In situ wafer heat for reduced backside contamination

Information

  • Patent Grant
  • 6704913
  • Patent Number
    6,704,913
  • Date Filed
    Friday, November 8, 2002
    22 years ago
  • Date Issued
    Tuesday, March 9, 2004
    20 years ago
Abstract
A substrate processing system and a computer-readable storage medium for directing operation of a substrate processing system are provided for preparing a substrate for processing. The substrate processing system has a chamber with a substrate receiving portion and systems equipped to implement plasma processes. The computer-readable storage medium has a program that directs operation of the systems. The substrate is positioned within the chamber in a location not on the substrate receiving portion. A gaseous flow is provided to the chamber, from which a plasma is struck to heat the substrate. After the substrate has been heated, it is moved to the substrate receiving portion for processing.
Description




BACKGROUND OF THE INVENTION




The present invention relates to the manufacture of integrated circuits on a substrate. More particularly, the invention relates to a method and apparatus for reducing backside contamination of substrates during processing.




One of the primary steps in the fabrication of modern semiconductor devices is the formation of a thin layer on a semiconductor substrate by chemical reaction of gases. Such a deposition process is referred to generally as chemical-vapor deposition (“CVD”). Conventional thermal CVD processes supply reactive gases to the substrate surface where heat-induced chemical reactions take place to produce a desired layer. Plasma-enhanced CVD (“PECVD”) techniques, on the other hand, promote excitation and/or dissociation of the reactant gases by the application of radio-frequency (“RF”) energy to a reaction zone near the substrate surface, thereby creating a plasma. The high reactivity of the species in the plasma reduces the energy required for a chemical reaction to take place, and thus lowers the temperature required for such CVD processes as compared to conventional thermal CVD processes. These advantages are further exploited by high-density-plasma (“HDP”) CVD techniques, in which a dense plasma is formed at low vacuum pressures so that the plasma species are even more reactive. “High-density” is understood in this context to mean having an ion density that is equal to or exceeds 10


11


ions/cm


3


.




Because these processes are used in the precise manufacture of small-scale devices, it is especially desirable to limit the incidence of damage to the substrates during processing. Generally, silicon substrates used for processing are positioned onto a support, typically made of alumina, within a process chamber. The substrate is subject to expansion during processes that heat it with the plasma, which typically has a temperature of 400-800° C. While the heat of the plasma also causes the alumina support to expand, there may be a considerable difference in the degree of expansion of the silicon substrate when compared with the alumina support. This is because alumina has a lower coefficient of thermal expansivity than does silicon (or most other semiconductors) and because the alumina surface coating is actively cooled to at or near 65° C. The different expansions of the substrate and the support may result in scratching on the side of the substrate in contact with the support.




In some instances, the alumina support may be covered with a SiO


2


layer. The temperature changes resulting from the plasma heating may similarly cause damage to that layer, such that some SiO


2


flakes may adhere to the back side of the substrate. In further subsequent processing of the substrate, the flakes may fall off the substrate onto the front side of another substrate, thereby reducing overall device yield.




SUMMARY OF THE INVENTION




Embodiments of the invention are directed to a method for preparing a substrate that reduces the level of contamination of the back side of the substrate. The substrate is positioned within a chamber that has a substrate receiving portion, but in a location not on the substrate receiving portion. A gaseous flow is provided to the chamber, from which a plasma is struck to heat the substrate. After the substrate has been heated, it is moved to the substrate receiving portion for processing. In one embodiment, the plasma is a high-density plasma.




In certain embodiments, the substrate is positioned within the chamber by situating it on a plurality of lift pins, which may be electrically conductive. The substrate may then be moved to the substrate receiving portion when it is ready for processing by retracting the lift pins.




In some embodiments, the temperature of the substrate is monitored, with the substrate being moved to the substrate receiving portion when it reaches a predetermined temperature. This predetermined temperature may be the processing temperature at which the substrate is processed. The substrate temperature may be monitored by detecting infrared emission. In another embodiment, the substrate is moved to the substrate receiving portion after a predetermined time since striking the plasma has elapsed.




The methods of the present invention may be embodied in a computer-readable storage medium having a computer-readable program embodied therein for directing operation of a substrate processing system. Such a system may include a process chamber, a plasma generation system, a substrate holder, a gas delivery system, and a system controller. The computer-readable program includes instructions for operating the substrate processing system to form a thin film on a substrate disposed in the processing chamber in accordance with the embodiments described above.











A further understanding of the nature and advantages of the present invention may be realized by reference to the remaining portions of the specification and the drawings.




BRIEF DESCRIPTION OF THE DRAWINGS




In the figures, similar components and/or features may have the same reference label. Where reference is made in the detailed description to a figure without specifying a particular subpart, the reference is intended to refer collectively to all subparts of the figure.





FIG. 1A

is a simplified diagram of one embodiment of a high-density plasma chemical vapor deposition system according to the present invention.





FIG. 1B

is a simplified cross section of a gas ring that may be used in conjunction with the exemplary CVD processing chamber of FIG.


1


A.





FIG. 1C

is a simplified diagram of a monitor and light pen that may be used in conjunction with the exemplary CVD processing chamber of FIG.


1


A.





FIG. 1D

is a flow chart of an exemplary process control computer program product used to control the exemplary CVD processing chamber of

FIG. 1A

;




FIG.


2


(


a


) is a simplified diagram showing the position of a substrate and lift pins in a loading position;




FIG.


2


(


b


) is a simplified diagram showing the position of a substrate and lift pins in a pre-processing position;




FIG.


2


(


c


) is a simplified diagram showing the position of a substrate and lift pins in a processing position; and





FIG. 3

is a flow diagram illustrating steps in one embodiment of the invention.











DESCRIPTION OF THE SPECIFIC EMBODIMENTS




I. Introduction




Embodiments of the present invention are directed to a method and apparatus for reducing the incidence of substrate backside contamination. In particular, embodiments of the invention use a set of lift pins to keep the substrate above the substrate receiving portion while it is heated by the plasma. The lift pins are made of a material having an electric conductivity sufficient to mitigate any storing of charges from the plasma, but not so electrically conductive as to produce arcing from the plasma. The wafer may be cooled by radiation and a small amount of heat conduction through the conductive lift pins. In the case of higher chamber pressures, a small amount of convective and/or conductive heat transfer may also occur with the gases supporting the plasma.




II. Exemplary Substrate Processing System





FIG. 1A

illustrates one embodiment of a high density plasma chemical vapor deposition (HDP-CVD) system


10


in which a substrate can be processed according to the present invention. System


10


includes a chamber


13


, a vacuum system


70


, a source plasma system


80


A, a bias plasma system


80


B, a gas delivery system


33


, and a remote plasma cleaning system


50


.




The upper portion of chamber


13


includes a dome


14


, which is made of a ceramic dielectric material, such as aluminum oxide or aluminum nitride. Dome


14


defines an upper boundary of a plasma processing region


16


. Plasma processing region


16


is bounded on the bottom by the upper surface of a substrate


17


and a substrate support member


18


.




A heater plate


23


and a cold plate


24


surmount, and are thermally coupled to, dome


14


. Heater plate


23


and cold plate


24


allow control of the dome temperature to within about ±10° C. over a range of about 100° C. to 200° C. This allows optimizing the dome temperature for the various processes. For example, it may be desirable to maintain the dome at a higher temperature for cleaning or etching processes than for deposition processes. Accurate control of the dome temperature also reduces the flake or particle counts in the chamber and improves adhesion between the deposited layer and the substrate.




The lower portion of chamber


13


includes a body member


22


, which joins the chamber to the vacuum system. A base portion


21


of substrate support member


18


is mounted on, and forms a continuous inner surface with, body member


22


. Substrates are transferred into and out of chamber


13


by a robot blade (not shown) through an insertion/removal opening (not shown) in the side of chamber


13


. Lift pins (shown in

FIG. 2

) are raised and then lowered under the control of a motor (not shown) to move the substrate to different positions within the chamber


13


. The lift pins may be configured to move the substrate from the robot blade at an upper loading position


57


to a pre-processing position


58


where, as explained further below, the substrate is prepared for processing. Subsequently, the lift pins may move the substrate to a lower processing position


56


in which the substrate is placed on a substrate receiving portion


19


of substrate support member


18


. Substrate receiving portion


19


includes an electrostatic chuck


20


that secures the substrate to substrate support member


18


during substrate processing. In a preferred embodiment, substrate support member


18


is made from an aluminum oxide or aluminum ceramic material.




Vacuum system


70


includes throttle body


25


, which houses twin-blade throttle valve


26


and is attached to gate valve


27


and turbo-molecular pump


28


. It should be noted that throttle body


25


offers minimum obstruction to gas flow, and allows symmetric pumping. Gate valve


27


can isolate pump


28


from throttle body


25


, and can also control chamber pressure by restricting the exhaust flow capacity when throttle valve


26


is fully open. The arrangement of the throttle valve, gate valve, and turbo-molecular pump allow accurate and stable control of chamber pressures from between about 1 millitorr to about 2 torr.




The source plasma system


80


A includes a top coil


29


and side coil


30


, mounted on dome


14


. A symmetrical ground shield (not shown) reduces electrical coupling between the coils. Top coil


29


is powered by top source RF (SRF) generator


31


A, whereas side coil


30


is powered by side SRF generator


31


B, allowing independent power levels and frequencies of operation for each coil. This dual coil system allows control of the radial ion density in chamber


13


, thereby improving plasma uniformity. Side coil


30


and top coil


29


are typically inductively driven, which does not require a complimentary electrode. In a specific embodiment, the top source RF generator


31


A provides up to 5,000 watts of RF power at nominally 2 MHz and the side source RF generator


31


B provides up to 5,000 watts of RF power at nominally 2 MHz. The operating frequencies of the top and side RF generators may be offset from the nominal operating frequency (e.g. to 1.7-1.9 MHz and 1.9-2.1 MHz, respectively) to improve plasma-generation efficiency.




A bias plasma system


80


B includes a bias RF (“BRF”) generator


31


C and a bias matching network


32


C. The bias plasma system


80


B capacitively couples substrate portion


17


to body member


22


, which act as complimentary electrodes. The bias plasma system


80


B serves to enhance the transport of plasma species (e.g., ions) created by the source plasma system


80


A to the surface of the substrate. In a specific embodiment, bias RF generator provides up to 5,000 watts of RF power at 13.56 MHz.




RF generators


31


A and


31


B include digitally controlled synthesizers and operate over a frequency range between about 1.8 to about 2.1 MHz. Each generator includes an RF control circuit (not shown) that measures reflected power from the chamber and coil back to the generator and adjusts the frequency of operation to obtain the lowest reflected power, as understood by a person of ordinary skill in the art. RF generators are typically designed to operate into a load with a characteristic impedance of 50 ohms. RF power may be reflected from loads that have a different characteristic impedance than the generator. This can reduce power transferred to the load. Additionally, power reflected from the load back to the generator may overload and damage the generator. Because the impedance of a plasma may range from less than 5 ohms to over 900 ohms, depending on the plasma ion density, among other factors, and because reflected power may be a function of frequency, adjusting the generator frequency according to the reflected power increases the power transferred from the RF generator to the plasma and protects the generator. Another way to reduce reflected power and improve efficiency is with a matching network.




Matching networks


32


A and


32


B match the output impedance of generators


31


A and


31


B with their respective coils


29


and


30


. The RF control circuit may tune both matching networks by changing the value of capacitors within the matching networks to match the generator to the load as the load changes. The RF control circuit may tune a matching network when the power reflected from the load back to the generator exceeds a certain limit. One way to provide a constant match, and effectively disable the RF control circuit from tuning the matching network, is to set the reflected power limit above any expected value of reflected power. This may help stabilize a plasma under some conditions by holding the matching network constant at its most recent condition.




Other measures may also help stabilize a plasma. For example, the RF control circuit can be used to determine the power delivered to the load (plasma) and may increase or decrease the generator output power to keep the delivered power substantially constant during deposition of a layer.




A gas delivery system


33


provides gases from several sources,


34


A-


34


F chamber for processing the substrate via gas delivery lines


38


(only some of which are shown). As would be understood by a person of skill in the art, the actual sources used for sources


34


A-


34


F and the actual connection of delivery lines


38


to chamber


13


varies depending on the deposition and cleaning processes executed within chamber


13


. Gases are introduced into chamber


13


through a gas ring


37


and/or a top nozzle


45


.

FIG. 1B

is a simplified, partial cross-sectional view of chamber


13


showing additional details of gas ring


37


.




In one embodiment, first and second gas sources,


34


A and


34


B, and first and second gas flow controllers,


35


A′ and


35


B′, provide gas to ring plenum


36


in gas ring


37


via gas delivery lines


38


(only some of which are shown). Gas ring


37


has a plurality of source gas nozzles


39


(only one of which is shown for purposes of illustration) that provide a uniform flow of gas over the substrate. Nozzle length and nozzle angle may be changed to allow tailoring of the uniformity profile and gas utilization efficiency for a particular process within an individual chamber. In a preferred embodiment, gas ring


37


has


12


source gas nozzles made from an aluminum oxide ceramic.




Gas ring


37


also has a plurality of oxidizer gas nozzles


40


(only one of which is shown), which in a preferred embodiment are co-planar with and shorter than source gas nozzles


39


, and in one embodiment receive gas from body plenum


41


. In some embodiments it is desirable not to mix source gases and oxidizer gases before injecting the gases into chamber


13


. In other embodiments, oxidizer gas and source gas may be mixed prior to injecting the gases into chamber


13


by providing apertures (not shown) between body plenum


41


and gas ring plenum


36


. In one embodiment, third and fourth gas sources,


34


C and


34


D, and third and fourth gas flow controllers,


35


C and


35


D′, provide gas to body plenum via gas delivery lines


38


. Additional valves, such as


43


B (other valves not shown), may shut off gas from the flow controllers to the chamber.




In embodiments where flammable, toxic, or corrosive gases are used, it may be desirable to eliminate gas remaining in the gas delivery lines after a deposition. This may be accomplished using a 3-way valve, such as valve


43


B, to isolate chamber


13


from delivery line


38


A and to vent delivery line


38


A to vacuum foreline


44


, for example. As shown in

FIG. 1A

, other similar valves, such as


43


A and


43


C, may be incorporated on other gas delivery lines. Such 3-way valves may be placed as close to chamber


13


as practical, to minimize the volume of the unvented gas delivery line (between the 3-way valve and the chamber). Additionally, two-way (on-off) valves (not shown) may be placed between a mass flow controller (“MFC”) and the chamber or between a gas source and an MFC.




Referring again to

FIG. 1A

, chamber


13


also has top nozzle


45


and top vent


46


. Top nozzle


45


and top vent


46


allow independent control of top and side flows of the gases, which improves layer uniformity and allows fine adjustment of the layer's deposition and doping parameters. Top vent


46


is an annular opening around top nozzle


45


. In one embodiment, first gas source


34


A supplies source gas nozzles


39


and top nozzle


45


. Source nozzle MFC


35


A′ controls the amount of gas delivered to source gas nozzles


39


and top nozzle MFC


35


A controls the amount of gas delivered to top gas nozzle


45


. Similarly, two MFCs


35


B and


35


B′ may be used to control the flow of oxygen to both top vent


46


and oxidizer gas nozzles


40


from a single source of oxygen, such as source


34


B. The gases supplied to top nozzle


45


and top vent


46


may be kept separate prior to flowing the gases into chamber


13


, or the gases may be mixed in top plenum


48


before they flow into chamber


13


. Separate sources of the same gas may be used to supply various portions of the chamber.




A remote microwave-generated plasma cleaning system


50


is provided to periodically clean deposition residues from chamber components. The cleaning system includes a remote microwave generator


51


that creates a plasma from a cleaning gas source


34


E (e.g., molecular fluorine, nitrogen trifluoride, other fluorocarbons or equivalents) in reactor cavity


53


. The reactive species resulting from this plasma are conveyed to chamber


13


through cleaning gas feed port


54


via applicator tube


55


. The materials used to contain the cleaning plasma (e.g., cavity


53


and applicator tube


55


) must be resistant to attack by the plasma. The distance between reactor cavity


53


and feed port


54


should be kept as short as practical, since the concentration of desirable plasma species may decline with distance from reactor cavity


53


. Generating the cleaning plasma in a remote cavity allows the use of an efficient microwave generator and does not subject chamber components to the temperature, radiation, or bombardment of the glow discharge that may be present in a plasma formed in situ. Consequently, relatively sensitive components, such as electrostatic chuck


20


, do not need to be covered with a dummy wafer or otherwise protected, as may be required with an in situ plasma cleaning process. In one embodiment, this cleaning system is used to dissociate atoms of the etchant gas remotely, which are then supplied to the process chamber


13


. In another embodiment, the etchant gas is provided directly to the process chamber


13


. In still a further embodiment, multiple process chambers are used, with deposition and etching steps being performed in separate chambers.




System controller


60


controls the operation of system


10


. In a preferred embodiment, controller


60


includes a memory


62


, such as a hard disk drive, a floppy disk drive (not shown), and a card rack (not shown) coupled to a processor


61


. The card rack may contain a single-board computer (SBC) (not shown), analog and digital input/output boards (not shown), interface boards (not shown), and stepper motor controller boards (not shown). The system controller conforms to the Versa Modular European (“VME”) standard, which defines board, card cage, and connector dimensions and types. The VME standard also defines the bus structure as having a 16-bit data bus and 24-bit address bus. System controller


31


operates under the control of a computer program stored on the hard disk drive or through other computer programs, such as programs stored on a removable disk. The computer program dictates, for example, the timing, mixture of gases, RF power levels and other parameters of a particular process. The interface between a user and the system controller is via a monitor, such as a cathode ray tube (“CRT”)


65


, and a light pen


66


, as depicted in FIG.


1


C.





FIG. 1C

is an illustration of a portion of an exemplary system user interface used in conjunction with the exemplary CVD processing chamber of FIG.


1


A. System controller


60


includes a processor


61


coupled to a computer-readable memory


62


. Preferably, memory


62


may be a hard disk drive, but memory


62


may be other kinds of memory, such as ROM, PROM, and others.




System controller


60


operates under the control of a computer program


63


stored in a computer-readable format within memory


62


. The computer program dictates the timing, temperatures, gas flows, RF power levels and other parameters of a particular process. The interface between a user and the system controller is via a CRT monitor


65


and a light pen


66


, as depicted in FIG.


1


C. In a preferred embodiment, two monitors,


65


and


65


A, and two light pens,


66


and


66


A, are used, one mounted in the clean room wall (


65


) for the operators and the other behind the wall (


65


A) for the service technicians. Both monitors simultaneously display the same information, but only one light pen (e.g.


66


) is enabled. To select a particular screen or function, the operator touches an area of the display screen and pushes a button (not shown) on the pen. The touched area confirms being selected by the light pen by changing its color or displaying a new menu, for example.




The computer program code can be written in any conventional computer-readable programming language such as 68000 assembly language, C, C++, or Pascal. Suitable program code is entered into a single file, or multiple files, using a conventional text editor and is stored or embodied in a computer-usable medium, such as a memory system of the computer. If the entered code text is in a high level language, the code is compiled, and the resultant compiler code is then linked with an object code of precompiled windows library routines. To execute the linked compiled object code, the system user invokes the object code causing the computer system to load the code in memory. The CPU reads the code from memory and executes the code to perform the tasks identified in the program.





FIG. 1D

shows an illustrative block diagram of the hierarchical control structure of computer program


100


. A user enters a process set number and process chamber number into a process selector subroutine


110


in response to menus or screens displayed on the CRT monitor by using the light pen interface. The process sets are predetermined sets of process parameters necessary to carry out specified processes, and are identified by predefined set numbers. Process selector subroutine


110


identifies (i) the desired process chamber in a multichamber system, and (ii) the desired set of process parameters needed to operate the process chamber for performing the desired process. The process parameters for performing a specific process relate to conditions such as process gas composition and flow rates, temperature, pressure, plasma conditions such as RF power levels, and chamber dome temperature, and are provided to the user in the form of a recipe. The parameters specified by the recipe are entered utilizing the light pen/CRT monitor interface.




The signals for monitoring the process are provided by the analog and digital input boards of system controller


60


, and the signals for controlling the process are output on the analog and digital output boards of system controller


60


.




A process sequencer subroutine


120


comprises program code for accepting the identified process chamber and set of process parameters from the process selector subroutine


110


and for controlling operation of the various process chambers. Multiple users can enter process set numbers and process chamber numbers, or a single user can enter multiple process set numbers and process chamber numbers; sequencer subroutine


120


schedules the selected processes in the desired sequence. Preferably, sequencer subroutine


120


includes a program code to perform the steps of (i) monitoring the operation of the process chambers to determine if the chambers are being used, (ii) determining what processes are being carried out in the chambers being used, and (iii) executing the desired process based on availability of a process chamber and type of process to be carried out. Conventional methods of monitoring the process chambers can be used, such as polling. When scheduling which process is to be executed, sequencer subroutine


120


can be designed to take into consideration the “age” of each particular user-entered request, or the present condition of the process chamber being used in comparison with the desired process conditions for a selected process, or any other relevant factor a system programmer desires to include for determining scheduling priorities.




After sequencer subroutine


120


determines which process chamber and process set combination is going to be executed next, sequencer subroutine


120


initiates execution of the process set by passing the particular process set parameters to a chamber manager subroutine


130


A-C, which controls multiple processing tasks in chamber


13


and possibly other chambers (not shown) according to the process set sent by sequencer subroutine


120


.




Examples of chamber component subroutines are substrate positioning subroutine


140


, process gas control subroutine


150


, pressure control subroutine


160


, and plasma control subroutine


170


. Those having ordinary skill in the art will recognize that other chamber control subroutines can be included depending on what processes are selected to be performed in chamber


13


. In operation, chamber manager subroutine


130


A selectively schedules or calls the process component subroutines in accordance with the particular process set being executed. Chamber manager subroutine


130


A schedules process component subroutines in the same manner that sequencer subroutine


120


schedules the process chamber and process set to execute. Typically, chamber manager subroutine


130


A includes steps of monitoring the various chamber components, determining which components need to be operated based on the process parameters for the process set to be executed, and causing execution of a chamber component subroutine responsive to the monitoring and determining steps.




Operation of particular chamber component subroutines will now be described with reference to

FIGS. 1A and 1D

. Substrate positioning subroutine


140


comprises program code for controlling chamber components that are used to load a substrate onto substrate support number


18


. Substrate positioning subroutine


140


may also control transfer of a substrate into chamber


13


from, e.g., a plasma-enhanced CVD (“PECVD”) reactor or other reactor in the multi-chamber system, after other processing has been completed.




Process gas control subroutine


150


has program code for controlling process gas composition and flow rates. Subroutine


150


controls the open/close position of the safety shut-off valves and also ramps up/ramps down the mass flow controllers to obtain the desired gas flow rates. All chamber component subroutines, including process gas control subroutine


150


, are invoked by chamber manager subroutine


130


A. Subroutine


150


receives process parameters from chamber manager subroutine


130


A related to the desired gas flow rates.




Typically, process gas control subroutine


150


opens the gas supply lines, and repeatedly (i) reads the necessary mass flow controllers, (ii) compares the readings to the desired flow rates received from chamber manager subroutine


130


A, and (iii) adjusts the flow rates of the gas supply lines as necessary. Furthermore, process gas control subroutine


150


may include steps for monitoring the gas flow rates for unsafe rates and for activating the safety shut-off valves when an unsafe condition is detected.




In some processes, an inert gas, such as argon, is flowed into chamber


13


to stabilize the pressure in the chamber before reactive process gases are introduced. For these processes, the process gas control subroutine


150


is programmed to include steps for flowing the inert gas into chamber


13


for an amount of time necessary to stabilize the pressure in the chamber. The steps described above may then be carried out.




Additionally, when a process gas is to be vaporized from a liquid precursor, for example, tetraethylorthosilane (TEOS), the process gas control subroutine


150


may include steps for bubbling a delivery gas such as helium through the liquid precursor in a bubbler assembly or for introducing the helium to a liquid injection valve. For this type of process, the process gas control subroutine


150


regulates the flow of the delivery gas, the pressure in the bubbler, and the bubbler temperature to obtain the desired process gas flow rates. As discussed above, the desired process gas flow rates are transferred to process gas control subroutine


150


as process parameters.




Furthermore, the process gas control subroutine


150


includes steps for obtaining the necessary delivery gas flow rate, bubbler pressure, and bubbler temperature for the desired process gas flow rate by accessing a stored table containing the necessary values for a given process gas flow rate. Once the necessary values are obtained, the delivery gas flow rate, bubbler pressure and bubbler temperature are monitored, compared to the necessary values and adjusted accordingly.




The process gas control subroutine


150


may also control the flow of heat-transfer gas, such as helium (He), through the inner and outer passages in the wafer chuck with an independent helium control (IHC) subroutine (not shown). The gas flow thermally couples the substrate to the chuck. In a typical process, the wafer is heated by the plasma and the chemical reactions that form the layer, and the He cools the substrate through the chuck, which may be water-cooled. This keeps the substrate below a temperature that may damage preexisting features on the substrate.




Pressure control subroutine


160


includes program code for controlling the pressure in chamber


13


by regulating the size of the opening of throttle valve


26


in the exhaust portion of the chamber. There are at least two basic methods of controlling the chamber with the throttle valve. The first method relies on characterizing the chamber pressure as it relates to, among other things, the total process gas flow, the size of the process chamber, and the pumping capacity. The first method sets throttle valve


26


to a fixed position. Setting throttle valve


26


to a fixed position may eventually result in a steady-state pressure.




Alternatively, the chamber pressure may be measured, with a manometer for example, and the position of throttle valve


26


may be adjusted according to pressure control subroutine


360


, assuming the control point is within the boundaries set by gas flows and exhaust capacity. The former method may result in quicker chamber pressure changes, as the measurements, comparisons, and calculations associated with the latter method are not invoked. The former method may be desirable where precise control of the chamber pressure is not required, whereas the latter method may be desirable where an accurate, repeatable, and stable pressure is desired, such as during the deposition of a layer.




When pressure control subroutine


160


is invoked, the desired, or target, pressure level is received as a parameter from chamber manager subroutine


130


A. Pressure control subroutine


160


measures the pressure in chamber


13


by reading one or more conventional pressure manometers connected to the chamber; compares the measured value(s) to the target pressure; obtains proportional, integral, and differential (PID) values from a stored pressure table corresponding to the target pressure, and adjusts throttle valve


26


according to the PID values obtained from the pressure table. Alternatively, pressure control subroutine


160


may open or close throttle valve


26


to a particular opening size to regulate the pressure in chamber


13


to a desired pressure or pressure range.




Plasma control subroutine


170


comprises program code for controlling the frequency and power output setting of RF generators


31


A and


31


B and for tuning matching networks


32


A and


32


B. Plasma control subroutine


370


, like the previously described chamber component subroutines, is invoked by chamber manager subroutine


330


A.




An example of a system that may incorporate some or all of the subsystems and routines described above would be the ULTIMA™ system, manufactured by APPLIED MATERIALS, INC., of Santa Clara, Calif., configured to practice the present invention. Further details of such a system are disclosed in the commonly assigned U.S. patent application Ser. No. 08/679,927, filed Jul. 15, 1996, entitled “Symmetric Tunable Inductively-Coupled HDP-CVD Reactor,” having Fred C. Redeker, Farhad Moghadam, Hirogi Hanawa, Tetsuya Ishikawa, Dan Maydan, Shijian Li, Brian Lue, Robert Steger, Yaxin Wang, Manus Wong and Ashok Sinha listed as co-inventors, the disclosure of which is incorporated herein by reference. The described system is for exemplary purpose only. It would be a matter of routine skill for a person of skill in the art to select an appropriate conventional substrate processing system and computer control system to implement the present invention.




III. Substrate Preparation




Preparation of the substrate before processing is used to reduce the possibility of contamination and damage to the back side of the substrate. In particular, embodiments of the invention heat the substrate from room temperature approximately to the process temperature, within the process chamber, before the substrate is brought in contact with the substrate receiving portion


19


. With the wafer temperature near the process temperature, any expansion of the substrate has already occurred so the possibility of inconsistent expansion between the substrate and the substrate receiving portion is essentially removed. The result is that damage to and/or contamination of the back side of the substrate is substantially reduced during processing. One means of heating the substrate to the desired temperature before bringing it in contact with the substrate receiving portion is to support it with lift pins that can be recessed into the substrate receiving portion.




An example illustrating the operation of such lift pins is shown in

FIG. 2

, where the various components are not shown to scale. As configured in the example, the lift pins


92


are adapted to position the substrate


90


in one of three positions relative to the substrate receiving portion. The lift pins


92


may reside within chambers


93


and be driven with a motor (not shown) such that the three positions are achieved by moving the lift pins


92


out from or into the substrate receiving portion a specific distance. In a first position, shown in FIG.


2


(


a


), the lift pins


92


are positioned such that the substrate


90


can be received from the robot blade at the upper loading position


57


. The upper loading position


57


is determined so as to be convenient for receiving the substrate


90


from the robot blade. In a second position, the pre-processing position


58


shown in FIG.


2


(


b


), the lift pins


92


are further recessed into the substrate receiving portion


19


and positioned so that the substrate


90


is not in contact with the substrate receiving portion


19


. In a third position, shown in FIG.


2


(


c


) as the processing position


56


, the substrate


90


is in contact with the substrate receiving portion


19


, where it may be electrostatically chucked into a secure position for processing.




Certain aspects of the invention may be understood more fully with reference to

FIG. 3

, which is a flow diagram depicting a particular embodiment. At step


204


, the substrate


90


is received within the chamber


13


at the upper loading position


57


, resting on the lift pins


92


. The substrate


90


is then moved to the pre-processing position


58


at step


208


by lowering the lift pins. For a circular 200 or 300 mm substrate in the pre-processing position


58


, the substrate


90


may be approximately 50-150 mil above the substrate receiving portion


19


. If higher than about 150 mil, the substrate


90


may acquire a charge from the plasma before deposition gases are introduced into the chamber


13


. The lower limit is dictated primarily by the range of electrostatic forces from the electrostatic chuck. There is no a priori limitation on how close the substrate


90


may be to the substrate receiving portion


19


provided there is no contact between them, with the substrate remaining unchucked.




Once the substrate


90


is properly positioned, initial gases are flowed into the process chamber at step


208


. Such initial gases may include, for example, an inert gas such as argor from which a plasma may be struck at step


212


. The plasma may be a high-density plasma, which is understood in this context to mean having an ion density that is equal to or exceeds 10


11


ions/cm


3


. The substrate


90


is heated by the plasma, and the temperature of the substrate


90


is monitored at step


216


. A small amount of heat may radiate away from the substrate


90


and some may be conducted through the lift pins


92


. In the case of higher chamber pressures, there may additionally be a small amount of convective or conductive heat transfer with the gases supporting the plasma. There are various methods for monitoring the substrate temperature, and the invention is not limited by a particular method. For example, the substrate receiving portion


19


may be configured with an infrared sensor. With the substrate


90


sufficiently close to the infrared sensor, the temperature may be measured from infrared emissions from the substrate


90


, perhaps with reference to previously derived correlations established for certain separations between the substrate and the infrared sensor. In an alternative embodiment, a fixed time period is used to allow the substrate


90


to reach the desired temperature. That time may be optimized, for example, by examining process output parameters or by examining the incidence of backside contamination on the substrate after it has been processed. Such incidence is minimized when the substrate is heated by the plasma for the optimal time.




There are several considerations useful in determining the specific structure of the lift pins


92


. In one embodiment, they are configured to be electrically conductive. This has the effect of grounding the outer surface of the substrate


90


, thereby suppressing the accumulation of charge on the substrate


90


while it is in direct contact with the plasma. The conductivity of the lift pins


92


is preferably within a range sufficient to prevent charge accumulation but not so large that there is a danger of arcing with the plasma. If the electrical conductivity is too low, the lift pins may be too resistive to ground the substrate


90


sufficiently, while conductivity that is too high increases the possibility of indesireable arcing.




A further consideration involves balancing the desire to minimize the contact area with the substrate


90


while also providing adequate support to the substrate


90


. This may be accomplished by varying several parameters, including the cross-sectional area of the lift pins


92


as well the number of lift pins


92


. To minimize contact area, the lift pins


92


may be beveled where they contact the substrate in some embodiments. In one embodiment, four lift pins are used in a square configuration to support a circular substrate. In one embodiment suitable for processing a circular substrate having a nominal diameter of 300 mm, each of the lift pins has a circular cross section with a diameter less that 1 cm. The material used to fabricate the lift pins


92


should be chosen so that it will not be damaged by the plasma nor will contaminate the plasma. Appropriate materials include alumina or SiC. Once it is determined at step


220


that the substrate temperature has reached the desired level, i.e. approximately at the process temperature to be used subsequently, the substrate


90


is moved to the processing position


56


at step


224


.




When in the processing position


56


, the substrate


90


is in contact with the substrate receiving portion


19


, where it may be secured by electrostatic chucking. The process gases are then flowed into the chamber


13


at step


228


to perform the desired processing, such as deposition or etching, on the substrate


90


at step


229


. Once the substrate has been processed, the flow of process gases is stopped at step


230


without terminating the plasma. The substrate is subsequently returned to the pre-processing position at step


231


so that it remains in contact with the plasma in order to allow charges to expel. At step


232


, the plasma is terminated and the substrate is then moved back to the loading position at step


236


by decoupling the electrostatic chuck


20


and moving the lift pins


92


. At this point, the processed substrate can be removed from the chamber


13


. The time interval between steps


232


and


236


should be short so that there is insufficient time for the processed substrate and the substrate receiving portion


19


to contract at different rates.




This process may be clarified with a specific example in which embodiments of the invention are used for deposition of a layer on a substrate


90


. In such an embodiment, a flow of substantially inert gas is provided into the chamber


13


, from which a plasma is formed. The substrate


90


is maintained in the preprocessing position


58


while it is heated by the plasma. Once heated, the substrate


90


is moved to the substrate receiving portion


19


. Deposition gases for forming the layer on the substrate


90


are flowed into the chamber


13


only after the substrate has been moved to the substrate receiving portion


19


. A similar procedure may be used for embodiments used to etch a substrate


90


, with additional gases being provided to the chamber


13


for etching only after the substrate has been heated by the plasma and moved to the substrate receiving portion


19


. As used herein, “substantially inert gas” refers to a gas or combination of gases that does not result in appreciable processing of the substrate


90


, i.e. does not result in appreciable deposition for a deposition process or does not result in appreciable etching for an etch process.




In one alternative embodiment, instead of having a single set of lift pins configured to move the substrate to at least three different positions, a plurality of sets of lift pins may be provided, each having only two positions. Thus, one set of lift pins may be used to move the substrate between the upper loading position and the substrate receiving portion while another may be used to move the substrate between the pre-processing position and the substrate receiving portion. Other configurations may also be used.




Having described several embodiments, it will be recognized by those of skill in the art that various modifications, alternative constructions, and equivalents may be used without departing from the spirit of the invention. In particular, while embodiments have been described in detail for high-density plasma system, ,those of skill in the art will recognize the general applicability of the invention to any substrate processing system that uses a plasma to heat the substrate. Accordingly, the above description should not be taken as limiting the scope of the invention, which is defined in the following claims.



Claims
  • 1. A computer-readable storage medium having a computer-readable program embodied therein for directing operation of a substrate processing system including a chamber having a substrate receiving portion; a plasma generation system; and a gas delivery system configured to introduce gases into the chamber, the computer-readable program including instructions for operating the substrate processing system to process a substrate disposed in the chamber in accordance with the following:receiving the substrate within the chamber not on the substrate receiving portion; providing a gaseous flow to the chamber; striking a plasma from the gaseous flow to heat the substrate; and moving the substrate to the substrate receiving portion for processing after the substrate has been heated by the plasma.
  • 2. The computer-readable storage medium recited in claim 1 wherein the substrate receiving portion includes a plurality of retractable lift pins, wherein receiving the substrate within the chamber comprises receiving the substrate on the lift pins, and wherein moving the substrate to the substrate receiving portion comprises retracting the lift pins within the substrate receiving portion.
  • 3. The computer-readable storage medium recited in claim 1 wherein the substrate processing system further includes an infrared sensor, and wherein the computer-readable program further includes instructions for operating the infrared sensor to monitor a temperature of the substrate and to perform the step of moving the substrate to the substrate receiving portion when the substrate has reached a predetermined temperature.
  • 4. A substrate processing system comprising:a housing defining a chamber; a plasma generating system operatively coupled to the chamber; a substrate receiving portion within the chamber configured to hold a substrate during substrate processing; a gas-delivery system configured to introduce gases into the chamber; a pressure-control system for maintaining a selected pressure within the chamber; a controller for controlling the plasma generating system, the gas-delivery system, and the pressure-control system; and a memory coupled to the controller, the memory comprising a computer-readable medium having a computer-readable program embodied therein for directing operation of the substrate processing system, the computer-readable program including instructions to receive the substrate within the chamber not on the substrate receiving portion; instructions to provide a gaseous flow to the chamber; instructions to strike a plasma from the gaseous flow to heat the substrate; and instructions to move the substrate to the substrate receiving portion for processing after the substrate has been heated by the plasma.
  • 5. The substrate processing system recited in claim 4 wherein the substrate receiving portion includes a plurality of retractable lift pins, wherein the instructions to receive the substrate within the chamber include instructions to receive the substrate on the lift pins, and wherein the instructions to move the substrate to the substrate receiving portion include instructions to retract the lift pins within the substrate receiving portion.
  • 6. The substrate processing system recited in claim 4, further comprising an infrared sensor, wherein the computer-readable program further includes instructions for operating the infrared sensor to monitor a temperature of the substrate, and wherein the instructions to move the substrate to the substrate receiving portion are executed when the substrate has reached a predetermined temperature.
  • 7. The computer-readable storage medium recited in claim 2 wherein the retractable lift pins are electrically conductive.
  • 8. The computer-readable storage medium recited in claim 2 wherein the lift pins are composed of alumina.
  • 9. The computer-readable storage medium recited in claim 2 wherein the lift pins are composed of AlN.
  • 10. The computer-readable storage medium recited in claim 2 wherein the lift pins are composed of SiC.
  • 11. The computer-readable storage medium recited in claim 1 wherein the plasma is a high-density plasma.
  • 12. The computer-readable storage medium recited in claim 1 wherein moving the substrate to the substrate receiving portion is performed a predetermined time after striking the plasma.
  • 13. The substrate processing system recited in claim 5 wherein the retractable lift pins are electrically conductive.
  • 14. The substrate processing system recited in claim 5 wherein the retractable lift pins are composed of AlN.
  • 15. The substrate processing system recited in claim 5 wherein the retractable lift pins are composed of SiC.
  • 16. The substrate processing system recited in claim 4 wherein the plasma is a high-density plasma.
  • 17. The substrate processing system recited in claim 4 wherein the instructions to move the substrate to the substrate receiving portion are executed a predetermined time after striking the plasma.
Parent Case Info

This application is a Divisional application of U.S. Ser. No. 09/771,085 filed on Jan. 26, 2001 now U.S. Pat. No. 6,514,870.

US Referenced Citations (17)
Number Name Date Kind
4269137 Johnson May 1981 A
5227337 Kadomura Jul 1993 A
5494854 Jain Feb 1996 A
5693238 Schmitt et al. Dec 1997 A
5782974 Sorensen et al. Jul 1998 A
5804259 Robles Sep 1998 A
5937323 Orczyk et al. Aug 1999 A
5968610 Liu et al. Oct 1999 A
6056825 Sumnitsch May 2000 A
6083567 Vesnovsky et al. Jul 2000 A
6130397 Arai Oct 2000 A
6162709 Raoux et al. Dec 2000 A
6183565 Granneman et al. Feb 2001 B1
6221781 Siefering et al. Apr 2001 B1
6316367 Sumnitsch Nov 2001 B1
6559026 Rossman et al. May 2003 B1
20010003064 Ohio Jun 2001 A1
Foreign Referenced Citations (4)
Number Date Country
1 041 171 Apr 2000 EP
62185877 Aug 1987 JP
10135186 May 1998 JP
WO 9633098 Oct 1996 WO
Non-Patent Literature Citations (2)
Entry
Weigand et al., “High Density Plasma CVD oxide deposition: the effect of sputtering on the film properties,” VMIC Conference, Jun. 18-20, 1996; 1996 ISMIC—106/96/0075©, pp. 75-80.
Wei et al., “Characterization of High Density Plasma CVD USG Film,” SPIE vol. 3214, pp. 94-103.