Not applicable.
Not applicable.
This invention relates to the sealing of microelectromechanical systems (MEMS) devices in an enclosure and the method of manufacture of the sealed enclosure. In particular, this invention relates to the formation of a hermetic seal at a low temperature between a fabrication wafer supporting a MEMS device, and a lid wafer enclosing the MEMS device.
Microelectromechanical systems (MEMS) are devices often having moveable components which are manufactured using lithographic fabrication processes developed for producing semiconductor electronic devices. Because the manufacturing processes are lithographic, MEMS devices may be batch fabricated in very small sizes. MEMS techniques have been used to manufacture a wide variety of sensors and actuators, such as accelerometers and electrostatic cantilevers.
MEMS techniques may be used to manufacture small detectors and emitters, such as infrared bolometers. These devices may require evacuated cavities to function properly, so that the emitter or detector may be placed in a sealed device cavity during or after fabrication. The sealed cavity may be formed by placing a lid wafer and a device wafer in an evacuated wafer bonding chamber, and bonding the two wafers to form a two-wafer assembly with a hermetic seal to form the evacuated device cavity enclosing the infrared device.
MEMS techniques have also been used to manufacture electrical relays or switches of small size, generally using an electrostatic actuation means to activate the switch. In the MEMS switches, a thin cantilevered beam of silicon is etched into the silicon device layer, and a cavity is created adjacent to the cantilevered beam, typically by etching the thin silicon dioxide layer to allow for the electrostatic deflection of the beam. Electrodes provided above or below the beam may provide the voltage potential which produces the attractive (or repulsive) force to the cantilevered beam, causing it to deflect within the cavity.
Because the MEMS devices often have moveable components such as the electrical relay, or require a vacuum, such as the infrared bolometer, they typically require the enclosure of the device by sealing it with a protective cap or lid wafer, to form a device cavity as mentioned. The lid wafer may be secured to the device wafer by some adhesive means, such as a low outgassing epoxy.
However, the epoxy bond may not be hermetic, such that the gas with which the MEMS device is initially surrounded during fabrication, escapes over time and may be replaced by ambient air, or the vacuum is eventually lost via gas leakage through the seal. Accordingly, it may be preferable to seal the MEMS device in a hermetic, i.e., non-leaking enclosure.
Furthermore, the deposition techniques used to form the thin layers often result in gases incorporated in the layers during deposition. These devices may then be encapsulated in an evacuated cavity for proper functioning. However, the gases incorporated in the films may escape from the layers during the lifetime of the device, raising the pressure in the evacuated cavities. Accordingly, many designs include a “getter” material, namely a reactive, generally metal layer, whose purpose is to absorb these gases, and maintain the vacuum levels within the package. Because of the reactive nature of these materials, they also tend to oxidize at the surface, forming an oxide layer that must be removed in order to activate the getter.
Infrared applications in particular, may require very low pressure environments, such as sub 10-Torr. Achieving such a pressure over the lifetime of the device generally requires such a gettering material to be sealed in the cavity to absorb impurity gases released or leaked into the cavity over time. Thus, in order to maintain the environment around the MEMS device, the seal may need to be hermetic, and a getter may also need to be provided in the device cavity.
Current packaging techniques for vacuum-encapsulated packages require high temperatures, in excess of 400 C, to activate the getters. At this temperature, the oxide layers on the surface of the getter are generally driven into the bulk of the getter material, leaving the surface relatively clean and able to absorb additional impurity gases. These high temperatures are consistent with those required to fuse glass frit, which is often used for vacuum encapsulation, because the melting temperatures simultaneously fire, or activate, the getter. Accordingly, the step of sealing the device in the frit also activates the getter.
However, because the MEMS devices may be made with thin, delicate metal layers, the device may not be able to withstand the high temperatures required to form a hermetic seal or activate the getter. While low temperature bonding materials exist, the device must still be exposed to high temperatures in order to activate the getter. For this reason, vacuum applications requiring a low temperature bonding mechanism have been hampered in development.
The systems and methods described here form a hermetic seal between a device wafer and a cap or lid wafer using a hermetic bonding material, to form a two-wafer assembly. The seal construction may include a bonding material which is applied to at least one of the wafers of the two-wafer assembly. This wafer may then be heated preferentially within the wafer bonding chamber to activate the bonding material, whereas the device wafer remains cool. Thus, the wafers inside the bonding chamber may be held at two substantially different temperatures. These substantially different temperatures may be achieved by one or more: heating the upper lid wafer; cooling the lower device wafer; providing a heat shield between the upper and lower wafers; illuminating the upper wafer with a radiation source such as a laser; cooling the lower wafer by applying an inert gas or refrigerated liquid to the backside of the wafer chuck; and heating only specific structures in the device by providing an magnetically permeable layer under the structure, and heating that layer by inductive coupling to a coil driven by an RF signal. These are examples of different embodiments, and the list is not meant to be exhaustive, but instead to provide examples of the inventive concept.
One example of a useful hermetic seal is a metal alloy bond, such as an indium layer deposited over a gold layer. The gold and indium layers are then heated to a temperature beyond the melting point of the indium (156 C.°). The heat required to produce this temperature may be applied only to one of the wafers, that is, the lid wafer may be heated to this temperature, whereas the lower device wafer remains cool. In this way, the delicate features of the device wafer are protected from the higher temperatures.
The AuInx alloy is an example of a class of bonding mechanisms known generally as solid/liquid interdiffusion bonds (SLID). These bonds generally make use of a lower melting temperature first component which forms a bond with a higher temperature solid second component. The bond is often a metallic alloy of a low melting temperature metal such as indium and the higher temperature metal such as gold. The requirement to heat the components is limited because of the low melting temperature of the first component of the SLID bond. The metal layer for the SLID bond may also be deposited over a rigid raised feature formed on the surface of one substrate, which in turn forms a raised region in the metal layer. This raised region then penetrates the opposing layer of the other metal deposited on the other substrate, thereby ensuring a region relatively rich in composition of metal of the raised feature.
The wafer bonding chamber may include a plurality of fixtures, each supporting one wafer on a frontside of the fixture, and at least one of a heating mechanism and a cooling mechanism, configured so as to maintain one of the wafers in one of the fixtures at a substantially different temperature than another wafer in another of the plurality of fixtures. Several embodiments of these ideas are described below, as examples of the inventive concept.
Various exemplary details are described with reference to the following figures, wherein:
As mentioned previously, many vacuum encapsulated devices have used a glass frit adhesive to bond two substrates together, wherein the substrates define an evacuated device cavity in the wafer assembly that encloses a microdevice. The glass frit provides a hermetic seal around the device cavity, maintaining the vacuum therein. Glass frit requires high melting or bonding temperatures, which may destroy the delicate structures of the microdevice. However, these high temperatures are also needed to activate the getter enclosed in the device cavity. Therefore, if using a lower temperature bonding method is used, some other means must be devised for activating the getter which requires the higher temperatures.
Many devices and especially so-called microelectromechanical systems (MEMS) devices, have delicate structures which cannot withstand these 400+ degree centigrade temperatures. For these devices, a lower temperature bond may be used, for example, a metal alloy bond such as that described in U.S. patent application Ser. No. 11/211,622, filed Aug. 26, 2005 and U.S. patent application Ser. No. 11/304,601, now U.S. Pat. No. 7,569,926. Each of these documents is incorporated by reference in their entireties. For such applications, the getter must be fired some other way than raising the temperature of the wafer assembly to 400+ degrees centigrade. Furthermore, the getter must be activated within a vacuum cavity, for example within the wafer bonding chamber, and that vacuum maintained in order to avoid the reformation of the passivation layer over the getter surface. This may be done by, for example, heating the lid and device wafers within an evacuated bonding chamber, and then bonding the lid wafer to the device wafer in the bonding chamber. However, the bonding material is generally already placed on the lid wafer before insertion in the bonding chamber, thus requiring a bonding technology to withstand the high temperatures required to activate the getter. If a low temperature metal alloy bonding material is used on the lid wafer, these metal films may be melted, damaged or degraded by the heat.
Accordingly, to date, there has been no way of using a low temperature bond with a device requiring a getter, which has greatly inhibited the development of such devices. There are, indeed, many such devices such as infrared imaging devices or bolometers, which because of their need for an evacuated operating environment, require getters, but their delicate structures cannot withstand high temperatures, and thus they also require both a low temperature bond and getter activation.
Accordingly, the systems and methods described herein may be particularly applicable to the manufacture of microdevices, wherein the manufacturing process makes use of a low temperature bonding methodology, such as a metal alloy SLID bond. The microdevices may be, for example, MEMS devices formed on a semiconductor substrate. Alternatively, they may be integrated circuit devices formed on a semiconductor substrate.
The systems and methods disclosed here may apply a heating or cooling source locally and specifically, using the techniques described herein. The system and method are consistent with bonds that may be formed at low temperature, for example using metal alloy bonds as described in the '926 patent. These materials form a hermetic seal at temperatures less than about 250 degrees centigrade. Depending on the application, the heat applied may be sufficient for melting the adhesive material on the lid wafer, as well as activating the getter material on the lid wafer, while the device wafer is maintained at a substantially lower temperature. Accordingly, the devices supported on the device wafer are not exposed to these higher temperatures.
A unique feature about system 1000 is that the two wafers, lid wafer 520 and device wafer 720, are held at two substantially different temperatures. For example, lid wafer 520 may be approximately 100 F, or more, warmer or cooler than device wafer 720. In one embodiment, device wafer 720 is heated to about 180 F, in order to melt the indium layer of the Au/In bond as described in the '622 application. The lid wafer 520 is brought into contact with the device wafer 720, forming a hermetic AuIn2 alloy bond. The alloy has a much higher melting temperature, so that the material freezes upon formation, bonding the lid wafer 520 to the device wafer 720 with a hermetic seal. During this process, the device wafer stays cool relatively cool, under 200 F, so that the delicate structures on the device wafer 720 are not damaged or destroyed by the heat. As this entire process takes place within a sealed wafer bonding chamber, some additional and unique features may be added to the bonding chamber to accomplish this task.
A getter material which may be disposed on the lid wafer, may be heated to a higher temperature in order to activate the getter. For example, the lid wafer may support both the getter material and the high melting temperature component of the SLID bond, such as gold (Au). Thus in this case, the two wafers are once again held at substantially different temperatures.
Because there is a necessary gap between the lid wafer 520 and the device wafer 720 in this embodiment, care may be required in aligning the wafers properly before bonding. Self-aligning methods may be used, such as ball-in-socket techniques known to those of ordinary skill in the art.
Alternatively, the inert gas, helium for example, may be introduced directly into the wafer bonding chamber 1000 through a vent, where it circulates around both the lid wafer fixture 500 and the device wafer fixture 700. In this way, inert gas flowing over the device wafer 720 surface may remove heat from that surface, keeping the structures on the device wafer 720 cool relative to the lid wafer 520.
The systems and methods presented here which maintain the lid wafer at a substantially different temperature than the device wafer, may also be implemented using an inductive coupling approach. This approach is described with respect to heating a getter material to activate the getter material, in co-owned U.S. patent application Ser. No. 13/137,883, filed Sep. 20, 2011, and incorporated by reference in its entirety.
In the systems and methods described in the incorporated '883 application, an inductive heating approach is used to heat a getter material preferentially in order to activate the getter material. This application extends the idea to the heating of an adhesive bonding material disposed on the lid wafer, while keeping the device wafer relatively cool. The process may also include the heating of the getter material, as set forth in the '883 patent application.
The concept is illustrated in
A bonding adhesive 540 is deposited over the magnetically permeable material 530. The magnetic and bonding materials may be either be suspended over an empty cavity or deposited over an insulating layer (not shown), in order to promote a local rise in temperature in the vicinity of the magnetically permeable layer 530. These options are described in greater detail below. Then, using a method similar to that described in the '883 patent application, the permeable layer 530 and the bonding adhesive 540 are heated by inductive coupling to an RF coil 400.
A power supply 560 is used to generate an RF signal which is applied to a coil 400 as shown in
Because the bonding adhesive 540 is deposited over and is in direct contact with the magnetically permeable material 530 over much of its surface, the heat would flow by conduction specifically into the bonding material, heating it preferentially to the rest of the wafer and device structure, which would remain at a relatively low temperature. To increase the efficiency of this heat transfer, the magnetic material may be suspended over a cavity or void formed beneath it, reducing the heat leakage into the substrate thereby. This is described in greater detail below with respect to
While the system illustrated in
The coil 400 or 600 may also be wrapped around a core of permeable magnetic material which will also dramatically increase the magnetic flux produced. This core may be, but need not necessarily be, the same material as magnetically permeable material 5300. A core permeability of between about 10 and 20 T may be suitable. This core may be a composition including iron (Fe), nickel (Ni), cobalt (Co), neodymium (Nd), manganese (Mn) or their alloys. The coil may be brought into proximity to the magnetic layer, but need not be in contact or coupled to the wafer either mechanically or electrically. The coil may be conveniently brought to a distance of about 5 cm to the magnetic layer, or even closer. Alternatively, the coil 600 may be embedded in the wafer fixture which may include permeable material, as was illustrated in
As with the embodiment illustrated in
As shown in
A bonding material 5400 and optionally a getter material 5500 may then be deposited over the magnetic material 5300. The bonding material 5400 may be one component of a solid-liquid interdiffusion bond (SLID) bond, such as indium in a gold/indium SLID bond as described in the incorporated '926 patent. The metal layer 5400 may be, for example, 2 microns thick and deposited by sputter deposition over the permeable layer 5300. The other, higher melting temperature component of the SLID bond, for example, gold, may be formed in a layer 6000 on the other wafer.
The getter material 5500 is typically a reactive metal or metal alloy, such as, for example, an alloy of zirconium (Zr), vanadium (V), and iron (Fe) as that described in U.S. patent application Ser. No. 11/819,338, incorporated by reference in its entirety. The getter material 5500 may be deposited over the entire surface of the wafer, or it may be localized to certain areas by patterning. This patterning step may pattern the underlying magnetic layer at the same time. The getter material may be 0.2-3 microns thick and extend over about a 3-4 micron area.
As described previously, the bonding material 5400 and the getter material 5500 may be melted, cured, fired, or otherwise activated, by heating the bonding material 5400 and the getter material 5500 to a temperature at which the layer melts or its passivation layer is driven off. Typically, an indium layer will melt at about 200 F, but the getter material may require higher temperatures, in the range of at least three hundred degrees Centigrade. For the zirconium/vanadium alloy mentioned above, this temperature may be about 450 C. Using the method described here, this temperature may be achieved in the getter material 5500 and the indium layer 5400, while the rest of the structure and the device wafer remains relatively cool.
As with the embodiment illustrated in
Upon heating the bonding material 5400 to a sufficient temperature, the lid wafer 5000 may be brought into contact with the device wafer 3000. The bonding adhesive, for example indium 5400, may be pressed against the other component 6000, until the bond is formed. This bond may form a hermetic alloy seal around the device cavity 8000, so that the microfabricated device 4000 is enclosed in a controlled, or vacuum environment.
Using the inductive heating method disclosed herein, it may also be possible to fabricate the device in the device cavity with a two-step process. The first step is the bonding process, whereby the low temperature bonding material is heated to the melting point of the low melting temperature component, at which point the SLID alloy is formed, making a hermetic seal around the cavity. This alloy has a much higher melting temperature, so that the getter, now enclosed in the cavity, may be reheated to a higher temperature, in order to activate its surface. As before, this heat is largely confined to the getter material, so that the rest of the structures within the device cavity remain substantially cooler. This process allows the low temperature component to be protected from the higher activation temperatures, by incorporating it first into the alloy bond.
Since the device 4000 and getter 5500 are already enclosed in the evacuated device cavity, the getter may begin to functioning immediately, and no further processing is needed. The devices can then be singulated from the wafer if they have not yet been.
The device wafer 3000 or the lid wafer 5000 may have the low temperature bonding material 5400 formed substantially in a perimeter around the microdevice 4000. This bonding material 5400 may be combined with a raised feature 7000 as is described more fully in U.S. Pat. No. 7,569,926 and U.S. Pat. No. 7,960,208, incorporated by reference in their entireties, and assigned to the same assignee as the instant application. This low temperature bonding material may be referred to as a SLID bond described previously, a combination of a low melting temperature such as elemental indium (In) and a high melting temperature material such as elemental gold (Au). The raised feature 7000 may be deposited first on the device wafer, followed by conformal deposition of a gold layer, the raised feature produces a corresponding raised feature in the deposited gold layer. When assembling the wafers, the gold protrusion penetrates into the molten layer of the lower melting point metal, here the indium metal 5400, to produce a region which is rich in concentration of the gold. Adjacent to this region will be regions which are indium-rich/gold poor. Between these two regions will occur a region having nearly the exact desired relative concentration of the metals to form the preferred stoichiometry of the alloy.
Accordingly, the raised feature 7000 and other component of the bonding material 6000 may be placed on the device wafer 3000. The lid wafer 3000 and the device wafer 5000 may then be bonded together as described above. After bonding the lid wafer 5000 to the device wafer 3000 in the evacuated bonding chamber 100 described above, the wafer assembly may be removed from the bonding chamber. The getter material 5500, now encapsulated in the device cavity 8000 with the microdevice 4000, may be activated as described above and in the '883 patent application. The getter may be fired using this inductive procedure either before or after bonding the lid wafer to the device wafer. The process may be conducted on either individual devices after singulation, or on the entire wafer before singulation.
While various details have been described in conjunction with the exemplary implementations outlined above, various alternatives, modifications, variations, improvements, and/or substantial equivalents, whether known or that are or may be presently unforeseen, may become apparent upon reviewing the foregoing disclosure. Furthermore, details related to the specific methods are intended to be illustrative only, and the invention is not limited to such embodiments. It should be understood that the techniques disclosed herein may be applied to any microdevice, including integrated circuits, which may require a vacuum cavity with a getter enclosed therein, for proper functioning. The techniques may also be combined with other wafer bonding technologies, such as fusion bonding rather than metal alloy or glass frit bonding. Accordingly, the exemplary implementations set forth above, are intended to be illustrative, not limiting.
This application is related to U.S. patent application Ser. No. 13/137,883, filed Sep. 20, 2011, and incorporated by reference in its entirety.