This application is based upon and claims the benefit of priority from the prior Japanese Patent Application No. 2022-193000, filed on Dec. 1, 2022, the entire contents of which are incorporated herein by reference.
The present invention relates to a heater life prediction method, a heat treatment apparatus, and a computer-readable storage medium.
A resistive heater (hereinafter, also “heater”) constituted of carbon and the like, which is used in environments where hydrogen (H2) gas is primarily adopted as the atmosphere gas often deteriorates with progress of a chemical reaction between the heater and a reactive gas, and finally fractures. If a heater provided in a film forming apparatus that forms a film on the surface of a substrate unexpectedly fractures, various problems such as defective products or unforeseen addressing of apparatus restoration occur. This results in a great decrease in the productivity of the film forming apparatus. Therefore, establishment of a method that can prevent unexpected fracture of a heater is demanded.
In order to prevent unexpected fracture of a heater, techniques of predicting the life of a heater using the resistance value of the heater have been proposed in JPA2009-245978 and JPA2011-108596.
A heater life prediction method according to one aspect of the present invention includes predicting a life of a heater in a semiconductor manufacturing apparatus including a treatment chamber in which a treatment of a substrate is performed, and the heater configured to heat the substrate loaded into the treatment chamber, wherein prediction of the life of the heater includes: calculating a resistance change amount being a difference between a resistance value of the heater and an initial value of the resistance value, or a resistance change rate obtained by dividing the resistance change amount by the initial value in a step in which constant output control is executed on the heater between the treatments of different substrates; and predicting the life of the heater on a basis of the calculated resistance change amount or the calculated resistance change rate.
In the heater life prediction method described above, it is possible to configure that the life of the heater is predicted based on a relation between the resistance change amount or the resistance change rate and a preset threshold.
In the heater life prediction method described above, it is possible to further include notifying a user that the heater is close to an end of the life.
In the heater life prediction method described above, it is possible to configure that the step in which the constant output control is executed is at least one of a film forming step of forming a film on the substrate, a temperature decreasing step of decreasing a temperature of the substrate, and an unloading step of unloading the substrate from the treatment chamber.
A heat treatment apparatus according to another aspect of the present invention includes: a treatment chamber in which a treatment of a substrate is performed; a heater configured to heat the substrate loaded into the treatment chamber; and a life predictor configured to predict a life of the heater, wherein the life predictor calculates a resistance change amount being a difference between a resistance value of the heater and an initial value of the resistance value, or a resistance change rate obtained by dividing the resistance change amount by the initial value in a step in which constant output control is executed on the heater between the treatments of different substrates, and predicts the life of the heater on a basis of the calculated resistance change amount or the calculated resistance change rate.
In the heat treatment apparatus described above, it is possible to configure that the life predictor predicts the life of the heater on a basis of a relation between the calculated resistance change amount or the calculated resistance change rate and a preset threshold.
In the heat treatment apparatus described above, it is possible to configure that the life predictor notifies a user that the heater is close to an end of the life.
In the heat treatment apparatus described above, it is possible to configure that the step in which the constant output control is executed is at least one of a film forming step of forming a film on the substrate, a temperature decreasing step of decreasing a temperature of the substrate, and an unloading step of unloading the substrate from the treatment chamber.
A computer-readable storage medium according to still another aspect of the present invention has a heater life prediction program stored therein to cause a computer to perform a procedure for predicting a life of a heater in a heat treatment apparatus including a treatment chamber in which a treatment of a substrate is performed, and the heater configured to heat the substrate loaded into the treatment chamber, the procedure including: calculating a resistance change amount being a difference between a resistance value of the heater and an initial value of the resistance value, or a resistance change rate obtained by dividing the resistance change amount by the initial value in a step in which constant output control is executed on the heater between the treatments of different substrates; and predicting the life of the heater on a basis of the calculated resistance change amount or the calculated resistance change rate.
In the computer-readable storage medium described above, it is possible to configure that predicting the life of the heater is based on a relation between the calculated resistance change amount or the calculated resistance change rate and a preset threshold.
In the computer-readable storage medium described above, it is possible to configure that the heater life prediction program causes the computer to further perform a procedure for notifying a user that the heater is close to an end of the life.
In the computer-readable storage medium described above, it is possible to configure that the step in which the constant output control is executed is at least one of a film forming step of forming a film on the substrate, a temperature decreasing step of decreasing a temperature of the substrate, and an unloading step of unloading the substrate from the treatment chamber.
Embodiments of the present invention will be explained below with reference to the accompanying drawings. The embodiments do not limit the present invention.
The chamber 2 performs film formation, which is an example of a treatment to wafers W which is an example of a substrate. The chamber 2 is a single-wafer chamber where film formation is performed to wafers W one by one. The wafers W are, for example, compound semiconductor wafers containing a compound semiconductor such as SiC and GaN. The wafers W are not limited to compound semiconductor wafers and may be, 35 for example, silicon wafers containing single-crystal silicon. The chamber 2 has a shape (for example, a cylindrical shape) that can house a wafer W as a film formation target. The susceptor 5, the heater 7, a part of the rotator 6, and the like are housed in the chamber 2. A gate valve (not illustrated) controlled to open and close by the controller 12 is provided on the chamber 2. When the gate valve is opened, a transfer robot (not illustrated) can load and unload a wafer W with respect to the chamber 2.
The gas supplier 3 supplies a source gas to the wafer W in the chamber 2. The gas supplier 3 includes a plurality of gas reservoirs 3a that individually retain a plurality of gases, a plurality of gas pipes 3b that connect these gas reservoirs 3a to the source emitting portion 4, and a plurality of gas valves 3c that adjust the flow rates of the gases flowing through these gas pipes 3b. Each of the gas valves 3c is connected to an associated one of the gas pipes 3b. The gas valves 3c are controlled by the controller 12. Actual pipe arrangement may have other configurations in which a plurality of gas pipes are coupled, one gas pipe is branched into a plurality of gas pipes, branching and coupling of gas pipes are combined, and the like.
The source emitting portion 4 is positioned on the upper part of the chamber 2. The source gas supplied from the gas supplier 3 passes the source emitting portion 4 to be emitted into the chamber 2. The source gas (process gas) emitted into the chamber 2 is supplied to the surface of the wafer W, whereby a desired film is formed on the surface of the wafer W. The source gas to be used is not particularly limited to a particular type. The source gas can be variously changed according to the type of a film to be formed.
A shower plate 4a is provided on the bottom side of the source emitting portion 4. The shower plate 4a can be constituted of a metallic material such as stainless steel or an aluminum alloy. The gases from the gas pipes 3b are mixed in the source emitting portion 4 and pass through gas spouts 4b of the shower plate 4a to be supplied into the chamber 2. The source emitting portion 4 may be provided with a plurality of gas flow channels to separate the plural types of gases and supply the gases to the wafer W in the chamber 2 using nozzles or the like.
The structure of the source emitting portion 4 needs to be selected in view of in-plane uniformity of a formed film, consumption efficiency of the supplied source gas, reproducibility, manufacturing cost, and the like. However, the structure is not limited to a particular one and a known structure can be properly used as long as these requirements are met.
The susceptor 5 supports the wafer W in the chamber 2. The susceptor 5 is provided on the upper part of the rotator 6 that rotates while holding the susceptor 5. The susceptor 5 has a structure supporting the wafer W while placing the wafer W in a counterbore provided on an inner circumferential side of the susceptor 5. While the susceptor 5 has an annular shape having an opening at the center in the example illustrated in
The heater 7 heats the susceptor 5 and the wafer W. The heater 7 heats the wafer W loaded in the chamber 2. A resistive heater constituted of carbon and the like is used as the heater 7.
The heater driver 8 drives the heater 7 by supplying power to the heater 7. For example, the heater driver 8 supplies a power-supply voltage to the heater 7 to pass a current through the heater 7 and cause the heater 7 to generate heat. The specific mode of the heater driver 8 is not limited to a particular one as long as it can drive the heater 7. For example, the heater driver 8 may have a transformer, a primary circuit connected to the primary side of the transformer, and a secondary circuit connected to the secondary side of the transformer. The primary circuit may have a thyristor and, for example, a commercial power-supply voltage may be applied to the primary circuit. The transformer may perform voltage conversion between an AC voltage on the primary circuit side and an AC voltage on the secondary circuit side. The heater 7 may be connected to the secondary circuit. A voltmeter and an ammeter may be connected to the secondary circuit. The voltmeter may measure the voltage applied to the heater 7 and the ammeter may measure the current flowing through the heater 7. The measurement values of the voltmeter and the ammeter may be supplied to the controller 12.
The gas discharging portion 9 discharges the gas in the chamber 2. The ejection mechanism 10 ejects the gas from the gas discharging portion 9. The ejection mechanism 10 ejects the reacted source gas from the inside of the chamber 2 through the gas discharging portion 9 and controls the inside of the chamber 2 to a desired pressure using an ejection valve 10a and a vacuum pump 10b.
The radiation thermometer 11 measures the temperature of the wafer W. The radiation thermometer 11 is provided on the top surface of the source emitting portion 4. The radiation thermometer 11 exposes the wafer W to light from a light source (not illustrated) and receives reflected light from the wafer W to measure reflected light intensity of the wafer W. The radiation thermometer 11 receives heat radiation light from a film growth face of the wafer W and measures heat radiation light intensity. While only one radiation thermometer 11 is illustrated in
The top surface of the source emitting portion 4 is provided with a light-permeable window (not illustrated). The light from the light source of the radiation thermometer 11, and the reflected light and the heat radiation light from the wafer W pass through the light-permeable window. The light-permeable window can have any shape such as a slit shape, a rectangular shape, or a circular shape. A transparent member to a wavelength range of light to be measured by the radiation thermometer 11 is used as the light-permeable window. For example, in a case of measuring temperatures from the room temperature to about 1500° C., it is preferable to measure the wavelengths of light from the visible region to the near-infrared region. In this case, quartz or the like is preferably used as the member of the light-permeable window. The result of the measurement of the temperature of the wafer W by the radiation thermometer 11 is used by the controller 12 that functions as a temperature adjustor to control power supply to the heater 7 by means of the heater driver 8 on the basis of the temperature of the wafer W.
The controller 12 includes a computer (not illustrated) that concentrically controls the film forming apparatus 1, and a storage (not illustrated) that stores a process control program, an apparatus history, and the like. The controller 12 controls the gas supplier 3, a rotating mechanism of the rotator 6, the ejection mechanism 10, heating of the wafer W by the heater 7, and the like by executing the process control program stored in the storage. The controller 12 controls the heater 7 to have an output to maintain the temperatures measured by the radiation thermometer 11 at a desired temperature, or a constant output previously determined.
The controller 12 also predicts the life of the heater 7 and notifies a user that the heater 7 is close to the end of the life as required.
A method of predicting the life of the heater 7 is explained below.
The present inventors sequentially performed single-wafer treatments of a plurality of wafers W in a film forming apparatus having the same configuration as that illustrated in
In the loading step and the temperature increasing step, the temperature of the wafer W at the same time differs between the film formation treatment of a first wafer and the film formation treatments of second and subsequent wafers carried in a state in which the temperature in the chamber 2 is kept as illustrated in
Another possible factor of the variation in the resistance value of the heater is individual differences of wafers. For example, when there is a difference in warp of wafers, the carrier concentration of wafers, the in-plane distribution thereof, or the like, it is considered that there may be contact between the wafer and the susceptor or variation in the infrared absorption coefficient on the wafer, or both thereof and that this results in variation of the heater output in wafer temperature control by means of the temperature adjuster. Therefore, the resistance value of the heater 7 varies in the film forming step to which the temperature control of the wafer W is applied.
In the temperature decreasing step, the temperature of the wafer W shows the same behavior among the wafers W. However, since the temperature is decreased by turning off the heater 7, the apparent power of the heater 7 becomes zero [kVA] or a considerably small value, and the resistance value of the heater 7 cannot be calculated or the calculation accuracy is significantly low. In the unloading step, the output of the heater 7 is controlled to be constant, so that variation in the temperature of the heater 7 among the film formation treatments (among runs) of different wafers W is small and fluctuation of the resistance value of the heater 7 is also small. That is, it can be said that predicting the life of the heater 7 in the unloading step where the constant output control is executed is preferable.
As illustrated in
For example, in a case of a heater constituted of conductive thin films (for example, pyrolytic graphite and pyrolytic boron nitride) formed on the surface of a base material, the initial value of the resistance value easily changes by 10% or 20% depending on variation in the thicknesses of the thin films. Therefore, the resistance change amount changes 1.1 times or 1.2 times in some cases. In these cases, changes of the resistance value and the resistance increase amount differ according to examples as illustrated in
First, as illustrated in
After detecting start of the unloading step, the controller 12 calculates the resistance value of the heater 7 (Step S2).
After calculating the resistance value of the heater 7, the controller 12 calculates the resistance increase amount by calculating a difference between the calculated resistance value of the heater 7 and an initial value of the resistance value of the heater 7 calculated in advance (Step S3).
After calculating the resistance increase amount, the controller 12 calculates the resistance increase rate by dividing the resistance increase amount by the initial value of the resistance value of the heater 7 (Step S4). Processing at Steps S2 to S4 may be performed in one step.
After calculating the resistance increase rate, the controller 12 determines whether the resistance increase rate has exceeded a preset first threshold for the first time (Step S5). The first threshold is, for example, the threshold of the warning level described above.
When the resistance increase rate has exceeded the first threshold for the first time (Step S5: YES), the controller 12 predicts that the heater 7 is close to the end of the life and performs first notification processing to a user (Step S6). For example, the controller 12 performs the first notification processing using an alarm sound source or a display device (both not illustrated) connected to the controller 12. The first notification processing is, for example, causing the alarm sound source to ring and alerting by voice that the heater 7 is close to the fracture period, or displaying that the heater 7 is close to the fracture period on the display device to call for attention.
On the other hand, when the resistance increase rate is not above the first threshold (Step S5: NO “< the first threshold”), the controller 12 repeats calculation of the resistance value of the heater 7 after detecting start of the unloading step again (Steps S2 to S4).
After performing the first notification processing, the controller 12 determines, after detecting start of the next unloading step, whether the resistance increase rate has exceeded a preset second threshold as a case in which it is not the first time for the resistance increase rate to exceed the first threshold at Step S5 (Step 5: NO “> the first threshold is not the first time”) (Step S7). The second threshold is a threshold larger than the first threshold and is, for example, the threshold of the alarm level described above.
When the resistance increase rate exceeds the second threshold (Step S7: YES), the controller 12 predicts that the heater 7 is closer to the end of the life and performs second notification processing to the user (Step S8). The controller 12 performs the second notification processing using, for example, the alarm sound source or the display device (both not illustrated) connected to the controller 12. In the second notification processing, notifying that the heater 7 is closer to the end of the life by ringing or display in a manner enabling to inform that the heater 7 is closer to fracture is possible. In the second notification processing, it is possible to cause the heater driver 8 to stop power supply to the heater 7.
On the other hand, when the resistance increase rate is not above the second threshold (Step S7: NO), the controller 12 repeats the calculation of the resistance value of the heater 7 after detecting start of the unloading step again (Steps S2 to S4).
As described above, according to the present embodiment, the resistance increase rate is calculated in the unloading step in which the output control on the heater 7 is executed, and the life of the heater 7 can be predicted at a high accuracy on the basis of the calculated resistance increase rate while being hardly affected by dimension tolerance of the heater 7 and individual differences of the deterioration tendency. Accordingly, unexpected fracture of the heater 7 can be prevented and occurrence of defective products due to heater fracture and downtime caused by unforeseen addressing of apparatus restoration can be suppressed.
The present embodiment is not limited to the examples described above and are applicable to various modifications illustrated as below.
In a case in which the tendency to heater deterioration does not change, the life of the heater 7 may be predicted based on the resistance increase amount calculated in the unloading step. At that time, a plurality of thresholds may be set as thresholds for the resistance increase amount to notify the user similarly to the embodiment. The life of the heater 7 can be predicted highly accurately similarly to the embodiment.
Under certain conditions, the resistance calculation may be performed in a step other than the unloading step. For example, in a case in which there is a period when the heater output is controlled to be constant in the film forming step, the life of the heater 7 can be predicted based on the resistance increase rate or the resistance increase amount of the heater 7 calculated in the constant output control period in the film forming step. Also in this case, the life of the heater 7 can be predicted highly accurately similarly to the embodiment.
In a case in which the output of the heater 7 is controlled to be constant, for example, so as to stepwise decrease the heater output, without causing the heater output to be zero in the temperature decreasing step between the treatments of different wafers W, the life of the heater 7 can be predicted based on the resistance increase rate or the resistance increase amount of the heater 7 calculated in the temperature decreasing step. Also in this case, the life of the heater 7 can be predicted highly accurately similarly to the embodiment. Furthermore, by stepwise decreasing the output of the heater 7, the environments in the furnace can be gradually changed and load on the wafer W can be suppressed. Accordingly, deformation of the wafer W resulting from thermal stress due to temperature differences in the plane of the wafer W can be reduced. While certain embodiments have been described, these embodiments have been presented by way of example only, and are not intended to limit the scope of the inventions. Indeed, the embodiments may be embodied in a variety of other forms and various omissions, substitutions and changes may be made without departing from the spirit of the inventions. While a film forming device has been explained as the embodiment, any heat treatment apparatus including a resistive heater is applicable and such embodiments and modifications are included in the accompanying claims and their equivalents as would be included in the scope and the spirit of the inventions.
Number | Date | Country | Kind |
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2022-193000 | Dec 2022 | JP | national |