Fabrication method of semiconductor integrated circuit device

Abstract
At the time of performing resin molding for a matrix frame in the fabrication of semiconductor integrated circuit devices, a predetermined amount of air is fed into each of first cavities in a first row and second cavities in a second row, the first and second cavities being formed in a matrix arrangement in a lower mold of a molding die, so as to pressurize the interiors of the cavities, and a sealing resin is charged into the cavities, while the pressure therein is regulated in such a manner that the charging speeds of the sealing resin become equal in all of the cavities, whereby it is possible to stabilize the quality of the product being obtained.
Description




BACKGROUND OF THE INVENTION




The present invention relates to a technique for use in fabricating a semiconductor integrated circuit device, and, more particularly, to a technique which is effective when applied to resin molding in an assembly using a matrix frame.




Resin molding techniques are described, for example, in Japanese Unexamined Patent Publication Nos. 2000-68305, Hei 11(1999)-297731, and 2000-164615.




Unexamined Patent Publication No. 2000-68305 discloses a technique in which the interior of a cavity is pressure-reduced prior to injection of resin into the cavity then, the cavity is pressurized almost simultaneously with the entry of the resin into the cavity and, thereafter, is pressure-reduced.




Unexamined Patent Publication No. Hei 11(1999)-297731, discloses a technique in which resin is charged into a cavity while pressurizing the interior of the cavity through air vents.




Unexamined Patent Publication No. 2000-164615, discloses a technique in which an air bleeder is formed in a press and cut relief plane of a resin sealing die, and residual air in a cavity and gas issuing from the molten resin are discharged to the exterior through the air bleeder.




SUMMARY OF THE INVENTION




If resin molding is performed in an assembly using a matrix frame, the charging speed of sealing resin differs between a first row of cavities located close to the pots of a molding die and a second row of cavities more widely spaced therefrom, the cavities being arranged in a matrix form, thus giving rise to the problem that the quality of the resulting product is deteriorated. That is, since the distance of the second row of cavities from the pots is longer than that of the first row of cavities, the resin charging speed for the second row of cavities is lower than that for the first row of cavities, thus leading to the deterioration of the quality of the produced product.




It is an object of the present invention to provide a method of fabricating a semiconductor integrated circuit device, which method can attain stabilization of the product quality.




It is another object of the present invention to provide a method of fabricating a semiconductor integrated circuit device, which method provides for an improvement in the freedom in developing a resin material of a sealing resin.




It is a further object of the present invention to provide a method of fabricating a semiconductor integrated circuit device, which method provides an improvement in the freedom of assembling conditions.




It is a still further object of the present invention to provide a method of fabricating a semiconductor integrated circuit device, which method can attain a reduction in the manufacturing cost.




The above and other objects and novel features of the present invention will become apparent from the following description and the accompanying drawings.




As to typical examples of in the present invention, a brief description will be given below.




In accordance with the present invention, the interiors of cavities arranged in a matrix form are pressurized and charged with a sealing resin in such a manner that the resin is charged at the same speed for all of the cavities.




Other more specific examples of the present invention will be described below:




1. A method of fabricating a semiconductor integrated circuit device, comprises the steps of:




(a) providing a lead frame on which plural device forming regions are arranged in a matrix form, the device forming regions each having a chip mounting portion and plural leads;




(b) mounting semiconductor chips, respectively, onto the chip mounting portions of the lead frame;




(c) disposing the lead frame with the semiconductor chips mounted thereon on a mold surface of a molding die, which mold surface includes cavities, and thereafter closing the molding die;




(d) pressurizing the interiors of the matrix cavities at a pressure in the range from 1 to 10 kg/cm


2


and charging a sealing resin into the thus-pressurized cavities; and




(e) after the step (d), dividing the lead frame into individual device forming regions.




2. A method of fabricating a semiconductor integrated circuit device, comprises the steps of:




(a) providing a multi-chip substrate on which plural device forming regions are arranged in a matrix form, the device forming regions each having a chip mounting region and plural leads;




(b) mounting semiconductor chips, respectively, onto the chip mounting regions of the multi-chip substrate, the semiconductor chips each having a thickness of 220 μm or less;




(c) disposing the multi-chip substrate with the semiconductor chips mounted thereon on a mold surface of a molding die, which mold surface includes a single cavity, and thereafter closing the molding die, while allowing the single cavity to cover all of the plural device forming regions;




(d) pressurizing the interior of the cavity, and charging a sealing resin into the thus-pressurized cavity; and




(e) after the step (d), dividing the multi-chip substrate into individual device forming regions.











BRIEF DESCRIPTION OF THE DRAWINGS





FIG. 1

is a plan view showing a structural example of a semiconductor integrated circuit device, which is assembled by a semiconductor integrated circuit device fabricating method according to a first embodiment of the present invention;





FIG. 2

is a side view of the device of

FIG. 1

;





FIG. 3

is a sectional view of the device of

FIG. 1

;





FIG. 4

is a constructional block diagram showing the structure of a back pressure supply system used in the semiconductor integrated circuit device fabricating method of the first embodiment, and also showing an example of a state of connection with a molding die;





FIG. 5

is a partial plan view showing a structural example of a matrix frame as used in the semiconductor integrated circuit device fabricating method of the first embodiment;





FIG. 6

is a plan view showing a structural example of an upper mold in a molding die used in the semiconductor integrated circuit device fabricating method of the first embodiment;





FIG. 7

is a plan view showing a structural example of a lower mold in the molding die used in the semiconductor integrated circuit device fabricating method of the first embodiment;





FIG. 8

is a timing chart showing an example of the timing of molding die operations and back pressure feed operations of the back pressure supply system in a molding step in the semiconductor integrated circuit device fabricating method of the first embodiment;





FIG. 9

is a diagrammatic plan view showing an example of a cavity pressurizing state in the molding step;





FIG. 10

is a diagrammatic plan view showing an example of a resin filled state of cavities in the molding step;





FIG. 11

is a diagrammatic plan view showing an example of a pressure reduction start timing (fastest) in the molding step;





FIG. 12

is a diagrammatic plan view showing an example of a pressure reduction start timing (slowest) in the molding step;





FIG. 13

is a partial plan view showing the structure of a matrix frame according to a modification of the first embodiment;





FIG. 14

is a diagrammatic plan view showing the structure of an upper mold according to a modification of the molding die used in the first embodiment;





FIG. 15

is a diagrammatic plan view showing the structure of a lower mold according to a modification of the molding die used in the first embodiment;





FIG. 16

is a diagrammatic partial sectional view showing a back pressure adjusting method according to a modification in the molding step adopted in the first embodiment;





FIG. 17

is a diagrammatic partial sectional view showing a back pressure adjusting method according to a modification in the molding step adopted in the first embodiment;





FIG. 18

is a sectional view showing a structural example of a semiconductor integrated circuit device assembled by a semiconductor integrated circuit device fabricating method according to a second embodiment of the present invention;





FIG. 19

is a diagrammatic plan view showing a structural example of an upper mold in a molding die used in the semiconductor integrated circuit device fabricating method of the second embodiment;





FIG. 20

is a diagrammatic plan view showing a structural example of a lower mold in the molding die used in the semiconductor integrated circuit device fabricating method of the second embodiment;





FIG. 21

is a diagrammatic plan view showing a structural example of a multi-chip substrate used in the semiconductor integrated circuit device fabricating method of the second embodiment;





FIG. 22

is a diagrammatic plan view showing a structural example after resin molding in the semiconductor integrated circuit device fabricating method of the second embodiment;





FIG. 23

is a diagrammatic plan view showing an example of a dicing line used in dividing the multi-chip substrate into individual chips after resin molding in the semiconductor integrated circuit device fabricating method of the second embodiment;





FIG. 24

is a diagrammatic plan view showing a structural example of runner and culls after resin molding in the semiconductor integrated circuit device fabricating method of the second embodiment;





FIG. 25

is a diagrammatic top plan view showing a structural example after the division into individual chips in the semiconductor integrated circuit device fabricating method of the second embodiment;





FIG. 26

is a diagrammatic bottom view showing a structural example after the division into individual chips in the semiconductor integrated circuit device fabricating method of the second embodiment;





FIG. 27

is a diagrammatic plan view showing a structural example of a multi-chip substrate after the mounting of chips thereon in the semiconductor integrated circuit device fabricating method of the second embodiment; and





FIG. 28

is a diagrammatic plan view showing an example of a resin filled state of the multi-chip substrate illustrated in FIG.


27


.











DETAILED DESCRIPTION OF THE PREFERRED EMBODIMENTS




Various embodiments of the present invention will be described in detail hereinunder with reference to the accompanying drawings.




In the following description of the embodiments, if necessary for convenience sake, a description of the subject matter will be given in a divided manner in plural sections or embodiments, but unless otherwise mentioned, they are not unrelated to each other, but are in a relation such that one is a modification, represents details, or is a supplementary explanation, of a part or the whole of the other.




In the following description of the embodiments, when reference is made, for example, to a number of elements (including the number, numerical values, quantities, and ranges), it is to be understood that no limitation is placed on the specific number referred to, but that numbers above and below the specific number are also employable, unless otherwise specified, and except for the case where a limitation is placed on a specific number basically obviously.




In the following description of the embodiments, it goes without saying that the constituent elements thereof (including element steps) are not always essential unless otherwise specified, and except for the case where they are considered essential basically obviously.




In the following description of the embodiments, when reference is made, for example, to the shapes and positional relations of constituent elements or the like, it is to be understood that those substantially similar or closely similar to the said shapes, etc. are also included, unless otherwise specified, and except for the case where they are not so considered basically obviously.




In all of the drawings, components having the same functions are identified by like reference numerals and repeated explanations thereof will be omitted.




First Embodiment




A first embodiment of the present invention will be described with reference to

FIGS. 1-17

of the accompanying drawings.




The semiconductor integrated circuit device fabricating method of this first embodiment is a method for assembling a thin QFP (Quad Flat Package)


1


, such as shown in

FIGS. 1

,


2


, and


3


.




The QFP


1


is made up of a semiconductor chip


4


having a semiconductor integrated circuit; plural inner leads (leads)


2




a


arranged radially around the semiconductor chip


4


; plural wires (fine wires)


5


, such as gold wires, for connection between bonding electrodes


4




b


, which serve as surface electrodes formed on a main surface


4




a


of the semiconductor chip


4


, and the inner leads


2




a


corresponding thereto; a tab (chip mounting portion)


2




c


to which the semiconductor chip


4


is fixed through a die bonding material; a seal member


3


formed by resin molding to seal both the semiconductor chip


4


and the plural wires


5


; and plural outer leads


2




b


formed integrally with the inner leads


2




a


and projecting outwards from the seal member


3


.




The QFP


1


of this first embodiment is a thin type package in which the thickness of the seal member


3


is, for example, 1.2 mm or less. For example, the wires


5


comprise gold wires of 30 μm or less in diameter, and the plural bonding electrodes


4




b


formed on the main surface


4




a


of the semiconductor chip


4


are arranged at a pitch of 65 μm or less, for example. According to this construction it is possible to attain a QFP


1


having a multi-pin structure. That is, by thinning the wire diameter and narrowing the pad pitch, it is possible to attain a QFP


1


having a multi-chip structure or to achieve chip-shrinkage of the QFP


1


.




As to the thickness, wire diameter and pad pitch in the QFP


1


, no limitation is placed on the above ranges, but even those various outside the above ranges are also employable. The inner leads


2




a


, outer leads


2




b


and tab


2




c


are formed using a thin plate of copper alloy or iron-nickel alloy, for example. The seal member


3


is formed by molding an epoxy resin, for example.




Next, a description will be given concerning a back pressure supply system, as shown in

FIG. 4

, which is used in a resin sealing step in assembling the QFP


1


of this first embodiment.




The back pressure supply system, indicated at


23


, is connected to a molding die


6


in molding equipment so as to apply or reduce the pressure within the cavities of the molding die


6


in a resin molding step.




In the back pressure supply system


23


, mainly, there are provided regulators (mist separator combination)


11


, pressure intensifying valves (air tank combination)


12


, solenoid valves


13




a


and


13




b


, exhaust valves


14




a


and


14




b


for atmospheric pressure exhaust, exhaust valves


17




a


and


17




b


for vacuum exhaust, silencers


15


and


21


, pressure gauges


16


and


19


, vacuum regulators


18


, a vacuum pump


20


, and a sequencer


22


.




In the molding die


6


, first cavities


7




a


in a first row arranged on a side close to pots


8




d


(see

FIG. 7

) and second cavities


7




b


in a second row arranged on a side remote from the pots


8




d


have separate pressurizing/reducing systems corresponding to the matrix frame (lead frame)


2


shown in

FIG. 5

, so that each system operates independently in the first and second cavities


7




a


,


7




b


, thereby to make it is possible to individually control the amounts of pressurization and pressure reduction in the cavities of each row.




As shown in

FIG. 4

, using factory air


32


as an initial pressure, a predetermined amount of air


9


is fed from the back pressure supply system


23


to the first and second cavities


7




a


,


7




b


in the molding die


6


by means of the pressure intensifying valves


12


or the vacuum pump


20


.




At this time, the amount of air


9


to be pressurized is set such that a back pressure


28


acting as a flow resistance to the sealing resin


10


becomes a preset value. The flow, i.e., charging speed, of the sealing resin


10


is controlled by adjusting the amount of air


9


to be pressurized so as to adjust the back pressure


28


against a resin injection pressure


27


.




For example, the first row of cavities have a higher resin charging speed than the second row of cavities; and, therefore, the interior of each cavity is pressurized at a predetermined pressure (a pressure of a magnitude capable of delaying the charging speed of the sealing resin


10


in the first row of cavities) to delay the resin charging speed in the first row, so that the charging speed of the sealing resin


10


in a first row cavity and that in a second row cavity become almost equal to each other.




That is, in the first and second rows of cavities, in order to mitigate instability, uncontrollability, and oversensitivity to external factors, of the resin front caused by the injection of the sealing resin


10


in a strong dynamic imbalance state, a dynamic imbalance at the resin interface is weakened by increasing the back pressure to the sealing resin


10


. The interiors of the first and second cavities


7




a


,


7




b


are pressurized so that the charging speed of the sealing resin


10


in the first row cavities and that in the second row cavities become equal to each other.




Therefore, if the preset back pressure


28


is applied into each cavity at the time of resin filling, the charging speed of the sealing resin


10


in the first cavities


7




a


of the first row, which charging speed is high in an unpressurized stage, becomes low and equal to the charging speed of the sealing resin


10


in the second cavities


7




b


of the second row, which charging speed is low in an unpressurized state.




The air supply systems for the first and second cavities


7




a


,


7




b


in the molding die


6


are independent, and so the back pressure


28


can be set independently for each of both systems. A back pressure


28


of a magnitude not larger than the initial pressure can also be set by the regulators


11


. Further, it is possible to set the pressure from positive to negative by the selection of intensifying valves


12


and vacuum pump


20


.




The solenoid valves


13




a


,


13




b


, exhaust valves


14




a


,


14




b


, and exhaust valves


17




a


,


17




b


each can be controlled independently by the sequencer


22


. With signals received by the sequencer


22


from the molding equipment in which the molding die


6


is provided, it is possible to set the opening/closing timings of the solenoid valves


13




a


,


13




b


, exhaust valves


14




a


,


14




b


, and exhaust valves


17




a


,


17




b


in accordance with the operations of the molding equipment.




Further, data from the pressure gauges


16


can be monitored or analyzed using a personal computer or the like through the sequencer


22


. The pressure gauges


16


may be replaced by pressure sensors buried in the cavities.




The following description is directed to a method of fabricating the semiconductor integrated circuit device (QFP


1


) of this first embodiment.




First, the matrix frame


2


shown in

FIG. 5

is provided. This matrix frame


2


has plural device regions (device forming regions)


2




d


each for forming one QFP


1


, the device regions


2




d


being arranged in a matrix form of plural rows×plural columns. Each device region


2




d


has a tab (chip mounting portion)


2




c


, inner leads (leads)


2




a


, and outer leads (leads)


2




b.






A gate resin sump portion


2




f


, corresponding to each gate


8




f


in the molding die


6


, is formed at one corner portion of each device region


2




d


. For example, the matrix frame


2


is formed using a thin plate of copper alloy.




Thereafter, semiconductor chips


4


are mounted, respectively, onto the tabs


2




c


of the matrix frame


2


through a die bonding material. In this case, if the QFP


1


is to attain a multi-pin structure, it is preferable that bonding electrodes


4




b


on the main surface


4




a


of each semiconductor chip


4


be formed at a mounting pitch of 65 μm or less.




Subsequently, wire bonding is performed. More specifically, the bonding electrodes


4




b


on each semiconductor chip


4


and corresponding inner leads


2




a


are connected together through wires


5


. In the case where the QFP


1


is to attain a multi-pin structure, it is preferable that gold wires having a diameter of 30 μm or less, for example, be used as the wires


5


.




Thereafter, resin molding is performed. Here reference will first be made to the structure of the molding die


6


in the molding equipment for assembling the QFP


1


.





FIG. 6

shows the mold surface


7




g


of an upper mold


7


in the molding die


6


. Five first cavities


7




a


are arranged as cavities in the first row, and, likewise, five second cavities


7




b


are arranged as cavities in the second row, all of the cavities being arranged in a matrix form corresponding to the matrix frame


2


. There are culls


7




d


, corresponding to pots


8




d


of a lower mold


8


shown in

FIG. 7

, and a runner


7




e


serving as a resin flow path to the culls


7




d


. Further, in each of the first and second cavities


7




a


,


7




b


, air vents


7




c


are formed in three corners, but not in the corner corresponding to each gate


8




f


in the lower mold


8


.





FIG. 7

shows the mold surface


8




i


of the lower mold


8


in the molding die


6


. Five first cavities


8




a


are arranged as cavities in the first row, and, likewise, five second cavities


8




b


are arranged as cavities in the second row, all of the cavities being arranged in a matrix form as in the case of the upper mold


7


. Further, there are pots


8




d


, sub-runners


8




e


and air vents


8




c


, as well as plural suction holes


8




g


for effecting the application and reduction of pressure. The suction holes


8




g


are arranged adjacent to the first and second cavities


8




a


,


8




b


in correspondence therewith. In the example of the lower mold


8


, as shown in

FIG. 7

, two suction holes


8




g


are formed for each cavity.




For the application or reduction of pressure in each cavity, air


9


is fed from the suction holes


8




g


, or air is exhausted therefrom. In this first embodiment, therefore, the application or reduction of pressure in each cavity can be effected by performing, for each cavity, a supplying or exhausting of air


9


through the suction holes


8




g.






A ring-like packing


8




h


is buried around the periphery of the region including the pots B


d


, the cavities and the plural suction holes


8




g


, so that the molding region is hermetically closed upon closure of both the upper and lower molds


7


,


8


.




The application of pressure in each cavity is performed by the supply of air


9


through air vents


7




c


and


8




c


, which are in communication with the cavity, while the reduction of pressure in each cavity is performed by the exhausting of air


9


through the air vents


7




c


and


8




c.






Within each pot


8




d


, there is disposed a plunger


8




j


, as shown in

FIG. 8

, for extruding the sealing resin


10


in a molten condition. Resin molding is carried out using the molding die


6


thus constructed.




Resin molding will now be described with reference to the time chart of FIG.


8


.

FIG. 8

shows an example of the preferred operation times and the operation time tolerances of the plungers


8




j


, solenoid valves


13




a


,


13




b


, and exhaust valves


14




a


,


14




b


,


17




a


,


17




b.






First, the matrix frame


2


, with semiconductor chips


4


mounted thereon, and which has gone through wire bonding, is disposed on the mold surface


8




i


of the lower mold


8


in the molding die


6


; and, then, the upper and lower molds


7


,


8


are closed, thereby to clamp the matrix frame, as indicated by the molding operations in FIG.


8


.




After making sure that the mold has been clamped, a plunger operation is started to inject the sealing resin


10


into each cavity. At this time, according to this first embodiment, as shown in

FIG. 9

, the interiors of the first and second cavities


8




a


,


8




b


in the first and second rows, respectively, in the matrix arrangement are pressurized at a predetermined pressure, and the sealing resin


10


is charged into the cavities so as to achieve the same charging speed in all of the cavities.




To be more specific, a predetermined amount of air


9


is fed into the first and second cavities from the air vents


7




c


through the suction holes


8




g


, thereby making the charging speed of sealing resin


10


equal in the first and second rows of cavities. The application of pressure into each cavity is performed by opening/closing operations of the solenoid valves


13




a


and


13




b


in accordance with the solenoid valve operation shown in FIG.


8


.




First, as shown in

FIG. 8

, when a plunger


8




j


begins to move upward from below, the sealing resin


10


in a molten condition begins to be extruded. In this first embodiment, however, it is preferable that the interior of each cavity be held in a state in which it is at atmospheric pressure until the molten sealing resin


10


reaches the gates


8




f


in the molding die


6


. By the state of atmospheric pressure, it is meant that the internal pressure of each cavity is made almost equal to the pressure present outside the molding die


6


, i.e., a state free of a difference in pressure between the interior and the exterior. In other words, it means that the interior of each cavity is maintained in a state free of any intentional application or reduction of pressure. For example, this requirement is satisfied if the interior of each cavity is open to the atmosphere before the mold is clamped, and if neither the application nor reduction of pressure is performed until the sealing resin


10


reaches the gates


8




f.






A pressure value indicating the state of atmospheric pressure is 1 Atm, for example, but the tolerance thereof is about 0.5 to 1.5 Atm.




By thus performing neither pressurization nor pressure reduction in each cavity until the arrival of the sealing resin


10


at the gates


8




f


, it is possible to prevent the inclusion of air in the sealing resin within culls


7




d


during the rising motion of the plungers


8




j


, whereby it is possible to prevent the formation of voids in the sealing resin


10


and the seal member


3


.




To be more specific, if air


9


enters into a cull


7




d


under pressure at the operation start point of the associated plunger


8




j


((A) in the state of resin fill in FIG.


8


), then after operation of the plunger


8




j


, the sealing resin


10


, which has entered the cull


7




d


, will have included therein air


9


at a high pressure, resulting in voids being formed within the sealing resin. At this time, the high-pressure air


9


is difficult to crush and is apt to remain. On the other hand, in the case of air


9


of atmospheric pressure or the like, it can be crushed in response to the resin injection pressure; and, therefore, it is preferable to avoid pressurization in each cavity until arrival of the sealing resin


10


at the associated gate


8




f.






It is also preferable to avoid the reduction of pressure. This is because, if a reduction in the pressure occurs in the cavities after operation of the plungers


8




j


and before arrival of the sealing resin


10


at the gates


8




f


, the molten sealing resin is pulled toward the cavities within the culls


7




d


and air becomes included therein; and, the air


9


stays within the sealing resin


10


, resulting in voids being formed. Thus, by preventing a reduction in the pressure before arrival of the sealing resin


10


at the gates


8




f


, it is possible to prevent the formation of voids in the sealing resin or in the seal member


3


.




Next, a description will be given concerning the application of pressure in each cavity. The time taken from the start of movement of each plunger


8




j


until arrival thereof at an upper-limit position corresponds to the charging time of the sealing resin


10


, which charging time is about 8 to 20 seconds. Within this charging time, the solenoid valves


13




a


and


13




b


are opened and closed in accordance with the solenoid valve operation to start and stop the pressurization in each cavity.




In this case, the application of pressure is started when (B) in the state of resin fill is assumed, as seen in FIG.


8


. That is, the application of pressure is started substantially simultaneously with the start of entry of the molten sealing resin


10


into each cavity after arrival thereof at the associated gate


8




f


. As shown in

FIG. 8

, the time (T


1


) required from the plunger operation start point (A) up the pressurization start point (B) is about 3 to 10 seconds. Further, the time of operation (opening time) of the solenoid valves


13




a


and


13




b


, i.e., the pressurization time (T


2


) is about 2 to 100 seconds.




The above pressurization is carried out by the supply of air


9


, intentionally, into the cavities through air vents


7




c


and


8




c


, which are formed in communication with the cavities. The magnitude of the pressurization is, for example, 5 kg/cm


2


in terms of a mid value, ranging from 1 to 10 kg/cm


2


. The said numerical value indicates a pressure to be further added from the foregoing state of atmospheric pressure (for example, 1 Atm, tolerance: 0.5 to 1.5 Atm) in each cavity.




By thus setting the magnitude of pressurization in the range of 1 to 10 kg/cm


2


, it is not necessary to install a high pressure tank in the back pressure supply system


23


, and, hence, it is possible to avoid an increase in the size of the equipment. However, this pressurization magnitude range does not constitute any limitation, but an upper limit thereof may be larger than 10 kg/cm


2


in relation to the resin injection pressure.




In this way the charging of the sealing resin


10


is carried out under the supply of air


9


at a pressurization magnitude preferably in the range of 1 to 10 kg/cm


2


, while establishing a setting such that the charging speeds of the sealing resin in the cavities become almost equal in all the cavities.




To be more specific, if the interior of each cavity is pressurized in the range of 1 to 10 kg/cm


2


, the charging speeds of the sealing resin


10


in the first cavities


8




a


in the first row, which charging speeds are originally high, become low due to the back pressure


28


acting as a flow resistance, to the extent that there is scarcely any difference among the sealing resin charging speeds in the cavities. Consequently, it is possible to diminish variations in the state of resin fill among the cavities, and, hence, it is possible to stabilize the quality of the product, i.e., QFP


1


.




Moreover, in selecting the sealing resin


10


, it is possible to mitigate the limitation on its fluidity. More particularly, if there are different charging speeds among the cavities, a fluid sealing resin


10


is selected to match any of the cavities, thus resulting in a larger limitation in the selection of a sealing resin


10


. In this first embodiment, however, it is possible to diminish variations in the state of resin fill among the cavities, so that, in the selection of sealing resin


10


, it is possible to mitigate the limitation on its fluidity. As a result, it is possible to enhance the degree of freedom in the development of a sealing resin material.




Besides, since it is possible to mitigate the limitation on the fluidity of the sealing resin


10


in the selection of the same resin, it is no longer necessary to change the sealing resin according to the type of semiconductor integrated circuit device being produced, whereby the commonness of the sealing resin


10


can be enhanced.




Moreover, if there are different charging speeds among the cavities, the sealing resin


10


in cavities having a low charging speed becomes hard and is apt to cause wire deformation, and so it is necessary to establish molding conditions on the basis of cavities of low charging speeds. Thus, the assembling conditions are significantly limited. In this embodiment, however, since the commonness of the sealing resin


10


can be enhanced, it is possible to improve the freedom in establishing assembling conditions for the QFP


1


.




Further, if the charging speeds of the sealing resin


10


are almost equal between the first and second cavities


8




a


,


8




b


, the angle of formation of gates


8




f


in the first cavities


8




a


and that in the second cavities


8




b


can be made equal to each other without direction, so that it is possible to attain a desired shape of the molding die


6


easily, whereby it is possible to reduce not only the cost of the molding die


6


, but also the manufacturing cost of the QFP


1


.




Further, since the molding die


6


can be formed into a desired shape easily, it is possible to shorten the period required for the development of the QFP


1


.




Next, a description will be provided concerning the reduction of pressure in each cavity. As indicated at (C) in the state of resin fill, as seen in

FIG. 8

, the reduction of pressure is started after the stopping of pressurization in each cavity and before the completion of the charging of the sealing resin


10


into each cavity.




More specifically, the solenoid valves


13




a


and


13




b


are closed to stop the pressurization in each cavity and thereafter, before completion of the filling of sealing resin


10


into each cavity, the exhaust valves


14




a


and


14




b


, or the exhaust valves


17




a


and


17




b


, are opened to start the reduction of pressure.




The time (T


3


) taken from the stopping of pressurization until the start of pressure reduction is about 0 to 100 seconds. However, the stopping of pressurization and the start of pressure reduction may be substantially simultaneous.




In connection with pressure reduction start timings, a state of fill at the fastest timing and that at the slowest timing are shown in

FIG. 11

(fastest timing) and

FIG. 12

(slowest timing), respectively. As shown in

FIG. 11

, the fastest pressure reduction start timing corresponds to a time point at which the state of fill of the sealing resin


10


in each cavity has passed a half of the volume of the cavity. As shown in

FIG. 12

, the slowest pressure reduction start timing corresponds to a time point at which the filling of the sealing resin


10


in each cavity is about to end. Therefore, it is preferable that the reduction of pressure be started during the period from the time when the filling of the charging resin


10


in each cavity has passed a half of the cavity volume until just before completion of the filling.




By thus performing the pressure reduction, the air


9


which has entered each cavity with the application of pressure can be exhausted, and, hence, it is possible to prevent the air


9


from being included in the sealing resin


10


. As a result, it is possible to prevent voids from being formed in the seal member


3


of QFP


1


.




The reduction of pressure is stopped after the completion of resin filling, as shown at (D) in

FIG. 8

, and before opening the molding die


6


. Resin molding is now over. Then, the molding die


6


is opened and the matrix frame


2


is taken out from the die.




Subsequently, the matrix frame


2


is cut, device region


2




d


by device region


2




d


, into individual device regions. In this case, a frame portion


2




e


of the matrix frame


2


and the outer leads


2




b


in each device region are cut off from each other, and the outer leads


2




b


are bent in a gull wing shape. Now, the assembly of QFP


1


is over.




In this way, it is possible to assemble the QFP


1


having a thickness of the seal member


3


of not larger than 1.2 mm. Thus, the resin molding method of this first embodiment is effective in assembling a thin semiconductor package, such as a QFP


1


, having a thickness of the seal member


3


of not larger than 1.2 mm.




Reference is now made to the case where the molding die


6


is additionally provided with flow cavities (auxiliary recesses)


7




f


and


8




k


located respectively in an upper mold


7


and a lower mold


8


, according to the modifications illustrated in

FIGS. 14 and 15

. The flow cavities


7




f


and


8




k


are auxiliary recesses for retaining therein the air


9


extruded from the cavities, and they are each formed, for example, in a corner portion remote from the gate


8




f


in each cavity so as to be in communication with the cavity.




In the case of the upper mold


7


and lower mold


8


shown in

FIGS. 6 and 7

, respectively, the flow cavities


7




f


and


8




k


are not provided, so that, at the time of charging the sealing resin into each cavity, the air


9


present in the cavity is allowed to escape from only the air vents


7




c


and


8




c


that are in communication with the cavity. In contrast, the upper mold


7


and the lower mold


8


shown in

FIGS. 14 and 15

are provided with flow cavities


7




f


and


8




k


, respectively, so that in the matrix frame


2


used for the molding die


6


in question, as shown in

FIG. 13

, there are flow cavity resin sump portions


2




g


at positions corresponding to the flow cavities


7




f


and


8




k.






Thus, the upper mold


7


and the lower mold


8


shown in

FIGS. 6 and 7

are not provided with the flow cavities


7




f


and


8




k


, respectively, and, therefore, resin sump portions corresponding to the flow cavities


7




f


and


8




k


are not formed in the matrix frame


2


shown in

FIG. 5

, that is used as a frame for the molding die


6


in question.




By adopting an upper mold


7


and lower mold


8


in the molding die


6


, such as shown in

FIGS. 6 and 7

, which are not provided with flow cavities


7




f


and


8




k


, it is possible to save the amount of the sealing resin


10


being used in an amount corresponding to the resin buried in the flow cavities


7




f


and


8




k


, so that in comparison with the case of using the molding die


6


provided with flow cavities


7




f


and


8




k


, it is possible to attain resin-saving, and, hence, it is possible to reduce the manufacturing cost of the QFP


1


.




Besides, since a flow cavity resin portion is not formed on the seal member


3


, the cutting of the flow cavity resin portion is not needed, and, therefore, it is possible to supply the cutting step.




Moreover, in the molding die


6


that is not provided with flow cavities


7




f


and


8




k


, it is possible to form a resin flow passage easily, so that the molding die


6


can be easily formed in a desired shape, and so it is possible to reduce the manufacturing cost of the molding die


6


.




Further, in the molding die


6


that is not provided with flow cavities


7




f


and


8




k


, it is possible to use a matrix frame


2


that is not formed with flow cavity resin sump portions


2




g


, and, hence, it is possible to employ the lead frame in common and, thereby, decrease the number of lead frame types.




On the other hand, in the case of using a molding die


6


provided with flow cavities


7




f


and


8




k


, it is possible to let the air


9


that is present in each cavity remain in the flow cavities


7




f


and


8




k


, so that a sufficient amount of air


9


can be allowed to escape from the interior of each cavity, whereby the formation of voids can be prevented in a more positive manner.





FIGS. 16 and 17

show modifications of the method for adjusting the back pressure in each cavity by means different from the back pressure supply system


23


illustrated in FIG.


4


.




In

FIG. 16

, a piston


24


is operated by a drive source, such as a motor or air pressure, causing the volume of an air tank


25


to vary and, thereby, adjusting the back pressure


28


which acts as a flow resistance against the flow of the sealing resin


10


in each cavity. That is, the air in each cavity, which is discharged under the resin injection pressure


27


, is compressed into the air tank


25


, thereby affording the back pressure


28


.




On the other hand, in

FIG. 17

, the amount of air being discharged is throttled of a valve member


29


to adjust the back pressure


28


in each cavity. According to the illustrated method, the amount of air to be discharged, as indicated at


30


, is adjusted so as to become larger than the actual amount of air being discharged, as indicated at


31


, thereby changing the magnitude of the back pressure


28


. In this modification, the valve member


29


is provided in each of the air vents


7




c


,


8




c


to throttle the intra-cavity air discharged under the resin injection pressure


27


, thereby affording the back pressure


28


.




Also, by the methods for adjusting the back pressure


28


according to the modifications shown in

FIGS. 16 and 17

, it is possible to adjust the back pressure


28


in each cavity, and the same effects can be obtained as were obtained in the use of the back pressure supply system shown in FIG.


4


.




Second Embodiment





FIG. 18

is a sectional view showing a structural example of a semiconductor integrated circuit device that has been assembled by a semiconductor integrated circuit device fabricating method according to a second embodiment of the present invention;

FIG. 19

is a plan view showing a structural example of an upper mold in a molding die used in the semiconductor integrated circuit device fabricating method of the second embodiment;

FIG. 20

is a plan view showing a structural example of a lower mold in the molding die used in the semiconductor integrated circuit device fabricating method of the second embodiment;

FIG. 21

is a plan view showing a structural example of a multi-chip substrate used in the semiconductor integrated circuit device fabricating method of the second embodiment;

FIG. 22

is a plan view showing a structural example after resin molding in the semiconductor integrated circuit device fabricating method of the second embodiment;

FIG. 23

is a plan view showing an example of a dicing line used in dividing the multi-chip substrate into individual chips after resin molding in the semiconductor integrated circuit device fabricating method of the second embodiment;

FIG. 24

is a plan view showing a structural example of runner and culls, after resin molding, in the semiconductor integrated circuit device fabricating method of the second embodiment;

FIG. 25

is a plan view showing a structural example, after the division into individual chips, in the semiconductor integrated circuit device fabricating method of the second embodiment;

FIG. 26

is a bottom view showing a structural example, after the division into individual chips, in the semiconductor integrated circuit device of the second embodiment;

FIG. 27

is a plan view showing a structural example of a multi-chip substrate, after the mounting of chips thereon, in the semiconductor integrated circuit device fabricating method of the second embodiment; and

FIG. 28

is a plan view showing an example of a resin filled state of the multi-chip substrate illustrated in FIG.


27


.




This second embodiment is directed to a method of fabricating a CSP (chip size package)


43


, which is assembled using a multi-chip substrate


40


.




The CSP


43


shown in

FIG. 18

is a thin semiconductor package of a chip laminate type, and it comprises: a wiring substrate


41


, the wiring substrate


41


having a main surface


41




a


and a back side


41




b


, with a chip mounting region


40




b


, as shown in

FIG. 21

, and plural leads


41




c


serving as wiring lines being formed on the main surface


41




a


; two semiconductor chips


4


vertically stacked in the chip mounting region


40




b


on the main surface


41




a


of the wiring substrate


41


; plural wires


5


for connecting bonding electrodes


4




b


on each semiconductor chip


4


with corresponding leads


41




c


; a seal member


44


, which seals the two semiconductor chips


4


and plural wires


5


with resin; and plural solder balls


42


serving as external terminals provided on the back side


41




b


of the wiring substrate


41


.




The CSP


43


is a thin type package. The thickness of one semiconductor chip


4


is 220 μm or so, for example. In the CSP


43


, the thickness from the back side


41




b


of the wiring substrate


41


up to the surface of the seal member


44


is 1 mm or less, for example.




The CSP


43


is formed in the following manner. As seen in

FIG. 21

, there is a multi-chip substrate


40


having a main surface


40




a


, on which plural device regions (device forming regions)


40




c


, each having chip mounting region


40




b


, are formed in a matrix arrangement. In a resin molding step after wire bonding, the plural device regions


40




c


, that are arranged in a matrix form, are covered with a single cavity of a molding die


6


and are sealed, followed by block molding with resin (such a resin sealing method will hereinafter be referred to as “block molding”), and the substrate is subsequently diced into individual chips.




Next, a description will be given of the structure of an upper mold


7


, as shown in

FIG. 19

, and a lower mold


8


, as shown in

FIG. 20

, which are used in the resin molding step in the semiconductor integrated circuit device fabricating method of this second embodiment.




In the upper mold


7


shown in

FIG. 19

, there is a block molding cavity


7




h


which can cover the main surface


40




a


of the multi-chip substrate


40


. Around the block molding cavity


7




h


, there are plural air vents


7




c


, plural culls


7




d


, plural gates


7




i


, and plural suction holes


7




j


for back pressure and pressure reduction. The plural air vents


7




c


are provided around three sides of the block molding cavity


7




h


, which is quadrangular in shape, but they are not provided one side located close to the culls


7




d


. Further, the plural suction holes


7




j


are formed near the air vents


7




c


. Therefore, the supplying and exhausting of the air


9


at the time of application and reduction of pressure in the block molding cavity


7




h


can be performed in three directions in the cavity.




In the lower mold


8


, as shown in

FIG. 20

, there are one block molding cavity


8




l


and plural pots


8




d


. Further, a ring-like packing


8




h


is buried outside the block molding cavity


8




l


and the plural pots


8




d


. When the upper and lower molds


7


,


8


are closed to effect mold clamping, a hermetically sealed region capable of vacuum exhaust is formed by the packing


8




h.






Also, in the case of the molding die


6


used in this second embodiment, as is the case with the molding die


6


used in the first embodiment, a back pressure supply system


23


, such as shown in

FIG. 4

, is connected to the molding die. At the time of resin molding, therefore, the interiors of the block molding cavities


7




h


and


8




l


can be pressurized or pressure-reduced by the supplying or exhausting of air


9


to or from the cavities


7




h


and


8




l


from the air vents


7




c


through the suction holes


7




j.






Next, a description will be given as to how to fabricate the semiconductor integrated circuit device (CSP


43


) of this second embodiment.




First, a multi-chip substrate


40


, as shown in

FIG. 21

, is formed so as to have plural device regions


40




c


, each having a chip mounting region


40




b


and plural leads (wiring lines)


41




c


, formed in a matrix arrangement.




Thereafter, semiconductor chips


4


are mounted respectively through a die bonding material or the like onto the chip mounting regions


40




b


in the device regions


40




c


of the main surface


40




a


of the multi-chip substrate


40


. The CSP


43


of this second embodiment is a chip laminate type package. Here, the lower semiconductor chips


4


are first mounted, respectively, onto the chip mounting regions


40




b


in the device regions


40




c


, and, subsequently, the upper semiconductor chips


4


are mounted onto the lower semiconductor chips


4


.




In this case, since it is an objective for the CSP


43


to attain a reduced of thickness, it is preferable that the thickness of each semiconductor chip


4


be 220 μm or so, for example, provided no limitation is made thereto.




In assembling the CSP


43


, due to a defect in a certain device region


40




c


in the multi-chip substrate


40


, there sometimes is a case where a device region


40




c


that is incapable of forming the CSP


43


is included among the plural device regions


40




c


arranged in a matrix form. As to such a multi-chip substrate


40


, a semiconductor chip


4


is not mounted in the defective device region


40




c


, but semiconductor chips


4


are mounted in only non-defective device regions


40




c


, so that, in the assembling step after the end of chip mounting, as shown in

FIG. 27

, the multi-chip substrate


40


, in which one or more semiconductor chips


4


are missing, may flow through the subsequent step.




Thus, there can be a case where the multi-chip substrate


40


, after the mounting of chips, is in a state where there are device regions


40




c


with semiconductor chips


4


mounted therein and also device regions


40




c


with semiconductor chips


4


not mounted therein. In connection with such a multi-chip substrate


40


(the multi-chip substrate


40


which is in such a state will hereinafter be referred to as a “partial chip missing multi-chip substrate


40


”), after the mounting of chips in this second embodiment, reference will be made below to an assembling operation. It is to be understood, however, that the assembly of CSP


43


in this second embodiment is applicable not only to a partial chip missing multi-chip substrate


40


, but also to a multi-chip substrate


40


with semiconductor chips


4


mounted in all the device regions


40




c


on the main surface


40




a.






After the chips have been stacked, wire bonding is performed. To be more specific, bonding electrodes


4




b


that are formed on the lower semiconductor chip


4


and corresponding leads


41




c


are connected together through wires


5


. Likewise, bonding electrodes


4




b


that are formed on the upper semiconductor chip


4


and corresponding leads


41




c


are connected together through wires


5


. Thereafter, resin molding is performed.




Also, in the resin molding according to this second embodiment, as shown in the timing chart of

FIG. 8

, resin filling and the application and reduction of pressure in each cavity are performed in a timed sequence, but as to the timings of plunger operation, solenoid valve operation and exhaust valve operation, as well as the tolerances of the respective operation times, they may be just the same as in the first embodiment, or they may be changed according to various types, for example.




First, the multi-chip substrate


40


, in a partial chip missing state and after wire bonding, is placed on the lower mold


8


of the molding die


6


; then, the plural device regions


40




c


on the multi-chip substrate


40


are together covered with the single block molding cavity


7




h


of the upper mold


7


; and the upper and lower molds


7


,


8


of the molding die


6


are closed so as to clamp the substrate.




After making sure that the mold has been clamped, the plunger operation shown in

FIG. 8

is started so as inject the sealing resin


10


into the block molding cavities


7




h


and


8




l


. In this case, according to this second embodiment, as shown in

FIG. 28

, the sealing resin


10


is charged in such a manner that the charging speeds thereof for the plural semiconductor chips


4


, which are arranged in rows in a direction (longitudinal direction of the multi-chip substrate


40


) orthogonal to the resin injecting direction in the block molding cavities


7




h


and


8




l


on the multi-chip substrate


40


, become almost equal in the plural semiconductor chips arranged in a respective row.




More specifically, a predetermined amount of air


9


is fed from the plural air vents


7




c


during resin filling into the block molding cavities


7




h


and


8




l


to pressurize the interiors of the cavities, whereby a flow resistance of a nearly uniform magnitude can be imparted to the whole of the sealing resin


10


during resin filling, and the charging speeds of the sealing resin


10


for the plural semiconductor chips


4


arranged in rows in a direction orthogonal to the resin injecting direction become almost equal in the semiconductor chips arranged in a respective row, as shown in FIG.


28


.




The sealing resin


10


is injected into the block molding cavities


7




h


and


8




l


at a resin injection pressure of about 490 MPa (50 kg/cm


2


) or lower. By so doing, it is possible to prevent the occurrence of a chip cracking caused by the resin injection pressure, even in the case of a semiconductor chip


4


as thin as 220 μm or less.




After the pressurization, as in the first embodiment, the interiors of the block molding cavities


7




h


and


8




l


are pressure-reduced to prevent pressurized air from being included in the sealing resin


10


, thereby preventing the formation of voids.




In the resin molding performed in this second embodiment, as in the first embodiment, the pressure in the interiors of the block molding cavities


7




h


and


8




l


are not regulated during the period after mold clamping until arrival of the sealing resin


10


at the gates


7




i


. Further, how to perform pressurization and pressure reduction, as well as the timing of pressurization and that of pressure reduction, are the same as in the first embodiment.




By thus pressurizing the interiors of the block molding cavities


7




h


and


8




l


during resin filling into the cavities, a predetermined flow resistance can be imparted to the whole of the sealing resin


10


during resin filling. Consequently, the charging speeds of the sealing resin


10


for plural semiconductor chips


4


, that are arranged in rows in a direction orthogonal to the resin injecting direction, can be made almost equal in the plural semiconductor chips arranged in a respective row.




As a result, it is possible to eliminate the occurrence of an unfilled portion within the block molding cavities


7




h


and


8




l


, and, hence, it is possible to stabilize the quality of the product, i.e., CSP


43


.




Moreover, even when the multi-chip substrate


40


is in a state of partial chip missing, since it is possible to substantially equalize the resin charging speeds among plural semiconductor chips


4


in a respective row, it is not necessary to perform the mounting of a dummy chip, which has been so far performed for the multi-chip substrate


40


which is in a state of partial chip missing. Consequently, it is possible to omit a dummy chip mounting step, and, hence, possible to simplify the fabrication process for the CSP


43


. Further, CSP


43


can be fabricated at a lower cost because a dummy chip is not needed.




Resin molding is now over. The molding die


6


is opened, and, thereafter, the multi-chip substrate


40


is taken out from the molding die


6


. In this case, as shown in

FIG. 24

, a block molding portion


45


formed by block molding is provided on a main surface


40




a


of the multi-chip substrate


40


. Further, runner resin


47


, cull resin


48


, and gate resin


49


are formed on the main surface


40




a.






Thereafter, the runner resin


47


, cull resin


48


and gate resin


49


are removed from the block molding portion


45


to provide the state shown in FIG.


22


. Further, the multi-chip substrate


40


is cut, device region


40




c


, by device region


40




c


into individual chips.




At this time, dicing is performed along a dicing line


46


, as shown in

FIG. 23

, to dice the multi-chip substrate together with the block molding portion


45


, thereby to obtain individual chips, as shown in FIG.


25


.




Subsequently, as shown in

FIG. 26

, plural solder balls


42


are attached to the back side


41




b


of the wiring substrate


41


obtained by the dicing. Now the assembly of the CSP


43


is over. Mounting of the solder balls


42


also may be carried out on the multi-chip substrate


40


prior to the dicing thereof into individual chips.




In the assembly of the CSP


43


according to this second embodiment, it is possible to stabilize the product quality even in the case of a chip laminate type thin CSP


43


having a thickness of not larger than 1 mm from the back side


41




b


of the wiring substrate


41


up to the surface of the seal member


44


.




Although the present invention has been described herein on the basis of first and second embodiments, it goes without saying that the invention is not limited to those embodiments, but that various changes may be made within a scope not departing from the gist of the invention.




For example, although the semiconductor integrated circuit device in the first embodiment is a QFP, it may be any other semiconductor integrated circuit device than a QFP insofar as the device adopted is a thin type device formed by using the matrix frame


2


.




Although, in the first embodiment, the number of cavity rows in the molding die


6


is two, the invention is not limited to two cavity rows, but any other plural number of rows may be adopted, so long as it is not less than two.




Further, although the CSP


43


in the second embodiment is a chip laminate type CSP, the invention is not limited thereto, but it may carry only one semiconductor chip


4


.




The following is a brief description of an effect obtained by typical features of the present invention.




By pressurizing the interiors of cavities arranged in a matrix form and charging a sealing resin into the pressurized cavities, it is possible to equalize the resin charging speeds for all of the cavities, and, hence, it is possible to stabilize the product quality.



Claims
  • 1. A method of fabricating a semiconductor integrated circuit device, comprising the steps of:(a) providing a multi-chip substrate on which a plurality of device forming regions are arranged in a matrix form, the device forming regions each having a chip mounting region and a plurality of leads; (b) mounting semiconductor chips respectively onto the chip mounting regions of the multi-chip substrate; (c) disposing the multi-chip substrate with the semiconductor chips mounted thereon onto a mold surface of a molding die, which mold surface includes a single cavity, and thereafter closing the molding die, while allowing the single cavity to cover all of the plural device forming regions; (d) pressurizing the interior of the cavity upon charging of a sealing resin into the thus-pressurized cavity; and (e) after the step (d), dividing the multi-chip substrate into individual device forming regions.
  • 2. A method according to claim 1, wherein the multi-chip substrate is sealed with the sealing resin, the multi-chip substrate having device forming regions on which semiconductor chips are mounted and a device forming region on which no semiconductor chip is mounted.
  • 3. A method according to claim 1, wherein the semiconductor chips are stacked in the device forming regions of the multi-chip substrate.
  • 4. A method according to claim 3, wherein the thickness from a back side of a wiring substrate of the semiconductor integrated circuit device up to a surface of a seal member is not larger than 1 mm.
  • 5. A method according to claim 1, wherein, in the step (d), the sealing resin is injected into the cavity at a resin injection pressure of not higher than 490 MPa.
  • 6. A method according to claim 1, wherein the interior of the cavity is maintained in a state of atmospheric pressure until the sealing resin reaches gates of the molding die.
  • 7. A method according to claim 1, wherein the pressurization of the interior of the cavity is started almost simultaneously with the start of entry of the sealing resin into the cavity.
Priority Claims (1)
Number Date Country Kind
2002-037204 Feb 2002 JP
US Referenced Citations (4)
Number Name Date Kind
4126292 Saeki et al. Nov 1978 A
5071334 Obara Dec 1991 A
5624691 Bednarz et al. Apr 1997 A
20020115237 Williams Aug 2002 A1
Foreign Referenced Citations (5)
Number Date Country
11-297731 Oct 1999 JP
11-297731 Oct 1999 JP
2000-68305 Mar 2000 JP
2000-68305 Mar 2000 JP
2000-164615 Jun 2000 JP