The present invention relates to the field of ultrasound transducers, and in particular to ultrasound transducers grown from thin films.
Ultrasound is used for investigating the interiors of opaque components where visual inspection is unsuitable. This may be where visual inspection is impossible or inadequate, or where important information can be obtained from ultrasound analysis. Piezoelectric transducers are used to generate and detect ultrasonic signals, with a pulse being directed into a component or material under investigation. A reflected signal, characterised by discontinuities in the component or material, is detected by transducers and is used to derive information on the discontinuities. These pulse-echo mode techniques are used for a variety of applications.
Conventionally, transducers are separate devices coupled to the test component or material. Effective acoustic coupling of the test component with the transducer presents a number of difficulties, resulting in a ultrasound pulses being inefficiently transmitted to the component. Waves reflected from the transducer-component interface impact on the detection of the reflected pulse. Typically, multilayer backing layers are required on the transducer to absorb unwanted reflections. This increases the size, weight, and material costs of the transducer unit. The shape of the transducer itself is also affected. The increased size, weight and cost, and effect on shape limits the practical applications of the transducers.
It would therefore be desirable to provide a transducer having improved coupling with a material or component to be investigated.
In addition, use of conventional transducers in high temperature systems requires complicated cooling or heat shielding arrangements. This increases the bulk of the transducers and increases capital costs, rendering them unsuitable for many applications. If coupling gel is necessary for effective acoustic coupling, the suitability for high temperature applications is further reduced, since the gel tends to solidify or evaporate when exposed to heat.
It would therefore be desirable to provide a transducer suitable for use in high temperature systems.
The market has an increasing demand for high frequency ultrasound transducers, capable of operating in the 50 to 300 MHz frequency range. Currently available high frequency transducers are expensive to produce and suffer from reliability problems.
It would therefore be desirable to provide an alternative ultrasound transducer with high frequency capabilities.
Polycrystalline aluminium nitride (AlN) thin films are known for their piezoelectric electric properties, and as such are used in thin film applications such as surface acoustic wave devices and resonators. AlN films can be deposited on substrates using a variety of deposition techniques, including RF-sputtering at low temperatures, as described in “Low temperature growth of RF reactively planar magnetron sputtered AlN films”, by M. Penza et al., Thin Solid Films, 259, (1995) pp. 154-162.
Various sputtering parameters affect the characteristics of the AlN films. “Condition monitoring with ultrasonic arrays at elevated temperatures” by K. Kirk et al, Insight Vol 45 No 2 Feb. 2003 discloses the deposition of AlN films by RF sputtering with no substrate heating. In a nitrogen atmosphere, the AlN film grows in the (002) orientation with the c-axis normal to the substrate surface, this orientation being preferred for some piezoelectric applications.
It is one aim of the invention to provide a thin film aluminium nitride ultrasound transducer and a method of manufacture thereof.
It is further aim of the invention to provide a test component having a thin film aluminium nitride ultrasound transducer deposited thereon.
It is further aim of the invention to provide a method for depositing a thin film aluminium nitride ultrasound transducer on a test component.
Further aims and objects of the invention will become apparent from reading the following description.
According to a first aspect of the invention, there is provided an ultrasound transducer comprising a thin film of aluminium nitride provided on a substrate.
Preferably, the aluminium nitride film is (002) orientated with its c-axis normal to the surface of the substrate.
The substrate may comprise metal. Alternatively, the substrate may comprise glass or a composite material.
More preferably, the substrate comprises a component of an apparatus of which ultrasound inspection is required.
The component may be a part of an engine.
The component may a bearing. The thin film of aluminium nitride may be deposited on the outer surface of the bearing.
Alternatively, the substrate is adapted to be coupled to an apparatus of which ultrasound inspection is required.
The thin film of aluminium nitride may be deposited on the substrate in a patterned arrangement.
Alternatively, the thin film of aluminium nitride may cover an entire surface of the substrate.
According to a second aspect of the invention, there is provided a system for non-destructive testing comprising a test component, an ultrasound transducer, ultrasound control apparatus and signal processing apparatus communicating with the ultrasound transducer, wherein a pulse is emitted from the ultrasound transducer to propagate the test component and a reflected pulse is detected by the ultrasound transducer, wherein the ultrasound transducer comprises a thin film of aluminium nitride deposited on the test component.
Preferably, the aluminium nitride film is (002) orientated with its c-axis normal to the surface of the substrate.
The component may be a part of an engine, or an assembly of parts of an engine.
The component may be a bearing assembly. The thin film of aluminium nitride may be deposited on the surface of a part of the bearing assembly. The surface may be a surface of a dust cap. Alternatively, the surface may be a surface of a raceway of a bearing.
The thin film of aluminium nitride may be deposited on the test component in a patterned arrangement.
Alternatively, the thin film of aluminium nitride may cover an entire surface of the test component.
The thin film of aluminium nitride may be provided with an electrode. The thin film of aluminium nitride may be provided with a plurality of electrodes.
The electrodes may be patterned such that an array of operable ultrasound transducers is defined.
According to a third aspect of the invention, there is provided a method of non-destructive testing a test component, comprising the steps of emitting a pulse from an ultrasound transducer to propagate in the test component and detecting a reflected pulse, wherein the transducer comprises a thin film of aluminium nitride deposited on the test component.
According to a fourth aspect of the invention, there is provided a component of a mechanical apparatus, wherein the component is provided with an ultrasound transducer formed from a thin film of aluminium nitride deposited on the component, and the transducer is adapted to emit or receive an ultrasound pulse into or from the component during ultrasound inspection.
Preferably, the aluminium nitride film is (002) orientated with its c-axis normal to the surface of the substrate.
Preferably, the component is a metal component.
Optionally, the component comprises two sub-components joined to one another at an interface, and the ultrasound transducer is adapted to direct an ultrasound pulse towards the interface.
Optionally, the component comprises two sub-components joined to one another at an interface, and the ultrasound transducer is adapted to receive an ultrasound pulse reflected from or transmitted through the interface.
The component may be a part of an engine.
The component may a bearing. The thin film of aluminium nitride may be deposited on the outer surface of a raceway of the bearing.
The thin film of aluminium nitride may be deposited on the component in a patterned arrangement.
Alternatively, the thin film of aluminium nitride may cover an entire surface of the component.
The system may be provided with an array of ultrasound transducers defined by a pattern of discrete areas of the aluminium nitride film.
Alternatively, an array of electrodes may be provided on a single area of the aluminium nitride film.
According to a fifth aspect of the invention there is provided a method of monitoring a bearing, the method comprising the step of emitting an ultrasound pulse from an ultrasound transducer, characterised in that the ultrasound transducer is formed from a thin film of aluminium nitride deposited on a part of the bearing.
According to a sixth aspect of the invention there is provided a method of ultrasonically imaging a test component, the method comprising the step of emitting pulses from an array ultrasound transducers formed from a thin film of aluminium nitride material deposited on the test component.
According to a seventh aspect of the invention there is provided a method of ultrasonically imaging a test component, the method comprising the step of detecting, using a receiving pulses from an array ultrasound transducers formed from a thin film of aluminium nitride material deposited on the test component.
According to an eighth aspect of the invention, there is provided a method of manufacturing an ultrasound transducer, the method comprising the step of depositing a thin film of AlN on a substrate.
Preferably, the step of depositing a thin film of AlN is carried out by RF-sputtering in a nitrogen atmosphere.
More preferably, the sputtering pressure is in the range of 650 to 950 kPa.
More preferably, the RF-power is approximately 800 W.
The present invention will now be described, by way of example only with reference to the following drawings, of which:
a and 14b respectively show measurements of pulse amplitude and pulse frequency for the apparatus of
The present invention in its various aspects utilises the growth of thin films of AlN on various substrates. The following is an example of how such growth is achieved for a glass substrate.
A Cryo Vacuum Chamber (CVC) RF magnetron sputtering machine was used, with an aluminium target of 99.999% purity and a diameter of 20.3 cm (8 inches). The target to substrate distance was 24 cm.
The substrates were cleaned in an ultrasonic bath with isopropyl alcohol for 15 minutes to remove impurities on the substrate surface and to improve adhesion. The pressure in the chamber was reduced to around 10−6 Torr (˜10−4 Pa) using a cryo pump. Different sputtering conditions were applied, as described below. In each case, the target was pre-sputtered at the same deposition conditions for 10 minutes with the shutter closed in order to remove oxides present on the surface of the target. After opening the shutter, the AlN thin film was deposited for 7 hours with no substrate heating.
Three different sets of deposition conditions were investigated, as follows:
The deposition rate, defined as the film thickness divided by sputtering time, was measured for RF power from 300 W to 800 W. The results are shown in
The crystallographic structure of the film was determined using X-ray diffraction with a Siemens D5000 machine.
The experimental results show the optimal deposition conditions for deposition of a (002) AlN film to be an RF power of 800 W, in a pure N2 atmosphere at about 6 mTorr (800 kPa).
However, it should be appreciated that optimal RF power can vary with the individual sputtering machine, and for extended deposition times additional orientations may become apparent, even under optimum conditions.
The above experimental results provide a deposition method for growing a highly (002) orientated AlN thin film with c-axis normal to the substrate surface.
The highly (002) orientated AlN thin films grown were investigated for piezoelectric activity using a Piezoelectric Force Microscope as follows. AlN was deposited on a layer of aluminium under the sputtering conditions described above, and a small Al contact was deposited on the upper surface of the AlN using a metal mask.
The experimental data relates to a glass substrate, but the above techniques can be used to grow thin film AlN transducers on a variety of substrates, including metallic and crystalline substrates.
No substrate heating is required for effective, reliable, reproducible results, enabling deposition on substrates for which other deposition techniques are unsuitable. In particular, the above-described techniques are suitable for growing highly (002) orientated AlN films on delicate and/or shaped substrates, or other components on which a uniform substrate temperature would be difficult to achieve.
The above-described techniques can also be used to deposit AlN thin films on curved surfaces.
The described method allows the production of effective ultrasonic thin film transducers. Transducers produced by this method offer the following benefits and advantages.
Deposition on a wide range of amorphous and crystalline substrates is possible, for example, glass, metal, and silicon.
No substrate heating is required for deposition, enabling the coating of bulk objects.
AlN is capable of withstanding high temperatures and is chemically stable.
Use of thin films makes it easy to achieve high frequency, and high bandwidth transducers. Transducers operational at frequencies of around 38 to 200 MHz are achievable.
The films are strongly crystalline and can be made several microns thick allowing increased energy generation by the material.
The surface of the blocks does not require extensive preparation, and good films have been made using only simple surface preparation techniques such as sandpapering or grinding, and surface cleaning by wiping with methanol using a lint-free cloth was sufficient.
A thin film grown on a component transfers ultrasound more efficiently to and from the component than a separate transducer, and avoids the need for backing materials to absorb unwanted reflections.
The thin film is low profile and does not add significant weight or bulk to the components, and thus is non-intrusive.
The AlN films have high electrical breakdown field, enabling larger transmitted power.
AlN has high acoustic velocity, and is lead free.
Instrumentation redesign is not required and good signal-to-noise ratios can be achieved.
Multilayers of AlN are possible, enabling design of transducers with advanced properties.
The above properties enable to the production of robust, inexpensive, high frequency transducers and arrays to replace conventional transducers. The AlN films can be grown on a support material, which is then attached in an appropriate manner to the material under investigation.
High frequency transducers and arrays can be used for example in layer thickness measurements in non-destructive testing and manufacturing control, and for high resolution real time acoustic microscopy.
The above-described technology has numerous additional applications. One application is in the field of non-destructive testing of important components, for example engineered metallic components or tools. In one implementation, a highly oriented AlN film is grown directly on a component to be tested to form an integrated ultrasonic transducer. Electrodes painted on the film define an array of ultrasound transducers capable of operation in conjunction with existing equipment.
Depending on the type of component, the sputtering process may need to be adapted in order to provide a satisfactory AlN film growth on the shaped component. For example, any directional sputtering and masking techniques known to one skilled in the art may be employed. The film can be deposited over the surface of the components to any extent required, or merely deposited in discrete patches.
The integrated transducer and test component improves acoustic coupling, and the thin film nature of the transducer does not add bulk or weight to the component, allowing it to perform its function.
In an alternative implementation, the film is deposited on a coupon, which is attached to a parent component to be monitored.
The foregoing has applications in, for example, monitoring the wear of precision components or high technology machine tools. In addition, engineering components under high stress or strain can be monitored for defects and flaws. Active condition monitoring of important components, such as brake components, parts in gearboxes, and critical regions of pipework in petrochemical processing plants can be achieved.
In use, the electrode excites the AlN film to cause an ultrasound pulse to propagate in the metal component 142. The pulse detected will be characterised by the integrity of the joint between the components 142 and 141, allowing detection of defects and flaws in the weld. The low profile and extremely good coupling of the AlN thin film transducers make them particularly suitable for this application.
It will be appreciated that pulse-echo, through transmission or acoustic emission and spectroscopic measurements could be used in this application. In some embodiments, the thin film may be formed in an array, and the test component may be imaged. In another embodiment, an array of electrodes may be formed on a continuous area of aluminium nitride thin film.
The present technology also has applications in the monitoring of oil films in bearings to check for the presence of cavities, discontinuities, drying out and breakdown of the oil film. At present, the investigation of oil films by ultrasound techniques is being researched using conventional transducers. The techniques described herein allow a thin film transducer to be grown on an outer surface of a bearing, thereby improving acoustic contact and avoiding the use of bulky and relatively heavy conventional transducers.
Activation of the outer surfaces of bearings allows monitoring of the internal oil film, giving the capability to identify lubrication problems and mitigate the risk of seizure. In particular, the reflected pulse will be characterised by the absence of an oil film adjacent the internal surface of the raceway.
In use, the electrode activates the aluminium nitride thin film to generate an ultrasound pulse.158 that propagates first in the metal raceway 152, and then in the lubricant 154. The signal reflected from the interface between the ball bearing 151 and the lubricant 154 is characterised by the lubricant layer, allowing detection of cavities, discontinuities, drying out and breakdown of the lubricant film.
An aluminium nitride thin film ultrasound transducer is particularly suitable for this application due to its low profile, high temperature operation and broadband characteristics.
A yet further application of the technology is to process monitoring at high temperatures, for example in sintering powdered metals, monitoring green-state ceramic extrusion, and high frequency monitoring of colloid processing in the food industry.
Presently, there is significant unfulfilled demand for process monitoring at high temperatures. For example, there is very significant wastage in the food industry because of process variations that cause off-flavours and require the disposal of whole batches of food. The use of thin film AlN transducers produced in accordance with aspects of the present invention allows real-time physical analysis of textures, particle sizes and consistencies, to supplement chemical analyses.
Other applications result from the drive for miniaturisation, integration and cost-reduction in the sensor market and include:
The reproducible, reliable properties of the AlN transducers also renders then suitable for monitoring of the output of existing transducers.
Improvements and modifications may be incorporated herein without deviating from the scope of the invention.
Number | Date | Country | Kind |
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0414705.4 | Jul 2004 | GB | national |
Filing Document | Filing Date | Country | Kind | 371c Date |
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PCT/GB05/02571 | 7/1/2005 | WO | 00 | 5/20/2008 |