The hard magnetic material layer 103 constituting the thin film magnet 20 is composed of, for example, an alloy that contains Co as a main component and also contains at least one of Cr and Pt (hereinafter, referred to as a Co alloy constituting the thin film magnet 20). Examples of the Co alloy constituting the thin film magnet 20 include CoCrPt, CoCrTa, CoNiCr and CoCrPtB. Note that Fe may be contained. The hard magnetic material layer 103 is polycrystalline composed of a set of different crystal orientations, and each crystal has the magnetic anisotropy in the in-plane direction. The magnetic anisotropy is derived from crystal magnetic anisotropy.
The dielectric layer 104 is configured with a nonmagnetic dielectric material and electrically insulates the thin film magnet 20 and the sensitive part 30. Specific examples of the dielectric material constituting the dielectric layer 104 include oxide, such as SiO2, Al2O3, or TiO2, or nitride, such as Si3N4 or AlN.
The sensitive element 31 in the sensitive part 30 is provided with uniaxial magnetic anisotropy in a direction crossing the longitudinal direction, for example, an intersecting short direction. Note that the direction crossing the longitudinal direction may have an angle exceeding 45° with respect to the longitudinal direction. In the exemplary embodiment, the direction crossing the longitudinal direction corresponds to a first direction.
As the soft magnetic material layer 105 constituting the sensitive element 31, it is preferable to use an amorphous alloy, which is an alloy containing Co as a main component doped with a high melting point metal, such as Nb, Ta or W (hereinafter, referred to as a Co alloy constituting the sensitive element 31). Examples of the Co alloy constituting the sensitive element 31 include CoNbZr, CoFeTa and CoWZr.
The hard magnetic material layer 103 and the dielectric layer 104 are processed to have a quadrangular planar shape (refer to
In the magnetic sensor 100, the lines of magnetic force outputted from the north pole of the thin film magnet 20 once go to the outside of the magnetic sensor 100. Then, a part of the lines of magnetic force passes through the sensitive element 31 via the yoke 40a and goes to the outside again via the yoke 40b. The magnetic force lines that have passed through the sensitive element 31 return to the south pole of the thin film magnet 20 together with the magnetic force lines that have not passed through the sensitive element 31. In other words, the thin film magnet 20 applies the magnetic field (a bias magnetic field) to the longitudinal direction of the sensitive element 31. In the exemplary embodiment, the longitudinal direction corresponds to a second direction.
Subsequently, characteristics of the magnetic sensor 100 will be described. In the magnetic sensor 100 shown in
As shown in
Consequently, in the magnetic sensor 100, by use of a portion where the amount of change ΔV in the voltage V with respect to the amount of change ΔH in the magnetic field H to be applied is steep (in other words, the portion where ΔV/ΔH is large), it is possible to extract extremely weak change in the magnetic field H as the amount of change ΔV in the voltage V. In
When the pulse current is supplied to the magnetic sensor 100, as shown in
According to the magnetization measurement device 1 of the exemplary embodiment, it is possible to measure the change in the magnetization M of the sensitive element 31 in response to the supply of the pulse current over time.
Subsequently, description will be given of the measurement method of the magnetization of the magnetic sensor 100 (the sensitive element 31) by the magnetization measurement device 1.
As described above, the magnetization measurement device 1 supplies the pulse current to the magnetic sensor 100 via the terminal parts 33 at a predetermined repetition period by the current supply part 7. Consequently, the pulse current flows along the longitudinal direction in the sensitive element 31 of the magnetic sensor 100.
In addition, the magnetization measurement device 1 irradiates the surface of the sensitive element 31 in the magnetic sensor 100 with the pulse light by the pulse laser 2. As shown in
The pulse light emitted from the pulse laser 2 is, as described above, linearly polarized by the polarizer 3 to have a predetermined polarized surface. Then, the linearly polarized pulse light enters the surface of the sensitive element 31 after the pulse current was supplied to the sensitive element 31 and after the delay time T has elapsed.
Here, in the exemplary embodiment, the sensitive element 31 is irradiated with the pulse light so that the advancing direction of the pulse light that is to enter the surface of the sensitive element 31 and the advancing direction of the reflected light reflected by the surface of the sensitive element 31 are in parallel with the short direction of the sensitive element 31. In the exemplary embodiment, the advancing direction of the pulse light that is to enter the surface of the sensitive element 31 and the advancing direction of the reflected light reflected by the surface of the sensitive element 31 that are in parallel with the short direction of the sensitive element 31 (the direction perpendicular to the direction in which the bias magnetic field Hb is applied) make it possible to detect the reflected light with a polarized surface rotated by the longitudinal Kerr effect by use of the detection device 4.
Note that, in the description of the exemplary embodiment, the advancing direction of the pulse light and the advancing direction of the reflected light being in parallel with the short direction of the sensitive element 31 mean that the advancing directions of the pulse light and the reflected light projected onto the surface of the sensitive element 31 are the same as the short direction of the sensitive element 31. The advancing direction of the pulse light can be controlled by an optical member, such as a not-shown reflecting mirror, for example.
By the surface of the sensitive element 31, the pulse light is reflected. In the reflected light of the pulse light, in response to the magnetization M of the sensitive element 31, the polarized surface is rotated by the magneto-optical Kerr effect (in this example, by the longitudinal Kerr effect). Then, the reflected light passes through the analyzer 5 and enters the detection device 4.
The detection device 4 detects the intensity (the light quantity) of the reflected light that has passed through the analyzer 5 and has entered, and based on the result, measures the magnetization M on the surface of the sensitive element 31 at the delay time T.
As described above, the polarized surface of the light passing through the analyzer 5 is perpendicular to the polarized surface of the light passing through the polarizer 3. In this case, the intensity (the light quantity) of the reflected light passing through the analyzer 5 and entering the detection device 4 corresponds to the rotation angle of the polarized surface of the reflected light rotated on the surface of the sensitive element 31 by the magneto-optical Kerr effect. In addition, the rotation angle of the polarized surface of the reflected light rotated on the surface of the sensitive element 31 corresponds to the state of the magnetization M on the surface of the sensitive element 31.
Consequently, the detection device 4 detects the intensity (the light quantity) of the reflected light, and based on the result, it is possible to obtain the magnetization M on the surface of the sensitive element 31. To additionally describe, the detection device 4 can measure the magnetization M on the surface of the sensitive element 31 after the delay time T has elapsed since the rise of the pulse current based on the reflected light.
Moreover, the magnetization measurement device 1 measures the magnetization M with slightly different delay times T for irradiating the sensitive element 31 with the pulse light and combines the measurement results of the magnetization M at the respective delay times T, and thereby the change in the magnetization M over time in response to the supply of the pulse current.
As shown in
Note that, in the magnetization measurement device 1, in the case where the change in the magnetization M over time is obtained by measuring the magnetization M with the different delay times T and combining the measurement results, it is preferable to measure the magnetization M plural times for each delay time T and adopt the average value of the plural measurement results. By measuring the magnetization M plural times for each delay time T, it is possible to reduce the error in the measurement results at each delay time T.
As described so far, according to the magnetization measurement device 1 of the exemplary embodiment, it becomes possible to measure the change in the magnetization M over time, which occurs in the sensitive element 31 when the current periodically changes, such as the pulse current, is supplied to the magnetic sensor 100.
Note that, in the exemplary embodiment, the current supply part 7 supplies, as the periodically changing current to be supplied, the pulse current with a predetermined repetition period to the magnetic sensor 100; however, the periodically changing current is not limited thereto. As the periodically changing current, the current supply part 7 may supply a high-frequency current with a predetermined frequency, for example. In this case, the magnetization measurement device 1 measures the magnetization M with different delay times T in relation to a specific phase of the high-frequency current, and thereby it is possible to confirm how the magnetization M of the sensitive element 31 changes with respect to the phase of the high-frequency current.
In addition, in the exemplary embodiment, the sensitive element 31 is irradiated with the pulse light from the pulse laser 2 so that the advancing direction of the pulse light to enter the surface of the sensitive element 31 and the advancing direction of the reflected light reflected by the surface of the sensitive element 31 are in parallel with the short direction of the sensitive element 31; however, irradiation is not limited thereto. For example, pulse light irradiation by the pulse laser 2 may be performed so that the advancing direction of the pulse light to enter the surface of the sensitive element 31 and the advancing direction of the reflected light reflected by the surface of the sensitive element 31 are in parallel with the longitudinal direction of the sensitive element 31.
Further, in the exemplary embodiment, the sensitive element 31 of the magnetic sensor 100 is taken as an example of an object (the sample) of measuring the magnetization M by the magnetization measurement device 1, but the object of measuring is not limited thereto. The object of measuring the magnetization M by the magnetization measurement device 1 is not particularly limited as long as the object is a soft magnetic material with uniaxial magnetic anisotropy in a predetermined first direction and a bias magnetic field applied in a second direction crossing the first direction. In addition, the configuration of applying the bias magnetic field to the soft magnetic material, which is the object of measuring, may be integrated with the object of measuring (the sensitive element 31), such as the thin film magnet 20 of the magnetic sensor 100, or may be separated from the object of measuring.
Number | Date | Country | Kind |
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2019-171903 | Sep 2019 | JP | national |
Filing Document | Filing Date | Country | Kind |
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PCT/JP2020/025555 | 6/29/2020 | WO |