The present invention relates to plasma generators, and more particularly, to a method and apparatus for generating a plasma in the fabrication of semiconductor devices.
Radio frequency (RF) generated plasmas have become convenient sources of energetic ions and activated atoms which can be employed in a variety of semiconductor device fabrication processes including surface treatments, depositions, and etching processes. For example, to deposit materials onto a semiconductor wafer, substrate, or other workpiece using a sputter deposition process, a plasma is produced in the vicinity of a sputter target material which is negatively biased. Ions created within the plasma impact the surface of the target to dislodge, i.e., “sputter” material from the target. The sputtered materials are then transported and deposited on the surface of the semiconductor wafer.
Sputtered material has a tendency to travel in paths from the target to the substrate being deposited at angles which are oblique to the surface of the substrate. As a consequence, materials deposited in etched trenches and holes of semiconductor devices having trenches or holes with a high depth to width aspect ratio, can bridge over causing undesirable cavities in the deposition layer. To prevent such cavities, the sputtered material can be redirected into substantially vertical paths between the target and the substrate by negatively charging the substrate or substrate support if the sputtered material is sufficiently ionized by the plasma. However, material sputtered in a low density plasma often has an ionization degree of less than 1% which may be insufficient to avoid the formation of an excessive number of cavities. Accordingly, in some applications, it is desirable to increase the ionization rate of the sputtered material in order to decrease the formation degree of unwanted cavities in the deposition layer.
One technique for increasing the ionization rate is to inductively couple RF energy from a coil to a plasma between the target and the workpiece. In order to maximize the energy being coupled from the coil to the plasma, it is desirable to position the coil as close as possible to the plasma itself. At the same time, however, it is also desirable to minimize the number of chamber fittings and other parts exposed to the material being sputtered so as to facilitate cleaning the interior of the chamber and to minimize the generation of particles being shed from interior surfaces. These particles shed from interior surfaces can fall on the wafer itself and contaminate the product. Accordingly, many sputtering chambers have a generally annular-shaped shield enclosing the plasma generation area between the target and the pedestal supporting the wafer. The shield provides a smooth gently curved surface which is relatively easy to clean and protects the interior of the chamber from being deposited with the sputtering material.
Thus, on the one hand, it would be desirable to place the coil outside the shield so that the coil is shielded from the material being deposited. Such an arrangement would minimize generation of particles by the coil and its supporting structure and would facilitate cleaning of the chamber. On the other hand, it is desirable to place the coil as close as possible to the plasma generation area inside the shield to avoid any attenuation by the spacing from the plasma or by the shield itself to thereby maximize energy transfer from the coil to the plasma. Accordingly, it has been difficult to increase energy transfer from the coil to the plasma while at the same time minimizing particle generation.
In accordance with one aspect of the invention, a coil is carried internally in a semiconductor fabrication chamber by a plurality of novel coil standoffs and RF feedthrough standoffs which reduce generation of particulates. In the illustrated embodiment, the coil has an outer face facing a shield wall, in which the outer face defines a fastener recess extending partially through the coil. A standoff includes a fastener member adapted to fasten the coil to the shield wall. The coil outer face fastener recess is adapted to receive the fastener member. As explained below, such an arrangement can reduce the generation of particulates by the coil and the coil standoffs.
There are additional aspects to the present inventions as discussed below. It should therefore be understood that the preceding is merely a brief summary of one embodiment of the present inventions. It should further be understood that numerous changes to the disclosed embodiments can be made without departing from the spirit or scope of the inventions. The preceding summary, therefore is not meant to limit the scope of the inventions. Rather, the scope of the inventions are to be determined only by the appended claims and their equivalents.
Referring first to
Radio frequency (RF) energy from an RF generator is radiated from the coil 104 into the interior of the plasma chamber 100, which energizes a plasma within the plasma containment region of the plasma chamber 100. A plasma ion flux strikes a negatively biased target 110 positioned above the plasma chamber 100. The plasma ions eject material from the target 110, which may then be deposited onto a wafer or other substrate or workpiece 112 supported by a pedestal 114 at the bottom of the plasma chamber 100. Deposition material may also be sputtered from the coil 104 onto the substrate to supplement the deposition material from the target 110. The coil 104 is carried on the shield 106 by a plurality of novel coil standoffs 500 which electrically insulate the coil 104 from the supporting shield 106. In addition, the standoffs 500 permit repeated deposition of conductive materials from the target 110 onto the coil standoffs 500 while preventing the formation of a complete conducting path of deposited material from the coil 104 to the shield 106 which could short the coil 104 to the shield 106 (which is typically at ground). As will be explained in greater detail below, in accordance with one aspect of the present invention, the insulating coil support standoffs 500 support the coil 104 in a manner which reduces the generation of particulate matter from the face of the coil 104.
To enable use of the coil as a circuit path, RF power is passed through the vacuum chamber walls and through the shield 106 to ends of the coil 104. Vacuum feedthroughs (not shown) extend through the vacuum chamber wall to provide RF current from a generator preferably located outside the vacuum pressure chamber. RF power is applied through the shield 106 to the coil 104 by feedthrough standoffs 600 (
As best seen in
In the illustrated embodiment, the dark space shield 130 is a closed continuous ring of titanium or stainless steel having a generally inverted frusto-conical shape. It is recognized, of course, that the dark space shield may be made from a variety of other conductive materials and have other shapes which shield the coil 104 and its associated supporting structures from at least some of the material being deposited from the target.
The plasma chamber shield 106 is generally bowl-shaped and includes a generally cylindrically shaped, vertically oriented wall 140 to which the standoffs 500 and 600 are attached to insulatively support the coil 104. The shield further has a generally annular-shaped floor wall 142 which surrounds the chuck or pedestal 114 which supports the workpiece 112. A clamp ring 154 clamps the wafer to the chuck 114 and covers the gap between the floor wall 142 of the shield 106 and the chuck 114. Thus, it is apparent from
The vacuum chamber wall 108 has an upper annular flange 150. The plasma chamber 100 is supported by a vacuum chamber adapter ring assembly 152 which engages the vacuum chamber wall flange 150. The plasma chamber shield 106 has a horizontally extending outer flange member 160 which is fastened by a plurality of fastener screws (not shown) to a horizontally extending flange member 162 of the adapter ring assembly 152. The plasma chamber shield 106 is grounded to the system ground through the adapter ring assembly 152.
The dark space shield 130 also has an upper flange 170 which is fastened to the horizontal flange 162 of the adapter ring assembly 152. The dark space shield 130, like the plasma chamber shield 106, is grounded through the adapter ring assembly 152. It should be appreciated that there are numerous alternatives for supporting a shield and dark space shield within a chamber.
The target 110 is generally disk-shaped and is also supported by the adapter ring assembly 152. However, the target 110 is negatively biased and therefore should be insulated from the adapter ring assembly 152 which is at ground. Accordingly, seated in a circular channel formed in the underside of the target 110 is a ceramic insulation ring assembly 172 which is also seated in a corresponding channel 174 in the upper side of the target 110. The insulator ring assembly 174 which may be made of a variety of insulative materials including ceramics, spaces the target 110 from the adapter ring assembly 152 so that the target 110 may be adequately negatively biased. The target, adapter and ceramic ring assembly are provided with O-ring sealing surfaces (not shown) to provide a vacuum tight assembly from the vacuum chamber flange 150 to the target 110.
As set forth in greater detail in copending application Ser. No. 08/680,335, entitled Sputtering Coil for Generating a Plasma, filed Jul. 10, 1996 (Attorney Docket 1390-CIP/PVD/DV) and assigned to the assignee of the present application, the coil 104 may also be positioned and biased in such a manner that the coil may sputter as well as the target. As a result, the deposited material may be contributed by both the target and the coil. Such an arrangement has been found to improve the uniformity of the deposited layer. In addition, the coil may have a plurality of turns formed in a helix or spiral or may have as few turns as a single turn to reduce complexity and costs and facilitate cleaning. Turning now to
The hub member 504 has a central portion 504a which defines a threaded bore 504b which receives a fastener member which, in the illustrated embodiment, is a bolt 505 used to secure the coil 104 to the shield wall 140. It should be appreciated that the bore 504b is preferably formed as a recess on the rear face 104a of the coil 104, in which the recess 504b extends partially through the hub member 504 and does not extend entirely through the coil 104. As a consequence, the front or inner face 104b of the coil 104 facing the wafer and the plasma generation area above the wafer is free of any protruding fastener elements or fastener openings which could generate particulates.
As noted above, the fastener member 505 in the illustrated embodiment is a bolt which is received in the fastener recess 504b which, in the illustrated embodiment, is a threaded bore. It should be appreciated that other types of couplers and fastener members may be used including pins, clips, cams and other structures for mechanically coupling elements together. In addition, the coil 104 may have a male portion of the coupler or fastener such as a bolt, and the standoff may include a female portion of the coupler or fastener, such as a threaded bore.
A channel 507 through the central portion 504a and a side wall 504c of the hub member 504 is coupled to the threaded bore 504b for the bolt 505 to vent gases that might inadvertently be trapped by the bolt 505 in the bore 504b. The electrically insulative base member 502 insulates the hub member 504 which is at the same RF potential as the coil 104, from the shield wall 140 which, in the illustrated embodiment, is at ground potential. The bolt 505 passes through a central aperture 502a of the base member 502 such that the base member 502 also insulates the bolt 505 from the grounded shield wall 140.
The cylindrically shaped end 502c of the insulative base member 502 is received in an annular shaped channel 504d positioned between a side wall 504c and the central portion 504a of the hub member 504. The cylindrically shaped side wall 504c of the hub member 504 is spaced from the lateral side 508 of the base member 502 to form a labyrinthine passageway 510 oriented substantially transverse to the wall 140 of the shield. It is believed that for many applications, the passage way 510 of the standoff 500 inhibits the formation of a path of deposition material across the standoff which could short the coil 104 to the shield 106.
The standoff 500 of
The second cup-shaped cover member 512, spaced from the first hub cover member 504, is maintained at ground. On the other hand, the hub member 504 is affixed to the rear face 104a of the coil 104. Consequently, as mentioned above, the hub member 504 is at the same potential as the coil 104 and hence may sputter. Because the second cover member 512 is at ground potential and is positioned to cover most of the exposed surfaces of the hub member 504, it is believed that the second cover member 512 can substantially reduce sputtering of the hub member 504 in those applications in which sputtering of the standoffs is undesirable. Even in those applications in which the coil 104 is sputtered to enhance the uniformity of deposition on the substrate, sputtering of the standoffs may introduce nonuniformities since the standoffs are typically not arrayed in a continuous ring around the substrate. Hence, retarding sputtering of the standoffs may be useful in a number of applications.
The insulative base member 502 extends through an opening 140c in the shield wall 140. In addition, the base member 502 has a reduced diameter portion 502b which extends through an opening 524a of a retainer plate 524 received in a recess 140a on the outer side of the shield wall 140.
The second cover member 512 and the retainer plate 524 are fastened to opposite sides of the shield wall 140 by screws or other suitable fasteners to support the feedthrough 500 on the shield wall 140. In addition, the cover member fasteners ensure that the second cover member 512 is tightly engaged against and in good electrical contact with the shield wall 140 and therefore grounded to retard sputtering of the second cover member 512. An annular shaped channel 512a in the second cover member is coupled to the threaded holes for the fasteners to vent gases that might inadvertently be trapped in the fastener holes.
The reduced diameter portion 502b of the base member 502 also extends through an opening 530a of a second electrically insulative base member 530 positioned on the outer side of the shield wall 140. Seated in a metal sleeve or bushing 531 is the bolt 505 which passes through an interior opening 531a in the sleeve 531, and the central aperture 502a of the base member 502 and is threaded into the threaded bore 504b of the hub member 504. A shoulder 502e of the insulative base member 502 which is received in the annular shaped channel 504d of the hub member 504, compresses the retainer plate 524 on one side as the bolt 505 is threaded into the hub member 504. The second electrically insulative member 530 compresses the retainer plate on the other side as the head 505a of the bolt 505 compresses the bushing 531 against the second insulative base member 530. In this manner, tightening the bolt 505 compresses the assembly of the standoff 500 together to insulatively secure the standoff and coil 104 to the shield wall 140.
The first electrically insulative base member 502 electrically insulates the hub member 504 of the coil 104 and the bolt 505 from the grounded shield wall 140. However, the base member 502 is preferably formed from an electrically insulative material which is also a good thermal conductor. The RF coil 104 may generate substantial heat which can be thermally coupled by the electrical insulator base member 502 to the wall 140 of the shield 106 to be dissipated. In the illustrated embodiment, the base member 502 is formed from an aluminum nitride ceramic material. Other electrically insulative materials may be used but it is preferred that the material be a good thermal conductor as well. Additional electrically insulative materials include aluminum oxide ceramic and quartz.
A space 538 is provided between the end of the reduced diameter portion 502b and the bushing 531 so that the compressive force of the bolt 532 and the hub member 504 does not damage the insulative members which may be made of breakable materials such as ceramics. The end of the bolt 505 may be covered by a third electrically insulative member 540 which, in the illustrated embodiment is button-shaped. The second insulative base member 530 has a flange 530b spaced from the retaining plate which receives a lip 540b of the insulative cover member 540 to retain the cover member 540 in place.
The insulative base member 530 and the insulative member 540 may be made of electrically insulative materials including ceramic materials such as aluminum oxide. Alternatively, electrically insulative materials which are also good thermal conductors may be used such as aluminum nitride ceramics.
The coil 104 and the hub members 504 of the coil 104 are preferably made of the same material which is being deposited. Hence, if the material being deposited is made of titanium, the hub member 504 is preferably made of titanium as well. To facilitate adherence of the deposited material (here for example, titanium), exposed surfaces of the metal may be treated by bead blasting which will reduce shedding of particles from the deposited material. Besides titanium, the coil and target may be made from a variety of deposition materials including tantalum, copper, and tungsten.
The passageways 510, 516a and 516b form a labyrinth between the standoff components including the hub member 504 of the coil 104, the insulative member 502 and the cover member 512. As set forth in greater detail incopending application Ser. No. 08/853,024, filed May 8, 1997, which is assigned to the present assignee and incorporated herein by reference in its entirety, the labyrinth should be dimensioned to inhibit formation of a complete conducting path from the coil to the shield. Such a conducting path could form as conductive deposition material is deposited onto the coil and standoffs. It should be recognized that other dimensions, shapes and numbers of passageways of the labyrinth are possible, depending upon the particular application. Factors affecting the design of the labyrinth include the type of material being deposited and the number of depositions desired before the standoffs need to be cleaned or replaced.
The second cover member 612 is fastened to the shield wall 140 by screw fasteners which ensure that the second cover member 612 is tightly engaged against and in good electrical contact with the shield wall 104 and therefore grounded to retard sputtering of the first cover member 604. An annular shaped channel 612a in the second cover member is coupled to the threaded holes for the fasteners to vent gases that might inadvertently be trapped in the fastener holes.
The first electrically insulative base member 602 extends through an opening 140d in the shield wall 140. The standoff 600 further includes a 25 second electrically insulative base member 632 positioned in a recess 140b on the outer side of the shield wall 140. Seated in a recess 632a of the the second insulative base member 632 and engaging the end of the central portion 604a of the hub member 604 is a conductive metal bar 633. Seated in a recess 633a of the conductive metal bar 633 is the head 605a of a bolt 605 which passes through interior opening 633b in the bar 633 and is threaded into the threaded bore 604b of the hub member 604 of the coil 104 on the interior side of the shield wall 140. This compresses the assembly of the standoff 600 together to insulatively secure the feedthrough standoff and coil 104 to the shield wall 140.
The first electrically insulative base member 602 insulates the bar member 633 (and the bolt 634) from the grounded shield wall 140. The second electrically insulative member 632 in turn insulates the conductive bar 633 from the grounded shield wall 140. RF current travels along the surface of the conductive bar 633 from an RF source exterior to the vacuum chamber, along the surfaces of the hub member 604 and the remainder of the coil 104. The conductive bar 633 may have a flexible portion 633c to accomodate movement of the shield and coil during deposition. A space 638 is provided between the end 602b of the insulative member 602 and the conductive bar 633 so that the compressive force of the bolt 605 and the hub member 604 does not damage the insulative members which may be made of breakable materials such as ceramics.
As set forth above, the conductive bar 633 carrying RF currents from the exterior generator to the feedthrough is seated in a second electrically insulative member 632. Covering the other side of the conductive bar 633 and the end of the bolt 634 is a third electrically insulative member 640. The electrically insulative members 632 and 640 conform around the RF conductive members to fill the available space to avoid leaving spaces larger than a darkspace to inhibit formation of a plasma and arcing from the conductive bar 633 and the bolt 605.
As best seen in
The support standoffs may be distributed around the remainder of the coil to provide suitable support. In the embodiment illustrated in
Each of the embodiments discussed above utilized a single coil in the plasma chamber. It should be recognized that the present invention is 15 applicable to plasma chambers having more than one coil. For example, the present invention may be applied to chambers having multiple coils for launching helicon waves or for providing additional sources of RF energy or deposition material.
The coil 104 of the illustrated embodiment is made of ½ by ¼ inch heavy duty bead blasted titanium or copper ribbon formed into a single turn coil. However, other highly conductive materials and shapes may be utilized.
For example, the thickness of the coil may be reduced to 1/16 inch and the width increased to 2 inches. Also, hollow tubing may be utilized, particularly if water cooling is desired.
In another aspect of the present inventions, the upper edge of the of the coil 104 adjacent the rear face 104a of the coil 104 may be beveled to form a flat angled face as indicated at 104e in
The appropriate RF generators and matching circuits are components well known to those skilled in the art. For example, an RF generator such as the ENI Genesis series which has the capability to “frequency hunt” for the best frequency match with the matching circuit and antenna is suitable. The frequency of the generator for generating the RF power to the coil is preferably 2 MHz but it is anticipated that the range can vary at other A.C. frequencies such as, for example, 1 MHz to 100 MHz and non-RF frequencies.
In the illustrated embodiment, the shield 106 has an inside diameter of 16″ but it is anticipated that good results can be obtained with a width in the range of 6″-25″. The shields may be fabricated from a variety of materials including electrically insulative materials such as ceramics or quartz. However, the shield and all metal surfaces likely to be coated with the target material are preferably made of a material such as stainless steel or copper unless made of the same material as the sputtered target material. The material of the structure which will be coated should have a coefficient of thermal expansion which closely matches that of the material being sputtered to reduce flaking of sputtered material from the shield or other structure onto the wafer. In addition, the material to be cooled should exhibit good adhesion to the sputtered material. Thus, for example if the deposited material is titanium, the preferred metal of the shields, coils, brackets and other structures likely to be coated is bead blasted titanium. Of course, if the material to be deposited is a material other than titanium, the preferred metal is the deposited material, stainless steel or copper. Adherence can also be improved by coating the structures with molybdenum prior to sputtering the target.
A variety of precursor gases may be utilized to generate the plasma including Ar, H2, O2 or reactive gases such as NF3, CF4 and many others. Various precursor gas pressures are suitable including pressures of 0.1-50 mTorr. For ionized PVD, a pressure between 10 and 100 mTorr is preferred for best ionization of sputtered material.
It will, of course, be understood that modifications of the present inventions, in their various aspects, will be apparent to those skilled in the art, some being apparent only after study others being matters of routine mechanical and electronic design. Other embodiments are also possible, their specific designs depending upon the particular application. As such, the scope of the inventions should not be limited by the particular embodiments herein described but should be defined only by the appended claims and equivalents thereof.
Number | Date | Country | |
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Parent | 10733983 | Dec 2003 | US |
Child | 11602134 | Nov 2006 | US |
Parent | 09515880 | Feb 2000 | US |
Child | 10733983 | Dec 2003 | US |