This disclosure relates to a susceptor for placing a wafer thereon within an epitaxial wafer growth device, an epitaxial growth device having the susceptor, and an epitaxial wafer that can be produced by the epitaxial growth device.
An epitaxial wafer is formed by growing an epitaxial film on the surface of a semiconductor wafer by vapor phase growth. For example, when crystal integrity is further required, when a multi-layer structure of different resistivity is needed, or the like, an epitaxial silicon wafer is produced by growing a single crystal silicon thin film on a silicon wafer by vapor phase growth or epitaxial growth.
For epitaxial wafer production, a single wafer type epitaxial growth device (apparatus) is used for example. Here, a typical single wafer type epitaxial growth device will be described with reference to
In such an epitaxial growth device, the wafer W is directly supported and lifted by the lift pins. Therefore, to a part of the back surface of the wafer W abutting against the lift pins, the lift pins ascend and abut, and contact with the upper end of the lift pins is continuously maintained. Thus, there has been a problem that scratches or pin marks having a depth more than 0.5 μm occur in the above mentioned part of the back surface of the wafer W.
Moreover, JP 2001-313329 A (PTL 1) discloses the technique of lifting a wafer directly by a part of a susceptor, instead of supporting and lifting the wafer directly by lift pins. More specifically,
PTL 1: JP 2001-313329 A
According to the technique of PTL 1, since the wafer is, when lifted, supported by a part of the susceptor at an edge part of the wafer, without being locally supported by lift pins, occurrence of scratches on the back surface of the wafer attributable to lift pins can be prevented. However, since a beveled part or edge part of the wafer is supported by point contact using three lift members 36, i.e., projections protruding inside from the soft ring 32, it is concerned that scratches having a depth more than 0.5 μm occur on the beveled part of the wafer. Additionally, the inventors have newly recognized that the technique of PTL 1 has a problem as follows.
More specifically, in PTL 1, the recessed part for accommodating the soft ring therein is located in the periphery of the susceptor main body, and outside the edge of the wafer. Therefore, at the time of vapor phase growth, the front surface of the soft ring and the front surface of the susceptor main body around the recessed part are in contact with a source gas to grow an epitaxial film, and the epitaxial film may even connect at a horizontal separation part between the soft ring and the susceptor main body. Thereafter, when the soft ring is relatively lifted from the susceptor main body, the epitaxial film connected at the separation part breaks and generates dust. It is desirable to reduce this dust, which attaches to the surface of the produced epitaxial wafer and generates many defects.
Therefore, in consideration of the above problems, this disclosure has the purpose of providing a susceptor and an epitaxial growth device, capable of preventing occurrence of deep scratches on the back surface and beveled part of a wafer attributable to contact with lift pins or the susceptor and reducing dust generation from the susceptor. Moreover, this disclosure has the purpose of providing an epitaxial wafer that has no observed scratches having a depth more than 0.5 μm which can occur due to contact with the lift pins or the susceptor.
The brief configuration of this disclosure for solving the above problems is as follows.
1. A susceptor for placing a wafer thereon within an epitaxial growth device, wherein
a counterbore part for placing the wafer thereon is formed on a front surface of the susceptor,
the susceptor has a susceptor main body, and two or more arc-shaped members placed on two or more recessed parts provided in an outer circumferential part of a front surface of the susceptor main body,
a bottom surface of the counterbore part is constituted of entire front surfaces of the arc-shaped members, and a part of the front surface of the susceptor main body,
the susceptor main body is provided with two or more penetration holes, for lift pins that support a back surface of the two or more arc-shaped members, and ascend and descend the two or more arc-shaped members, to be inserted therethrough, and
when the wafer is being placed on the counterbore part and when the wafer is carried out of the counterbore part, the entire front surfaces of the arc-shaped members ascended by the lift pins act as a supporting surface for supporting only an outer circumferential part of a back surface of the wafer by surface contact.
2. The susceptor according to the above item 1, the number of the arc-shaped members is two, located in substantially line symmetry from a front view.
3. The susceptor according to the above item 1 or 2, wherein the lift pins are fixed to the arc-shaped members.
4. An epitaxial growth device comprising: the susceptor according to any one of the above items 1 to 3; and an ascending/descending mechanism for ascending and descending the lift pins by supporting a lower end of the lift pins.
5. An epitaxial wafer comprising: a wafer; and an epitaxial layer formed on a surface of the wafer, wherein scratches having a depth more than 0.5 μm are not observed when a back surface and a beveled part of the epitaxial wafer are observed using a laser microscope.
6. The epitaxial wafer according to the above item 5, wherein scratches having a depth as small as 0.3 μm or less are not observed when a central part of the back surface of the epitaxial wafer is observed using a laser microscope.
The susceptor and the epitaxial growth device according to this disclosure can prevent occurrence of deep scratches on the back surface and beveled part of a wafer attributable to contact with the lift pins or the susceptor and reduce dust generation from the susceptor. Moreover, by using this susceptor and epitaxial growth device, an epitaxial wafer that has no observed scratches having a depth more than 0.5 μm which can occur due to contact with the lift pins or the susceptor.
This disclosure will be further described with reference to the accompanying drawings, in which:
With reference to
Epitaxial Growth Device
The epitaxial growth device 100 illustrated in FIG, 6 and
Chamber
The chamber 10 includes the upper dome 11, the lower dome 12 and the dome mounting body 13, and this chamber 10 defines the epitaxial film forming chamber. The chamber 10 is provided with the gas supply opening 15 and the gas exhaust opening 16 for supplying and exhausting a reaction gas at opposing positions on the side surface thereof.
Heat Lamp
The heat lamp 14 is arranged in the upper side region and the lower side region of the chamber 10, and generally a halogen lamp or infrared lamp having a high temperature increase/decrease rate, and excellent temperature controllability is used.
Main Configuration of Susceptor
With reference to
With reference to
With reference to
With reference to
Two lift pins 44 extend from each of the back surfaces 42A and 42B. These four lift pins 44 in total are respectively inserted through the four penetration holes 35 provided in the susceptor main body. The lift pins 44 can attach and detach the arc-shaped members 40A and 40B, and the susceptor main body 30, while supporting the back surfaces 42A and 42B of the arc-shaped members, by being ascended and descended in the vertical direction by the ascending/descending shaft 60 described below. This motion will be described below. From the perspective of stably ascending and descending the arc-shaped members, it is preferable to provide each arc-shaped member with two lift pins, and to provide these two lift pins in the vicinity of both ends of the arc-shaped member. Although the lift pins 44 are fixed to the arc-shaped members 40A and 40B in this embodiment, the lift pins 44 may not be fixed to the arc-shaped members 40A and 40B.
As illustrated in
Meanwhile, as illustrated in
Moreover, in the specification, “the central part of the back surface of the wafer” means a region inside the outer circumferential part of the back surface of the wafer, i.e., a region within less than 70% of the wafer radius from the wafer center. Furthermore, in this embodiment, since the arc-shaped members 40A and 40B support only the outer circumferential part of the back surface of the wafer W, the central part of the back surface does not have contact, not only point contact but also surface contact, with any members. Therefore, when the central part of the back surface of the produced epitaxial wafer is observed using a laser microscope, even scratches or contact scratches having a depth as small as 0.3 μm or less are not observed. During the epitaxial growth treatment, a phenomenon such as warp projecting upward or downward occurs in the wafer W under a high temperature heat treatment. Thus, if contact scratches are present on the back surface central part of the wafer W, slip dislocation is more likely to occur from these scratches as a starting point, which is not a concern in this embodiment.
The wafer W supported by the arc-shaped members 40A and 40B are conveyed out of the chamber, while the back surface central part of the wafer W is supported by a wafer supporting part 72 of a U-shaped conveying blade 70 inserted from the direction illustrated in
The surface part of the arc-shaped members 40A and 40B or the entirety of the arc-shaped members 40A and 40B is preferably made of a soft material such as glassy carbon. It is because occurrence of scratches when the back surface of the wafer W is supported by surface contact can be prevented.
In addition, the bottom of the recessed parts 31A and 31B of the susceptor main body, and the arc-shaped members 40A and 40B are also preferably porous structures. It is because by promoting hydrogen gas to sneak into the back surface of the wafer W, occurrence of halo or haze on the wafer back surface can be prevented.
Susceptor Support Shaft
With reference to
Ascending/Descending Shaft
As illustrated in
Production Procedure for Epitaxial Wafer
Next, a series of actions of carrying the wafer W into the chamber 10, vapor phase growth of an epitaxial film onto the wafer W, and carrying the produced epitaxial wafer out of the chamber 10 will be described with appropriate reference to
The wafer W carried into the chamber 10 while being supported by the conveying blade 70 illustrated in
Then, by ascending the susceptor support shaft 50, the susceptor main body 30 is moved to a position of the arc-shaped members 40A and 40B, and the wafer W is placed on the counterbore part 21 of the susceptor 20. Subsequently, an epitaxial wafer is produced by, while heating the wafer W to a temperature not lower than 1000° C. by the heat lamp 14, supplying a reaction gas from the gas supply opening 15 into the chamber 10, and growing an epitaxial film having a predetermined thickness by vapor phase growth. During vapor phase growth, by rotating the susceptor support shaft 50 using the main column 52 as a rotation axis, the susceptor 20 and the wafer W thereon are rotated.
Thereafter, by descending the susceptor support shaft 50, the susceptor main body 30 is descended. This descending is performed until the lift pins 44 are supported by the ascending/descending shaft 60 and the arc-shaped members 40A and 40B are separate from the susceptor main body 30, and the produced epitaxial wafer is supported by the front surfaces 41A and 41B of the arc-shaped members 40A and 40B supported by the lift pins 44. Then, the conveying blade 70 is introduced into the chamber 10, and the epitaxial wafer is placed on the wafer supporting part 72 of the conveying blade by descending the lift pins 44. Thus, the epitaxial wafer is passed from the arc-shaped members 40A and 40B to the conveying blade 70. Subsequently, the epitaxial wafer is carried out of the chamber 10 along with the conveying blade 70.
Configuration of Characteristic Part of Susceptor
Here, the position of the arc-shaped members 40A and 40B, as a characteristic configuration of this disclosure, will be described in detail.
With reference to
The technical significance of adopting such a configuration will be described with comparison to
Contrarily, in this embodiment illustrated in
Using the susceptor illustrated in
Similarly to Example except for using the susceptor illustrated in
Using the conventional epitaxial growth device illustrated in
[Vapor Phase Growth Conditions]
For producing epitaxial wafers, a silicon wafer was introduced into the chamber, and placed on the susceptor in the previously described method. Then, a hydrogen bake out was performed under a hydrogen gas atmosphere at 1150° C., and a silicon epitaxial film was grown on the silicon wafer surface by 4 μm at 1150° C., to obtain an epitaxial silicon wafer. Here, trichlorosilane gas was used as a raw material source gas, diborane gas as a dopant gas, and hydrogen gas as a carrier gas. Subsequently, by the previously described method, the epitaxial silicon wafer was carried out of the chamber.
[Evaluation of Back Surface Quality]
Each of the epitaxial wafers produced in Examples and Conventional Example was subject to observation of the back surface region corresponding to the position of supporting members, which are lift pins in Conventional Example and arc-shaped members in Example, using a confocal laser microscope with a magnification of 1000×. The results are illustrated in
Additionally, scratches having a depth more than 0.5 μm were also not observed in the beveled part of the epitaxial wafer in Example. Moreover, when the central part of the back surface was observed using the laser microscope, scratches having a depth or Peak-Valley as small as 0.3 μm or less were also not observed in the epitaxial wafer of Example. Thereby, occurrence of slip dislocation in the epitaxial wafer central part can be certainly prevented.
Furthermore, the epitaxial wafers produced in Example and Comparative Example were subject to observation of the back surface region corresponding to the position of lift pins using a surface examination device, manufactured by KLA-Tencor: Surfscan SP-2, in DCO mode, and measurement of the area of the region having a scattering strength not lower than the value set for laser reflection, or pin mark strength, to evaluate scratches on the epitaxial wafer back surface attributable to lift pins. The result was 0 mm2, and no scratches on the epitaxial wafer back surface attributable to lift pins were observed for both Comparative Example and Example.
[Evaluation of Number of Defects in Epitaxial Wafer]
10 epitaxial wafers produced in each of Example and Comparative Example were subject to observation of the epitaxial film using a surface examination device, manufactured by KLA-Tencor: Surfscan SP-2, in DCO mode or Dark Field Composite Oblique mode, to count the number of LPDs or Light Point Defects having a diameter not less than 0.25 μm. From this measurement result, the particle generation status due to dust generation can be evaluated. While the result was 20.1 defects per wafer with a standard deviation of 9.1 in Comparative Example, the value decreased to 6.4 defects per wafer with a standard deviation of 3.7 in Example. This suggests that dust generation from the susceptor could be reduced in Example.
The susceptor and the epitaxial growth device according to this disclosure, which can prevent occurrence of deep scratches on the wafer back surface and beveled part attributable to contact with lift pins or the susceptor, and reduce dust generation from the susceptor, can preferably be applied to epitaxial wafer production.
100 Epitaxial growth device
10 Chamber
11 Upper dome
12 Lower dome
13 Dome mounting body
14 Heat lamp
15 Gas supply opening
16 Gas exhaust opening
20 Susceptor
21 Counterbore part
30 Susceptor main body
31A, 31B Recessed part
32 Front surface outer circumferential part of susceptor main body
32A Wafer supporting surface
32B Vertical wall surface
33 Front surface central part of susceptor main body
34A, 34B Bottom surface of recessed part
35 Penetration hole
40A, 40B Arc-shaped member
41A, 40B Front surface of arc-shaped member
42A, 42B Back surface of arc-shaped member
43A, 43B Outer circumferential surface of arc-shaped member
44 Lift pin
45A, 45B inner circumferential surface of arc-shaped member
50 Susceptor support shaft
52 Main column
54 Arm
56 Penetration hole
58 Supporting pin
60 Ascending/descending shaft
62 Main column
64 Support column
66 Tip part of support column
70 Wafer conveying blade
72 Wafer supporting part
W Wafer
Number | Date | Country | Kind |
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2015-090563 | Apr 2015 | JP | national |
Filing Document | Filing Date | Country | Kind |
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PCT/JP2016/002165 | 4/22/2016 | WO | 00 |