The present disclosure relates to a micro-electro-mechanical device for transducing acoustic waves in a propagation medium and to the manufacturing process thereof. In particular, the disclosure refers to a PMUT (“Piezoelectric Micromachined Ultrasonic Transducer”) ultrasonic transducer for high intensity focused ultrasound (HIFU) applications.
As known, ultrasonic transducers are devices capable of emitting and receiving acoustic waves (in particular, ultrasounds at a frequency comprised between 20 kHz and 100 MHz) in fluid (liquid or gaseous) and/or solid propagation media, by converting electro-mechanical, acoustic or light energy.
In particular, MUT (“Micromachined Ultrasonic Transducers”) semiconductor ultrasonic transducers are known that are manufactured using silicon bulk micromachining and/or surface micromachining processes. The MUT transducers comprise membranes capable of vibrating in both acoustic waves transmission condition and acoustic waves reception condition; currently, the membrane vibrational operation is based on piezoelectric effects (piezoelectric MUTs, PMUTs) or electrostatic effects (capacitive MUTs, CMUTs).
The efficiency of the emitted/received energy electroacoustic conversion, the frequency response gain and the bandwidth are identification parameters of the MUTs. They depend both on factors typical of the MUTs (such as geometric structure and materials of the transducers, which determine a mechanical impedance of the MUT) and on factors typical of the acoustic wave propagation media (such as density of the propagation media and speed of conveyed sound, which determine an acoustic impedance thereof).
Different air ultrasonic applications are known, such as distance measure and object and environment imaging, based on the detection of the pulse echo, i.e., on the transmission of acoustic waves (e.g., of an ultrasonic pulse) and on the reception of ultrasonic echoes generated by the reflection and diffusion of the acoustic waves in the environment. The spatial distribution and harmonic content of ultrasonic echoes are caused by density variations in the propagation medium, and are indicative of objects and/or inhomogeneities present therein.
In this application, the usable frequencies also depend on the dimensions of the objects or on their characteristics; in particular, for the detection of objects having very small dimensions (e.g., up to 30 μm), very high-frequency acoustic waves are to be used, e.g., of the order of MHz.
Another example of air ultrasonic application is ultrasonic communication, which involves transmitting and receiving a modulated signal through an acoustic channel. In this application, the bandwidth directly affects the measurement resolution (pulse echo detection) or data transmission/reception (ultrasonic communication).
Another possible ultrasonic application is the minimally invasive treatment of patient tissues, where focused ultrasonic waves are used for the ablation of tissues, which are destroyed due to high heat. In this case, high-power ultrasonic waves are focused towards a target point, so as to obtain a rise in temperature up to 70-80° C.
Starting therefrom, it is desirable to manufacture piezoelectric micromachined ultrasonic devices that may work both in air and in aqueous environment, with high detection accuracy, even at much greater distances than the wavelengths used, in various fields of application, in a flexible manner.
The present disclosure provides a piezoelectric micromachined ultrasonic device that meets the indicated requirements.
According to the present disclosure, a PMUT ultrasonic transducer and the manufacturing process thereof are provided, as defined in the attached claims.
For example, in at least one embodiment, a PMUT acoustic transducer may include: a body of semiconductor material having a face; a plurality of first buried cavities, having an annular shape, arranged concentrically to each other and extending at a distance from the face of the body; a plurality of first membranes formed by the body, each first membrane extending between a respective first buried cavity of the plurality of first buried cavities and the face of the body; a plurality of piezoelectric elements on the face of the body, each piezoelectric element extending above a respective first membrane of the plurality of first membranes; wherein the first membranes have different widths.
For a better understanding of the present disclosure, some embodiments thereof are now described, purely by way of non-limiting example, with reference to the attached drawings, wherein:
In the article “Phased Array Focusing for Acoustic Wireless Power Transfer” by Victor Far-Guoo Tsemg, Sarah S. Bedair IEEE TRANSACTIONS ON ULTRASONIC FERROELECTRICS, AND FREQUENCY CONTROL, VOL. 65, NO. 1, January 2018 it is emphasized that wireless power transfer (WPT) through acoustic waves may achieve higher efficiencies than inductive coupling when the distance exceeds the dimension of the transducer by several times. This document teaches that arrays of ultrasonic phased elements have high power concentration on the receivers and allow the efficiency of power transfer to be increased.
The article “CONCENTRIC PMUT ARRAYS FOR FOCUSED ULTRASOUND AND HIGH INTENSITY APPLICATIONS” by Benjamin E. Eovino, Yue Liang and Liwei Lin, MEMS 2019, Seoul, Korea, 27-31 Jan. 2019, 978-1-7181-1610-5/19, IEEE, describes a PMUT device formed by an array of piezoelectric micromachined ultrasonic transducers (PMUTs) having the shape of concentric rings and demonstrates how this configuration allows manufacturing of miniaturized devices capable of generating very high acoustic and high focused intensities.
The following description refers to the arrangement shown; consequently, expressions such as “above,” “below,” “top,” “bottom,” “right,” “left” relate to the attached figures and are not to be intended in a limiting manner.
The present disclosure originates from inventors' research performed on PMUT ultrasonic transducers with concentric ring structure.
To this end, reference is made to
The body 2 has a face 2A having a piezoelectric element 3, of annular-shape, deposited thereon, and accommodates a cavity 4, also of annular-shape and underlying the piezoelectric element 3.
The cavity 4 has an internal diameter D_int and a width w_c; the piezoelectric element 3 has a width w_r, smaller than the width w_c of the cavity 3.
In practice, the body 2 defines a membrane 5 overlying the cavity 4 and carrying the piezoelectric element 3.
In the inventors' studies, it has been noted that the resonance frequency of the test structure 1 of
These data are shown in
In particular,
The inventors' studies have also highlighted that the acoustic pressure measured on the surface (in proximity to the face 2A of the body 2) significantly depends on the width w_c of the cavity 4 and, to a lesser extent, on the internal diameter D_int.
Taking into account the above, the present disclosure includes an acoustic transducer capable of emitting and detecting multi-frequency acoustic waves, as discussed hereinbelow with reference to
In detail, the acoustic transducer 10 comprises a body 11 of semiconductor material, such as silicon, for example with a monocrystalline structure, having a face 12A.
The body 11 accommodates a plurality of concentric buried cavities 12A-12H; of these, the concentric buried cavity 12A arranged in a central position (hereinafter also referred to as central buried cavity 12A) has a circular shape and the other concentric buried cavities 12B-12H have an annular shape.
The concentric buried cavities 12A-12H (generically referred to as the concentric buried cavities 12 when it is not desired to distinguish them) have widths w1-w8 increasing in the radial direction, here from the central buried cavity 12A, where w1 represents the radius of the central buried cavity 12A. The concentric buried cavities 12B-12H, which may be referred to as peripheral cavities, are spaced outward in the radial direction from the central buried cavity 12A, which may be referred to as a central cavity.
According to an embodiment, the widths w1-w8 of the concentric buried cavities 12A-12H are chosen so that they have a linearly decreasing resonance frequency (see
For example, w1=106 μm; w2=159 μm; w3=162 μm; w4=166 μm; w5=171 μm; w6=176 μm; w7=181 μm and w8=187 μm.
In general terms, the widths wi (e.g., w1, w2, w3, w4, w5, w6, w7, w8, etc.) of the first cavities may vary between a minimum value of 20 μm and a maximum value of 500 μm.
The concentric buried cavities 12 are mutually spaced in a uniform manner, for example by 2-20 μm.
The concentric buried cavities 12 also have a depth, e.g., of 2-20 μm, in particular of 4 μm.
The concentric buried cavities 12 are coplanar with each other and extend at a short distance from the face 11A of the body 11. For example, the distance d1 between the top side of the concentric buried cavities 12 and the face 11A of the body 11 (
The concentric buried cavities 12A-12H delimit from below, inside the body 11, respective thin membranes 13A-13H; therefore each thin membrane 13A-13H extends between a respective concentric buried cavity 12A-12H and the face 11A of the body 11.
A plurality of piezoelectric elements 15A-15H extends on the face 11A of the body 11. The piezoelectric elements 15A-15H (generically referred to as the piezoelectric elements 15 when it is not desired to distinguish them) each extend on a respective thin membrane 13A-13H (see in particular the enlarged detail of
The piezoelectric elements 15A-15H have a circular/annular shape similar to that of the respective concentric buried cavities 12A-12H and therefore comprise, in the embodiment shown, a piezoelectric element 15A, of circular shape and central position, also referred to as the central piezoelectric element 15A, and a plurality of piezoelectric elements 15B-15H, of annular shape and arranged concentrically with each other and with the central piezoelectric element 15A.
In practice, each piezoelectric element 15A-15H forms, with the respective concentric buried cavity 12A-12G, a transducer unit, indicated by 40A-40H.
As visible in particular in
A passivation layer 21 may cover, upwardly and laterally, the layer stacks 17-19. For example, as shown in
The piezoelectric layer 18 may be formed, for example, by PZT (Pb, Zr, TiO3) or by other piezoelectric material, i.e., capable of transforming electrical energy into vibrational mechanical energy or vice versa.
The insulating layer 20 may be of TEOS (tetraethylorthosilicate); the bottom electrode 17 is of electrically conductive material, e.g., of titanium (Ti) or platinum (Pt); the top electrode is of electrically conductive material, e.g., of TiW; the protection layers 21A and 21B are of insulating material. For example, the first protection layer 21A may be of silicon oxide and the second protection layer 21B may be of silicon nitride deposited by CVD (Chemical Vapor Deposition).
A deep buried cavity 25 extends below some of the concentric buried cavities 12 and, precisely, of the concentric buried cavities 12 having smaller width, for the reasons explained hereinbelow. In the embodiment shown, the deep buried cavity 25 extends below the central buried cavity 12A and the two concentric buried cavities 12B, 12C adjacent thereto.
In the embodiment shown, therefore, the deep buried cavity 25 is centrally arranged and has a circular shape; for example, it may have a radius R of 550 μm (diameter of 1100 μm).
In general, the second buried cavity 25 has a diameter comprised between 500 μm and 1500 μm and a depth comprised between 100 μm and 200 μm.
Furthermore, the top surface of the deep buried cavity 25 extends at a distance d2 from the face 11A of the body 11 which is comprised between 10 μm and 200 μm, for example of 140 μm.
The deep buried cavity 25 has a depth, e.g., of 2-20 μm, in particular of 4 μm, and delimits on the bottom a thick membrane 35 having a thickness d2, in the example considered, of 140 μm.
As shown in
The conductive tracks 23, 24 may be separated, for example as shown in
In particular, in the first part of the conductive tracks 23, 24, near the electrodes 17, 19, the conductive tracks 23, 24 of the piezoelectric elements 15A-15C (as well as of the piezoelectric elements 15D-15G, not visible) extend through interruptions in the piezoelectric elements 15 that are respectively more external.
Alternatively,
In both cases, the conductive tracks 23, 24 are connected to electronics 30 (
The electronics 30 comprises, in a known manner and not shown, a power supply unit, configured to generate the biasing voltages, and a control unit, configured to control the transduction steps (acoustic wave emission and/or acoustic wave detection).
The electronics 30 may be integrated into the body 11 together with the acoustic transducer 10 or may be integrated in a separate die and coupled to the conductive tracks 23, 24 through pads, as shown schematically in
In use, in a known manner, the application of a variable voltage, for example an alternating voltage, to the piezoelectric elements 15A-15B, causes generation of a strain and vibration of the respective thin membranes 13A-13H and emission of acoustics waves in the medium where the acoustic transducer 10 is located (acoustic wave generator operating mode).
Conversely, in the rest condition of the thin membranes 13A-13H (in presence of a DC bias or in absence of applied voltage, depending on the material of the piezoelectric layer 18), an acoustic wave hitting the thin membranes 13A-13H causes vibration of the latter and therefore the onset of a variable stress in the relative piezoelectric elements 15A-15H; these elements therefore generate corresponding electrical signals usable by the electronics 30 for detecting the parameters of the received acoustic wave (acoustic wave receiver operating mode).
The acoustic transducer 10, due to the different widths of the concentric buried cavities 12A-12G, is capable of rapidly switching from the acoustic wave emitter operating mode to the acoustic wave detector operating mode.
In fact, as discussed above, due to the different widths of the thin membranes 13A-13H, each transducer unit 40A-40H has a different resonance frequency.
For example, with the widths w1-w8 and the dimensions of the thin membranes 13A-13H indicated above, for silicon membranes, the resonance frequency values indicated in the following table I have been experimentally detected:
Due to the different resonance frequencies of the thin membranes 13A-13H and to their adjacent arrangement, the acoustic transducer 10 has a resonance frequency comprised between the minimum frequency value (resonance frequency of the maximum width cavity, here the concentric buried cavity 12H) and the maximum frequency value (resonance frequency of the minimum width cavity, here the first cavity 12A) and therefore is broadband.
By neglecting for the moment the effect of the thick membrane 35, as a result, the acoustic transducer 10 has a reduced quality factor Q with respect to the single transducer units 40A-40G and therefore tends to rapidly damp oscillations.
This is advantageous, for example, when the acoustic transducer 10 is used as a distance meter.
In fact, in this case, the acoustic transducer 10 may be controlled to operate, in a first step, in the generator operating mode and generates a high-frequency acoustic wave and, in a second step, in the receiver operating mode, and detects the echo of the emitted acoustic wave.
To this end, in the first step, the thin membranes 13A-13H are caused to vibrate by the respective piezoelectric elements 15A-15H, but they are rapidly damped, due to the high band of the system, and are rapidly caused to rest, to be able to operate in a detection condition.
In this manner, the acoustic transducer 10 may perform distance measurement operations very rapidly, without having to wait long times between the two operating steps. As a result, it is capable of operating even at a short distance.
According to another embodiment, the transducer units 40A-40G may be controlled individually and/or in selected groups, applying control voltages only to the selected transducer unit(s) 40A-40G. This may be useful in some applications, such as for example for focusing an acoustic beam for tumor ablation in the brain.
As mentioned above, in the acoustic transducer 10, the deep buried cavity 25 allows the acoustic waves emitted at high frequency to be amplified.
In fact, the acoustic power emitted by a PMUT acoustic transducer is subject to a damping dependent on the wave frequency and on the propagation medium, according to the equation:
p(x,t)=Pe−αx cos(ωt−kx) (1)
wherein:
For example, at the frequency of 1 MHz, the coefficient α has a value of 0.0022 in water and 12 in air.
In general, therefore, the waves emitted at higher frequencies are subject to greater attenuation than those at lower frequency. Furthermore, if the acoustic transducer 12 works at frequencies of the order of MHz and the propagation medium is air, the attenuation is rather high.
The deep buried cavity 25 obviates this problem. In fact, the acoustic pressure of a wave emitted by a membrane depends on the square of the ratio between the thickness and the radius of the membrane, as well as on its stiffness (Young's Modulus and on the density of the material of the membranes 13, 25, here monocrystalline silicon). By designing the thick membrane 35 so that it has a resonance frequency in the operational field of the narrower membranes 13A-13D (and where the attenuation in air is maximum), the acoustic wave emitted by the narrower membranes 13A-13D may be amplified.
For example, for a thickness of the thick membrane 35 of 140 μm (distance d2 in
In practice, the thick membrane 35 resonates with the overlying thin membranes 13A-13H which are actuated. Due to the large diameter of the thick membrane 35, the latter is subject to a high deformation which originates a very high acoustic pressure at a near resonance frequency, in the example considered, at 1.1 MHz. Since this frequency is inside the frequency band where the acoustic propagation is strongly attenuated by the air (or other medium which the acoustic transducer immersed in and which has strong attenuation at high-frequency), the membrane 35 contributes to making the acoustic transducer 10 operative even in such operating conditions.
The acoustic transducer 10 may be formed as shown in
In
For example, the deep buried cavity 25 may be formed with the process described in EP1577656 (corresponding to U.S. Pat. No. 8,173,513), according to which, starting from an initial silicon wafer, a plurality of adjacent and communicating trenches are formed, separated by silicon pillars; then an epitaxial growth is performed in an oxidizing environment, which leads to the top closure of the trenches and to a migration of the silicon atoms of the pillars, with formation of the buried cavity 25.
Then,
Thus, the thin membranes 13A-13G (only some shown in
The wafer thus obtained, indicated by 51, is formed by a substrate 52 (intended, after dicing the wafer 50, to form the body 11) having for example a depth of 712 μm and a face 51A.
Subsequently,
After dicing the wafer 51, a plurality of acoustic transducers 10 are obtained (
According to another embodiment, shown in
In detail, with reference to
In
In a manner known to the person skilled in the art, the porous silicon of the first structural layer 153 is characterized by the presence of micropores which make it permeable to liquids, in particular to etchants, such as, in case of a deep sacrificial region 152 of silicon oxide, HF (hydrofluoric acid).
Then,
In
The first structural layer 153 and the second structural layer 155 together form an intermediate structural layer 156, having a thickness equal to about the distance between the deep buried cavity 25 and the concentric buried cavities 12A-12H.
In
In
The third structural layer 156 and the intermediate structural layer 156 together form a final structural layer 162, having a thickness equal to the distance d2 (
Then,
In
After dicing the wafer 151, a plurality of acoustic transducers 10 are obtained (
The acoustic transducer 10 and the manufacturing processes described herein have numerous advantages.
In fact, forming transducer units 40A-40H with thin membranes 13A-13G, concentric with each other and having variable dimensions, as described above, allows a multifrequency acoustic transducer, with high detection accuracy and quick response, to be obtained.
Thanks to the presence of the deep buried cavity 25, the acoustic transducer 10 is capable of emitting high-power acoustic waves, detectable at a long distance, and has high sensitivity even when operating in media having high attenuation, such as air, and high frequencies. Advantageously, this amplification occurs by exploiting the portion of the body 11 underlying the thin membranes 13A-13G, and therefore without requiring further space for forming the thick membrane 35. This contributes to maintaining the dimensions of the acoustic transducer 10 small.
By operating several transducer units 40A-40H simultaneously, wide band acoustic signals, with rapid vibration damping, may be emitted and detected.
The acoustic transducer 10 may also be manufactured using usual semiconductor technique process steps and therefore at reduced costs.
It also has small overall dimensions which allow it to be used in portable devices.
Finally, it is clear that modifications and variations may be made to the acoustic transducer and to the manufacturing process described and illustrated herein without thereby departing from the scope of the present disclosure, as defined in the attached claims.
For example, the concentric buried cavities 12A-12G may be in different number.
They may also have dimensions variable in a different manner than shown. In particular, according to a different embodiment, the cavities might have a decreasing dimension starting from the center. In this case, the deep buried cavity 25 might have an annular shape and extend below the first outermost cavities.
Or, the concentric buried cavities 12 might have variable width in groups, so that the buried cavities of each group have the same width, and each group is arranged between a first group of larger dimension cavities and a second group of smaller dimension cavities.
Alternatively, the dimension sequence of the first cavities 12 might not be monotonous, and therefore not always increasing (or decreasing, depending on the direction of observation).
The number of concentric buried cavities 12 having the deep buried cavity 25 extending therebelow may vary, in particular depending on the desired resonance frequencies.
The central buried cavity 25 might also have an annular shape.
The embodiment with porous silicon of
A PMUT acoustic transducer (10), may be summarized as including a body (11) of semiconductor material having a face (11A); a plurality of first buried cavities (12A-12H), having an annular shape, arranged concentrically to each other and extending at a distance from the face (11A) of the body (11); a plurality of first membranes (13A-13H) formed by the body (11), each first membrane (13A-13H) extending between a respective first buried cavity (12A-12H) of the plurality of first buried cavities and the face (11A) of the body (11); a plurality of piezoelectric elements (15A-15H) on the face of the body, each piezoelectric element extending above a respective first membrane (13A-13H) of the plurality of first membranes; wherein the first membranes (13A-13H) have different widths (w1-w8).
The plurality of first membranes (13A-13H) may include a central membrane (13A) surrounded by other first membranes (13B-13H) of the plurality of first membranes (13A-13H) and a peripheral membrane (13H) surrounding the other first membranes of the plurality of first membranes and wherein the first membranes (13A-13H) of the plurality of first membranes have widths (w1-w8) that are monotonously variable from the central membrane (13A) towards the peripheral membrane (13H).
The first membranes (13A-13H) of the plurality of first membranes may have widths (w1-w8) increasing from the central membrane (13A) towards the peripheral membrane (13H).
The first buried cavities (12A-12H) may extend at a first distance (d1) from the face (11A) of the body (11) and the PMUT acoustic transducer (10) may further include a second buried cavity (25) extending at a second distance (d2) from the face of the body, the second distance greater than the first distance (d1), the second buried cavity (25) extending below at least one minimum width membrane (13A) of the plurality of first membranes (13A-13H).
The second buried cavity (25) may extend below at least the central membrane (13A).
The second buried cavity (25) may have a diameter between 500 μm and 1500 μm.
The second distance (d2) may be between 10 μm and 200 μm.
The first membranes may have a variable width between a minimum value and a maximum value, the minimum value (w1) being less than or equal to 20 μm and the maximum value (w8) being greater than or equal to 500 μm.
The first buried membranes (13A-13H) may have a thickness (d1) between 1 μm and 100 μm.
The piezoelectric elements (15A-15H) of the plurality of piezoelectric elements each may include a first and a second electrode (17, 19), the first electrodes (17) of the piezoelectric elements (15A-15H) of the plurality of piezoelectric elements being mutually coupled and the second electrodes (19) of the piezoelectric elements of the plurality of piezoelectric elements being mutually coupled.
The piezoelectric elements (15A-15H) of the plurality of piezoelectric elements each may include a first electrode (17) and a second electrode (19), the second electrodes (19) of the piezoelectric elements (15A-15H) of the plurality of piezoelectric elements being mutually decoupled.
A process for manufacturing a PMUT acoustic transducer (10), may be summarized as including forming a plurality of first buried cavities (12A-12H) in a wafer (50; 150) of semiconductor material, the first buried cavities being arranged concentrically to each other and extending at a distance from the face (52A) of the first wafer (50; 150), the first buried cavities (12A-12H) defining a plurality of first membranes (13A-13H) each extending between a respective first buried cavity (12A-12H) of the plurality of first buried cavities and the face (52A) of the body (50; 150); and forming a plurality of piezoelectric elements (15A-15H) on the face (52A) of the body (50; 150), each piezoelectric element extending above a respective first membrane (13A-13H) of the plurality of first membranes; wherein the first membranes (13A-13H) have different widths (w1-w8).
The process may further include forming a second buried cavity (25), wherein the first buried cavities (12A-12H) extend at a first distance (d1) from the face (52A) of the body (50; 150) and the second buried cavity (25) extends at a second distance (d2) from the face of the body, below at least one first minimum width membrane (13A) of the plurality of first membranes (13A-13H), the second distance greater than the first distance (d1).
After forming the second buried cavity (25), a semiconductor material layer (56; 155) may be grown epitaxially; and the step of forming the plurality of first buried cavities (12A-12H) may be performed.
Forming the second buried cavity (25) may include forming a first sacrificial region (152) of material other than the semiconductor material and etchable by an etching solution ineffective on the semiconductor material; forming a first porous semiconductor material layer (153) covering the first sacrificial region (152); removing the first sacrificial region through the first porous semiconductor material layer (153); forming a plurality of second sacrificial regions (160) on the first semiconductor material layer (155), the second sacrificial regions (160) being of material other than the semiconductor material and etchable by an etching solution ineffective on the semiconductor material; forming a second porous semiconductor material layer (161) covering the second sacrificial regions (160); and removing the second sacrificial regions through the second porous semiconductor material layer.
The various embodiments described above can be combined to provide further embodiments. Aspects of the embodiments can be modified, if necessary to employ concepts of the various patents, applications and publications to provide yet further embodiments.
These and other changes can be made to the embodiments in light of the above-detailed description. In general, in the following claims, the terms used should not be construed to limit the claims to the specific embodiments disclosed in the specification and the claims, but should be construed to include all possible embodiments along with the full scope of equivalents to which such claims are entitled. Accordingly, the claims are not limited by the disclosure.
Number | Date | Country | Kind |
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102021000027425 | Oct 2021 | IT | national |