Patent Application
20190047111
The present invention relates to a surface plate for finish polishing, a finish polishing device, and a polishing method.
In the related art, as polishing devices in which a polishing film is provided on a surface plate, there are known a polishing device in which the polishing film is fixed to the surface plate via an elastic body on the surface plate, and a polishing device in which the polishing film is directly fixed to the surface plate. These well-known polishing devices are disclosed, for example, in Patent Document 1. Patent Document 1 discloses a polishing device in which two types of polishing films including a polishing film for rough processing and a polishing film for finish polishing are mounted on a polishing surface plate, and an elastic body is mounted between the polishing target surface plate and the polishing film if necessary.
In a case where the elastic body is mounted between the polishing target surface plate and the polishing film or in a case where a polishing cloth having loose abrasive grains dispersed thereon is used, an edge sagging may be caused. The edge sagging is a phenomenon in which a soft part of a polishing sample may be excessively polished and excavated, and a circumferential edge of a hard part surrounded by the soft part may also be excessively polished. Particularly in a case where polishing is performed with the loose abrasive grains interposed, the edge sagging is likely to occur.
If a film of lubricant, such as water, is thick in a case where a fixed abrasive grain film is mounted on a smooth polishing surface plate, there is a concern that the lubricant may be interposed between the fixed abrasive grain film and the polishing sample and polishing may not be performed. Additionally, there is also a concern that the polishing target surface of the polishing sample may be sucked to the fixed abrasive grain film like a suction cup and polishing may not be easy. Moreover, there is also a concern that shavings may enter between the polishing target surface of the polishing sample and the fixed abrasive grain film and may damage the polishing target surface of the polishing sample.
As a technique of solving these problems, Patent Document 2 discloses a finishing polishing surface plate in which a number of grooves, having a width of several millimeters, parallel to a planar glass plate are formed.
A polishing wrapping film disclosed in the above Patent Document 1 and Patent Document 2 is a film that is sufficient in smoothly polishing materials. On the other hand, in a case where a flat polishing sample is made using the polishing wrapping film, the polishing wrapping film is placed on a hard plate (glass plate) having high planarity, and the sample is manually polished while causing the lubricant, such as water, flow to the polishing wrapping film. In this case, as the degree of the abrasive grains becomes smaller, the sample to be polished and the film are brought into closer contact with each other, and resistance increases. Accordingly, there is a case where the polishing sample may not smoothly slide on the polishing film and may not be cleanly polished. As the polishing target surface of the polishing sample becomes larger, it is noticeable that the polishing sample does not smoothly slide on the polishing film.
Additionally, there is a case where a lot of scratches may be formed on the polishing target surface of the polishing sample due to shavings. As the polishing target surface of the polishing sample becomes larger, the scratches become conspicuous.
Moreover, in Patent Document 2, particularly as the polishing target surface of the polishing sample becomes larger for manual polishing, there is a concern that prolonged work is required for mirror-finishing the sample. For that reason, there is a demand to shorten the time required for the mirror finishing.
Additionally, due to polishing in a certain direction (length), in manual polishing, a skillful technique is required for evenly polishing the sample surface. For this reason, particularly as the polishing target surface of the polishing sample becomes larger, there is a case where a polishing state may change depending on a worker's skill level.
Additionally, in a case where the above-described edge sagging has occurred and in a case where the polishing target surface of the polishing sample is analyzed by secondary ion mass spectroscopy (SIMS), there is a case where the flatness of an analysis surface (polishing target surface) may be insufficient, and the analysis may not be performed well. For this reason, particularly as the polishing target surface of the polishing sample becomes larger, there is a concern that analysis processing time may increase.
Additionally, if the polishing sample is small, time relating to flattening processing by polishing is also short. On the other hand, since there is a concern that the time related to flattening processing by polishing may become long if the polishing sample is large, there is demand to shorten this time. Moreover, if the polishing sample becomes large, the flattening processing by polishing will become difficult. As a result, the efficiency and accuracy of the sample making will be dependent on a worker's skill level. For that reason, there is a demand to eliminate the dependability onto the worker's skill level.
The present invention has been made in view of the above situation to achieve the following objects.
A finish polishing surface plate related to a first aspect of the present invention is configured such that a polishing film is mounted thereon. The finish polishing surface plate includes a plate body having a planar surface; and a plurality of island shaped protrusions formed on the surface of the plate body. In the plurality of island shaped protrusions, continuous grooved recesses are formed between the respective island shaped protrusions.
A diameter dimension of the island shaped protrusions may be set within a range of 1.5 to 2.5 times a width dimension of the grooved recesses.
The island shaped protrusions adjacent to each other may be arranged such that a separation distance therebetween is equal to the width dimension of the grooved recesses on the whole surface of the plate body.
Each of the island shaped protrusions may have a polygonal shape in plan view.
A diameter dimension of the island shaped protrusions may be set within a range of ½ to 3/2 with respect to a diameter dimension of a polishing target surface of a polishing sample.
A polishing target surface of a polishing sample may have a region having different hardnesses, and a Mohs hardness difference between a high-hardness region and a low-hardness region in the polishing target surface may be 3 or more.
A finish polishing device related to a second aspect of the present invention includes the finish polishing surface plate related to the first aspect; and a rotating device that rotates the finish polishing surface plate with respect to a rotational axis orthogonal to the surface of the plate body.
The rotating device may have rotating plate that rotates around the rotational axis, and a holding part that holds the finish polishing surface plate to the rotating plate.
The finish polishing surface plate may be formed of stainless steel having magnetism, and the holding part may be capable of magnetizing the finish polishing surface plate.
A polishing method related to a third aspect of the present invention includes performing polishing using a planar surface plate and polishing abrasive grains to generate edge sagging in a polishing sample; and performing polishing using the finish polishing device related to the above second aspect and a polishing film to eliminate the edge sagging to flatten the polishing target surface of the polishing sample.
According to the finish polishing surface plate related to the first aspect, since the continuous grooved recesses are formed between the respective island shaped protrusions in the plurality of island shaped protrusions, it is possible to efficiently exhibit a drainage effect from the grooved recesses extending in multiple directions rather than one direction. For that reason, it is possible to improve the ease of drainage of lubricant, such as water. The polishing target surface of the polishing sample and the polishing film can easily come into contact with each other, and polishing efficiency can be improved. Additionally, since shavings generated from the polishing sample are easily discharged to the outside of a working plane via the grooved recesses of the surface plate, a frequency at which the polishing target surface is damage can be remarkably lowered.
Additionally, since the island shaped protrusions are split by the grooved recesses, edge parts of the island shaped protrusions corresponding to regions to be subjected to polishing extend in the multiple directions rather than one direction. As a result, even in a case where the polishing target surface has regions having different hardnesses, it is possible to prevent occurrence of sagging.
Simultaneously, since the island shaped protrusions are split by the grooved recesses extending in the multiple directions rather than one direction, it is possible to prevent a situation where the polishing target surface of the polishing sample and the polishing film may be brought into close contact with each other and polishing may not be performed, when the polishing target surface of the polishing sample and the polishing film perform polishing by moving relative to each other.
Additionally, since the drainage of the lubricant is easily performed by the grooved recesses, the polishing target surface of the polishing sample and the polishing film can easily come into contact with each other, the polishing efficiency can be performed, and the processing time can be shortened even in a case where the polishing target surface of the polishing sample becomes large.
Additionally, in the finish polishing surface plate related to the first aspect, since the diameter dimension of the island shaped protrusions is set within a range of 1.5 to 2.5 times the width dimension of the grooved recesses, the drainage of the lubricant, prevention of sticking of the polishing sample, and prevention of the sagging can be effectively realized.
Additionally, in the finish polishing device related to the first aspect, since the separation distance between the island shaped protrusions adjacent to each other is equal to the width dimension of the grooved recesses on the whole surface of the plate body, the drainage of the lubricant, prevention of sticking of the polishing sample, and prevention of the sagging can be effectively realized.
Additionally, in the finish polishing surface plate related to the first aspect, since the shapes of the island shaped protrusions in plan view are the polygonal shapes, the drainage of the lubricant, and the island shaped protrusions are split by the grooved recesses extending in the multiple directions rather than one direction, the drainage of the lubrication, prevention of sticking of the polishing sample, and prevention of the sagging can be effectively realized.
Additionally, in the finish polishing surface plate related to the first aspect, since the diameter dimension of the island shaped protrusions is set within a range of ½ to 3/2 with respect to the diameter dimension of the polishing target surface of the polishing sample, the drainage of the lubricant, prevention of sticking of the polishing sample, and prevention of the sagging can be effectively realized.
Additionally, in the finish polishing device related to the first aspect, even in a case where the polishing target surface of the polishing sample has regions having different hardnesses, and the Mohs hardness difference between the high-hardness region and the low-hardness region in the polishing target surface is 3 or more, the drainage of the lubricant, prevention of sticking of the polishing sample, and prevention of the sagging can be effectively realized.
Additionally, since the finish polishing device related to the above second aspect includes the finish polishing surface plate related to the first aspect; and the rotating device that rotates the finish polishing surface plate with respect to the rotational axis orthogonal to the surface of the plate body, polishing can be performed by changing a state where the polishing target surface of the polishing sample and the polishing film come into contact with each other. For that reason, ease of drainage of the lubricant can be further improved using rotation, and prevention of sticking of the polishing sample and prevention of the sagging can be effectively realized.
Additionally, in the finish polishing device related to the first aspect, since the rotating device has the rotating plate that rotates around the rotational axis, and the holding part that holds the finish polishing surface plate to the rotating plate, the drainage of the lubricant, prevention of sticking of the polishing sample, and prevention of the sagging can be effectively realized. Accordingly, it is possible to perform polishing processing without being dependent on a worker's skill level.
Additionally, in the finish polishing device related to the first aspect, since the finish polishing surface plate is formed of stainless steel having magnetism, and the holding part is capable of magnetizing the finish polishing surface plate, ease of replacement of the polishing film and close contact of the polishing film with the surface plate can be improved.
Additionally, the polishing method related to the third aspect of the present invention includes performing polishing using a planar surface plate and polishing abrasive grains to generate edge sagging in a polishing sample; and performing polishing using the finish polishing device related to the second aspect and a polishing film to eliminate the edge sagging to flatten the polishing target surface of the polishing sample. Additionally, the polishing abrasive grains may be alumina paste. Accordingly, since the amount (surface area) of the polishing sample to be cut with the polishing film can be made small, it is possible to further shorten working hours required for flattening to quickly perform polishing by the planar surface plate and polishing abrasive grains.
Therefore, since further gaps can also be formed between the polishing film and the polishing sample, the shavings are not easily brought into contact with the polishing target surface, and can also be easily discharged, thereby reducing a rate at which a sample surface is damaged.
According to the above aspects of the present invention, the occurrence of the sagging in the polishing sample can be prevented. Additionally, occurrence of uneven polishing or the like in each region resulting from a hardness difference on the polishing target surface of the polishing sample can be prevented. Additionally, the sticking of the polishing sample to the polishing film can be prevented. Additionally, occurrence of the damage on the polishing target surface resulting from the shavings can be prevented. Additionally, damage of the polishing film by the sticking or other causes can be prevented. Additionally, the possibility of coping with the size of the polishing sample can be realized, and producing the polishing sample without depending on a worker's skill level can be realized.
Hereinafter, a finish polishing surface plate and a finish polishing device related to a first embodiment of the present invention will be described with reference to the drawings. The present invention is not to be interpreted as being limited to this, and various changes, modifications, and improvements can be made on the basis of the knowledge of those skilled in the art without departing from the scope of the present present invention.
A finish polishing surface plate 1 related to the present embodiment is used when polishing a composite material with different hardnesses to form a thin sample piece. As shown in
In the present embodiment, the plate body 2 has a flat disk shape. As the plate body 2, for example, a metal plate or the like having well-known magnetism can be used. It is preferable that the plate body 2 is formed of a stainless plate having magnetism. The size of the plate body 2 is ϕ100 to 300 mm and particularly preferably about ϕ150 mm (±15 mm) or 200 mm (±20 mm). Additionally, the thickness of the plate body 2 is 1.5 to 3 mm and particularly preferably about 2 mm (±0.2 mm). Additionally, SUS 200 series can be applied.
As shown in
A diameter dimension T1 of each island shaped protrusion 5 can be set to correspond to the size of a polishing target surface in a polishing sample 8. For example, T1 can be set to a range of ½ to 3/2 with respect to the diameter dimension of the sample polishing target surface (polishing target surface) of the polishing sample 8. Specifically, the diameter dimension T1 of the island shaped protrusion 5 can be set to about 12 mm (±1.2 mm) within a range of 8 mm to 20 mm. In addition, the diameter dimension T1 of the island shaped protrusion 5 is a distance between opposed sides of the island shaped protrusion 5.
Separation distances between adjacent island shaped protrusions 5 (distances between opposed sides of two adjacent island shaped protrusions 5) may be equal to each other. In addition, although the profiles of the island shaped protrusions 5 are not hexagonal shapes in portions that interferes with an edge part of the plate body 2, these portions may be formed such that separation distances between adjacent island shaped protrusions 5 are equal to each other.
Although the planar profiles of the island shaped protrusions 5 have a regular hexagonal shape in the present embodiment, the planar profiles are not limited to this as long as the island shaped protrusions are arranged on a plane in the closest state. A circular shape, an elliptical shape, or a polygonal shape with a larger number of corners than 6 can also be adopted. In this case, although the width of each grooved recess 3 to be described below becomes uneven depending on locations, the arrangement state of the island shaped protrusion 5 may be maintained in the same manner as in the case of the regular hexagonal shape.
At the profile position of each island shaped protrusion 5, an end part of the island shaped protrusion 5 is formed in a state where the grooved recess 3 is formed by polishing, that is, in a state where the end part is cut upright such that a side surface of the island shaped protrusion 5 or the grooved recess 3 is equal to a normal direction of a principal surface of the plate body 2.
As shown in
Additionally, the grooved recess 3 is engraved such that the depth dimension from a top part of the island shaped protrusion 5 is within a range of 50 to 300 μm, preferably about 100 to 200 μm (±10 μm). The grooved recess 3 extends between the island shaped protrusion 5 and island shaped protrusion 5 adjacent to each other, and all the grooved recesses 3 are brought into a continuous state on the surface of the plate body 2.
The grooved recesses 3 can be formed on the surface of the plate body 2 made of metal by well-known methods, such as etching, polishing, and cutting.
A corner part 6 of a boundary line between each grooved recess 3 and each island shaped protrusion 5 can also be formed by rounding off a corner to the same extent as a curvature radius that is half of the depth of the grooved recess 3.
Although a polishing film 7 mounted on the finish polishing surface plate 1 in the present embodiment is not particularly described, for example, a well-known fixed abrasive grain film for finishing application having an abrasive grain diameter of about 0.3 μm to 3 μm is used.
The present embodiment can also be applied to the polishing sample 8 in which a polishing target surface has regions having different hardnesses, and a Mohs hardness difference between a high-hardness region and a low-hardness region in this polishing target surface is 3 or more. If there is a hardness difference on the polishing target surface, sagging is likely to occur. However, in the finish polishing surface plate 1 of the present embodiment, polishing can be suitably performed even in such a polishing sample.
Additionally, the high-hardness region has a Mohs hardness of about 4 to 8 and can include glass, a mineral, metal, or the like, and the low-hardness region can include a mineral or the like having a lower viscosity than resin. The low-hardness region has a Mohs hardness of about 1 to 3 and can include indium.
The polishing sample includes, for example, a sample in which a plurality of polishing samples, such as rock, are embedded on a surface of a resinous cylindrical base material having a diameter dimension of about 25 mm.
As shown in
As shown in
As shown in
As shown in
In this way, for example, excessive lubricant 9, such as water, on the working plane of the plate body 2 is discharged from the working plane of the plate body 2 by the grooved recesses 3 and the arcuate recesses 4a formed in the surface of the polishing film 7. Accordingly, the lubricant 9 is not substantially interposed between the polishing target surface of the polishing sample 8 and the polishing film 7 immediately above the island shaped protrusions 5. Accordingly, the polishing target surface of the polishing sample 8 and the polishing film 7 can easily come into contact with each other above the island shaped protrusions 5, and polishing efficiency can be improved.
Additionally, since the contact area between the polishing target surface of the polishing sample 8 and the polishing film 7 is limited by the formation of the arcuate recesses 4a. Therefore, suction of the polishing target surface of the polishing sample 8 to the polishing film 7 is suppressed. Therefore, an acting force required for the polishing can be reduced, and polishing processing time can be shortened. Moreover, since shavings K generated from the polishing sample 8 accumulates within the arcuate recesses 4a of the polishing film or are discharged to the outside via the arcuate recesses 4a, the frequency at which the shavings K damages the polishing target surface decreases remarkably.
Even in a case where the polishing sample 8 made of a composite material having a hardness difference on the polishing target surface is polished, it is possible to prevent sagging or prevent partial variation of a polishing state to realize polishing having planarity and flatness.
According to the present embodiment, even if the operation skill level is low, it is possible to easily produce a polishing sample 8 having high planarity and flatness in a short time. Therefore, the possibility that the polishing sample 8 itself is damaged can be reduced, and the present embodiment can also be applied to a valuable sample without alternatives, such as a single article.
Hereinafter, a finish polishing surface plate related to a second embodiment of the present invention will be described with reference to a drawing.
The present embodiment is different from the above-described first embodiment in terms of the dimensions of the island shaped protrusions 5 and the grooved recesses 3, and corresponding constituent elements other than this will be designated by the same reference signs and the description thereof will be omitted.
In the present embodiment, the width T2 of each grooved recess 3 is made smaller than the diameter T1 of each island shaped protrusion 5, and the diameter T1 of the island shaped protrusion 5 can be set to about 4 mm (±4 mm) within a range of 2 to 8 mm.
The width T2 of the grooved recess 3 is provided so as to be equal to a separation distance between two adjacent island shaped protrusions 5. The widths T2 of the grooved recesses 3 are equal to each other on the whole surface of the working plane of the plate body 2. Specifically, the width T2 of each grooved recess 3 can be set to about 2 mm (±0.2 mm) within a range of 1 to 4 mm.
The present embodiment can also be applied to the polishing sample 8 in which a polishing target surface has regions having different hardnesses and a Mohs hardness difference between a high-hardness region and a low-hardness region in this polishing sample surface is 3 or more. If there is a hardness difference on the polishing target surface, sagging is likely to occur. However, in the finish polishing surface plate 1 of the present embodiment, polishing can be suitably performed even in such a polishing sample.
The present embodiment can also be applied to, for example, a polishing sample in which a plurality of polishing samples, such as rock, are embedded on a surface of a resinous cylindrical base material having a diameter of about 5 to 10 mm.
In the present embodiment, polishing can be performed so as to correspond to a polishing sample 8 smaller than the polishing sample 8 in the first embodiment by setting the width T2 of the grooved recess 3 and the diameter T1 of the island shaped protrusion 5 as described above.
Additionally, in the present embodiment, first, a first polishing step is performed by supplying alumina paste to a surface plate without the ordinary grooved recesses 3, and then, a second polishing step is performed using the finish polishing surface plate 1 and the polishing film 7 of the present embodiment.
In the first polishing step, the processing of forming a polishing target surface having area and flatness sufficient to perform finish polishing on the polishing sample 8 is performed. On the other hand, in a case where the high-hardness region and the low-hardness region having different hardnesses on the polishing target surface are included because the surface plate having no grooved recesses 3 and island shaped protrusions 5 are included on the working plane, there is a case where the sagging may occur. Additionally, there is a case where the low-hardness region may be excessively polished.
However, in the present embodiment, by performing the second polishing step after the first polishing step, the amount (surface area) of the polishing sample to be cut with the polishing film can be made small by the first polishing step (first step), and flattening can be made by the second polishing step (second step). Accordingly, it is possible to further shorten working hours to quickly perform polishing.
Additionally, gaps resulting from the further arcuate recesses can also be formed between the polishing film 7 and the polishing sample 8. Therefore, the shavings K are not easily brought into contact with the polishing target surface and can also be easily discharged, thereby reducing a rate at which a sample surface is damaged.
Hereinafter, examples related to the present invention will be described.
Here, polishing processing was performed, using 0.3 μm alumina paste as loose abrasive grains. As shown in
In addition, in
Here, after polishing was performed for 1 minute in a state where the rotating plate 11 was rotated at 300 rpm using one having an abrasive grain diameter of 3 μm as a polishing film (wrapping film), finish polishing was performed for 2 minutes in a state where the rotating plate 11 was rotated at 300 rpm using one having an abrasive grain diameter of 0.5 μm as a polishing film (wrapping film).
As shown in
Here, polishing processing was performed, using 0.3 μm alumina paste as loose abrasive grains. As shown in
In addition, in
Here, polishing was performed for 3 minutes in a state where the rotating plate 11 was rotated at 300 rpm, using one having an abrasive grain diameter of 0.5 μm as a polishing film (wrapping film).
As shown in
In addition, those including a pyroxene (Mohs hardness 6.5 to 7) olivines (Mohs hardness 7) spinel (Mohs hardness 8) indium metal (Mohs hardness 1.2) kaolinite; or clay (Mohs hardness 1-2) iron nickel alloy (Mohs hardness 4) can be included as the polishing sample 8.
From these results, it can be seen that sufficient planarizing and flattening can be realized for a polishing sample subjected to the second step using the finish polishing surface plate 1 in the embodiment.
Accordingly, it is possible for the polishing sample 8 flattened in the present invention to sufficiently satisfy smoothness required for application to SIMS (secondary ion mass spectroscopy). Specifically, a state where a sample surface can be suitably observed using an objective lens (Nikon L Plan 2.5×0.075 EPI) having a relatively shallow depth of focus with reflected light of a polarization microscope that is a criterion for determining whether or not analysis performed by the SIMS is possible can be satisfied.
The present invention makes it possible to quickly and smoothly polish a composite material having remarkably different hardnesses, and can be widely utilized in individual fields involved in processing of hard-to-work materials, including the materials science field.
| Number | Date | Country | Kind |
|---|---|---|---|
| 2016-026048 | Feb 2016 | JP | national |
This application is a 371 National Stage Application of International Application No. PCT/JP2017/004746, filed on Feb. 9, 2017, published as International Publication No. WO 2017/141812, which claims priority to Japanese Patent Application No. 2016-026048, filed Feb. 15, 2016, the content of which is incorporated herein by reference.
| Filing Document | Filing Date | Country | Kind |
|---|---|---|---|
| PCT/JP2017/004746 | 2/9/2017 | WO | 00 |
