This application claims the priority of European Patent Application No. 06405117.0, dated Mar. 16, 2006, the disclosure of which is incorporated herein by reference.
The invention relates to a target holder for a target, which is used in a coating method. The coating method includes in particular a gas flow sputtering method for the application of high temperature resistant adhesive layers on a substrate, such as in particular on a turbine blade. The target contains the coating material, which can be sputtered out of the target by means of ions of an ionised inert gas plasma. The targets are accommodated on target holders in the housing of a coating source. The coating material sputtered from the target reaches the substrate to be coated via the ionised inert gas plasma flux. The coating source is located in a closed vacuum chamber, which is continually pumped down. The ionised inert gas and the deposited coating particles of the target reach the substrate inside the chamber or are pumped off by the vacuum pump. Each target has to be mechanically fastened in the target holder, by which means stresses arise in the target. Stresses of this kind are undesirable in the target because the coating material, from which the target is made, is neither resistant to tensile stresses nor to compressive stresses, nor to torsional stresses. The coating material is, as a rule, at least partially sintered powder or melts.
A target is soldered onto a target holder, or screwed directly to the target holder. A possible solution is to drill a blind hole into the target holder in which the target is screwed. The target is exposed to a high heat input during operation. This heat has to be dissipated via the target holder however. With both a soldered connection, and also with a screwed in realisation, overheating can occur in the target, in particular in temperature ranges above 400° C., since the heat can not be dissipated via the contact surfaces of the soldered connection or of the screwed connection. Overheating of this kind results in high residual stresses occurring in the target, which lead to a formation of cracks and subsequently to premature failure of the target.
It is therefore the object of the invention to connect a target or a target segment to the cooling system by means of a target holding apparatus in such a way that overheating of this kind no longer occurs.
This object is satisfied by the characterising part of claim 1. An apparatus for the attaching of a target or target segment of a coating source includes a target or target segment and a target holder, which includes a cooling body and a connecting means for attaching the target or target segment on the cooling body. The connecting means include electrically and/or thermally conductive means, so that the current supply takes place in a uniform distribution across the target or target segment, and also the heat arising at the target or target segment during the coating method can be conducted away into the cooling body uniformly.
In the following the term target segment should also be used for target. The term target is admittedly usually used since one only uses a single target in conventional sputtering processes. Target stands for an element made of coating material, which is located in a coating source, which is used for a coating method, such as a gas flow sputtering process for example. A coating apparatus is used for the coating process, which includes the coating source, and also the substrate to be coated. The coating source includes the totality of the target segments, the target holder for each target segment, a distribution apparatus for a gas, which includes an inert gas, in particular argon or a reactive gas, in particular an oxygen-containing gas. The coating source further includes a cooling body with a coolant connection, in particular a water connection and also a housing for the accommodation of all the above-named components, and also means for isolating the whole coating source. These means for isolating effect the complete electrical isolation and the largely complete thermal isolation of the coating source from the sputtering space. The term sputtering space is used to describe the region of the coating apparatus, which is for the most part formed as a vacuum chamber, in which the coating takes place, which means that the component to be coated or the components to be coated are located in this region of the vacuum chamber. The coating material is arranged on the target segment. The coating source is used in particular in a gas flow sputtering method, for which the abbreviations GV-PVD (gas flow physical vapour deposition) or also HS-PVD (high speed physical vapour deposition) will be used in the following. For the most part two target segments lying opposite one another are used for the gas sputtering method. Depending on the size and sputter rate desired, these target segments can be designed as an single element or can comprise a plurality of individual segments, precisely the aforementioned target segments. Thus the expression target segment in this application, instead of target, means that at least one target segment is used per target holder. The segmentation of the targets permits the achievement of higher coating rates and power inputs. Should higher coating rates and power inputs be of secondary importance, the sputtering method can also be carried out without segmentation using the present arrangement of the coating source. By using target segments it is possible to input a higher electrical power into each target segment, by means of which the sputtering of layer material from the target segment is accelerated, so that a higher sputtering rate can be achieved. As a result of the higher sputtering rate, higher coating rates result on the component. The use of target segments also offers advantages, which concern the durability and mechanical characteristics of the target segments. Due to the low stresses in each target segment, cracks and breaks in the coating material do not arise. Thus hard and/or brittle coating materials, such as, in particular, MCrAlY, can be subjected to the same power input, without an alteration in the handling of the coating materials during installation and during the coating method being necessary. Very soft materials, in particular pure aluminium or magnesium, which can only be soldered badly or even not at all, can be used with the same power input, without an alteration in the handling of the coating materials during installation and during the coating method being necessary. Furthermore the temperature resistance of the arrangement of the target segments increases, because the heat can be conducted away in an improved manner, through which no material melts on any of the target segments. Each of the target segments has in particular its own power connection and also its own connection to the cooling body. The primary function of the cooling body is to conduct away the heat occurring during the coating method. The thermal energy to be conducted away is produced by the power input, which is caused by currents of in particular up to 150 A per target, and in particular creates power densities of in particular up to 220 W/cm2 on the target surface, and also by the impact of the gas atoms striking the target segment. An inert gas can be used on the one hand in a coating method for coating with a metallic coating material, and argon in particular has proved to be suitable. The impact energy of these argon atoms likewise leads to a heat input into the target element. By means of the impact, atoms of the coating material are released from their bond at the target surface. During this high temperatures are reached. In order to control the process, it can be heated additionally by means of a radiative heating apparatus in order to reach coating temperatures, depending on the substrate and the layer, of up to approximately 1150° Celsius in the coating chamber. The coating apparatus can also be used for a reactive gas flow sputtering method. Instead of or in addition to inert gas, reactive gas, in particular oxygen-containing gas is added, by which means reactions of the coating material with the gas molecules at the target segment or in the gas phase after separation from the target segment result, so that a rise in temperature occurs, through the mostly exothermally occurring chemical reactions, in particular oxidation reactions. In order to avoid overheating of the target segment in a coating time of several hours, each target segment is cooled, wherein in particular water cooling is used. For the coupling in of higher currents, which result in higher heat transfer at the target segment, it is advantageous to use a plurality of individual target segments in the coating apparatus. In order to avoid the above-mentioned stresses in the target segment or to reduce them until they are below the crack formation stress of the target segment material, the target holder described in the following is used.
The coating source thus includes the target segment or target segments, the power connection for each of the target segments, a connection of each of the target segments to the cooling system for the supply and discharge of a coolant. The supply of the inert gas and/or of the reactive gas takes place via gas connections, and also gas distributors, which are arranged in such a way that a uniform distribution of the quantity of gas takes place with a same mean impact speed on all target segments. Apparatus-wise each target segment is accommodated in a target holder. The target holder includes the cooling body or bodies, and also an outer wall and connection connection means for connecting the target segment to the cooling body and also the outer wall of the coating source. By means of the previously described construction of the coating source, target segments and also other parts of the coating source, such as the gas distribution unit, the receiving units for coating material, which was not transported out of the coating source by the stream of gas can be installed and removed independently of one another, so that an improved repair and cleaning of the target segments, and also other parts of the coating source can be achieved. This fact is of particular significance in high power applications and long-term use of the coating source. If damage should occur to a target segment, which leads to a break down of the coating source, it is possible to repair the damage quickly by the exchange of the target segment. This results in a cost advantage because all other target segments can still be used further. The proportion of no longer usable coating material includes at most the coating material of the target segment to be replaced. The time needed for the exchange of the target segment is reduced, since only the damaged target segment is to be exchanged and each target segment can be exchanged individually by means of the target holder in accordance with the invention. Each component of the target holder is likewise exchangeable independently of the remaining parts of the coating source. One consequence of this service friendliness is the reusability of the target holder and/or of the target segments during their entire life. The breakdown of a target holder and/or of a target segment only results in a short standstill time of the coating plant, causing, at the most, slight interruptions in production, particularly in series production applications. Coating tasks can also be realised using different coating materials in the same coating plant due to the exchangeability of the target segments. The target segments can be constructed from any desired coating materials, so that a target can have target segments of different coating materials. The conversion of the whole target to a new coating material is comparatively unproblematic by means of the target holder in accordance with the invention, since the targets can be exchanged quickly. The dimensions of the target segments can likewise vary in many areas, so that the composition of the coating on the component can be adjusted precisely by means of the dimensioning of the target segments, the arrangement of the target segments, and the variation of the gas distribution by displaceable gas distribution units or a change of the through flow in the gas distribution unit.
Further advantageous embodiments of the invention are the subject of the subsidiary claims. The apparatus includes a T-nut for accommodating an attachment screw for the connection of the target segment to the cooling body.
The T-nut and/or the attachment screw have a contact lamella, and a power and heat conducting contact can be established between the T-nut and the attachment screw and/or the target segment by means of the contact lamella.
The T-nut has a galvanic coating in the contact region of the T-nut with the attachment screw and/or the T-nut and the cooling body and/or the T-nut and the target segment. The cooling body and/or the target segment have a galvanic coating at least on the common contact surfaces.
The attachment screw is surrounded by a sleeve in the region of the through bore through the cooling body, and the sleeve can be formed as a hollow cylindrical body, which includes, in particular, an external screw thread, with which the sleeve can be screwed into a bore in the cooling body and through which the attachment screw can be inserted through with an accurate fit, or the sleeve can be screwed into a threaded hole of the cooling body together with the attachment screw, so that a good heat transfer from the attachment screw into the cooling body takes place for the conducting of the heat away from the target segment. The sleeve is also termed as a screw in lamella or a screw in lamella sleeve in technical terminology.
The electrically and/or thermally conductive means include a forked plug device for the plugging of a target segment into the cooling body.
A contact lamella is arranged between the target segment and the cooling body, in particular inside the forked plug device and/or in a recess of the cooling body and/or of the target segment adjoining the cooling body and/or of the T-nut arranged between the cooling body and the target segment.
The contact lamella includes a spring element, through which the heat transfer between the adjacent surfaces of the cooling body and/or of the target segment and/or of the T-nut and/or of the forked plug device can be improved.
The forked plug device is soldered onto the cooling body and/or plugged in a recess of the target segment and/or can be screwed to the cooling body. At least one coolant passage is provided for the conveying of the coolant through the cooling body. The cooling body includes at least one inlet and one outlet for the coolant, so that the coolant can be conveyed from the inlet through the coolant passage to the outlet. Water is used in particular as a coolant.
A receiving means is provided in the cooling body for connecting means, in particular for the attachment screw and/or the forked plug device and/or the target segment and the coolant passage is arranged around the receiving means.
The receiving means include bores for the attachment screw and/or sleeve and/or recesses for the target segment and/or a forked plug device.
The coolant passage is formed as an open coolant passage, which was manufactured by means of a chip forming machining process or by means of a chemical process, in particular an etching process. The open coolant passage is bounded by an exterior wall of a cooling body, wherein cooling body and cooling body exterior wall are soldered, brazed, bolted or secured by a clamping connection and sealing means are provided between the cooling body and the cooling body exterior wall, in order to prevent the escape of coolant from the cooling body.
The cooling body contains at least one bore for a screw head of the attachment screw, with the attachment screw being guided through the cooling body exterior wall and through the cooling body in order to be screwed in the T-nut with the internal thread of the bore.
The coolant passage in the cooling body is arranged in such a way that the bores are arranged in the cooling body base material and/or a sleeve is arranged in the bore, with the sleeve being directly or indirectly in heat conducting contact with the coolant.
Receiving means for the target segment and/or the forked plug device are provided at the inside of the cooling body, with the receiving means being designed as soldering or brazing points or as recesses.
A plurality of target segments is provided in the coating source, which can be secured in the target holder via electrically or thermal conductive means.
The T-nut, the contact lamellae and/or the sleeve and/or the forked plug device contain a copper and/or nickel alloy, in particular a copper and beryllium containing alloy or a copper and beryllium and cobalt containing alloy.
a shows a further variant for the connection of the target segment with the cooling body
b shows a further variant for the connection of the target segment with the cooling body
c shows a further variant for the connection of the target segment with the cooling body
d shows a further variant for the connection of the forked plug device with the cooling body
a shows the T-nut, the sleeve and the attachment screw in accordance with FIGS. 1 to 4
b shows a first variant for the connection of the attachment screw with the T-nut
c shows a second variant for the connection of the attachment screw with the T-nut
a shows the connection of the target segment with the T-nut
b shows a section through a first embodiment of a connection of the target segment and the T-nut.
c shows a section through a second embodiment of a connection of the target segment and the T-nut.
d shows a section through a third embodiment of a connection of the target segment and the T-nut.
e shows a section through a fourth embodiment of a connection of target segment and the T-nut.
The connection of the target segment 9 to the cooling body 13 and to the power contact which is not illustrated is achieved here by means of the contact lamellae 10 between the target segment 9 and the surface of the continuation 23 on the target segment side, by means of the rear side target segment surface of the target segment 9, of the T-nut 8, via the T-nut, via the internal thread 25 of the cylinder 22 of the T-nut, and also of one contact lamella 3 arranged in the internal thread 25, into the attachment screw 7 and also from the attachment screw 7 directly to the cooling body or alternatively to this via the sleeve 6 to the cooling body 13. The contact lamella 3 is either part of the attachment screw 7, as is illustrated in the upper part of
In a further embodiment in accordance with
In the first embodiment, the thermal transfer also takes place between the target segment 9 and the surface on the target segment side of the slit-like recess 29 via the rib 14 of the target segment, through the connector 26 via the internal thread 28 and a contact lamella 3 arranged optionally in the internal thread 28 into the attachment screw 7 and also from the attachment screw 7 directly to the cooling body or, alternative to this, via the sleeve 6 to the cooling body 13. The contact lamella 3 is either part of the attachment screw 7, as is illustrated in the upper part of
In a further embodiment in accordance with
According to a further embodiment in accordance with
The target segments are plugged and fixed directly into these forked plug devices. The target segments are machined using suitable machining methods (according to material: e.g. EDM, milling) in such a way that their rib fits precisely and with firm contact into the forked plug device 12 of the cooling body 13. Milling or EDM (electron discharge machining) are used in particular as machining methods. Electron discharge machining is a high precision machining process, by means of which material is cut or drilled. A machining of even extremely hard, tough or brittle material types is made possible by means of electro-physical vaporisation by the application of an electrical potential to an electrode.
In accordance with any one of the previous embodiments the target segments 9 can be plugged into place and can also be removed again in this manner. Individual target segments can thus be replaced in all versions completely independently from the other target segments. A large effective thermal transfer surface results by means of the areal contact from the target segments to the forked plug devices, so that the target holder is directly connected to the cooling system. The heat arising in the target segment can then be dissipated simply, so that a high cooling rate can be achieved.
a shows a further variant for the connection of the target segment 9 to the cooling body 13. A groove 30 is located in the cooling body 13, in which a rib 14 with a rounded surface 31 engages with positive locking. Contact lamellae 11 are arranged in the groove 30. The contact lamellae 11 improve the retention of the target segment 9 in the groove 30 and permit a precise fitting of the two parts. Additionally, a galvanic coating and/or a thermally conductive, viscous or pasty fluid can be inserted in the groove for the improvement of the thermal transfer prior to the assembly of the target segment with the cooling body. This is advantageously a releasable connection, so that a used target segment can simply be exchanged.
b shows that a contact lamella 11 can also be attached to the target segment 9 itself. The attaching of the target segment 9 to the cooling body is not shown. A contact lamella of this kind can be used in each of the embodiments in accordance with
c shows that a contact lamella 11 can be attached to the surface of the cooling body 13. The attaching of the target segment 9 to the cooling body 13 is not shown. A contact lamella of this kind can be used in each of the embodiments in accordance with
d shows a combination of the rib 14 shown in
a shows the T-nut, sleeve and attachment screw in accordance with the embodiments from FIGS. 1 to 4 in an exploded view. In this case the sleeve 6 is plugged onto the attachment screw 7, before the assembly with the not illustrated cooling body and the T-nut 8 takes place.
b shows a first variant for the connection of the attachment screw to the T-nut. The T-nut 8 is shown in section, with details such as the illustration of the cylinder 22, being omitted. In the present case a blind hole with a thread was used. As an alternative the possibility exists of providing a through bore in the T-nut 8, such as was shown in
A second variant for connecting the attachment screw 7 to the T-nut 8 is illustrated in
a again schematically shows the connection of the target segment 9 to the T-nut 8 in accordance with
b shows the use of a blind hole after the embodiment of
b shows the use of a dovetail groove 24 as a groove in the target segment. The head of the T-nut has a cross-section, which corresponds precisely to the dovetail groove in the target segment, so that a precise fit of the two parts results. Moreover, the connection of the attachment screw to the T-nut illustrated in
c shows a variant for the attachment of the target segments 9 to a T-nut with a head with a design for the fitting into a dovetail groove of the target segment. One T-nut is, however, used for each of two adjacent target segments. This solution is particularly advantageous when the target segment material is not suitable for the manufacture of partially hollow structures, such as T-shaped grooves or dovetail grooves. Target segment material has to be removed exclusively from respectively two edges of the target segment, which simplifies the machining of the target segment considerably.
Two variants of the connection of the T-nut to the attachment screw 7 are also illustrated in
e shows a sectional view corresponding to
| Number | Date | Country | Kind |
|---|---|---|---|
| 06405117.0 | Mar 2006 | EP | regional |