This invention relates to a vacuum pump and in particular a compound vacuum pump with multiple ports suitable for differential pumping of multiple chambers.
In a differentially pumped mass spectrometer system a sample and carrier gas are introduced to a mass analyser for analysis. One such example is given in
The high vacuum chamber 10, second interface chamber 12 and third interface chamber 14 can be evacuated by means of a compound vacuum pump 16. In this example, the vacuum pump has two pumping sections in the form of two sets 18, 20 of turbo-molecular stages, and a third pumping section in the form of a Holweck drag mechanism 22; an alternative form of drag mechanism, such as a Siegbahn or Gaede mechanism, could be used instead. Each set 18, 20 of turbo-molecular stages comprises a number (three shown in
In this example, a first pump inlet 24 is connected to the high vacuum chamber 10, and fluid pumped through the inlet 24 passes through both sets 18, 20 of turbo-molecular stages in sequence and the Holweck mechanism 22 and exits the pump via outlet 30. A second pump inlet 26 is connected to the third interface chamber 14, and fluid pumped through the inlet 26 passes through set 20 of turbo-molecular stages and the Holweck mechanism 22 and exits the pump via outlet 30. In this example, the pump 16 also includes a third inlet 27 which can be selectively opened and closed and can, for example, make the use of an internal baffle to guide fluid into the pump 16 from the second, optional interface chamber 12. With the third inlet open, fluid pumped through the third inlet 27 passes through the Holweck mechanism only and exits the pump via outlet 30. In this example, the first interface chamber 11 is connected to a backing pump 32, which also pumps fluid from the outlet 30 of the compound vacuum pump 16. The backing pump typically pumps a larger mass flow directly from the first chamber 11 than that from the outlet of the secondary vacuum pump 30. As fluid entering each pump inlet passes through a respective different number of stages before exiting from the pump, the pump 16 is able to provide the required vacuum levels in the chambers 10, 12, 14, with the backing pump 32 providing the required vacuum level in the chamber 11.
The backing pump 32 is typically a relatively large, floor standing pump. Depending on the type of backing pump used, the performance provided by the backing pump at the first interface chamber 11 can be significantly affected by the operational frequency. For example, a direct on line backing pump running from a 50 Hz electrical supply can produce a performance in the first chamber 11 as much as a 20% lower than the performance produced by the same pump operating at 60 Hz. As the remaining chambers 10, 12, 14 are all linked to the first chamber 11, any change in the performance in the first chamber 11 would have a significant affect on the performance in the other chambers.
In at least its preferred embodiments, the present invention seeks to solve these and other problems.
In a first aspect, the present invention provides a differentially pumped vacuum system comprising apparatus, for example, a mass spectrometer, having at least first and second chambers; and a vacuum pump for differentially pumping fluid from the chambers to generate a first pressure above 0.1 mbar, preferably above 1 mbar, in the first chamber and a second pressure lower than the first pressure in the second chamber, the pump comprising at least first and second pump inlets each for receiving fluid from a respective pressure chamber and a plurality of pumping stages positioned relative to the inlets so that fluid received from the first chamber passes through fewer pumping stages than fluid from the second chamber, the inlets being attached to the apparatus such that at least 99% of the fluid mass pumped from the apparatus passes through at least one of the pumping stages of the pump.
The differentially pumped vacuum system may have additional, lower pressure chambers than those described above, which may be pumped by the same pumping arrangement or by a separate pumping arrangement. However, in either case, the fluid mass pumped through these additional lower pressure chambers is typically much less than 1% of the total system mass flow.
Each pumping stage preferably comprises a dry pumping stage, that is, a pumping stage that requires no liquid or lubricant for its operation.
In one embodiment, the apparatus comprises a third chamber, and the pump comprises a third inlet for receiving fluid from the third chamber to generate a third pressure lower than the second pressure in the third chamber, the pumping stages being arranged such that fluid entering the pump from the third chamber passes through a greater number of pumping stages than fluid entering the pump from the second chamber. In other words, in this embodiment the pump comprises at least three pump inlets, an outlet from a first, relatively high, pressure chamber being connected to a first pump inlet, an outlet for a second, medium pressure chamber being connected to a second pump inlet, and an outlet for a third, relatively low pressure chamber being connected to a third pump inlet.
Preferably, the pump comprises at least three pumping sections, each comprising at least one pumping stage, for differentially pumping the first to third chambers. The pump preferably comprises a first pumping section, a second pumping section downstream from the first pumping section, and a third pumping section downstream from the second pumping section, the sections being positioned relative to the inlets such that fluid entering the pump from the third chamber passes through the first, second and third pumping sections, fluid entering the pump from the second chamber passes through, of said sections, only the second and third pumping sections, and fluid entering the pump from the first chamber passes through, of said sections, only at least part of the third pumping section.
Preferably at least one of the first and second pumping sections comprises at least one turbo-molecular stage. Both of the first and second pumping sections may comprise at least one turbo-molecular stage. The stage of the first pumping section may be of a different size to the stage of the second pumping section. For example, the stage of the second pumping section may be larger than the stage of the first pumping section to offer selective pumping performance.
Optionally, the third pumping section is arranged such that fluid passing therethrough from the second pump inlet follows a different path from fluid passing therethrough from the first pump inlet. For example, the third pumping section may be arranged such that fluid passing therethrough from the first pump inlet follows only part of the path of the fluid passing therethrough from the second pump inlet. Alternatively, the third pumping section may be arranged such that fluid passing therethrough from the first pump inlet follows a path which is separate from the path of the fluid passing therethrough from the second pump inlet. For example, the third pumping stage may comprise a plurality of channels, in which one or more of the channels communicate with the second pump inlet whilst the remaining channels communicate with the first pump inlet.
The third pumping section preferably comprises at least one molecular drag stage. In the preferred embodiments, the third section comprises a multi-stage Holweck mechanism with a plurality of channels arranged as a plurality of helixes. The Holweck mechanism may be positioned relative to the first and second pump inlets such that fluid passing therethrough from the first pump inlet follows only part of the path of the fluid passing therethrough from the second pump inlet.
In one embodiment, the third pumping section comprises at least one Gaede pumping stage and/or at least one aerodynamic pumping stage for receiving fluid entering the pump from each of the first, second and third chambers. The Holweck mechanism may be positioned upstream from said at least one Gaede pumping stage and/or at least one aerodynamic pumping stage, and such that fluid entering the pump from the first pump inlet does not pass therethrough.
The aerodynamic pumping stage may be a regenerative stage. Other types of aerodynamic mechanism may be side flow, side channel, and peripheral flow mechanisms. Preferably, in use, the pressure of the fluid exhaust from the pump outlet is equal to or greater than 10 mbar.
The apparatus may comprise a fourth chamber located between the first and second chambers. In this case, the vacuum pump preferably comprises an optional fourth inlet for receiving fluid from the fourth chamber, the fourth inlet being positioned such that fluid entering the pump from the fourth chamber passes through, of said sections, only the third pumping section towards the pump outlet, and with the fluid entering the pump from the fourth chamber passes through a greater number of stages of the third pumping section than fluid entering the pump from the first chamber.
The pump preferably comprises a drive shaft having mounted thereon at least one rotor element for each of the pumping stages. The rotor elements of at least two of the pumping sections may be located on, preferably integral with, a common impeller mounted on the drive shaft. For example, rotor elements for the first and second pumping sections may be integral with the impeller. Where the third pumping section comprises a molecular drag stage, an impeller for the molecular drag stage may be located on a rotor integral with the impeller. For example, the rotor may comprise a disc substantially orthogonal to, preferably integral with, the impeller. Where the third pumping section comprises a regenerative pumping stage, rotor elements for the regenerative pumping stage are preferably integral with the impeller.
The system preferably comprises a backing pump connected to the pump outlet such that, in use, at least 99% of the fluid mass pumped from the apparatus passes through both the vacuum pump and the backing pump.
In a second aspect, the present invention provides a method of differentially evacuating a plurality of chambers of an apparatus, the method comprising the steps of providing a vacuum pump comprising at least first and second pump inlets each for receiving fluid from a respective chamber and a plurality of pumping stages positioned relative to the inlets so that fluid entering the pump from the first inlet passes through fewer pumping stages than fluid entering the pump from the second inlet, attaching the inlets of the pump to the chambers such that, in use, at least 99% of the fluid mass pumped from the apparatus passes through at least one of the pumping stages of the pump, and operating the pump to generate a first pressure above 0.1 mbar in a first chamber and a second pressure lower than the first pressure in a second chamber.
In a third aspect, the present invention provides a deferentially pumped vacuum system comprising a plurality of pressure chambers; and a vacuum pump attached thereto and comprising a plurality of pump inlets each for receiving fluid from a respective pressure chamber, and a plurality of pumping stages for differentially pumping the chambers; wherein a pumping stage arranged to pump fluid from the pressure chamber in which the highest pressure is to be generated comprises a Gaede pumping stage or an aerodynamic pumping stage. This system may be a mass spectrometer system, a coating system, or other form of system comprising a plurality of differentially pumped chambers. Features described above in relation to the first aspect of the invention are equally applicable to this third aspect of the invention.
In a fourth aspect the present invention provides a method of differentially evacuating a plurality of chambers, the method comprising the steps of providing a vacuum pump comprising a plurality of pump inlets each for receiving fluid from a respective pressure chamber, and a plurality of pumping stages for differentially pumping the chambers; and attaching the pump to the chambers such that a pumping stage for pumping fluid from the pressure chamber in which the highest pressure is to be generated comprises a Gaede pumping stage or an aerodynamic pumping stage.
In a fifth aspect, the present invention provides a compound multi-port vacuum pump comprising first, second and third pumping sections, a first pump inlet through which fluid can enter the pump and pass through each of the pumping sections towards a pump outlet, a second pump inlet through which fluid can enter the pump and pass through only the second and third pumping sections towards the outlet, an optional third pump inlet through which fluid can enter the pump and pass through only the third pumping section towards the outlet, and a fourth inlet through which fluid can enter the pump and pass through only part of the third pumping section towards the outlet.
The present invention also provides a differentially pumped vacuum system comprising a plurality of chambers and a pump as aforementioned for evacuating each of the chambers. The system preferably comprises a backing pump having an inlet connected to the pump outlet for receiving fluid exhaust from the pump.
Features described above in relation to system or pump aspects of the invention are equally applicable to method aspects of the invention, and vice versa.
Preferred features of the present invention will now be described, by way of example only, with reference to the accompanying drawings, in which:
The pump includes at least three pumping sections 106, 108, 112. The first pumping section 106 comprises a set of turbo-molecular stages. In the embodiment shown in
The second pumping section 108 is similar to the first pumping section 106, and also comprises a set of turbo-molecular stages. In the embodiment shown in
Downstream of the first and second pumping sections is a third pumping section 112 in the form of a molecular drag mechanism, for example, a Holweck drag mechanism. In this embodiment, the Holweck mechanism comprises two rotating cylinders 113a, 113b and corresponding annular stators 114a, 114b having helical channels formed therein in a manner known per se. The rotating cylinders 113a, 113b are preferably formed from a carbon fibre material, and are mounted on a disc 115, which is located on the drive shaft 104. In this example, the disc 115 is also mounted on with the drive shaft 104.
Downstream of the Holweck mechanism 112 is a pump outlet 116. A backing pump 150 backs the pump 100 via outlet 116.
As illustrated in
In use, each inlet is connected to a respective chamber of the differentially pumped mass spectrometer system. Thus, inlet 120 is connected to a low pressure chamber 10, inlet 122 is connected to a middle pressure chamber 14 and inlet 124 is connected to the highest pressure chamber 11. Where another chamber 12 is present between the high pressure chamber 11 and the middle pressure chamber 14, as indicated by the dotted line 140, the optional inlet 126 is opened and connected to this chamber 12. Additional lower pressure chambers may be added to the system, and may be pumped by separate means, however, the mass flow of these additional chambers is typically much less than 1% of the total mass flow of the spectrometer system.
Fluid passing through inlet 120 from the low pressure chamber 10 passes through the first pumping section 106, through the second pumping section 108, through all of the channels of the Holweck mechanism 112 and exits the pump 100 via pump outlet 116. Fluid passing through inlet 122 from the middle pressure chamber 14 enters the pump 100, passes through the second pumping section 108, through all of the channels of the Holweck mechanism 112 and exits the pump 100 via pump outlet 116. Fluid passing through inlet 124 from the high pressure chamber 11 enters the pump 100, passes through at least a portion of the channels of the Holweck mechanism and exits the pump via pump outlet 116. If opened, fluid passing through inlet 126 from chamber 12 enters the pump 100, passes through all of the channels of the Holweck mechanism 112 and exits the pump 100 via pump outlet 116.
In this example, in use, and similar to the system described with reference to
A particular advantage of the embodiment described above is that, by enabling the high pressure chamber of the differentially pumped mass spectrometer system to be directly pumped by the same compound multi port vacuum pump 100 that pumps the second and third highest pressure chambers, rather than by the backing pump 150, the compound multi port vacuum pump is able to manage more than 99% of the total fluid mass flow of the mass spectrometer system. Thus, the performance of the first chamber and the rest of the internally linked spectrometer system can be increased without increasing the size of the backing pump.
The regenerative stage 210 comprises a plurality of rotors in the form of an annular array of raised rings 211a mounted on, or integral with, the disc 215 of the Holweck mechanism 212. As illustrated in
Stator 214b of the Holweck mechanism 212 can also form the stator of the regenerative stage 210, and has formed therein an annular channel 211b within which the rotors 211a rotate. As is known, the channel 211b has a cross sectional area greater than that of the individual rotors 211a, except for a small part of the channel known as a “stripper” which has a reduced cross section providing a close clearance for the rotors. In use of the pump 200, fluid pumped from each of the chambers of the differentially pumped mass spectrometer system enters the annular channel 211b via an inlet positioned adjacent one end of the stripper and the fluid is urged by means of the rotors 211a on the rotating disc 215 along the channel 211b until it strikes the other end of the stripper, and the fluid is then urged through the outlet 216 situated on that other end of the stripper.
In use, the vacuum pump 200 can generate a similar performance advantage in the chambers of the differentially pumped mass spectrometer system as the vacuum pump 100 of the first embodiment. In addition to the potential performance advantage offered by the first embodiment, this second embodiment can also offer two further distinct advantages. The first of these is the consistency of the system performance when backed by pumps with different levels of performance, for example a backing pump operating directly on line at 50 or 60 Hz.
In the case of this second embodiment it is anticipated that, in the system described with reference to
In summary, a differentially pumped mass spectrometer system comprising a mass spectrometer having a plurality of pressure chambers; and a vacuum pump attached thereto and comprising a plurality of pump inlets each for receiving fluid from a respective pressure chamber and a plurality of pumping stages for differentially pumping fluid from the chambers; whereby, in use, at least 99% of the fluid mass pumped from the spectrometer passes through one or more of the pumping stages of the vacuum pump.
Number | Date | Country | Kind |
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0322888.9 | Sep 2003 | GB | national |
0409139.3 | Apr 2004 | GB | national |
Filing Document | Filing Date | Country | Kind | 371c Date |
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PCT/GB2004/004046 | 9/23/2004 | WO | 00 | 3/23/2006 |
Publishing Document | Publishing Date | Country | Kind |
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WO2005/040615 | 5/6/2005 | WO | A |
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