Apparatus for accurately measuring local thickness of insulating layer on semiconductor wafer during polishing and polishing system using the same

Information

  • Patent Grant
  • 6322422
  • Patent Number
    6,322,422
  • Date Filed
    Tuesday, January 19, 1999
    25 years ago
  • Date Issued
    Tuesday, November 27, 2001
    22 years ago
  • Inventors
  • Original Assignees
  • Examiners
    • Hail, III; Joseph J.
    • Berry, Jr.; Willie
    Agents
    • Laff, Whitesel & Saret Ltd
    • Whitesel; J. Warren
Abstract
A polishing system has a polishing pad, a wafer retainer for pressing an insulating layer formed on a semiconductor wafer against polishing slurry spread over a polishing pad and a measuring apparatus for measuring the thickness of different portions of the insulating layer, and the measuring apparatus has measuring electrodes embedded in the polishing pad, a first calibration electrode also embedded in the polishing pad and a second calibration electrode embedded into the lower surface of the wafer retainer, wherein the first calibration electrode and the measuring electrodes are opposed to the second calibration electrode and an electrode formed in a dicing area of the semiconductor wafer during the polishing so that the measuring apparatus determines the thickness at the different portions on the basis of a first capacitance between the first calibration electrode and the second calibration electrode and a second capacitance between the measuring electrodes and the electrode in the dicing area.
Description




FIELD OF THE INVENTION




This invention relates to a measuring technology and, more particularly, to an apparatus for measuring local thickness of an insulating layer on a semiconductor wafer during a polishing and a polishing system using it.




DESCRIPTION OF THE RELATED ART




While a manufacturer is fabricating an integrated circuit on a semiconductor wafer, a semiconductor layer and an insulating layer are repeatedly deposited over the semiconductor wafer, and are patterned through a photolithography. The patterned layers deteriorate the step coverage, and the lower insulating layer is subjected to a polishing before deposition of a semiconductor layer. If the lower insulating layer is polished too much, the insulating layer can not offer good electrical isolation, and the detection of remaining thickness is important.




A typical example of the apparatus for measuring the thickness of the remaining insulating layer is disclosed in Japanese Patent Publication of Unexamined Application Ser. No. 4-357851, and

FIG. 1

illustrates the prior art measuring apparatus.




The prior art measuring apparatus is used for a semiconductor wafer


1


. An insulating layer


2


has been already deposited on the semiconductor wafer


1


, and is now being polished on a polishing pad


3


. Polishing slurry


4


is supplied onto the polishing pad


3


, and the polishing pad


3


is rotating with respect to the insulating layer


2


.




The prior art measuring apparatus comprises a measuring electrode


5


, a protective electrode


6


and an insulating layer


6




a


, and the measuring electrode and the protective electrode


6


are embedded in the polishing pad


3


. The measuring electrode


5


and the protective electrode


6


are exposed to the polishing slurry


4


. The measuring electrode


5


is spaced from the protective electrode


6


, and the insulating layer


6




a


electrically isolates the measuring electrode


5


from the protective electrode


6


.




The prior art measuring apparatus further comprises a measuring section


7


and an amplifier


8


. The measuring section


7


is directly connected to the measuring electrode


5


and to the non-inverted input node of the amplifier


8


. The output node of the amplifier


8


is connected to the protective electrode


6


and the inverted input node. A parasitic capacitor


9


is connected to the back surface of the semiconductor wafer


1


. The measuring section


7


supplies an alternating current signal DT


1


to the measuring electrode


5


and the non-inverted input node. The amplifier


8


shifts the phase of the alternating current signal DT


1


by 180 degrees, and produces an inverted alternating current signal CDT


1


.




While the insulating layer


2


is being polished, the measuring section


7


supplies the alternating current signal DT


1


to the measuring electrode


5


, and the inverted alternating current signal CDT


1


is supplied to the protective electrode


6


for bootstrapping. The alternating current signal DT


1


varies the amplitude in proportion to the thickness of the insulating layer


2


, and the measuring section


7


produces an output signal OUT


1


indicative of the thickness of the remaining insulating layer


2


.




The prior art measuring apparatus merely measures an average thickness. The semiconductor wafer


1


is getting large, and the manufacturer hardly polishes the insulating layer


2


uniformly. This means that the insulating layer


2


is locally different in thickness from the average thickness. The prior art measuring apparatus can not measure the locally different thickness. This is the first problem inherent in the prior art measuring apparatus.




The second problem is undesirable damage to the circuit components fabricated on the semiconductor wafer


1


. When the alternating current signal DT


1


is applied to the measuring electrode


5


, the electric field extends over the semiconductor wafer


1


. The electric field is liable to damage the circuit components.




SUMMARY OF THE INVENTION




It is therefore an important object of the present invention to provide a measuring apparatus, which can measure the thickness of an arbitrary portion of an insulating layer without damages to circuit components.




It is also an important object of the present invention to provide a polishing system, which realizes an insulating layer with completely uniform thickness.




In accordance with one aspect of the present invention, there is provided an apparatus for measuring a thickness of an insulating layer having a first surface held in contact with a first electrode means and a second surface opposite to the first surface and held in contact with a non-conductive liquid spread over a moving member, and the apparatus comprises a second electrode means stationary with respect to the moving member, changing a relative position with respect to the first electrode means and a first distance to the first electrode means together with the moving member and forming a first capacitor together with first electrode means, the insulating layer and the non-conductive liquid, a third electrode means stationary with respect to the insulating layer and with respect to the first electrode means, a fourth electrode means stationary with respect to the moving member, changing a second distance to the third electrode means and forming a second capacitor together with the third electrode means and the non-conductive liquid, a source of electric power connected between the first and third electrode means and the second and fourth electrode means, a measuring equipment connected to the second electrode and the fourth electrode for measuring a first capacitance between the first electrode means and the second electrode means and a second capacitance between the third electrode means and the fourth electrode means and a calculating means connected to the measuring equipment for determining a thickness of the insulating layer on the basis of the first capacitance and the second capacitance.




In accordance with another aspect of the present invention, there is provided a polishing system for polishing an insulating layer formed on a semiconductor wafer, and the polishing system comprises a measuring means for measuring a thickness of more than one portion of the insulating layer, a polishing pad for polishing a surface of the insulating layer, a feeding means for supplying non-conductive polishing slurry between the polishing pad and the surface of the insulating layer, a pressurizing means exerting variable force on a plurality of portions of the semiconductor wafer for pressing the insulating layer against the polishing pad and a controlling means connected to the measuring means and the pressurizing means for instructing the pressurizing means to vary the variable force at the plurality of portions depending upon the thickness of the more than one portion of the insulating layer.











BRIEF DESCRIPTION OF THE DRAWINGS




The features and advantages of the measuring apparatus will be more clearly understood from the following description taken in conjunction with the accompanying drawings in which:





FIG. 1

is a schematic cross sectional view showing the prior art measuring apparatus;





FIG. 2

is a plane view showing a semiconductor wafer to be polished;





FIG. 3

is a schematic cross sectional view showing the semiconductor wafer held by a retainer;





FIG. 4

is a plane view showing the arrangement of measuring electrodes and a calibration electrode;





FIG. 5

is a cross sectional view showing a polishing operation on an interlevel insulating layer locally pressed against a polishing pad;





FIG. 6

is a plane view showing portions of the inter-level insulating layer to be polished; and





FIG. 7

schematically shows a matrix of measuring electrodes for detecting the thickness of the insulating layer at a plurality of areas.











DESCRIPTION OF THE PREFERRED EMBODIMENT




Referring to

FIG. 2

of the drawings, a dicing area


11


is formed in a major surface of a semiconductor wafer


12


like a lattice, and an integrated circuit is to be fabricated in device areas


13


. The semiconductor wafer


12


will be broken into semiconductor chips along the lattice-like dicing area


11


. Conductive material is deposited on the dicing area


1


, and forms an electrode


14


.




Although circuit components such as, for example, field effect transistors have been already fabricated on the device areas


13


, the circuit components are too small to be shown. The major surface of the semiconductor wafer is covered with insulating material, and the insulating material forms an inter-level insulating layer


15


(see FIG.


3


). The inter-level insulating layer


15


is to be polished.

FIG. 3

shows the cross section of the semiconductor wafer


11


along line A—A.




The semiconductor wafer


12


is held by a wafer retainer


21


as shown in FIG.


3


. In detail, a recess


22


is formed in the wafer retainer


21


, and the wafer retainer


21


is broken down into a bottom wall portion


21




a


and a side wall portion


21




b


. The wafer retainer


21


accommodates the semiconductor wafer


12


in the recess


22


. Plural through-holes


21




c


are formed in the bottom wall portion


21




a


, and connect a high-pressure air source


23


to the recess


22


. The high-pressure air presses the inter-level insulating layer


15


against a polishing pad


24


. If the high-pressure air source


23


selectively supplies the high-pressure air to the through holes


21




c


, the force is locally exerted on the semiconductor wafer


12


, and a part of the inter-level insulating layer


15


is strongly pressed against the polishing pad


24


.




The wafer retainer


21


is connected to a driving mechanism (not shown), and is driven for rotation around an axis O


1


. An angle measuring equipment


26


is connected to the axis O


1


, and measures the rotating angle of the wafer retainer


21


. The polishing pad


24


is spread over a turn table (not shown), and the turn table is drive for rotation around an axis Q


2


by a driving mechanism (not shown). An angle measuring equipment


27


is connected to the axis O


2


, and detects the rotating angle of the polishing pad


24


. Polishing slurry


28


is supplied onto the polishing pad


24


, and is non-conductive. The axis O


2


is offset from the axis O


1


, and the inter-level insulating layer


15


is polished through two kinds of rotary motion.




A measuring apparatus


30


embodying the present invention is used for the insulating layer


15


during the polishing. The measuring apparatus


30


comprises the angular measuring equipments


26


/


27


, a source of electric power


31


, a pair of calibration electrodes


32




a


/


32




b


and plural measuring electrodes


33


. The source of electric power


31


has a first electrode


31




a


and a second electrode


31




b


, and the first electrode


31




a


is opposite in polarity to the second electrode


31




b


. The first electrode


31




a


is connected to the electrode


14


and the calibration electrode


32




a


, and the second electrode


31




b


is connected to the other calibration electrode


32




b


and the measuring electrodes


33


.




The calibration electrode


32




a


is embedded in the side wall portion


21




b


of the retainer


21


, and the other calibration electrode


32




b


is embedded in the polishing pad


24


. The calibration electrode


32




a


is opposed to the other calibration electrode


32




b


at a certain timing during the two kinds of rotary motion, and the calibration electrodes


32




a


/


32




b


form a capacitor C


1


together with the polishing slurry


28


therebetween.




On the other hand, the measuring electrodes


33


are also embedded in the polishing pad


24


, and are arranged in matrix. The measuring electrodes


33


are opposed to the crossing portions of the lattice-like electrode


14


at the certain timing during the two kinds of rotary motion. The measuring electrode


33


and the crossing portion form capacitors C


3


together with the non-conductive polishing slurry


28


and the inter-level insulating layer


15


.

FIG. 4

illustrates the calibration electrode


32




b


and the measuring electrodes


33


embedded in the polishing pad


24


.




Turing back to

FIG. 3

of the drawings, the measuring apparatus


30


further comprises a capacitive detector


34


and a controller


35


. The capacitive detector


34


are connected through parallel signal lines to the calibration electrode


32




b


and the measuring electrodes


33


, and measures the capacitance of the capacitor C


1


and the capacitance of each of the capacitors C


3


. The signal lines are sequentially connected to the capacitive detector


34


, and the capacitive detector


34


successively measures the capacitance of the capacitor C


1


and the capacitance of each capacitor C


3


. The controller


35


is connected to the angular measuring equipments


26


/


27


and the capacitive detector


34


, and produces an output signal indicative of the thickness of the inter-level insulating layer


15


as described hereinbelow.




After deposition of the inter-level insulating layer


15


on the semiconductor wafer


12


, the manufacturer attaches the semiconductor wafer


12


to the retainer


21


, and the inter-level insulating layer


15


is pressed against the polishing pad


24


. The polishing slurry


28


is supplied onto the polishing pad


24


, and the driving mechanisms (not shown) rotate the turn table (not shown) and the retainer


21


. The polishing pad


24


and the semiconductor wafer


12


are rotated around the axes O


1


/O


2


in the same direction, i.e., clockwise direction or counter-clockwise direction, and the inter-level insulating layer


15


is polished through the two kinds of rotary motion.




The angular measuring equipment


26


produces a detecting signal DT


10


indicative of the angular position of the retainer


21


, and the other angular measuring equipment


27


produces another detecting signal DT


11


indicative of the angular position of the polishing pad


24


. The detecting signals DT


10


and DT


11


are supplied to the controller


35


, and the controller checks the angular positions to see whether or not the calibration electrode


32




a


is just opposed to the other calibration electrode


32




b.






When controller


35


decides that the calibration electrodes


32




a


is opposed to the calibration electrode


32




b


, the measuring electrodes


33


are respectively opposed to the crossing portions of the lattice-like electrode


14


, and the controller


35


instructs the capacitive detector


34


to sequentially measure the capacitance C


1


/C


3


. The capacitive detector


34


sequentially selects the signal lines, and measures the capacitance of the capacitor C


1


and the capacitance of the capacitor C


3


between each measuring electrode


33


and the associated crossing portion. The capacitance C


1


/C


3


is successively reported to the controller


35


through a detecting signal DT


12


, and the controller


35


stores the values of the detecting signal DT


12


in an internal memory (not shown).




As shown in

FIG. 5

, the capacitor C


3


is equivalent to a combination of the capacitor C


1


and a capacitor C


2


. The non-conductive polishing slurry


28


serves as the dielectric layer of the capacitor C


1


, and the inter-level insulating layer


15


serves as a dielectric layer of the capacitor C


2


. For this reason, the controller


35


subtracts the capacitance of the capacitor C


1


from the capacitance of each capacitor C


3


, and determines the capacitance of the capacitor C


2


. The controller


35


sequentially calculates the capacitance of the capacitors C


2


at the measuring electrodes


33


, and determines the dispersion of thickness for the inter-level insulating layer


15


.




If the controller


35


reports that portions a/b/c/d of the inter-level insulating layer


15


are difference in thickness as c=d>a>b, the controller


35


instructs the high-pressure air source


23


to regulate the air pressure at the through-holes


21




a


to values respectively indicated by arrows AR


1


, AR


2


, AR


3


and AR


4


. The arrows AR


3


is as long as the arrow AR


4


, and the air pressure indicated by the arrow AR


3


is equal to the air pressure indicated by the arrow AR


4


. The arrow AR


1


is longer than the arrow AR


2


and shorter than the arrows AR


3


/AR


4


. For this reason, the air pressure indicated by the arrow AR


1


is lower than the air pressure indicated by the arrows AR


3


/AR


4


, and is higher than the air pressure indicated by the arrow AR


2


. As a result, the inter-level insulating layer


15


is non-uniformly pressed against the polishing pad


24


, and the inter-level insulating layer


15


is finished to be contact in thickness.




If the inter-level insulating layer


15


has thick portions


15




a


(see FIG.


7


), the matrix of the measuring electrodes


33


can detect the thick portions


15




a


, and the controller


35


instructs the high-pressure air source


23


to strongly presses the thick portions


15




a


against the polishing pad


24


. As a result, the polishing system finishes the inter-level insulating layer


15


to have a uniform thickness.




As will be appreciated from the foregoing description, the measuring apparatus changes the relative position of the measuring electrode


33


with respect to the electrode


14


, and determines the thickness of the inter-level insulating layer


15


at the relative position. Moreover, the electrode


14


is formed in the dicing area


11


, and the electric field between the electrode


14


and the measuring electrode


33


does not damage a circuit component fabricated in the device area


13


.




Although a particular embodiment of the present invention has been shown and described, it will be apparent to those skilled in the art that various changes and modifications may be made without departing from the spirit and scope of the present invention.




For example, if a single measuring electrode changes relative position to the electrode


14


, the controller


35


can determine the thickness of different points on the semiconductor wafer. Therefore, the plural measuring electrodes


33


do not directly relate to the gist of the present invention.



Claims
  • 1. An apparatus for measuring a thickness of an insulating layer on a semiconductor wafer, having a first surface held in contact with a non-conductive liquid spread over a moving member, comprising:a second electrode means stationary with respect to said moving member, changing a relative position with respect to said first electrode means and a first distance to said first electrode means together with said moving member, and forming a first capacitor together with first electrode means, said insulating layer and said non-conductive liquid; a third electrode means stationary with respect to said insulating layer and with respect to said first electrode means; a fourth electrode means stationary with respect to said moving member, changing a second distance to said third electrode means and forming a second capacitor together with said third electrode means and said non-conductive liquid; a source of electric power connected between said first and third electrode means and said second and fourth electrode means; a measuring equipment connected to said second electrode and said fourth electrode for measuring a first capacitance between said first electrode means and said second electrode means and a second capacitance between said third electrode means and said fourth electrode means; and a calculating means connected to said measuring equipment for determining a thickness of said insulating layer on the basis of said first capacitance and said second capacitance; said first electrode means being formed on a major surface of said semiconductor wafer, and said second surface being polished.
  • 2. The apparatus as set forth in claim 1, in which said semiconductor wafer is held by a wafer retainer, and said third electrode means is attached to said wafer retainer so that said second distance is varied together with said first distance during the polishing.
  • 3. The apparatus as set forth in claim 2, in which said polishing pad and said wafer retainer are driven for rotation around a first axis and a second axis offset from said first axis, respectively, so that said first electrode means and said third electrode means are intermittently opposed to said second electrode means and said fourth electrode means, respectively.
  • 4. The apparatus as set forth in claim 3, further comprising a first angle measuring equipment attached to said first axis for measuring a first angular position of said semiconductor wafer, a second angle measuring equipment attached to said second axis for measuring a second angular position of said polishing pad, and a controlling means giving a timing for determining said thickness of said insulating layer to said calculating means on the basis of said first and second angular positions.
  • 5. The apparatus as set forth in claim 2, in which said calculating means eliminates an influence of said second capacitor from said capacitance of said first capacitor.
  • 6. The apparatus as set forth in claim 1, in which said moving member and said non-conductive liquid serve as a polishing pad and polishing slurry between said second surface and said polishing pad.
  • 7. The apparatus as set forth in claim 1, in which said semiconductor wafer has a plurality of device areas for fabricating circuit components and a dicing area for breaking said semiconductor wafer into semiconductor chips, and said first electrode means is formed in said dicing area.
  • 8. An apparatus for measuring a thickness of an insulating layer having a first surface held in contact with a first electrode means and a second surface opposite to said first surface and held in contact with a non-conductive liquid spread over a moving member, said second surface being polished, said apparatus comprising:a second electrode means stationary with respect to said moving member, changing a relative position with respect to said first electrode means and a first distance to said first electrode means together with said moving member, and forming a first capacitor together with first electrode means, said insulating layer and said non-conductive liquid; a third electrode means stationary with respect to said insulating layer and with respect to said first electrode means; a fourth electrode means stationary with respect to said moving member, changing a second distance to said third electrode means and forming a second capacitor together with said third electrode means and said non-conductive liquid; a source of electric Power connected between said first and third electrode means and said second and fourth electrode means; a measuring equipment connected to said second electrode and said fourth electrode for continuously measuring a first capacitance between said first electrode means and said second electrode means and a second capacitance between said third electrode means and said fourth electrode means while said insulating layer is being relatively moved with respect to said moving member, said second electrode means having a plurality of electrodes isolated from one another and selectively connected to said measuring equipment, said plurality of electrodes being opposed to said first electrode means and formed on a major surface of a semiconductor wafer; and a calculating means connected to said measuring equipment for determining a thickness of said insulating layer on the basis of said first capacitance and said second capacitance.
  • 9. The apparatus as set forth in claim 8, in which said semiconductor wafer has a plurality of device areas for fabricating circuit components and a dicing area for breaking said semiconductor wafer into semiconductor chips, and said first electrode means is formed in said dicing area.
  • 10. The apparatus as set forth in claim 9, in which said dicing area is formed into a lattice surrounding said plurality of device areas, and said first electrode means has a lattice configuration.
  • 11. The apparatus as set forth in claim 10, in which said semiconductor wafer is held by a wafer retainer, and said third electrode means is attached to said wafer retainer so that said second distance is varied together with said first distance during the polishing.
  • 12. The apparatus as set forth in claim 11, in which said moving member and said non-conductive liquid serve as a polishing pad and polishing slurry between said second surface and said polishing pad.
  • 13. The apparatus as set forth in claim 12, in which said polishing pad and said wafer retainer are driven for rotation around a first axis and a second axis offset from said first axis, respectively, so that said first electrode means and said third electrode means are intermittently opposed to said second electrode means and said fourth electrode means, respectively.
  • 14. The apparatus as set forth in claim 13, further comprising a first angle measuring equipment attached to said first axis for measuring a first angular position of said semiconductor wafer, a second angle measuring equipment attached to said second axis for measuring a second angular position of said polishing pad, and a controlling means giving a timing for determining said thickness of said insulating layer to said calculating means on the basis of said first and second angular positions.
  • 15. The apparatus as set forth in claim 14, in which said calculating means eliminates an influence of said second capacitor from said capacitance of said first capacitor.
  • 16. A polishing system for polishing an insulating layer formed on a semiconductor wafer, said system comprising:measuring means for continuously measuring a thickness of more than one portion of said insulating layer responsive to variations of capacitance coupled to said semiconductor wafer during a polishing on said insulating layer; a polishing Dad for polishing a surface of said insulating layer; feeding means for supplying a non-conductive polishing slurry between said polishing pad and said surface of said insulating layer; pressurizing means exerting a variable force on a plurality of portions of said semiconductor wafer for pressing said insulating layer against said polishing pad; control means connected to said measuring means and said pressurizing means for instructing said pressurizing means to vary said variable force at said plurality of portions depending upon the thickness of said more than one portion of said insulating layer, said measuring means including: a first electrode means formed between said semiconductor wafer and said insulating layer, a second electrode means attached to said polishing pad, changing a relative position with respect to said first electrode means and a first distance to said first electrode means while said surface of said insulating layer is being polished, said second electrode forming a first capacitor together with first electrode means, and together with said insulating layer and said polishing slurry, a third electrode means stationary with respect to said insulating layer and with respect to said first electrode means, a fourth electrode means attached to said polishing pad, changing a second distance to said third electrode means and forming a second capacitor together with said third electrode means and said non-conductive polishing slurry, a source of electric power connected between said first and third electrode means and said second and fourth electrode means; a measuring equipment connected to said second electrode and said fourth electrode for measuring a first capacitance between said first electrode means and said second electrode means and a second capacitance between said third electrode means and said fourth electrode means, said second electrode means having a plurality of electrodes isolated from one another and selectively connected to said measuring equipment, said plurality of electrodes being opposed to said first electrode means formed on a major surface of said semiconductor wafer, and a calculating means connected to said measuring equipment for determining said thickness of said more than one portion on the basis of said first capacitance and said second capacitance.
  • 17. The polishing system as set forth in claim 16, in which said semiconductor wafer has a plurality of device areas for fabricating circuit components and a dicing area for breaking said semiconductor wafer into semiconductor chips, and said first electrode means is formed in said dicing area.
  • 18. The polishing system as set forth in claim 17, in which said dicing area is formed into a lattice surrounding said plurality of device areas, and said first electrode means has a lattice configuration.
  • 19. The polishing system as set forth in claim 18, further comprising a wafer retainer for holding said semiconductor wafer, and said third electrode means is attached to said wafer retainer so that said second distance is varied together with said first distance during the polishing.
  • 20. The polishing system as set forth in claim 19, in which said polishing pad and said wafer retainer are driven for rotation around a first axis and a second axis offset from said first axis, respectively, so that said first electrode means and said third electrode means are intermittently opposed to said plurality of electrodes and said fourth electrode means, respectively.
  • 21. The polishing system as set forth in claim 20, in which said measuring apparatus further includes a first angle measuring equipment attached to said first axis for measuring a first angular position of said semiconductor wafer, a second angle measuring equipment attached to said second axis for measuring a second angular position of said polishing pad, and a controller giving a timing for determining said thickness of said more than one portion to said calculating means on the basis of said first and second angular positions.
  • 22. The polishing system as set forth in claim 21, in which said calculating means eliminates an influence of said second capacitor from said capacitance of said first capacitor.
  • 23. The polishing system as set forth in claim 19, in which a plurality of through-holes are formed in said wafer retainer, and said pressurizing means includes a high pressure gas source and a plurality of gas conduits respectively connected to said plurality of through-holes.
US Referenced Citations (6)
Number Name Date Kind
5492594 Burke et al. Feb 1996
5562529 Kishii et al. Oct 1996
5851135 Sandhu et al. Dec 1998
5916009 Izumi et al. Jun 1999
5961369 Bartels et al. Oct 1999
6007405 Mei Dec 1999
Foreign Referenced Citations (6)
Number Date Country
58-115618 Jul 1983 JP
1-207929 Aug 1989 JP
1-306073 Dec 1989 JP
4-357851 Dec 1992 JP
9-134904 May 1997 JP
10-233-421 Sep 1998 JP