The present invention relates to a high-voltage insulating structure, a charged particle gun, and a charged particle beam device.
In general, devices such as electron microscopes and X-ray devices that use charged particles to observe and analyze objects are equipped with a charged particle gun (generally called an electron gun) that generates electrons in the form of a beam. In such devices, a very high voltage of several kV to several hundred kV is applied to the cathode disposed inside the electron gun, so that an electron beam (charged particle beam) is accelerated and emitted toward the anode.
An HV power cable is typically used to supply such a high voltage (hereinafter abbreviated as “HV”) from an HV power supply to the cathode. Here, an HV connector assembly is attached to each end of the HV power cable. In general, one end of the HV connector assembly is connected to the HV power supply, and the other end is connected to a connector portion of a housing of the electron gun.
The HV conductor having HV voltage is provided at the center of each of the HV connector assembly and the housing connector portion, and the perimeter of the HV conductor is filled with an insulating material to electrically shield the HV conductor from the ground portion. By coupling the HV connector assembly and the housing connector portion, the respective HV conductor portions are brought into electrical contact and power can be supplied to the cathode.
An insulating gasket is interposed between the connecting portion between the HV connector assembly and the housing connector portion to ensure or increase the adhesion of the connecting portion. Since the dielectric breakdown voltage of air is lower than that of solid insulating materials, discharge in the air layer between the connecting portions is a problem. Therefore, by inserting an insulating gasket, the air layer can be eliminated and a high withstand voltage can be implemented. Grease is generally applied to the surface of the gasket to further increase adhesion.
As described above, by electrically insulating the HV conductor portion having the HV voltage from the housing portion having the ground voltage, the occurrence of discharge that would destroy the electron gun is prevented. The electron gun should also prevent the occurrence of minute discharges that impair electron gun performance. Therefore, electron guns are designed with various measures to reduce the electric field.
Typically, the inside of the HV cable, and the periphery of the HV conductor, such as the connecting portion of the connector, have an axially symmetrical shape centering on the HV conductor. A radial electric field E in such an axially symmetric space follows Gauss's law given by the following Equation (1).
In the above equation, V0 is the HV voltage applied to the HV conductor, r is the distance from the central axis (R1≤r≤R2), R1 is the diameter of the HV conductor (HV voltage) on the inner peripheral portion, and R2 is the diameter of the housing (ground voltage) on the outer peripheral portion. According to Equation (1), the electric field E is inversely proportional to the distance r from the center axis, that is, the closer to the center, the higher the electric field. As a result, the point where the electric field is maximum is positioned on the surface (r=R1) of the HV conductor. Thus, the vicinity of the center where the electric field is high is a portion where the possibility of occurrence of discharge is particularly high. According to Equation (1), the electric field E decreases as the radius R2 of the outer peripheral portion or the radius R1 of the inner peripheral portion increases.
As a way to reduce the electric field, for example, the radius R2 can be increased by increasing the size of the housing. To increase the radius R1, for example, in the HV connector system disclosed in PTL 1, the HV connector assembly includes a Faraday cup disposed to surround the HV conductor. According to PTL 1, “one advantage of the present invention is that the Faraday cup provides substantial local field relief in the vicinity of HV wire junctions, thereby reducing partial discharge activity”.
In the HV connector system described in PTL 1, for example, by placing a Faraday cup so that the cup covers the HV conductor, the diameter of the inner peripheral portion, which is the HV voltage, is expanded, thereby reducing the concentration of the electric field to a certain extent. However, the technique described in PTL 1 still has an undesirable characteristic, that is, the closer to the center of the axis, the greater the value of the electric field.
An object of the present invention is to provide a high-voltage insulating structure, a charged particle gun and a charged particle beam device capable of reducing an electric field around an electrically conductive part to which a high voltage is applied.
The following briefly explains the outline of a representative example of the invention disclosed in the present application.
A high-voltage insulating structure according to a representative embodiment of the present invention is a high-voltage insulating structure in which an electrically conductive part, to which a high voltage is applied and which extends in an axial direction, is surrounded by an insulator, in which
The effect obtained by a representative example of the invention disclosed in the present application will be briefly described as follows.
That is, according to a representative embodiment of the present invention, a structure having good insulating properties against high voltage is obtained. Such a high-voltage insulating structure is capable of reducing an electric field around an electrically conductive part positioned at the center of the axis and minimizing the possibility of occurrence of partial discharge.
Hereinafter, embodiments of the present invention will be described with reference to the drawings. Each of the embodiments described below is an example for implementing the present invention, and are not to be construed as limiting the technical scope of the present invention. Throughout the embodiments, the members having the same functions are designated by the same reference numerals, and the repeated description thereof will be omitted unless particularly necessary.
First, an example of a charged particle beam device commonly applied to each embodiment will be described with reference to
As shown in
In the transmission electron microscope, the electron gun 101 includes a metal housing 104, and a first insulator 105, a cathode 106, an electron source 107, and an anode 108 that are provided in the metal housing 104. The electron gun 101 also includes an HV cable 103 and an HV connector 102 for introducing a high voltage (HV) output from the high voltage power supply 1007 into the metal housing 104 and applying the HV to the electron source (the cathode 106 and the electron source 107 in the present example).
Of the above, the cathode 106 and the electron source 107 form a part of the conductor positioned at the center of the axis of the electron gun 101 and are electrically insulated from the metal housing 104 forming ground voltage. The cathode 106 is electrically connected to the HV cable 103 and the HV connector 102, and is applied with a high voltage (HV) generated by the high voltage power supply 1007, to accelerate the electron beam (charged particle beam) emitted from the high-temperature electron source 107 toward the anode 108. Other configurations and features of the electron gun 101 will be described below with reference to
In the transmission electron microscope shown in
In such a transmission electron microscope (charged particle beam device), it is important to not only prevent the occurrence of discharges that destroy the electron gun 101, but also prevent minute discharges that may impair electron gun performance. Specifically, for example, when a minute discharge is generated in the metal housing 104, there is a concern that the electron beam 109 output from the electron gun 101 and the image of the electron microscope image of the sample 1001 detected by the detector 1006 may be distorted or the resolution may be degraded.
Next, a specific configuration example of the electron gun 101 for solving the problem described above will be described below with reference to
In the electron gun 101, a negative high voltage (HV voltage) of several kV to several hundreds of kV is applied to the cathode 106 and the electron source 107, generating a voltage difference corresponding to the HV voltage with respect to the anode 108 which is the ground voltage. The inside of the electron gun 101 is vacuum, and the electron beam 109 emitted from the electron source 107 is accelerated by the voltage difference and emitted toward the anode 108 without colliding with gas molecules in the space. The HV voltage is supplied to the cathode 106 and the electron source 107 through the HV cable 103, the HV connector 102 and a conductor embedded within the first insulator 105. In general, the HV connector 102 and the metal housing 104 are in separable structures to improve workability when replacing the electron source 107 or when baking to reduce the internal pressure of the electron gun 101.
For example, one of the conductors 201 and 204 is convex-shaped and the other is concave-shaped, such that when the HV connector 102 and the metal housing 104 are connected to each other, the conductors 201 and 204 are stably contacted and electrically as the convex-shaped conductor is inserted into the concave-shaped conductor. Although not shown in
The HV voltage portion and the ground voltage portion are electrically insulated by the first insulator 105, the second insulator 203 and the gasket 205. The first insulator 105 and the second insulator 203 are made of epoxy resin or ceramic, for example, and have a high electrical insulation performance with an electrical resistivity of about 1014 to 1018 Ωcm. The gasket 205 is also a material having electrical insulation performance, and an elastic insulating material such as rubber is used to ensure and increase the adhesion at the joining portion.
Referring to
In the first embodiment shown in
In other words, the second insulator 203 is positioned on the opposite side from the first insulator 105 to face the same in the axial direction, that is, in the direction in which the electrically conductive part extends. The gasket 205 is provided to be interposed between the first insulator 105 and the second insulator 203 in the axial direction (in the vertical direction).
In the first embodiment of the present disclosure, the gasket 205 serves as a third insulator and is made of a material having a lower electrical resistivity than the surrounding insulators, that is, the first insulator 105 and the second insulator 203. For example, when the electrical resistivity of the first and second insulators 105 and 203 is about 1014 to 1018 Ωcm, the gasket 205 is made of a material with an electrical resistivity lower than 1014 Ωcm. Examples of such material include chloroprene (neoprene) rubber having an electrical resistivity of 1010 to 1012 Ωcm.
Generally, according to the related art, it is believed that, from the viewpoint of high withstand voltage, the gasket interposed in the connecting portion between the first insulator 105 and the second insulator 203 should be made of a material having as high electrical resistivity as possible, and such a configuration has been used in practice.
On the other hand, in the related-art configuration described above, while it is possible to prevent a discharge due to a large current that would destroy the electron gun, it is considered difficult to prevent other discharges, that is, local or partial discharges (hereinafter referred to as “partial discharges”), which may affect the performance of the electron gun.
As a result of various studies and experiments on the structure of electron guns, the present inventors have thought the opposite the related way, that is, the inventors have found that it is better to make the electrical resistivity of the gasket lower than that of the surrounding insulators 105 and 203 to prevent the partial discharges while preventing discharge due to large current. Moreover, to obtain such an effect, the inventors have found that it is necessary to make the thickness of the gasket different at an inner diameter side and an outer diameter side as follows.
In the present disclosure, the gasket 205 is configured such that a first thickness at the outer diameter side is less than a second thickness at the inner diameter side. More specifically, the gasket 205 of the first embodiment has a tapered shape in which the thickness is continuously reduced in a radial direction from the portion with the second thickness to the portion with the first thickness. Although not shown, as another example, the gasket 205 may be configured such that the thickness decreases stepwise (for example, in a stepped or wavy cross-sectional shape) in the radial direction from the portion with the second thickness to the portion with the first thickness. Alternatively, the thickness may change in a curved line from the portion with the second thickness to the portion with the first thickness. Between the first thickness and the second thickness, there may be a flat area where the thickness does not change.
The inventors of the present invention have found that, with the configuration described above, the partial discharge generated from the conductor 201 or the Faraday cup 202 inside the metal housing 104 can be significantly prevented by the action of the gasket 205 (electrical properties of the third insulator).
As described above, according to the configuration that the gasket 205 has different thicknesses at the outer diameter side and the inner diameter side, it is desirable that the surfaces of the first insulator 105 and the second insulator 203 that come into contact with the gasket 205 are processed into shapes that follow the shape of the gasket 205. For example, in the example shown in
As shown in
As described above, since the surfaces of the first and second insulators 105 and 203 holding the gasket 205 (the upper and lower surfaces contacting the gasket 205) are formed into the surface shapes corresponding to the shapes of the corresponding contact surfaces (the lower and upper surfaces) of the gasket 205, the original shape of the gasket 205 can maintain the original shape even when it is pressed and held. Therefore, the gasket 205 and the insulators 105 and 203 can be brought into close contact with each other to improve electrical insulation performance.
As the comparison of
Here, the difference between the first embodiment and the related-art configuration will be described in more detail with reference to
The difference in effect is more clearly demonstrated in the electric field graph shown in
The effect of reducing the electric field concentration described above can be achieved by the following characteristics of the present disclosure.
Characteristic 1: By using a material with a lower electrical resistivity than the surrounding insulator as the third insulator (gasket in the present example), a minute current (leakage current) that inevitably leaks from the electrically conductive part during operation of the electron gun preferentially flows through the third insulator (gasket).
Characteristic 2: By making the outer diameter side thickness of the third insulator (gasket) less than the inner diameter side thickness thereof, the resistance value per unit distance in the radial direction of the third insulator (gasket) is controlled to equalize the current density of the leakage current shown in
As described above, according to the electron gun 101 and the transmission electron microscope of the present disclosure, by smoothing the distribution of the electric field generated over the radial direction of the third insulator (gasket), it is possible to reduce the local concentration of the electric field, thereby reducing the occurrence of undesirable partial discharges. As a resultant effect, the electric field on the surface of the third insulator (gasket) can be reduced, such that the grease applied to improve the withstand voltage performance can be removed, thereby eliminating the assembly process of applying grease, and improvement in maintainability can also be expected.
In the second embodiment of the present disclosure, modifications of each part included in the electron gun 101 will be described. Since other configurations are the same as that of the first embodiment, differences from the first embodiment will be mainly described below.
For example, in the configuration example of the second embodiment shown in
By placing the additional gasket as such, there is provided an advantageous effect that it is not necessary to process the insulator forming the HV connector 102 or the metal housing 104 into a tapered shape or the like, while maintaining the same effects as in the first embodiment. Therefore, cost reduction in the manufacturing process of the electron gun 101 can be achieved.
In the third embodiment of the present disclosure, a modification of each part included in the electron gun 101 will be described. Since other configurations are the same as those of the first embodiment, differences from the first embodiment will be mainly described below.
On the other hand, a gasket 801 used in the third embodiment has a third thickness that is less than the first thickness between a second thickness at the inner diameter side and a first thickness at the outer diameter side that is less than the second thickness, as shown in
The thickness of the gasket 801 between the first thickness and the third thickness and between the second thickness and the third thickness changes continuously in the radial direction. Although not shown, as another example, the gasket 801 may be configured such that the thickness between the first thickness and the third thickness and the thickness between the second thickness and the third thickness changes stepwise (for example, in a cross-sectional shape such as a stepped shape or a wavy shape) in the radial direction. Various modifications such as those described in the first embodiment can be adopted for the mode of change in thickness.
In the example shown in
Therefore, according to the third embodiment, by biasing the electric field to the middle portion of the gasket where partial discharge is generally less likely to occur, it is possible to further reduce the electric field at both ends of the gasket which become relatively prone to partial discharge. In the third embodiment, although an example in which there are three extreme points of variation in the thickness of the gasket (third insulator) has been described, as another example, the gasket may be configured such that there are four or more extreme points of variation in thickness.
Note that the present invention is not limited to the first, second, and third embodiments described above, and includes various modifications. For example, the embodiments described above have been described in detail with respect to electron guns specifically adapted to the field of electron microscopy for ease of understanding of the present invention. Accordingly, the present invention is not necessarily limited to having all the configurations described herein. A part of the configuration of an embodiment can be replaced with the configuration of another embodiment, and the configuration of another embodiment can be added to the configuration of an embodiment.
The configuration of the third insulator in the embodiment described above can be applied not only to an electron gun of an X-ray device, but also to a gas insulating device described in, for example, JP2007-14070A. Specifically, the configuration of the third insulator described above can be applied to an “insulating spacer” attached to a high voltage conductor in a closed container filled with an insulating gas in gas-insulated electrical equipment. Here, the insulating gas corresponds to both the first insulator and the second insulator described above, and the third insulator need not be a plate-like member or an elastic member. From another aspect, the phases of the first insulator and the second insulator are not particularly limited and may be solid, gaseous or liquid. The phase of the third insulator is also not necessarily solid. For example, when the first insulator and the second insulator are solid, the third insulator may be liquid or gas as well as solid.
Filing Document | Filing Date | Country | Kind |
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PCT/JP2021/018601 | 5/17/2021 | WO |