This application claims priority to Japanese Patent Application No. 2019-092434, filed on May 15, 2019, the entire contents of which are incorporated herein by reference.
The disclosure herewith relates to a method of measuring a film thickness.
Japanese Patent Application Publication No. 2019-9329 describes a method of measuring a thickness of a gallium nitride film that is formed on a gallium nitride substrate by epitaxial growth, by Fourier transform infrared spectroscopy or infrared spectroscopic ellipsometry.
The disclosure herein provides a technology that enables accurate measurement of a film thickness of an upper semiconductor layer out of stacked two semiconductor layers, which is different from the technology of Japanese Patent Application Publication No. 2019-9329.
The present disclosure discloses a method of measuring a film thickness of a second semiconductor layer covering a surface of a first semiconductor layer by using a film thickness measuring device. The first semiconductor layer and the second semiconductor layer may be mainly constituted of a same material and may be of a same conductivity type. The film thickness measuring device may comprise a light source, a stage, a half mirror, a photodetector, and a film thickness calculator. The method may comprise fixing a semiconductor substrate including the first semiconductor layer and the second semiconductor layer to the stage, and measuring the film thickness of the second semiconductor layer with the film thickness measuring device. The film thickness measuring device may be configured such that light emitted from the light source is reflected by the semiconductor substrate fixed to the stage after having been reflected by the half mirror, and the light reflected by the semiconductor substrate passes through the half mirror and enters the photodetector. The light reflected by the semiconductor substrate may include first reflected light reflected by a surface of the second semiconductor layer and second reflected light reflected by an interface between the second semiconductor layer and the first semiconductor layer. The film thickness calculator may calculate the film thickness of the second semiconductor layer based on the light detected by the photodetector.
The above-described method enables accurate measurement of the film thickness of the second semiconductor layer.
Representative, non-limiting examples of the present disclosure will now be described in further detail with reference to the attached drawings. This detailed description is merely intended to teach a person of skill in the art further details for practicing preferred aspects of the present teachings and is not intended to limit the scope of the disclosure. Furthermore, each of the additional features and teachings disclosed below may be utilized separately or in conjunction with other features and teachings to provide improved methods for measuring a film thickness.
Moreover, combinations of features and steps disclosed in the following detailed description may not be necessary to practice the disclosure in the broadest sense, and are instead taught merely to particularly describe representative examples of the disclosure. Furthermore, various features of the above-described and below-described representative examples, as well as the various independent and dependent claims, may be combined in ways that are not specifically and explicitly enumerated in order to provide additional useful embodiments of the present teachings.
All features disclosed in the description and/or the claims are intended to be disclosed separately and independently from each other for the purpose of original written disclosure, as well as for the purpose of restricting the claimed subject matter, independent of the compositions of the features in the embodiments and/or the claims. In addition, all value ranges or indications of groups of entities are intended to disclose every possible intermediate value or intermediate entity for the purpose of original written disclosure, as well as for the purpose of restricting the claimed subject matter.
The semiconductor substrate 10 contains a dopant.
Next, the film thickness measuring device 100 used in the measuring method of the present embodiment will be described. As shown in
The light source 102 is configured to emit light in a predetermined wavelength band. In the present embodiment, the light source 102 emits visible light (approximately 400 to 800 nm) or ultraviolet light (approximately 200 to 400 nm).
The semiconductor substrate 10 to be measured is fixed to the stage 104. The semiconductor substrate 10 is fixed such that a lower surface of the first semiconductor layer 12 abuts the stage 104. When the semiconductor substrate 10 is fixed on the stage 104, therefore, an upper surface of the second semiconductor layer 14 is oriented upward.
The half mirror 106 is configured to reflect a part of incident light and allows the remainder of the incident light to pass therethrough. The half mirror 106 is disposed above the stage 104. Specifically, the half mirror 106 is disposed directly above the semiconductor substrate 10 fixed on the stage 104. The half mirror 106 is disposed to be inclined relative to the normal to an upper surface of the stage 104. The half mirror 106 is inclined at an angle that allows the light emitted from the light source 102 and reflected by the half mirror 106 to be emitted onto the semiconductor substrate 10 mounted on the stage 104. The light emitted from the light source 102 is therefore reflected by the half mirror 106 and then enters an upper surface of the semiconductor substrate 10 at an angle substantially perpendicular thereto.
The light emitted onto the upper surface of the semiconductor substrate 10 is reflected by the upper surface thereof. A part of the light reflected by the upper surface of the semiconductor substrate 10 passes through the half mirror 106. The light passed through the half mirror 106 enters the photodetector 108.
The photodetector 108 is configured to generate an interference signal based on interference light obtained from the light reflected by the semiconductor substrate 10. The photodetector 108 includes a diffraction grating 114 and a photoreceptor 116. The diffraction grating 114 is configured to split the incident light to the photodetector 108 by wavelength to generate an interference fringe pattern. The photoreceptor 116 is configured to detect the light split by the diffraction grating 114 by wavelength to generate an interference signal. The film thickness calculator 110 is configured to perform various processes on the interference signal generated by the photoreceptor 116 to calculate a film thickness of the second semiconductor layer 14. The photodetector 108 and the film thickness calculator 110 will hereinafter be described in further details.
The objective lens 112 is disposed between the stage 104 and the half mirror 106. Moving the objective lens 112 in a direction of its optical axis (i.e., a direction linking the stage 104 and the half mirror 106) can change a focus position of the light emitted from the light source 102.
When the film thickness of the second semiconductor layer 14 of the semiconductor substrate 10 is to be measured with the film thickness measuring device 100, the semiconductor substrate 10 to be measured is firstly fixed on the stage 104. The light source 102 then emits light. The light emitted from the light source 102 is reflected by the half mirror 106, and then enters the semiconductor substrate 10 fixed on the stage 104 through the objective lens 112. The light that entered the semiconductor substrate 10 is reflected by the upper surface of the second semiconductor layer 14 and by the interface 13 between the second semiconductor layer 14 and the first semiconductor layer 12. The light reflected by the upper surface of the second semiconductor layer 14 will hereinafter be termed first reflected light, and the light that passed through the second semiconductor layer 14 and then was reflected by the interface 13 between the second semiconductor layer 14 and the first semiconductor layer 12 will hereinafter be termed second reflected light.
The first reflected light and the second reflected light pass through the half mirror 106 through the objective lens 112, and then enter the photodetector 108. The first reflected light and the second reflected light that have entered the photodetector 108 then enter the diffraction grating 114. Each of the first reflected light and the second reflected light that have entered the diffraction grating 114 is split by wavelength. Each split light is reflected by the diffraction grating 114 and inputted into the photoreceptor 116. A line sensor (polychromator) can be used as the photoreceptor 116. The photoreceptor 116 measures interferences between the first reflected light and the second reflected light by wavelength. The photodetector 108 then generates an interference signal in accordance with the intensity of the measured interference light, and inputs this interference signal into the film thickness calculator 110.
Based on the inputted interference signal, the film thickness calculator 110 calculates the film thickness of the second semiconductor layer 14. Specifically, the film thickness calculator 110 extracts each wavelength whose reflectivity is at its peak from the inputted interference signal, and calculates the film thickness of the second semiconductor layer 14 based on the extracted wavelengths. In the above-described manner, the film thickness of the second semiconductor layer 14 can be calculated. As such, the present embodiment enables measurement of the film thickness of the second semiconductor layer 14 by the film thickness measuring device in which the optical path of the light that enters the semiconductor substrate 10 partially overlaps the optical path of the light reflected from the semiconductor substrate 10.
In the present embodiment, the light source 102 emits visible light or ultraviolet light (approximately 200 to 800 nm). In other words, the emitted light has a wavelength shorter than a wavelength of light that is mainly used for infrared spectroscopy (approximately 0.8 to 4 μm). Generally, for accurate measurement of film thickness, emitted light is required to have a wavelength shorter than the film thickness to be measured. Thus, the present embodiment enables suitable measurement of the film thickness of the second semiconductor layer 14 of the semiconductor substrate 10 on the order of micrometers.
Moreover, in the present embodiment, the objective lens 112 is disposed between the stage 104 and the half mirror 106. In other words, the objective lens 112 is disposed on the optical path where the light entering the semiconductor substrate 10 overlaps the light reflected from the semiconductor substrate 10. The present embodiment therefore facilitates adjustment of the focus position of the light emitted from the light source 102.
Moreover, the semiconductor substrate 10 used for the measurement of the present embodiment contains the dopant, and the concentration of this dopant is at its peak at the interface 13 between the first semiconductor layer 12 and the second semiconductor layer 14. The interface 13 therefore has optical properties (e.g., refractive index, and the like) different from those of the other portion of the semiconductor substrate 10. This facilitates detection of the light reflected by the interface 13 (i.e., the second reflected light), and enables accurate detection of the position of the interface 13.
In the semiconductor substrate 10 of the above-mentioned embodiment, although the concentration of the dopant is at its peak at the interface 13 between the first semiconductor layer 12 and the second semiconductor layer 14, the concentration of the dopant may be at its peak at a portion other than the interface 13.
As shown in
When the semiconductor substrate 10 has the dopant concentration distribution shown in
As shown in
As shown in
The first semiconductor layer 22 of the above-described semiconductor substrate 20 contains B, and thus the first semiconductor layer 22 has a high crystal defect density as shown in
Although a crystal defect density has its peak (local maximum value) or a local minimum value at the interface 13 between the first semiconductor layer 12 and the second semiconductor layer 14, the crystal defect density may have a local maximum value or local minimum value at a portion other than the interface 13.
Some of the features characteristic to the technology disclosed herein will be listed below. It should be noted that the respective technical elements are independent of one another, and are useful solely or in combinations.
In a configuration disclosed herein as an aspect, the same material may be a wide gap semiconductor, and the light source may emit visible light or ultraviolet light.
In such a configuration, the light emitted by the light source has a relatively short wavelength. This enables suitable measurement for the semiconductor layer having a film thickness on the order of micrometers.
In a configuration disclosed herein as an aspect, the film thickness measuring device may further comprise an objective lens disposed between the half mirror and the stage, and the method may further comprise adjusting a focus position of the light emitted onto the semiconductor substrate by moving the objective lens.
In such a configuration, the objective lens is disposed on the optical path where the light entering the semiconductor substrate overlaps the light reflected from the semiconductor substrate. Therefore, moving the objective lens facilitates adjustment of the focus position of the light emitted onto the semiconductor substrate.
In a configuration disclosed herein as an aspect, the first semiconductor layer and the second semiconductor layer may contain a dopant, and a concentration of the dopant may be at its peak at the interface between the first semiconductor layer and the second semiconductor layer.
In such a configuration, the interface between the first semiconductor layer and the second semiconductor layer has optical properties different from those of the other portions of the semiconductor substrate. This facilitates detection of the light reflected by the interface, and enables accurate detection of the position of the interface.
In a configuration disclosed herein as an aspect, the same material may be an oxide semiconductor.
In a configuration disclosed herein as an aspect, the first semiconductor layer and the second semiconductor layer may be of n-type, and the first semiconductor layer and the second semiconductor layer may contain a group IV element.
In a configuration disclosed herein as an aspect, the group IV element may be carbon or silicon.
In a configuration disclosed herein as an aspect, a concentration of oxygen atoms in the semiconductor substrate may be at its peak at the interface between the first semiconductor layer and the second semiconductor layer.
In such a configuration, the semiconductor substrate has a low crystal defect density at the interface between the first semiconductor layer and the second semiconductor layer. The interface therefore has optical properties different from those of the other portions of the semiconductor substrate. This facilitates detection of the light reflected by the interface, and enables accurate detection of the position of the interface.
In a configuration disclosed herein as an aspect, the oxide semiconductor may be gallium oxide.
In a configuration disclosed herein as an aspect, a crystal defect density in the semiconductor substrate may have a local maximum or local minimum value at the interface between the first semiconductor layer and the second semiconductor layer.
In a configuration disclosed herein as an aspect, in a distribution of a crystal defect density in the semiconductor substrate measured along a thickness direction of the first semiconductor layer and the second semiconductor layer, a change amount of the crystal defect density may be at its maximum at the interface between the first semiconductor layer and the second semiconductor layer.
When the crystal defect density is distributed as in each of the above-described configurations, the interface between the first semiconductor layer and the second semiconductor layer has optical properties different from those of the other portions of the semiconductor substrate. This facilitates detection of the light reflected by the interface, and enables accurate detection of the position of the interface.
In a configuration disclosed herein as an aspect, a switching element may be disposed in the semiconductor substrate, a resistance of the second semiconductor layer may be higher than a resistance of the first semiconductor layer, and the second semiconductor layer may be a drift layer of the switching element.
While specific examples of the present disclosure have been described above in detail, these examples are merely illustrative and place no limitation on the scope of the patent claims. The technology described in the patent claims also encompasses various changes and modifications to the specific examples described above. The technical elements explained in the present description or drawings provide technical utility either independently or through various combinations. The present disclosure is not limited to the combinations described at the time the claims are filed. Further, the purpose of the examples illustrated by the present description or drawings is to satisfy multiple objectives simultaneously, and satisfying any one of those objectives gives technical utility to the present disclosure.
Number | Date | Country | Kind |
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2019-092434 | May 2019 | JP | national |