This application is based upon and claims the benefit of priority from prior Japanese Patent Application No. 2004-117237, filed on Apr. 12, 2004; the entire contents of which are incorporated herein by reference.
1. Field of the Invention
The present invention relates to a substrate heating device, which heats a substrate such as a semiconductor substrate, a liquid crystal substrate or the like. More specifically, the present invention relates to a substrate heating device which includes a ceramic base plate and resistance heating elements buried in the ceramic base plate.
2. Description of the Related Art
A ceramic heater which has a ceramic base plate and resistance heating elements buried in the ceramic base plate is widely used as a substrate heating device in a semiconductor manufacturing process or the like. The ceramic heater used in a semiconductor manufacturing process or the like is available over a wide range of temperatures for applications. Uniform heat on the heating surface of the heater is desired for increasing yield of semiconductor products.
In many ceramic heaters, a single resistance heating element, which is provided by forming a single continuous linear resistance heating element into a coil shape, is buried in the ceramic base plate. Recently, a multi-zone heater having independent resistance heating elements buried in respective zones into which the heating surface is divided has been adopted. A heating value may be specified for each zone in the multi-zone heater, thereby providing improved uniformity of heater surface temperature. A multi-zone heater with resistance heating element buried in respective nine zones of the ceramic base plate is disclosed in Japanese Patent Application Laid-Open No. 2001-52843,
In the conventional multi-zone heater, terminals are connected to the respective resistance heating elements. Lead wires are connected to the respective terminals and are connected to a power supply line. In the conventional ceramic heater, the lead wires are also buried in the ceramic base plate. Therefore, the lead wires are wired in the ceramic base plate and connected to the power supply line at the central of the underside of the ceramic base plate.
Meanwhile, in this case, since the buried lead wires themselves may become defects of the ceramic base plate, the thinnest available wire must be used as lead wires to prevent s generating tress. In addition, in the manufacturing process for the ceramic base plate, since a ceramic compact in which lead wires are buried is sintered, the lead wires must be made of a sintering temperature-proof refractory metal.
Therefore, conventionally, a refractory metal with high volume resistivity has been used for lead wires as with a resistance heating element material. As a result, the lead wires generate heat as with the resistance heating element. When extending the respective lead wires to the central of the ceramic base plate, the lead wires must always be arranged to pass through other zones. Therefore, it is difficult to precisely control the temperatures of the respective zones due to influence of heat generation of the lead wires.
An object of the present invention is to provide a substrate heating device including resistance heating elements for the respective zones into which a heating surface is divided, which can prevent influences of lead wires and precisely control temperature for respective zones.
A substrate heating device of an embodiment of the present invention includes a ceramic base plate having a heating surface on which a substrate is placed, resistance heating elements buried in the ceramic base plate for respective zones into which the heating surface is divided, terminals connected to the resistance heating elements respectively, and lead wires connected to the terminals respectively and wired on an outer surface of the ceramic base plate other than the heating surface.
According to such a substrate heating device, the lead wires connected to respective terminals of the resistance heating elements are not buried in the ceramic base plate and are wired on an outer surface of the ceramic base plate other than the heating surface, in the substrate heating device having resistance heating elements for the respective zones into which the heating surface is divided. Therefore, the substrate heating device can prevent influences of lead wires and precisely control temperature for respective zones.
A substrate heating device, according to a first embodiment of the present invention, is a ceramic heater including resistance heating elements buried in a ceramic base plate. More specifically, it is a multi-zone heater with independent resistance heating elements buried in respective zones into which a heating surface is divided. A substrate is placed on the heating surface. Lead wires connected to respective terminals of the resistance heating elements are not buried in the ceramic base plate, and are wired on an outer surface of the ceramic base plate other than the heating surface.
As shown in
The heating surface 11 may be arbitrarily divided into multiple zones. For example, as shown in
For example, in the vicinity of the periphery of the heating surface 11, the temperature tends to depend on the surrounding of the substrate heating device 1, as opposed to that of the central region of the heating surface 11. In addition, a tubular member or the like is often connected to the central region in the underside of the ceramic base plate 10. As a result, the heating surface 11 temperature tends to decrease due to influence of heat conduction to the tubular member. As described above, since heating conditions differ among those zones, it is preferable that heating values for the respective zones are adjusted to respective appropriate values so as to be uniform temperature of the heating surface 11.
Note that the heating surface 11 may be divided into two zones: an inner zone that is in the vicinity of the central region of the heating surface 11, and an outer zone that is the periphery of that inner zone. In addition, the periphery of the second zone shown in
As shown in
Furthermore, as shown in
As described above, in the substrate heating device 1, the lead wires L, which have conventionally been buried in the ceramic base plate 10 together with the resistance heating elements 30, are not buried in the ceramic base plate 10, and are wired on an outer surface of the ceramic base plate 10 instead. Therefore, the substrate heating device 10 can prevent influences of lead wires L and precisely control temperature for respective zones.
More specifically, the lead wires L are not defects of the ceramic base plate 10. In addition, it is unnecessary to carry out sintering while the lead wires are buried. As a result, diameters and materials of the lead wires L are not limited. This allows use of a conductor material with a lower resistance such as a metallic wire made of Ni or Al, i.e., a nickel wire, or an aluminum wire for the lead wires L. As a result, heat generation of the lead wires L themselves may be prevented, thereby preventing influences on temperature control due to heat generation of the lead wires L. More specifically, heat generation of the lead wires L does not influence the temperatures of the resistance heating elements 30 and the heating surface 11. This allows further precise temperature control for each zone of the heating surface 11.
Note that as shown in
Next, respective part in the substrate heating device 1 are described in further detail. Material of the ceramic base plate 10 is not limited, and aluminum nitride (AlN), alumina (Al2O3), silicon nitride (SiNx), silicon carbide (SiC), mullite (Al6Si2O13), boron nitride (BN), sialon (Si6-zAlzOzN8-z) and the like are available. Of these, particularly, aluminum nitride is preferably used. As a result, further increase temperature uniformity of the heating surface 11 can be achieved, because aluminum nitride has high thermal conductivity. Therefore, it is preferable that the ceramic base plate 10 includes aluminum nitride, and further preferable that it includes aluminum nitride as a main ingredient.
The shape of the ceramic base plate 10 is not limited to a disc shape shown in
Material of the resistance heating elements 30 is not limited, and a refractory conductive material such as molybdenum (Mo), tungsten (W), molybdenum carbide (MoC), or tungsten carbide (WC) is preferred. Other than a refractory conductive material, Ni, TiN, TiC, TaC, NbC, HfC, HfB2, ZrB2, or carbon is available. It is preferable that the resistance heating elements 30 include at least one of molybdenum and tungsten, and is further preferable to include molybdenum or tungsten as a main ingredient. In addition, the form of the resistance heating elements 30 is not limited. Other than the wire shown in
Since the resistance heating elements 30 are buried in the ceramic base plate 10, in other words, the base is made of highly corrosion-proof ceramics, and the resistance heating elements are not externally exposed, the substrate heating device 1 is highly corrosion proof. Therefore, it is preferable to use the substrate heating device 1 in a chemical vapor deposition (CVD) apparatus or a dry etching apparatus, which often use a corrosive gas.
In addition, it is preferable that the lead wires L are made of a low-resistance metallic wire, for example, a nickel (Ni) wire or an aluminum (Al) wire. It is preferable that the diameter of the lead wire is from about 0.5 mm to about 10 mm. The form of the lead wires L is not limited. Other than the wire made of lead wire material, a printing lead formed by printing a printing paste including lead wire material, and a thin film of lead wire material formed by CVD or PVD such as vapor deposition or sputtering are available.
Next, a manufacturing method for the substrate heating device 1, according to the first embodiment, is described. First, the ceramic base plate 10 in which the resistance heating elements 30 connected to the terminals T are buried is formed. Next, the lead wires L are connected to the respective terminals T and wired on an outer surface other than the heating surface 11 of the ceramic base plate 10, for example, on the underside of the ceramic base plate 10 (the opposite surface to the heating surface 11). Next, steps of the manufacturing method are described in further detail.
The ceramic base plate 10 is formed by preparing a ceramic compact in which the resistance heating element 30 connected to the respective terminals T are buried and then sintering it. A ceramic powder made by adding a rare-earth oxide such as yttrium, which is used as a sintering aid, to a main ingredient such as aluminum nitride, silicon carbide, silicon nitride, mullite, sialon or the like is available. First, slurry is made by beating and mixing to the ceramic powder a binder, a dispersing agent, water, etc. as necessary. The resulting slurry is granulated with a spray dryer. The resulting granules are filled in a mold and pressed, forming a preform. The coil-shaped resistance heating elements 30 connected to the terminals T into which heating surface 11 is divided are placed on the preform in respective zones. A ceramic compact in which the resistance heating element 30 connected to the terminals T are buried is formed by filling the ceramic powder on the preform and the resistance heating elements 30 and then press-forming. At this time, grooves may be formed in advance at positions on the preform where the resistance heating elements 30 are to be placed, and afterwards, the resistance heating elements 30 may be placed in those respective grooves.
Next, the ceramic compact is sintered by hot pressing or atmospheric sintering, for example. For example, in the case of using an aluminum nitride powder as the ceramic powder, it is sintered for about one to about ten hours at a temperature of about 1700° C. to about 2000° C. in a nitrogen atmosphere. In the case of hot pressing, pressure of about 20 kgf/cm2 to about 100 kgf/cm2, more preferably about 100 kgf/cm2 to about 400 kgf/cm2 is applied. Since pressure is applied in a uniaxial direction when sintering using the hot pressing method, excellent adhesiveness of the resistance heating elements 30 and the surrounding ceramic base plate 10 can be provided. Furthermore, when using a metallic bulk as the resistance heating elements 30, there is no deformation made by the applied pressure when hot press sintering. In this manner, the ceramic base plate 10 which is a disc-shaped ceramic sintered body with a diameter of about 200 mm to about 400 mm can be obtained.
Holes are formed in the ceramic base plate 10 in which the resistance heating elements 30 connected to the respective terminals T are buried so as to expose the terminals T of the respective buried resistance heating elements. The exposed terminals T are connected to the ends of the lead wires L by soldering, welding or the like. The lead wires L are then wired on the underside (the opposite surface to the heating surface 11) of the ceramic base plate 10. The lead wires may be fixed to the underside of the ceramic base plate 10 using an insulating adhesive or the like or by tightening screws at several places. Furthermore, in the case of forming the lead wires L by printing, a printing paste such as a Ni paste is patterned on the underside of the ceramic base plate 10 by screen printing and is then sintered. In this case, the lead wires should be connected to the respective terminals T of the resistance heating elements 30 by soldering or the like. Note that arrangement of the lead wires L is not limited to collectively wiring them in the central region on the underside of the ceramic base plate 10. Alternatively, an optimum position should be determined depending on the arrangement of the surrounding area of the substrate heating device 1, such as connection with power supply member or positional relationships with units provided therearound.
Note that in a hole-punching process, the heating surface 11 is embossed by sandblasting or the like, grooves are formed for placing the substrate on the heating surface 11, or through-holes or channels, which are for introducing purge gas to the heating surface 11, or through-holes for lift pins to be inserted are formed as necessary. In addition, guide channels for wiring the lead wires L i.e., guide channels in which the lead wires L are housed may be formed on the underside of the ceramic base plate 10. In this case, the lead wires L may be wired along the respective guide channels.
As described above, according to the substrate heating device 1 of the first embodiment, since the lead wires L are not buried in the ceramic base plate 10, and are wired on the outer surface other than the heating surface 11 of the ceramic base plate 10 instead, more specifically, on the underside of the ceramic base plate 10 (the opposite surface to the heating surface 11), a conductor with lower resistance such as a fine metallic wire made of nickel, aluminum or the like, different than materials of the resistance heating elements 30, may be used. This can prevent influences of the lead wires. More specifically, the lead wires L are not defects of the ceramic base plate 10. In addition, since heat generation of lead wires themselves may be prevented, further precise temperature control for respective zones on the heating surface 11 is possible.
Therefore, the substrate heating device 1 may be preferably used as a substrate heating device for heating a semiconductor substrate, a liquid crystal substrate, or the like in a semiconductor manufacturing process, a liquid crystal manufacturing process, or the like. For example, even when it is available over a wide range of temperatures from room temperature to a high temperature of 400° C. or greater for applications, the substrate heating device 1 may accurately control temperatures for respective zones by regulating the heating values for the respective zones into certain optimal values, allowing extremely precise temperature uniformity of the heating surface 1.
Accordingly, provision of the auxiliary plate 60 allows fixation of the lead wires wired on the underside of the ceramic base plate 10. In addition, since the auxiliary plate 60 can cover the lead wires L, the lead wires L can be protected from the surrounding environment with a simple structure even when the lead wires L are not buried in the ceramic base plate 10. For example, corrosion of the lead wires L may be prevented by using a simple way. More specifically, since the auxiliary plate 60 covers the lead wires L, the substrate heating device 2 may be used without exposing the lead wires L. This allows use of the substrate heating device 2 in various gaseous environments. For example, the substrate heating device 2 may be used in a corrosive gas atmosphere. Material of the lead wires L is not limited to a corrosion-proof material even in a corrosive gas atmosphere, and the lead wires L made of various materials are available.
Furthermore, as shown in
Note that the auxiliary plate 60 is not limited to a disc of almost the same size as the underside of the ceramic base plate 10 (not limited to the same shape as the ceramic base plate 10), as long as it can cover the lead wires L. Therefore, as shown in
The material of the auxiliary plate 60 is not particularly limited as long as it is insulating and has sufficient heat resistivity in an allowable temperature range of the substrate heating device 2. For example, when it is used at a relatively low temperature of 300° C. or less, an engineering plastic material such as polyimide, polyether-ether-ketone, or the like may be available. On the other hand, when it is used at a high-temperature atmosphere of 400° C. or greater, it is preferable that the auxiliary plate 60 includes ceramics such as alumina, aluminum nitride, silicon nitride, silicon carbide, mullite, boron nitride, sialon or the like. In addition, it is preferable to use ceramics with the same main ingredient as the ceramic base plate 10. This prevents thermal stress from generating due to difference in thermal expansion coefficient at the junction with the ceramic base plate 10.
Furthermore, as shown in
It is preferable that the auxiliary plate 60 is screwed to the ceramic base plate 10. In other words, it is preferable that the auxiliary plate 60 is screwed to the ceramic base plate 10 with bolts 70, as shown in
When used in a corrosive gas atmosphere, or when used at a high temperature of 200° C. or greater, it is preferable to use bolts made of Ni base alloy, such as Inconel, or carbon or ceramics. It is preferable that the ceramic base plate 10, the auxiliary plate 60, and the bolts 70 are made of the same ceramics, for example, aluminum nitride. This can prevent thermal stress due to difference in thermal expansion coefficient among them.
In addition, when Ni base alloy is used, a ‘helisert’ (helical coil wire screw thread insert) made of Ni base alloy should be inserted in the internal threads of the ceramic base plate 10. This can prevent chipping of the internal threads of the ceramic base plate 10, since torque of screwing can evenly work on the internal threads due to inserting the helisert made of elastic material. Note that it is preferable to use a ‘sacrificial material’ cover, which slows down corrosive gas entry due to activated reaction with corrosive gas, so as to protect bolts 70 made of metal from a corrosive gas atmosphere.
In addition, provision of a circular ring or a gasket at the interface between the ceramic base plate 10 and the auxiliary plate 60 allows securing of airtightness. As a result, the lead wires L may be almost completely shut off from the corrosive gas atmosphere. In addition, the auxiliary plate 60 may be fixed to the ceramic base plate 10 by solid-state welding, solid-liquid-state welding, soldering or the like, in addition to tightening screws.
When manufacturing the auxiliary plate 60 made of ceramics such as aluminum nitride, a sintered body should be provided by forming and sintering ceramic powder, and then processing it, as described in the manufacturing method for the ceramic base plate 10, according to the first embodiment. In addition, the auxiliary plate 60 made of a resin material may be provided by processing or forming the resin material into a disc shape.
According to the substrate heating device 2 of the second embodiment, since the lead wires L are not buried in the ceramic base plate 10, and are wired on an outer surface other than the heating surface 11 instead, more specifically, on the underside (the opposite surface to the heating surface 11) of the ceramic base plate 10, a resistance conductor with lower resistance such as a fine wire made of nickel, aluminum or the like, different than a material of the resistance heating elements 30, are available. This can prevent influences of the lead wires. More specifically, the lead wires L are not defects of the ceramic base plate 10. In addition, since heat generation of lead wires themselves may be prevented, further precise temperature control for respective zones on the heating surface 11 is possible.
In addition, the auxiliary plate 60 provided on the underside of the ceramic base plate 10 may cover the lead wires L. This allows fixation of the lead wires L wired on the underside of the ceramic base plate 10, and prevention of the lead wires L from being exposed. Accordingly, for example, it is possible to prevent corrosion of the lead wires even in a corrosive gas atmosphere. Therefore, for example, the substrate heating device 2 may be preferably used in a CVD apparatus or a dry etching apparatus often using a corrosive gas.
The tubular member 80 houses part of lead wires L and power supply member such as a power supply line or a power supply rod, and supports the ceramic base plate 10. Therefore, it is preferable that the tubular member 80 is made of a rigid body such as ceramics or metal. In other words, it is preferable that the tubular member 80 includes at least one of metal or ceramics. Note that the tubular member 80 may be fixed to the chamber wall, when the substrate heating device 3a is arranged in a chamber of a dry etching apparatus. In particular, when the tubular member 80 is made of a corrosion-proof material such as ceramics or the like, corrosion of the lead wires L and power supply member connected to the respective lead wires L which are housed in the tubular member 80 may be prevented. More specifically, corrosion of the lead wires L and power supply member may be further certainly prevented by sealing the edge of the tubular member 80 or purging the inside of the tubular member 80 with an inert gas. In addition, it is preferable that the plate 10, the auxiliary plate 60, and the tubular member 80 are made of the same ceramic material such as aluminum nitride. This can prevent thermal stress due to difference in thermal expansion coefficient among them.
The tubular member 80 is connected to the central region of the underside of the ceramic base plate 10 (i.e., the opposite surface to the heating surface 11) via the auxiliary plate 60. The tubular member 80 may be screwed to the auxiliary plate 60. For example, the tubular member 80 made of ceramics may be fixed to the auxiliary plate made of ceramics with bolts 75 or the like. In this case, internal threads for the bolts 75 are formed in the auxiliary plate 60. It is preferable that the bolts 75 are made of the same ceramics, for example, aluminum nitride as with the auxiliary plate 60 and tubular member 80. This can prevent thermal stress due to difference in thermal expansion coefficient at the junction. In addition, the tubular member 80 and the ceramic base plate 10 may be joined together by soldering or using adhesive.
Furthermore, the substrate heating device 3a shown in
A planar electrode may be used as the electrode 20, for example. In addition, the electrode 20 may be made of a refractory material such as molybdenum (Mo), tungsten (W), or tungsten carbide (WC). A form of the electrode 20 is not limited and may be made of a bulk of electrode material, a printed electrode formed by printing a printing paste including electrode material, or a thin film of electrode material formed by CVD or PVD such as vapor deposition or sputtering. In addition, the shape of the electrode 20 may be circular plate, a mesh, a perforated-shape or the like. Note that use of an electrode 20 which is bulk metal especially allows reduction in resistance. Therefore, it can be used as an electrode generating electrostatic chucking force and an RF electrode generating plasma. Note that such an electrode 20 is applicable to the substrate heating devices 1 and 2, according to the first and the second embodiment shown in
In addition, in the substrate heating device 3a shown in
To form the tubular member 80 shown in
Note that there are various forming methods for the tubular member 80 or the auxiliary plate with tubular member 100; however, it is preferable to use a cold isostatic pressing (CIP) method or a slip cast method, which is suitable for forming a relatively intricately shaped compact. In addition, it is preferable to use a atmospheric sintering because of an intricate compact shape. For example, in the case of using AlN as the ceramic material, it is sintered for about one to about ten hours at a temperature of about 1700° C. to about 2000° C. in a nitrogen atmosphere. In a processing step, a sintered body surface is lapped. In the case of the tubular member 80, the joining surface with the auxiliary plate 60 is lapped. The tubular member 80 is then screwed to the auxiliary plate 60, as shown in
To form the tubular member 80 by using metal, it may be formed by polishing a metallic tube. In addition, when the tubular member 80 is made of a metallic material, it is preferable to house the lead wires L in the insulating tube 90 made of alumina or the like so as to secure insulation, as shown in
Note that the tubular member 80 is not necessarily connected to the auxiliary plate 60. It may be connected to a device without the auxiliary plate 60 as with the substrate heating device 1 shown in
According to the substrate heating devices 3a and 3b of the third embodiment, since the lead wires L are not buried in the ceramic base plate 10, and are wired on the outer surface other than the heating surface 11 instead, more specifically, on the underside of the ceramic base plate 10 (i.e., the opposite surface to the heating surface 11), a conductor with lower resistance such as a fine wire made of nickel, aluminum or the like, different than a material of the resistance heating elements 30, may be available. This can prevent influences of the lead wires. More specifically, the lead wires L are not defects of the ceramic base plate 10. In addition, since heat generation of lead wires themselves may be prevented, further precise temperature control for respective zones on the heating surface 11 is possible.
In addition, the auxiliary plate 60 provided on the underside of the ceramic base plate 10 may cover the lead wires L. This allows fixation of the lead wires L wired on the underside of the ceramic base plate 10, and prevention of lead wires L from being exposed. Accordingly, for example, it is possible to prevent corrosion of the lead wires even in a corrosive gas atmosphere. Furthermore, since the substrate heating devices 3a and 3b include the tubular member 80, the ceramic base plate 10 may be supported, and the lead wires L and power supply member connected to the lead wires L may be housed in the tubular member 80. Accordingly, it is possible to prevent corrosion of the lead wires and power supply member.
Note that the auxiliary plate 60 and the tubular member 80 may be attached, not limited to a substrate heating device used in a corrosive gas atmosphere.
Although the inventions have been described above by reference to certain embodiments of the inventions, the inventions are not limited to the embodiments described above. Modifications and variations of the embodiments described above will occur to those skilled in the art, in light of the above teachings.
Number | Date | Country | Kind |
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P2004-117237 | Apr 2004 | JP | national |